Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:110-93-0
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:110-93-0
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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High Quality and Best Price of 6-Methyl-5-hepten-2-one from HENAN TIANFU CHEMICAL: Henan Tianfu Chemical Co.,LTD was built in 2009 with an ISO certificate in the past 5 years, we have grown up as a famous fine chemicals supplier in china and we h
Cas:110-93-0
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inquiryLIDE PHARMACEUTICALS LIMITED is a professional chemicals and APIs leading manufacturer in China. Our core business line covers APIs, Intermediates, Herb extract, etc.
Cas:110-93-0
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FOB Price: $0.9 / 1.0
Type:Lab/Research institutions
inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:110-93-0
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Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:110-93-0
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inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W
Cas:110-93-0
Min.Order:1 Kilogram
FOB Price: $7.0 / 9.0
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:110-93-0
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inquiry6-Methyl-5-hepten-2-one CAS:110-93-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic int
Cas:110-93-0
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:110-93-0
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiry6-Methyl-5-hepten-2-one CAS: 110-93-0 Specificatio Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard Shelf life 2 years Storage should be stored in a we
Cas:110-93-0
Min.Order:1 Kilogram
FOB Price: $100.0 / 150.0
Type:Other
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Hangzhou Fanda Chemical Co.,Ltd (FandaChem) , a China-based chemical company, specialize in exporting 6-Methyl-5-hepten-2-one;Methyl Heptenone CAS:110-93-0, Please contact us by email freely. We are leading exporter in China. If you r
Cas:110-93-0
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Type:Other
inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:110-93-0
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:110-93-0
Min.Order:0 Metric Ton
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:110-93-0
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquirySuperior quality, moderate price & quick delivery. Appearance:colourless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediat
Product Name: 6-Methyl-5-hepten-2-one Synonyms: 2-Methyl-2-hepten-6-one (=6-Methyl-5-hepten-2-one);METHYL HEPTENONE, NATURAL;6-Methyl-5-henten-2-one;2-Methyl-6-oxo-2-heptene;2-methylhept-2-en-6-one;2-Oxo-6-methylhept-5-ene;5-Hepten-2-one,6-meth
Cas:110-93-0
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:110-93-0
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryHangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:110-93-0
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:110-93-0
Min.Order:1 Metric Ton
FOB Price: $1.5
Type:Trading Company
inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Cas:110-93-0
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Trading Company
inquiryISO/factory/goodqualityAppearance:off white Storage:Dry,cool place Package:drum Application:active pharmaceutical ingredients Transportation:by air/sea/express Port:shenzhen/shanghai
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Cas:110-93-0
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiry3,7-dimethyloct-6-en-1-yn-3-ol
2-methyl-but-3-yn-2-ol
A
6-Methyl-hept-5-en-2-on
B
acetone
