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Cas:7677-24-9
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inquiryTrimethylsilyl cyanide CAS:7677-24-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic int
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A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquirymoderate price & quick delivery Appearance: clear colorless to yellow liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:100g/bottle,1kg/bottle,25kg/drum or as per your request Application:Reacts with alde
Product name: Trimethylsilyl Cyanide CAS No.:7677-24-9 Molecule Formula:C4H9NSi Molecule Weight:99.21 Purity: 97.0% Package: 140kg/drum Description:Colorless or light yellow liquid Manufacture Standards:Enterprise Standard
Cas:7677-24-9
Min.Order:1 Kilogram
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Min.Order:1 Gram
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inquiryProduct Name: Trimethylsilyl cyanide Synonyms: TRIMETHYLSILYL CYANIDE FOR SYNTHESIS;trimethylsilylformonitrile;trimethylsilylmethanenitrile;trimethyl-silanecarbonitril;trimethylsilycyanide;TMSCN;TRIMETHYLSILANECARBONITRILE;TRIMETHYLSILYL CYANID
Cas:7677-24-9
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With 1-methyl-pyrrolidin-2-one at 200℃; | 96% |
at 170 - 200℃; | 89% |
trimethylsilyl bromide
bis(triphenylphosphine)iminium cyanide
trimethylsilyl cyanide
Conditions | Yield |
---|---|
at 20℃; for 1h; | 93% |
Conditions | Yield |
---|---|
With 1-methyl-pyrrolidin-2-one; potassium iodide for 12h; Ambient temperature; | 88% |
With PEG400; zinc(II) iodide In dichloromethane at 20℃; for 20h; | 86% |
With 1-methyl-pyrrolidin-2-one; potassium iodide for 72h; Ambient temperature; | 78% |
benzyl thiocyanate
(trifluoromethyl)trimethylsilane
A
trimethylsilyl cyanide
B
benzyl trifluoromethyl sulfide
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran 0 deg C, 5 min then rt., 2.5 h; | A n/a B 87% |
Conditions | Yield |
---|---|
With PEG400; zinc(II) iodide In dichloromethane at 20℃; for 16h; | 83% |
With PEG400; zinc(II) iodide In dichloromethane at 20℃; for 4h; sonification; | 80% |
With sodium iodide solvent: N-methyl-2-pyrrolidone; | 70% |
With 1-methyl-pyrrolidin-2-one; AMBERLITE XAD-4 for 0.05h; Ambient temperature; |
trimethylsilyl iodide
A
trimethylsilyl cyanide
Conditions | Yield |
---|---|
In benzene at 65℃; for 36h; | A n/a B 81% |
terephthalonitrile
2-methallyltrimethylsilane
A
trimethylsilyl cyanide
B
4-(2-methyl-2-propenyl)benzonitrile
Conditions | Yield |
---|---|
In acetonitrile Irradiation; | A n/a B 80% |
octyl thiocyanate
(trifluoromethyl)trimethylsilane
A
trimethylsilyl cyanide
B
n-octyll trifluoromethyl sulfide
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran 0 deg C, 5 min then rt., 2.5 h; | A n/a B 76% |
ethyl isothiocyanate
diethyl trimethylsilyl phosphite
A
O,O,S-triethyl phosphorothioate
B
trimethylsilyl cyanide
Conditions | Yield |
---|---|
at 100 - 110℃; for 1h; | A 75% B n/a |
at 100 - 110℃; for 1h; Yields of byproduct given; |
1-octaneselenocyanate
(trifluoromethyl)trimethylsilane
A
trimethylsilyl cyanide
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran 0 deg C, 5 min then rt., 2.5 h; | A n/a B 75% |
