Index Name Specifications Appearance Colorless transparent liquid Assay 99%min Boiling range(
Cas:110-91-8
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryLonwin Industry group limited as a professional manufactor & exporter of chemical materials ,we totally haver more than 270 stuffs, we have been on this line for more than 9 years. Our chemical materials are exported to lot of countries and regio
Cas:110-91-8
Min.Order:100 Kilogram
FOB Price: $2.7 / 3.0
Type:Other
inquiryOur clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:110-91-8
Min.Order:1 Metric Ton
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inquiryProduct description: Product name Morpholine CAS number 110-91-8 Assay ≥99% Appearance Colorless transparent liquid Capacity 1000mt/year Application Analytical reagent, solve
Cas:110-91-8
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryGood products, good service. We have professional sales team working on sales service for 15 years. Good products can win good market but can not stand long without good service. We have strict sales regulation and service procedure to make sure yo
Cas:110-91-8
Min.Order:1 Metric Ton
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inquiryGood quality Promptly delivery Good price Appearance:white powder Storage:dry Package:fiber drum Application:OLED Transportation:By Sea Port:Shanghai Port
Cas:110-91-8
Min.Order:1 Kilogram
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Type:Manufacturers
inquirychengdu and import and export trade co., LTD., who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do res
Morpholine Typical Properties Melting point -5 °C Boiling point 129 °C(lit.) density 1.000 g/mL at 20 °C vapor density 3 (vs air)
1-Oxa-4-azacyclohexane Basic information Product Name: 1-Oxa-4-azacyclohexane Synonyms: 1,4-Oxazinan;1,4-oxazine,tetrahydro-;2H-1,4-Oxazine, tetrahydro-;4H-1,4-Oxazine, tetrahydro-;B
Item Standard Appearance Colorless oily liquid Purity by gas as chromatorraphy 99.0%min Moisture
Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:110-91-8
Min.Order:1 Kilogram
FOB Price: $54.0 / 60.0
Type:Trading Company
inquiryAppearance:Colorless water-absorbing fluid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used as raw material for medicine, rubber accelerant and fluorescent whi
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:110-91-8
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquirySuperior quality Appearance:Yellow liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used as a medicine, rubber accelerator and fluorescent w
Product name: Morpholine CAS No.:110-91-8 Molecule Formula:C4H9NO Molecule Weight:87.13 Purity: 99.0% Package: 25kg/drum Description:Colorless oily liquid Manufacture Standards:Enterprise Standard TESTING ITEMS
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:110-91-8
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryWe are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
Cas:110-91-8
Min.Order:1 Gram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryHANGZHOU THINK CHEMICAL CO., LTD. (THINKCHEM) is an integrative corporation of trade, research and contract manufacture. With about ten years of business experiences on the marketing & distribution, thinkchem specializes in exp
Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service an
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
Product Name: 1-Oxa-4-azacyclohexane Synonyms: 1,4-Oxazinan;1,4-oxazine,tetrahydro-;2H-1,4-Oxazine, tetrahydro-;4H-1,4-Oxazine, tetrahydro-;BASF 238;…Appearance:Solid powder Storage:Sealed,light and oxygen resistant Package:aluminum foil bag,carton
SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe
Cas:110-91-8
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryR & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates
Best service,high quality and cheap price. Storage:Keep away from heat,sparks and flames. Package:25kg/50kg/200kg drum or Customer demand Application:Used as pharmaceutical intermediates Transportation:BY sea/air or by courier
Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home
Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city?in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api,?intermediat
Conditions | Yield |
---|---|
In xylene for 6h; Heating; | A n/a B 100% |
under 0.075006 Torr; Pyrolysis; |
Conditions | Yield |
---|---|
With diethylamine; palladium diacetate; trisodium tris(3-sulfophenyl)phosphine In water for 0.166667h; Ambient temperature; | A 98% B 2% |
With formic acid; triphenylphosphine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex In tetrahydrofuran at 30℃; for 3h; | A 16 % Chromat. B 84 % Chromat. |
Conditions | Yield |
---|---|
With methylamine | A 98% B n/a |
4-Phenylsulfanyl-morpholine
diisopropyl phosphite
A
morpholine
B
thiophosphoric acid O,O'-diisopropyl ester S-phenyl ester
Conditions | Yield |
---|---|
A n/a B 96% |
prop-2-yn-1-yl morpholine-4-carboxylate
morpholine
Conditions | Yield |
---|---|
With benzyltriethylammonium tetrathiomolybdate In acetonitrile at 20℃; for 2.5h; | 95% |
With potassium tetrachloroplatinate(II) In d(4)-methanol; water-d2 at 20℃; for 14h; Reagent/catalyst; |
Conditions | Yield |
---|---|
With Ru-MACHO; potassium tert-butylate; hydrogen In tetrahydrofuran at 140℃; under 38002.6 Torr; for 2.5h; Catalytic behavior; Temperature; Glovebox; Autoclave; Cooling with ice; | 95% |
With [bis({2‐[bis(propan‐2‐yl)phosphanyl]ethyl})amide](carbonyl)(hydride)iron(II); hydrogen In tetrahydrofuran at 100℃; under 22801.5 Torr; for 4h; Catalytic behavior; |
2,6-difluorobenzaldehyde
Methyl thioglycolate
Benzo[b]thiophene
A
morpholine
Conditions | Yield |
---|---|
With triethylamine In NaH; dimethyl sulfoxide; acetonitrile | A 93% B n/a |
4-(9-fluorenylmethoxycarbonyl)morpholine
morpholine
Conditions | Yield |
---|---|
With triethylamine; 1-butyl-3-methylimidazolium Tetrafluoroborate In neat (no solvent) at 25℃; for 0.0666667h; Green chemistry; | 93% |
Conditions | Yield |
---|---|
With 1,3,5-trichloro-2,4,6-triazine; potassium carbonate In chloroform at 0 - 20℃; | 92% |
Conditions | Yield |
---|---|
With magnesium; acetic acid In methanol at 20℃; | 92% |
morpholine-4-carboxylic acid tert-butyl ester
morpholine
Conditions | Yield |
---|---|
With aluminium trichloride In dichloromethane for 3h; Ambient temperature; | 91% |
allyl morpholine-1-carboxylate
A
morpholine
B
N-allylmorpholine
C
propene
Conditions | Yield |
---|---|
With formic acid; triphenylphosphine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex In tetrahydrofuran at 30℃; for 3h; | A 16 % Chromat. B 84% C n/a |
4-Phenylsulfanyl-morpholine
Diethyl phosphonate
A
morpholine
B
Diethyl 4-morpholidophosphate
C
O,O-diethyl S-phenyl phosphorothioate
Conditions | Yield |
---|---|
A n/a B 5% C 83% |
Conditions | Yield |
---|---|
With ammonium formate; PdMCM-41 In methanol at 69.84℃; for 2h; | 80% |
With isocyanate de chlorosulfonyle In diethyl ether for 10h; Ambient temperature; | 75% |
With perchloric acid; ammonium sulfamate; sodium thiocyanide at 50℃; Rate constant; piperidinium perchlorate, 18h; transnitrosating studies; | |
With benzophenone In N,N-dimethyl-formamide at 25℃; Rate constant; var. organic electron carriers, object of study - homogeneous electrochemical reduction with the aid of organic electron carriers; |