Conditions | Yield |
---|---|
potassium hydroxide In water at 93℃; for 6.41667h; Heating / reflux; | A 95.2% B 95.8% |
Conditions | Yield |
---|---|
With Dimethyl phosphite at 150℃; for 14.6h; Reagent/catalyst; Time; Inert atmosphere; | 95.1% |
hydrogen tris(oxalato)phosphate In methanol at 124.84 - 149.84℃; for 17 - 25h; Product distribution / selectivity; | 77.3% |
hydrogen tris(oxalato)phosphate In acetone at 149.84℃; for 24h; Product distribution / selectivity; | 56.4% |
6-methylhept-5-en-2-one N,N-dimethylhydrazone
6-Methyl-hept-5-en-2-on
Conditions | Yield |
---|---|
With sodium perborate; sodium hydroxide; potassium dihydrogenphosphate; water In tert-butyl alcohol at 60℃; for 24h; | 94% |
3-chloro-3-methyl-1-butene
3,3-dimethyl-allyl chloride
6-Methyl-hept-5-en-2-on
Conditions | Yield |
---|---|
With N,N-dimethyl-formamide; sodium hydroxide In acetone at 50℃; for 2h; Reagent/catalyst; Temperature; Inert atmosphere; | 92.8% |
Conditions | Yield |
---|---|
With aluminum oxide; potassium permanganate; neutral In acetone for 4h; Ambient temperature; | A n/a B 92% |
(E/Z)-3,7-dimethyl-2,6-octadienal
A
6-Methyl-hept-5-en-2-on
B
acetaldehyde
Conditions | Yield |
---|---|
With tetra(n-butyl)ammonium hydroxide; water at 150℃; for 0.166667h; Microwave irradiation; Green chemistry; | A 91% B n/a |
With potassium carbonate |
2-methyl-3-buten-2-ol
acetoacetic acid methyl ester
6-Methyl-hept-5-en-2-on
Conditions | Yield |
---|---|
90.8% |
Conditions | Yield |
---|---|
With pyrrolidine; water In acetonitrile at 20℃; for 12h; | 90% |
With water; potassium carbonate man destilliert mit Wasserdampf und fraktioniert im Vakuum; | |
With potassium carbonate |
6-Methyl-hept-5-en-2-on
Conditions | Yield |
---|---|
With selenium(IV) oxide; dihydrogen peroxide In methanol at 20℃; pH=7; aq. phosphate buffer; | 89% |
1,2-diamino-benzene
(E/Z)-3,7-dimethyl-2,6-octadienal
A
2-Methyl-1H-benzimidazole
B
6-Methyl-hept-5-en-2-on
Conditions | Yield |
---|---|
With tetra(n-butyl)ammonium hydroxide; water at 150℃; for 0.166667h; Microwave irradiation; Green chemistry; | A 61% B 89% |
Conditions | Yield |
---|---|
With polymer-supported dicyanoketene acetal; water at 20℃; for 20h; | 88% |
With silica gel; toluene-4-sulfonic acid In dichloromethane for 3h; | 87% |
With polymer-supported dicyanoketene acetal; water In acetonitrile at 20℃; for 20h; Hydrolysis; | 73% |
palladium (II) ion In acetone for 1h; Ambient temperature; | 100 % Chromat. |
6-Methyl-hept-5-en-2-on
Conditions | Yield |
---|---|
Stage #1: C10H17NO2 With chromium dichloride; acrylic acid methyl ester In tetrahydrofuran at 25℃; Stage #2: With water In tetrahydrofuran Further stages.; | 88% |
2-Methoxypropene
3-(1-methoxy-1-methyl-ethoxy)-3-methyl-but-1-ene
6-Methyl-hept-5-en-2-on
Conditions | Yield |
---|---|
Stage #1: 3-(1-methoxy-1-methyl-ethoxy)-3-methyl-but-1-ene at 150℃; for 16h; autoclave; Stage #2: 2-Methoxypropene; phosphoric acid In acetone at 150℃; for 16h; autoclave; | 86% |
6-methylhept-5-en-2-ol
6-Methyl-hept-5-en-2-on
Conditions | Yield |
---|---|
With trimethylsilyl chromates In dichloromethane at 25℃; for 2h; | 85% |
With butyltriphenylphosphonium dichromate In chloroform for 3.5h; Oxidation; Heating; | 80% |
With [Fe[(S)-N-benzyl-2-phenyl-2-(pyridin-2-ylmethoxy)-N-(pyridin-2-ylmethyl)ethanamine](OTf)2]; dihydrogen peroxide In water; acetonitrile at 20℃; for 2h; Inert atmosphere; | 69% |
6-Methyl-3-(toluene-4-sulfonyl)-hept-5-en-2-one
6-Methyl-hept-5-en-2-on
Conditions | Yield |
---|---|
With disodium hydrogenphosphate; sodium amalgam In methanol at 0℃; for 2h; | 85% |
4-<(tert-Butyl)dimethylsilyl>-2-methyl-2-(4'-methylpent-3'-enyl)-1,3-dioxole