Conditions | Yield |
---|---|
for 15h; Heating; | 72% |
methyl thiocyanate
diisopropyl trimethylsily phosphite
A
trimethylsilyl cyanide
B
O,O-diisopropyl S-methyl phosphorothioate
Conditions | Yield |
---|---|
at 100 - 110℃; for 1h; | A n/a B 70% |
at 100 - 110℃; for 1h; Yields of byproduct given; |
phenyl thiocyanate
(trifluoromethyl)trimethylsilane
A
trimethylsilyl cyanide
B
phenyl trifluoromethylsulfide
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran 0 deg C, 5 min then rt., 2.5 h; | A n/a B 70% |
benzyl selenocyanate
(trifluoromethyl)trimethylsilane
A
trimethylsilyl cyanide
B
{[(trifluoromethyl)selanyl]methyl}benzene
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran 0 deg C, 5 min then rt., 2.5 h; | A n/a B 70% |
Conditions | Yield |
---|---|
68% |
phthalonitrile
allyl-trimethyl-silane
A
trimethylsilyl cyanide
B
2-allylbenzonitrile
Conditions | Yield |
---|---|
In acetonitrile Irradiation; | A n/a B 67% |
terephthalonitrile
allyl-trimethyl-silane
A
trimethylsilyl cyanide
B
4-allylbenzonitrile
Conditions | Yield |
---|---|
In acetonitrile Irradiation; | A n/a B 66% |
2-propyl thiocyanate
diisopropyl trimethylsily phosphite
A
O,O,S-triisopropyl phosphorothioate
B
trimethylsilyl cyanide
Conditions | Yield |
---|---|
at 100 - 110℃; for 1h; | A 64% B n/a |
at 100 - 110℃; for 1h; Yields of byproduct given; |
Conditions | Yield |
---|---|
With AMBERLITE XAD-4; sodium cyanide In various solvent(s) at 25℃; for 0.5h; | 61% |
With NaCN impregnated on Amberlite XAD-4 In acetonitrile at 60℃; for 1.5h; Product distribution; effect of other reagent, other solvents, reaction time and temperature; | 95 % Chromat. |
phenyl selenocyanate
(trifluoromethyl)trimethylsilane
A
trimethylsilyl cyanide
B
phenyl trifluoromethylselenide
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran 0 deg C, 5 min then rt., 2.5 h; | A n/a B 58% |
4-nitrophenyl thiocyanate
(trifluoromethyl)trimethylsilane
A
trimethylsilyl cyanide
B
p-nitrophenyl trifluoromethyl sulfide
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran 0 deg C, 5 min then rt., 2.5 h; | A n/a B 58% |
2-methallyltrimethylsilane
phthalonitrile
A
trimethylsilyl cyanide
B
2-(2-methyl-2-propenyl)benzonitrile
Conditions | Yield |
---|---|
In acetonitrile Irradiation; | A n/a B 44% |
Conditions | Yield |
---|---|
150 to 200 deg C; | 42% |
thiocyanatocyclohexane
(trifluoromethyl)trimethylsilane
A
trimethylsilyl cyanide
B
cyclohexyl(trifluoromethyl)sulfane
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran 0 deg C, 5 min then rt., 2.5 h; | A n/a B 33% |
1-methyl-1H-pyrrol-2-yl thiocyanate
(trifluoromethyl)trimethylsilane
A
1-methyl-2-trifluoromethylsulfanyl-pyrrole
B
trimethylsilyl cyanide
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran 0 deg C, 5 min then rt., 2.5 h; | A 32% B n/a |
(trifluoromethyl)trimethylsilane
A
trimethylsilyl cyanide
B
2,4-dimethoxy-1-[(trifluoromethyl)sulfanyl]benzene
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran 0 deg C, 5 min then rt., 2.5 h; | A n/a B 30% |
Conditions | Yield |
---|---|
With lithium | |
(i) LiH, ether, (ii) /BRN= 1209232/; Multistep reaction; |
trimethylsilyl cyanide
cyclohexanone
1-trimethylsilanyloxycyclohexanecarbonitrile
Conditions | Yield |