1,1-bis(N-morpholinyl)ethylene
malononitrile
A
morpholine
B
4-acetylmorpholine
C
2-(1-morpholinoethylidene)malononitrile
Conditions | Yield |
---|---|
In diethyl ether for 8h; Heating; | A n/a B n/a C 74% |
Conditions | Yield |
---|---|
With chloro-trimethyl-silane; sodium iodide In acetonitrile for 3h; Heating; | 70% |
A
morpholine
B
ethyl 4-aminopyrimido<1,2-a>benzimidazole-3-carboxylate
C
ethyl 4-<2-(2-hydroxyethyldithio)-1-(2-hydroxyethylthio)ethylideneamino>pyrimido<1,2-a>benzimidazole-3-carboxylate
Conditions | Yield |
---|---|
With hydrogenchloride; 2-hydroxyethanethiol In methanol for 4h; Ambient temperature; | A 69% B 5% C 64% |
2-hydroxyethanethiol
A
morpholine
B
ethyl 4-aminopyrimido<1,2-a>benzimidazole-3-carboxylate
C
ethyl 4-<2-(2-hydroxyethyldithio)-1-(2-hydroxyethylthio)ethylideneamino>pyrimido<1,2-a>benzimidazole-3-carboxylate
Conditions | Yield |
---|---|
With hydrogenchloride In methanol for 4h; Ambient temperature; | A 69% B 5% C 64% |
4-Phenylsulfanyl-morpholine
methyl phosphite
A
morpholine
B
thiophosphoric acid O,O'-dimethyl ester S-phenyl ester
Conditions | Yield |
---|---|
A n/a B 67% |
4-(trimethylsilyl)morpholine
morpholine
Conditions | Yield |
---|---|
With C8H20BO(1-)*Na(1+) In tetrahydrofuran at 80℃; for 6h; Reagent/catalyst; Inert atmosphere; Schlenk technique; High pressure; | 66% |
Stage #1: 4-(trimethylsilyl)morpholine With cesium fluoride at 100℃; for 0.5h; Inert atmosphere; Sealed tube; Stage #2: In chloroform-d1 Inert atmosphere; Acidic conditions; | 29% |
With potassium trimethylsilonate In dimethyl sulfoxide at 70℃; for 6h; Sealed tube; Schlenk technique; | 47 %Chromat. |
With Na(1+)*C6H15B*C2H5O(1-) In tetrahydrofuran at 80℃; for 6h; Reagent/catalyst; | 66 %Chromat. |
4,4'-<3,3'-Oxybis(2-methyl-1-phenyl-2-propenyliden)>dimorpholinium-bis(trifluormethansulfonat)
A
morpholine
B
3-Hydroxy-2-methyl-1-oxo-1-phenylprop-2-ene
Conditions | Yield |
---|---|
With water In acetonitrile for 96h; Product distribution; Ambient temperature; | A n/a B 62% |
ethanolamine
acetylene
A
morpholine
B
2-aminoethyl vinyl ether
C
2-vinyloxy-1,3-butadiene
D
N-Ethylideneethanolamine Vinyl Ether
Conditions | Yield |
---|---|
With potassium hydroxide In dimethyl sulfoxide at 100℃; under 760 Torr; for 2h; Product distribution; reaction under different conditions (temperature, pressure, time, base, solvent); | A n/a B 60% C n/a D n/a |
With potassium hydroxide In dimethyl sulfoxide at 100℃; under 760 Torr; for 2h; | A n/a B 60% C n/a D n/a |
Conditions | Yield |
---|---|
In acetonitrile at 20℃; for 0.5h; Michael Addition; diastereoselective reaction; | A n/a B 59% C n/a |
3-Morpholin-4-yl-propionitrile
A
morpholine
B
4-(3-Aminopropyl)morpholine
Conditions | Yield |
---|---|
With sodium tetrahydroborate; hydrogen; nickel dichloride In tert-butyl alcohol at 70℃; under 760.051 Torr; for 8h; | A 22% B 59% |
Conditions | Yield |
---|---|
In 2,2,2-trifluoroethanol at 20℃; for 6h; regioselective reaction; | 100% |
With copper(II) ferrite In dichloromethane at 20℃; regioselective reaction; | 95% |
With Montmorillonite K10 clay for 0.0166667h; aminolysis, ring cleavage; Irradiation; | 74% |
at 130 - 140℃; for 3h; | 60% |
morpholine
2,3-Dichloro-1,4-naphthoquinone
2-chloro-3-morpholin-4-yl-[1,4]naphthoquinone
Conditions | Yield |
---|---|
In water at 50℃; for 0.333333h; | 100% |
With water at 50℃; for 0.5h; | 98% |
With triethylamine In diethyl ether at 20℃; for 24h; | 64% |
morpholine
Succinimide
formaldehyd
N-[{morpholin-1-yl}-methyl]-pyrrolidine-2,5-dione
Conditions | Yield |
---|---|
With aluminum oxide In water for 0.2h; Condensation; microwave irradiation; | 100% |
In ethanol at 60℃; for 2h; | 88% |