6-Methyl-hept-5-en-2-on
Conditions | Yield |
---|---|
With water; oxalic acid Ambient temperature; | 85% |
1,1-dimethylprop-2-enyl 3-oxobutanoate
6-Methyl-hept-5-en-2-on
Conditions | Yield |
---|---|
With aluminum oxide at 60℃; for 3h; | 84% |
With aluminum oxide at 60℃; for 3h; Product distribution; substrate supported on Al2O3; Carrol rearrangement of allyl acetoacetates to γ,δ-unsaturated ketones on the surface of chromatographic absorbents; | 84% |
With aluminum isopropoxide at 160℃; |
3,7-dimethyloct-6-en-1-yn-3-ol
2-methylpropan-2-thiol
A
6-Methyl-hept-5-en-2-on
B
(Z)-1-tert-Butylsulfanyl-3,7-dimethyl-octa-1,6-dien-3-ol
Conditions | Yield |
---|---|
With potassium hydroxide In dimethyl sulfoxide at 50℃; for 6h; | A 10% B 83% |
With potassium hydroxide In dimethyl sulfoxide at 50℃; for 6h; | A 10% B 83% |
6-methylhept-5-en-2-one oxime
6-Methyl-hept-5-en-2-on
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; dipyridinium dichromate In dichloromethane at 0℃; for 4.5h; | 80% |
2,4-Dimethyl-2-(4'-methylpent-3'-enyl)-1,3-dioxole
6-Methyl-hept-5-en-2-on
Conditions | Yield |
---|---|
With hydrogenchloride for 24h; | 80% |
(E/Z)-3,7-dimethyl-2,6-octadienal
A
6-Methyl-hept-5-en-2-on
B
4,6-bis(4-methylpent-3-en-1-yl)-6-methylcyclohexa-1,3-diene-1-carbaldehyde
Conditions | Yield |
---|---|
With sodium hydride In diethyl ether for 0.5h; Heating; | A n/a B 80% |
6-methylhept-5-en-2-ol
A
6-Methyl-hept-5-en-2-on
B
6-methylhept-6-en-2-one
C
6-methylheptan-2-one
Conditions | Yield |
---|---|
With reusable unsupported rhenium nanocrystalline particle In neat (no solvent) at 180℃; for 10h; Green chemistry; | A 80% B 5% C 15% |
3-(1-methoxy-1-methyl-ethoxy)-3-methyl-but-1-ene
2,2-dimethoxy-propane
6-Methyl-hept-5-en-2-on
Conditions | Yield |
---|---|
phosphoric acid In acetone at 150℃; for 32h; Product distribution / selectivity; autoclave; | 78.8% |
2,3-epoxygeranial
A
2-methyl-2-(4-methyl-pent-3-enyl)-oxirane
B
6-Methyl-hept-5-en-2-on
Conditions | Yield |
---|---|
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In 1,2-dichloro-benzene at 140℃; for 14h; Sealed tube; Inert atmosphere; | A 73% B 23% |
tert-butyl acetoacetate
2-methyl-3-buten-2-ol
A
6-Methyl-hept-5-en-2-on
B
1,1-dimethylprop-2-enyl 3-oxobutanoate
Conditions | Yield |
---|---|
In toluene for 4h; Heating; | A 31% B 72% |
1,1-dimethylprop-2-enyl 3-oxobutanoate
A
6-Methyl-hept-5-en-2-on
B
3-methylbut-2-en-1-yl 3-oxobutanoate
Conditions | Yield |
---|---|
With silica gel at 60℃; for 5h; | A n/a B 70% |
Conditions | Yield |
---|---|
In diethyl ether at 0℃; for 3h; | 70% |
In diethyl ether at 0℃; for 1h; Methylation; | 70% |
3,7-dimethyloct-6-en-1-yn-3-ol
3-tert-Butylsulfanyl-but-3-en-2-ol
A
6-Methyl-hept-5-en-2-on
B
(Z)-1-tert-Butylsulfanyl-3,7-dimethyl-octa-1,6-dien-3-ol
Conditions | Yield |
---|---|
With potassium hydroxide In neat (no solvent) at 75 - 120℃; for 0.366667h; | A 33% B 64% |
2-methyl-3-buten-2-ol
ethyl acetoacetate
A
6-Methyl-hept-5-en-2-on
B
3-methylbut-2-en-1-yl 3-oxobutanoate
Conditions | Yield |
---|---|
In paraffin 1.) 160 deg C, 6 h, 2.) 180 deg C, 3 h; | A 60% B 5% |
3-(1-methoxy-1-methyl-ethoxy)-3-methyl-but-1-ene
6-Methyl-hept-5-en-2-on
Conditions | Yield |
---|---|
Stage #1: 3-(1-methoxy-1-methyl-ethoxy)-3-methyl-but-1-ene at 150℃; for 16h; autoclave; Stage #2: phosphoric acid In acetone at 150℃; for 16h; autoclave; | 60% |
6-Methyl-hept-5-en-2-on
6-methylhept-5-en-2-ol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In diethyl ether at 0℃; for 1h; | 100% |
With lithium aluminium tetrahydride In diethyl ether at 0℃; for 1h; | 99% |