---|---|
In 1-methyl-pyrrolidin-2-one at 20℃; for 4h; Inert atmosphere; | 100% |
With MgAlCO3-HT In n-heptane for 0.0833333h; Ambient temperature; | 99% |
With tris(2-hydroxyethyl)amine-N-oxide; N-benzyl-N,N-dimethylphenylmethylammonium bromide In dichloromethane at 23℃; for 16h; | 99% |
trimethylsilyl cyanide
4-nitrobenzaldehdye
2-(4-nitrophenyl)-2-[(trimethylsilyl)oxy]acetonitrile
Conditions | Yield |
---|---|
With 2Zn(2+)*10H2O*3C10H8N2*2H(1+)*Co2Mo10H4O38(6-) In neat (no solvent) at 25℃; for 7h; Reagent/catalyst; Inert atmosphere; | 100% |
With C42H50Mg2N4 In benzene-d6 at 25℃; Glovebox; Inert atmosphere; | 99% |
With cobalt incorporated covalent organic framework of 2,3-dihydroxyterephthalohydrazide with triformylphloroglucinol (NUS-51-Co) In dichloromethane at 24.84℃; for 10h; Catalytic behavior; | 99% |
trimethylsilyl cyanide
benzaldehyde
phenyl(trimethylsiloxy)acetonitrile
Conditions | Yield |
---|---|
tris(bis(trimethylsilyl)amido)samarium(III) In tetrahydrofuran at 0℃; for 4h; | 100% |
With lithium tetrafluoroborate In acetonitrile at 20℃; for 2h; | 100% |
iron(III) chloride In nitromethane at 0℃; for 0.5h; | 100% |
trimethylsilyl cyanide
acetaldehyde
2-<(trimethylsilyl)oxy>propanenitrile
Conditions | Yield |
---|---|
With Zr(IV) metal-organic framework with 1,4-benzenedicarboxylate in anhydrous form In dichloromethane at 40℃; for 46h; Inert atmosphere; Reflux; | 100% |
With Eu2(benzene-1,2,3,4,5,6-hexacarboxylate)(H2O)3 In acetonitrile at 20 - 100℃; for 3h; | 99% |
With Mn(5-((4-(tetrazol-5-yl)benzyl)oxy)isophthalic acid)2(H2O)2 In neat (no solvent) at 20℃; Catalytic behavior; Reagent/catalyst; | 99% |
trimethylsilyl cyanide
propionaldehyde
2-<(trimethylsilyl)oxy>butanenitrile
Conditions | Yield |
---|---|
With trans-{(iBu)2ATIGeiPr}2Pt(CN)2 In chloroform-d1 at 50℃; for 2h; Catalytic behavior; Schlenk technique; Glovebox; | 100% |
With C29H38AlN4O2(1+)*CF3O3S(1-) at 20℃; for 0.0833333h; Catalytic behavior; Inert atmosphere; Schlenk technique; | 99% |
With Mn(5-((4-(tetrazol-5-yl)benzyl)oxy)isophthalic acid)2(H2O)2 In neat (no solvent) at 20℃; Catalytic behavior; Reagent/catalyst; | 99% |
Conditions | Yield |
---|---|
With chloro-trimethyl-silane at 20℃; for 72h; Inert atmosphere; | 100% |
for 168h; Ambient temperature; | 63% |
trimethylsilyl cyanide
cyclododecanone
1-trimethylsilyloxy-1-cyclododecanecarbonitrile
Conditions | Yield |
---|---|
With zinc(II) iodide | 100% |
With lithium perchlorate; tetraethylammonium perchlorate In dichloromethane Ambient temperature; electrolysis: 0.28 F/mol; | 95% |
With n-butyllithium In tetrahydrofuran; hexane for 2h; Ambient temperature; | 90.6% |
With zinc(II) iodide |
1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose
trimethylsilyl cyanide
2,3,5-tri-O-benzoyl-β-D-ribofuranosyl-1-carbonitrile
Conditions | Yield |
---|---|
With tin(IV) chloride | 100% |
With trimethylsilyl trifluoromethanesulfonate In dichloromethane at 20℃; stereoselective reaction; | 100% |
With boron trifluoride diethyl etherate In nitromethane Ambient temperature; | 87% |
Conditions | Yield |
---|---|
With isopropoxydiisobutylaluminum In hexane Product distribution; Ambient temperature; other oxiranes; var. Lewis acids; var. solvents; var. temperatures; | 100% |