Conditions | Yield |
---|---|
chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II) at 100℃; | 100% |
With [RhCl2(p-cymene)]2; bis[2-(diphenylphosphino)phenyl] ether In toluene at 250℃; under 37503.8 Torr; Flow reactor; | 93% |
With Cu1-Mo1/TiO2 In neat liquid at 20℃; for 21h; Catalytic behavior; Inert atmosphere; UV-irradiation; | 82% |
morpholine
2-chloro-5-nitropyridine
4-(5-nitro-pyridin-2-yl)-morpholine
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 3h; | 100% |
With potassium carbonate In tetrahydrofuran at 80℃; for 4h; | 99% |
With potassium carbonate In tetrahydrofuran at 80℃; for 4h; | 99% |
Conditions | Yield |
---|---|
With oxalic acid at 100 - 120℃; Eschweiler-Clarke methylation; | 100% |
With hydrogen In methanol at 100℃; under 9750.98 Torr; for 3h; Autoclave; | 97% |
With acetic acid at 30℃; for 2h; | 96% |
Conditions | Yield |
---|---|
With cyano-hydroxyimino-acetic acid 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester; sodium hydrogencarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In water at 20℃; for 3h; Reagent/catalyst; Solvent; | 100% |
In butan-1-ol at 120℃; Solvent; Temperature; | 99.35% |
In ethanol at 140℃; for 24h; Solvent; Autoclave; | 98% |
Conditions | Yield |
---|---|
With sodium t-butanolate; palladium diacetate; [(μ-PPh2CH2PPh2)Co2(CO)4][μ,η-PhCCP(tBu)2] In toluene at 60℃; for 20h; Product distribution; Further Variations:; Catalysts; Reagents; Solvents; Temperatures; | 100% |
With C20H45N2OP; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In toluene at 105℃; for 20h; Reagent/catalyst; | 100% |
With bis(η3-allyl-μ-chloropalladium(II)); [(μ-Ph2PCH2PPh2)Co2(CO)4(μ,η-Me2NCH2CCP(C6H11)2)]; sodium t-butanolate In toluene at 80℃; for 2h; Inert atmosphere; | 99% |
morpholine
1,3,5-trichloro-2,4,6-triazine
2,6-Dichloro-4-morpholino-1,3,5-triazine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at -78℃; for 0.166667h; | 100% |
With triethylamine In dichloromethane at -78 - -30℃; for 1.5h; Inert atmosphere; | 99% |
With triethylamine In acetone for 0.5h; Cooling with ice; | 98% |
morpholine
1,3,5-trichloro-2,4,6-triazine
2-chloro-4,6-di-morpholin-4-yl-[1,3,5]triazine
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In dichloromethane at 0 - 40℃; for 3h; | 100% |
In dichloromethane; water at 0 - 5℃; for 3.25h; Large scale; | 98% |
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0℃; for 1h; | 95% |
Conditions | Yield |
---|---|
100% | |
With sodium hydrogencarbonate In dichloromethane; water at 0 - 20℃; | 86.5% |
With triethylamine In diethyl ether at 0℃; | 82% |
morpholine
1,4-dibromo-2-nitrobenzene
4-(4-bromo-2-nitro-phenyl)-morpholine
Conditions | Yield |
---|---|
In isopropyl alcohol | 100% |
With triethylamine In isopropyl alcohol at 70℃; for 24h; | 73% |
morpholine
ethyl 2-phenyl-2-bromoacetate
α-morpholine ethyl phenylacetate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 1.5h; | 100% |
With N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 1.5h; | 100% |
With triethylamine at 20℃; | 80% |
With isopropyl alcohol |
Conditions | Yield |
---|---|
With zirconium(IV) chloride at 20℃; for 0.25h; | 100% |
With zinc(II) perchlorate hexahydrate at 80℃; for 1h; | 100% |
With zinc(II) bis(tetrafluoroborate) hydrate at 20℃; for 2h; Neat (no solvent); | 97% |
Conditions | Yield |
---|---|
With copper(II) bis(trifluoromethanesulfonate) In water at 20℃; for 0.0333333h; | 100% |
In benzene at 20℃; for 16h; Inert atmosphere; | 99% |
In benzene Reflux; | 95% |
Conditions | Yield |
---|---|
With copper(II) bis(trifluoromethanesulfonate) In water at 20℃; for 0.0333333h; | 100% |
at 50℃; for 0.333333h; Molecular sieve; Microwave irradiation; | 98% |