With hydrogen; silver trifluoromethanesulfonate; potassium hexamethylsilazane In toluene at 25℃; under 15001.5 Torr; for 24h; Glovebox; chemoselective reaction; | 99% |
6-Methyl-hept-5-en-2-on
(S)-sulcatol
Conditions | Yield |
---|---|
In isopropyl alcohol at 50℃; for 24h; ADH T. brockii (growing), NADP, PAN 800; | 100% |
With NADH-dependent-formate-dehydrogenase; flavin adenine dinucleotide; NADH at 30℃; for 6h; pH=7.5; aq. buffer; Enzymatic reaction; optical yield given as %ee; enantiospecific reaction; | 99% |
With dichloro(benzene)ruthenium(II) dimer; mono(3-deoxy-3-[N-(2-hydroxyethyl)amino])-β-cyclodextrin; sodium formate In water; N,N-dimethyl-formamide at 50℃; for 12h; optical yield given as %ee; enantioselective reaction; | 95% |
Conditions | Yield |
---|---|
With sodium methylate In methanol at 0 - 5℃; for 0.5h; Inert atmosphere; | 99.1% |
86% | |
With diethyl ether unter Zusatz von Kaliumhydroxid; |
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethyl acetate under 2280 Torr; for 0.75h; Ambient temperature; | 99% |
With hydrogen In tetrahydrofuran at 24.84℃; under 15001.5 Torr; for 1h; | 98.2% |
With hydrogen; palladium/alumina at 60℃; under 1500.15 Torr; for 66h; Product distribution / selectivity; Autoclave; | 97.3% |
Conditions | Yield |
---|---|
With ytterbium(III) triflate at 20℃; for 4h; | 99% |
6-Methyl-hept-5-en-2-on
ketene t-butyldimethylsilyl methyl acetal
Conditions | Yield |
---|---|
Stage #1: 6-Methyl-hept-5-en-2-on With bis(trifluoromethanesulfonyl)amide In diethyl ether at -78 - 23℃; Mukaiyama Aldol Addition; Schlenk technique; Inert atmosphere; Stage #2: ketene t-butyldimethylsilyl methyl acetal In diethyl ether at -20℃; for 0.5h; Mukaiyama Aldol Addition; Schlenk technique; Inert atmosphere; | 99% |
6-Methyl-hept-5-en-2-on
trimethylsulfonium methylsulfate
2-methyl-2-(4-methyl-pent-3-enyl)-oxirane
Conditions | Yield |
---|---|
With N-benzyl-N,N,N-triethylammonium chloride In dichloromethane | 98% |
Conditions | Yield |
---|---|
With formic acid; chloro-(pentamethylcyclopentadienyl)-{5-methoxy-2-{1-[(4-methoxyphenyl)imino-N]ethyl}phenyl-C}-iridium(lll); triethylamine In methanol at 80℃; for 1h; Inert atmosphere; | 97% |
Conditions | Yield |
---|---|
Stage #1: Vinyl bromide With n-butyllithium; lithium bromide In tetrahydrofuran; diethyl ether; pentane at -127 - -105℃; for 3h; Inert atmosphere; Schlenk technique; Stage #2: 6-Methyl-hept-5-en-2-on In tetrahydrofuran; diethyl ether; pentane Inert atmosphere; Schlenk technique; | 97% |
6-Methyl-hept-5-en-2-on
vinylmagnesium chloride
3,7-dimethylocta-1,6-dien-3-ol
Conditions | Yield |
---|---|
With zinc(II) chloride In tetrahydrofuran at 20℃; for 4h; Reagent/catalyst; Solvent; Inert atmosphere; Cooling with ice; | 96.3% |
With tetrahydrofuran |
6-Methyl-hept-5-en-2-on
ethylene glycol
2-methyl-2-(4-methyl-3-pentenyl)-1,3-dioxolane
Conditions | Yield |
---|---|
With pyridinium p-toluenesulfonate In benzene Heating; | 96% |
With toluene-4-sulfonic acid In benzene | 94% |
With toluene-4-sulfonic acid In benzene for 5h; Condensation; Heating; | 92% |
6-Methyl-hept-5-en-2-on
2-propynyl chloride
4,8-dimethyl-non-7-en-1-yn-4-ol
Conditions | Yield |
---|---|
With manganese; TiCpCl2 In tetrahydrofuran at 20℃; for 1h; Reagent/catalyst; Inert atmosphere; | 96% |
With 2,4,6-trimethyl-pyridine; bis(cyclopentadienyl)titanium dichloride; manganese; chloro-trimethyl-silane In tetrahydrofuran at 20℃; for 7h; Barbier Coupling Reaction; Inert atmosphere; chemoselective reaction; | 96% |
dimethyltitanocene
6-Methyl-hept-5-en-2-on
2,6-dimethyl-hepta-1,5-diene
Conditions | Yield |
---|---|