With aluminum isopropoxide 1.) RT, 2 h, 2.) RT, 15 h; Yield given. Multistep reaction; |
trimethylene oxide
trimethylsilyl cyanide
4-<(trimethylsilyl)oxy>butyronitrile
Conditions | Yield |
---|---|
With diethylaluminium chloride for 18h; Ambient temperature; | 100% |
furfural
trimethylsilyl cyanide
2-(2-furyl)-2-(trimethylsilyloxy)acetonitrile
Conditions | Yield |
---|---|
With Eu2(benzene-1,2,3,4,5,6-hexacarboxylate)(H2O)3 In acetonitrile at 20 - 100℃; for 1h; | 100% |
With 1-methoxy-2-methyl-1-(trimethylsiloxy)propene at 19℃; for 10h; | 99% |
With potassium phtalimide at 20℃; for 1.16667h; solvent-free; | 99% |
4-methylpyridine-1-oxide
trimethylsilyl cyanide
2-Cyano-4-methylpyridin
Conditions | Yield |
---|---|
With N,N-Dimethylcarbamoyl chloride In dichloromethane for 120h; Ambient temperature; | 100% |
Stage #1: 4-methylpyridine-1-oxide; trimethylsilyl cyanide With N,N-Dimethylcarbamoyl chloride In dichloromethane at 20℃; for 24h; Stage #2: With potassium carbonate In dichloromethane; water for 0.5h; | 96% |
With triethylamine In acetonitrile at 100 - 110℃; for 20h; | 89% |
2-methylpyridine N-oxide
trimethylsilyl cyanide
2-Cyano-6-methylpyridine
Conditions | Yield |
---|---|
With N,N-Dimethylcarbamoyl chloride In dichloromethane for 120h; Ambient temperature; | 100% |
With dimethylcarbamide chloride In dichloromethane at 20℃; for 24h; | 98% |
With N,N-Dimethylcarbamoyl chloride In Nitroethane at 20℃; for 22h; | 28% |
3-methyl-butan-2-one
trimethylsilyl cyanide
2,3-dimethyl-2-((trimethylsilyl)oxy)butanenitrile
Conditions | Yield |
---|---|
With trans-{(iBu)2ATIGeiPr}2Pt(CN)2 In chloroform-d1 at 50℃; for 6h; Catalytic behavior; Schlenk technique; Glovebox; | 100% |
With C29H38AlN4O2(1+)*CF3O3S(1-) In neat (no solvent) at 20℃; for 0.0833333h; Catalytic behavior; Inert atmosphere; Schlenk technique; | 99% |
With C48H40N8Sm(1-)*C16H32LiO4(1+) at 20℃; for 4h; Inert atmosphere; Schlenk technique; | 99% |
(E)-3-phenylpropenal
trimethylsilyl cyanide
(E)-4-phenyl-2-(trimethylsiloxy)but-3-enenitrile
Conditions | Yield |
---|---|
With zinc(II) iodide In dichloromethane at 20℃; for 2h; Addition; | 100% |
With 1-methoxy-2-methyl-1-(trimethylsiloxy)propene at 19℃; for 36h; | 99% |
With tin-tungsten mixed oxide, Sn/W molar ratio = 2, calcined at 800 °C In 1,2-dichloro-ethane at 22 - 23℃; for 1h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With aluminium trichloride In dichloromethane | 100% |
1,3-Benzothiazole
trimethylsilyl cyanide
benzoyl chloride
3-benzoyl-2,3-dihydro-2-benzothiazolecarbonitrile
Conditions | Yield |
---|---|
With aluminium trichloride In dichloromethane other aroyl chlorides; | 100% |
With aluminium trichloride In dichloromethane | 100% |
With aluminium trichloride In dichloromethane for 72h; Ambient temperature; | 50% |
With aluminium trichloride In dichloromethane | 44% |
1,3-Benzothiazole
trimethylsilyl cyanide
4-methyl-benzoyl chloride
2,3-dihydro-3-(4-methylbenzoyl)-2-benzothiazolecarbonitrile
Conditions | Yield |
---|---|
With aluminium trichloride In dichloromethane | 100% |
With aluminium trichloride In dichloromethane for 72h; Ambient temperature; | 87% |