at 100℃; for 0.166667h; Microwave irradiation; Neat (no solvent); | 95% |
Conditions | Yield |
---|---|
at 0 - 20℃; for 48.3333h; | 100% |
In diethyl ether at 20℃; for 18h; | 99.2% |
In diethyl ether at 20℃; for 0.75h; Addition; | 97% |
Conditions | Yield |
---|---|
In benzene for 0.5h; Reflux; | 100% |
In toluene for 8h; | 92% |
In benzene for 0.5h; Alkylation; Heating; | 91% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 50℃; under 4500360 Torr; for 20h; | 100% |
With potassium carbonate In dimethyl sulfoxide at 120℃; for 19h; | 100% |
In tetrahydrofuran at 50℃; under 10000 Torr; for 2h; Product distribution; other pressure; | 99.7% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 50℃; under 4500360 Torr; for 20h; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 100℃; for 6h; | 99% |
With potassium phosphate; Al2O3#dotCo(2+) In water at 100℃; for 7h; | 90% |
morpholine
2-Bromo-4'-phenylacetophenone
1-biphenyl-4-yl-2-morpholin-4-yl-ethanone
Conditions | Yield |
---|---|
Stage #1: morpholine; 2-Bromo-4'-phenylacetophenone In diethyl ether; dichloromethane at 0 - 20℃; for 1h; Stage #2: With sodium hydrogencarbonate In dichloromethane; water Product distribution / selectivity; | 100% |
With triethylamine In diethyl ether at 0 - 20℃; for 2.5h; Product distribution / selectivity; | 93% |
Conditions | Yield |
---|---|
In methanol | 100% |
With zirconium(IV) chloride In dichloromethane at 20℃; for 1h; Michael addition; | 100% |
With poly(ethylene glycol) 2000; ruthenium trichloride at 50℃; for 6h; aza-Michael addition; | 99% |
Conditions | Yield |
---|---|
With potassium carbonate In toluene at 60℃; for 2h; | 100% |
Stage #1: morpholine; chloroacetyl chloride With triethylamine In dichloromethane at 0 - 27℃; for 2h; Stage #2: With hydrogenchloride In dichloromethane; water | 100% |
With triethylamine In dichloromethane at 0 - 20℃; for 6h; | 99% |
Conditions | Yield |
---|---|
In neat (no solvent) at 20℃; Inert atmosphere; | 100% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In 2-methyltetrahydrofuran at 40℃; for 4h; | 87% |
at 130℃; for 4h; | 75% |
morpholine
2,5-dichloronitrobenzene
4-(4-chloro-2-nitro-phenyl)morpholine
Conditions | Yield |
---|---|
In tetrahydrofuran at 50℃; under 4500360 Torr; for 20h; | 100% |
at 2℃; Heating; | 50% |
Conditions | Yield |
---|---|
With [NO(1+)*18-crown-6*H(NO3)2(1-)] In dichloromethane at 20℃; for 0.0833333h; | 100% |
With silica gel; zinc(II) chloride; sodium nitrite In dichloromethane at 20℃; for 0.75h; Nitrosation; | 99% |
With Iron(III) nitrate nonahydrate; tetrabutylammonium perchlorate In acetonitrile at 70℃; Kinetics; Reagent/catalyst; Inert atmosphere; Electrolysis; Green chemistry; | 99% |
Conditions | Yield |
---|---|
With sulfuryl dichloride In acetonitrile for 24h; Heating / reflux; | 100% |
With hydrogenchloride; sodium hypochlorite; sulfur dioxide; chlorine In dichloromethane; water | 60% |
With hydrogenchloride; sodium hypochlorite; sulfur dioxide; chlorine In dichloromethane; water | 60% |
morpholine
Phenyl glycidyl ether
4-(2-hydroxy-3-phenoxypropyl)morpholine
Conditions | Yield |
---|---|
In 2,2,2-trifluoroethanol at 20℃; for 6h; regioselective reaction; | 100% |
In water at 0 - 20℃; | 97% |
With sulfated zirconia In neat (no solvent) at 20℃; for 3h; regioselective reaction; | 97% |
Conditions | Yield |
---|---|
In ethanol for 24h; Heating; | 100% |
With zinc(II) chloride In water at 60℃; for 8h; regioselective reaction; | 96% |
In water at 0 - 5℃; for 4h; | 92% |
Conditions | Yield |
---|---|
at 120℃; for 9h; | 100% |
for 72h; Heating; | 95% |
at 100℃; for 4h; Neat (no solvent); | 95% |
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