Stage #1: dimethyltitanocene; 6-Methyl-hept-5-en-2-on In toluene at 20 - 80℃; for 5h; Inert atmosphere; Stage #2: With sodium hydrogencarbonate In methanol; water; toluene at 40℃; for 3h; Temperature; | 95.3% |
6-Methyl-hept-5-en-2-on
vinyl magnesium bromide
3,7-dimethylocta-1,6-dien-3-ol
Conditions | Yield |
---|---|
With zinc(II) chloride In tetrahydrofuran at 20℃; for 5h; Reagent/catalyst; Solvent; Inert atmosphere; Cooling with ice; | 95.2% |
With tetrahydrofuran; diethyl ether | |
In tetrahydrofuran at -78℃; Addition; |
methyl magnesium iodide
6-Methyl-hept-5-en-2-on
2,6-dimethylhept-5-en-2-ol
Conditions | Yield |
---|---|
In diethyl ether for 1h; | 95% |
analog verlaeuft die Reaktion mit Magnesiumaethyljodid; |
6-Methyl-hept-5-en-2-on
ethyl bromoacetate
3-hydroxy-3,7-dimethyl-oct-6-enoic acid ethyl ester
Conditions | Yield |
---|---|
With zinc In tetrahydrofuran for 2h; Reformatsky Reaction; Reflux; | 95% |
With zinc In tetrahydrofuran for 2h; Reformatsky Reaction; Reflux; | 95% |
With zinc In tetrahydrofuran for 2h; Reformatsky Reaction; Reflux; | 95% |
chloro-trimethyl-silane
6-Methyl-hept-5-en-2-on
6-methylhept-5-en-2-yl trimethylsilyl ether
Conditions | Yield |
---|---|
With tert-Amyl alcohol; sodium hydride; zinc(II) chloride In tetrahydrofuran for 0.25h; Ambient temperature; | 95% |
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran at -78℃; | 95% |
6-Methyl-hept-5-en-2-on
acetylenemagnesium bromide
3,7-dimethyloct-6-en-1-yn-3-ol
Conditions | Yield |
---|---|
In tetrahydrofuran at 0℃; for 1h; | 95% |
In tetrahydrofuran; diethyl ether Grignard reaction; | 90% |
In tetrahydrofuran at -78 - 20℃; | 87% |
6-Methyl-hept-5-en-2-on
3-hydroxy-3,7-dimethyl-oct-6-enoic acid ethyl ester
Conditions | Yield |
---|---|
With zinc Reformatsky reaction; | 95% |
6-Methyl-hept-5-en-2-on
Conditions | Yield |
---|---|
With sulfuric acid; dihydrogen peroxide; trifluoroacetic acid In dichloromethane at 0℃; for 6h; | 95% |
6-Methyl-hept-5-en-2-on
Conditions | Yield |
---|---|
With methanol; sodium tetrahydroborate at 0 - 35℃; | 95% |
Conditions | Yield |
---|---|
Stage #1: 6-Methyl-hept-5-en-2-on With (R,R)-N,N′-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediaminoaluminum(III) chloride; (tert-Butoxycarbonylmethylene)triphenylphosphorane; Triphenylphosphine oxide In dichloromethane at -30℃; for 0.5h; Inert atmosphere; Stage #2: trimethylsilyl cyanide In dichloromethane at -30℃; for 20h; Inert atmosphere; | 95% |
With (R,R)-N,N′-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediaminoaluminum(III) chloride; ethyl (triphenylphosphoranylidene)acetate In ethyl acetate at -30℃; for 33h; Solvent; Inert atmosphere; | 92% |
6-Methyl-hept-5-en-2-on
5,6-dihydroxy-6-methyl-heptan-2-one
Conditions | Yield |
---|---|
With osmium(VIII) oxide; 4-methylmorpholine N-oxide In water; acetone; tert-butyl alcohol at 0℃; for 4h; | 94% |
With water; oxygen bei der Sonnenbelichtung; | |
With potassium permanganate; water | |
With potassium permanganate |
6-Methyl-hept-5-en-2-on
N,N-Bis(trimethylsilyl)benzenesulphenamide
N-<(6-methyl)-5-hepten-2-ylidene>benzenesulfenamide
Conditions | Yield |
---|---|
tetrabutyl ammonium fluoride In tetrahydrofuran at 20℃; | 94% |
6-Methyl-hept-5-en-2-on
1,1-dimethylhydrazine
6-methylhept-5-en-2-one N,N-dimethylhydrazone
Conditions | Yield |
---|---|
With acetic acid at 20℃; for 3h; Condensation; | 94% |
Yield given; |
Conditions | Yield |
---|---|
Stage #1: dimethyl methane phosphonate With n-butyllithium In tetrahydrofuran; hexane at -70℃; for 0.25h; Stage #2: 6-Methyl-hept-5-en-2-on In tetrahydrofuran; hexane for 0.0833333h; Further stages.; | 94% |
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