With aluminium trichloride In dichloromethane for 72h; Ambient temperature; | 86% |
Conditions | Yield |
---|---|
With aluminium trichloride In dichloromethane | 100% |
Conditions | Yield |
---|---|
With aluminium trichloride In dichloromethane | 100% |
4-tert-butylpyridine N-oxide
trimethylsilyl cyanide
4-tert-butyl-2-cyanopyridine
Conditions | Yield |
---|---|
With N,N-Dimethylcarbamoyl chloride In dichloromethane at 20℃; | 100% |
With triethylamine In acetonitrile at 100℃; for 25h; | 97% |
With N,N-Dimethylcarbamoyl chloride In dichloromethane for 24h; Ambient temperature; | |
With N,N-Dimethylcarbamoyl chloride In dichloromethane cyanidation; |
glyoxylic acid ethyl ester
trimethylsilyl cyanide
(+/-)-ethyl 2-cyano-2-hydroxyacetate
Conditions | Yield |
---|---|
With sodium acetate buffer In ethanol; water for 0.166667h; Ambient temperature; | 100% |
With sodium acetate; acetic acid In ethanol for 0.166667h; Ambient temperature; | 1.29 g |
Stage #1: glyoxylic acid ethyl ester With copper(II) bis(trifluoromethanesulfonate) In dichloromethane at 20℃; for 0.25h; Stage #2: trimethylsilyl cyanide In dichloromethane at 20℃; for 18h; |
Conditions | Yield |
---|---|
In dichloromethane for 18h; | 100% |
Carvone
trimethylsilyl cyanide
5-Isopropenyl-2-methyl-3-trimethylsilanyloxy-cyclohex-2-enecarbonitrile
Conditions | Yield |
---|---|
With triethylaluminum In tetrahydrofuran for 6h; Heating; | 100% |
Conditions | Yield |
---|---|
With [Sc3(3,5-disulfobenzoic acid)2(μ-O2H3)(μ-OH)2(H2O)2] In neat (no solvent) at 40℃; for 2h; Catalytic behavior; Schlenk technique; Inert atmosphere; | 100% |
With 2Zn(2+)*10H2O*3C10H8N2*2H(1+)*Co2Mo10H4O38(6-) In neat (no solvent) at 25℃; for 7h; Reagent/catalyst; Inert atmosphere; | 100% |
With tin-tungsten mixed oxide, Sn/W molar ratio = 2, calcined at 800 °C In 1,2-dichloro-ethane at 22 - 23℃; for 0.5h; Inert atmosphere; | 99% |
hexan-1-amine
trimethylsilyl cyanide
4,4'-[decane-1,10-diylbis(oxy)]dibenzaldehyde
(4-{10-[4-(Cyano-hexylamino-methyl)-phenoxy]-decyloxy}-phenyl)-hexylamino-acetonitrile
Conditions | Yield |
---|---|
In dichloromethane for 120h; | 100% |
trimethylsilyl cyanide
3-oxo-propionic acid ethyl ester
(+/-)-ethyl 3-cyano-3-hydroxypropionate
Conditions | Yield |
---|---|
With sodium hydroxide; acetic acid In ethanol; water | 100% |
With sodium acetate buffer In ethanol; water for 1h; Ambient temperature; | 98% |
trimethylsilyl cyanide
1-Adamantanecarbaldehyde
adamantan-1-yltrimethylsilanyloxy-acetonitrile
Conditions | Yield |
---|---|
With zinc(II) iodide | 100% |
With zinc(II) iodide In dichloromethane at 0℃; for 1h; | 75.3% |
With zinc(II) iodide at 20℃; for 150h; | |
With zinc(II) iodide In chloroform for 1h; |
trimethylsilyl cyanide
bicyclo[3.3.1]nonane-2,6-dione
2,6-Bis(trimethylsilyloxy)bicyclo<3.3.1>nonan-2,6-dicarbonitril
Conditions | Yield |
---|---|
With zinc(II) iodide In dichloromethane at 40℃; for 0.5h; | 100% |
trimethylsilyl cyanide
5-Methoxy-1-tetralone
1-cyano-1-(trimethylsilyloxy)-5-methoxy-1,2,3,4-tetrahydronaphthalene
Conditions | Yield |
---|---|
With zinc(II) iodide In benzene at 25℃; for 3h; | 100% |
With zinc(II) iodide for 48h; Ambient temperature; | |
With zinc(II) iodide |
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