Factory direct production Hangzhou Verychem Science And Technology Co. Ltd. was set up in year 2004, it’s a young but fast growing company. In the twelve years history, it invested two pharmaceutical raw material production plants, one resea
Cas:14371-10-9
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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
Cas:14371-10-9
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Shanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
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inquirytrans-Cinnamaldehyde Basic information Product Name: trans-Cinnamaldehyde Synonyms: CINNAMALDEHYDE, TRANS-;FEMA 2286;LABOTEST-BB LT00939010;AKOS B004060;AKOS BBS-00003207;3-PHENYLPROPENA
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:14371-10-9
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inquirytrans-Cinnamaldehyde CAS:14371-10-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic int
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryProduct Detail Minimum Order Qty. 10 Gram
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Min.Order:20 Metric Ton
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inquiryProduct quality: Our company have high quality product , and also the product we have good manufacture . First of all, this product is of fine quality. Every finish should be checked by quality inspection system.And every one should be also tried
Cas:14371-10-9
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inquiryOur Advantage 1. Rich experience We specialize in this filed for many years, our APIs exported to all over the world and and we established long friendly relations of cooperation with our clients. 2. Great quality,purity and favorable Good qual
Cas:14371-10-9
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inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
Cas:14371-10-9
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Nanjing Spring & Autumn Biological Engineering Co., Ltd. Which was founded at 2008, has an R & D team composed very experienced natural products chemists. The company is a high-tech enterprise engaged in functional health care products raw ma
Cas:14371-10-9
Min.Order:500 Gram
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Type:Lab/Research institutions
inquiryWhy Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu
Specification: Our advantages: Name trans-Cinnamaldehyde EINECS 203-213-9 CAS No. 14371-10-9 Density 1.035 g/cm3 PSA 17.07000 LogP 1.89870 Solubility 1.1 g/L (20 °C)
Cas:14371-10-9
Min.Order:10 Gram
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:14371-10-9
Min.Order:10 Gram
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inquiryProduct name Cinnamic aldehyde Cas No. 104-55-2/14371-10-9 Fema No. 2286 Molecular Formula C9H8O Structural Formula
GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
Product Name: trans-Cinnamaldehyde Synonyms: CINNAMALDEHYDE, TRANS-;FEMA 2286;LABOTEST-BB LT00939010;AKOS B004060;AKOS BBS-00003207;3-PHENYLPROPENAL;trans-3-Phenylacrolein trans-3-Phenylacrylaldehyde trans-3-Phenyl-2-propenal;trans-CinnaMaldehy
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Min.Order:1 Gram
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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Min.Order:1 Kilogram
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inquiryHangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
(2E)-3-phenyl-2-propen-1-ol
(E)-3-phenylpropenal
Conditions | Yield |
---|---|
With 3-methyl-5-deaza-10-oxaflavin; toluene-4-sulfonic acid In 1,4-dioxane for 1h; Product distribution; Heating; other 3-methyl-5-deaza-10-oxaflavins; other alcohols; | 100% |
With manganese(IV) oxide In hexane for 2h; Ambient temperature; | 100% |
With molecular sieve; In dichloromethane for 0.5h; Ambient temperature; | 100% |
5-phenyl-4,5-dihydro-1H-pyrazole
(E)-3-phenylpropenal
Conditions | Yield |
---|---|
With benzeneseleninic anhydride In dichloromethane for 4h; Ambient temperature; | 100% |
(E)-cinnamaldehyde dimethylacetal
(E)-3-phenylpropenal
Conditions | Yield |
---|---|
With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone In acetonitrile for 1h; Ambient temperature; | 100% |
With polymer-supported dicyanoketene acetal; water In acetonitrile at 20℃; for 0.5h; Hydrolysis; | 100% |
With tin(ll) chloride; naphthalene In dichloromethane for 0.0833333h; Ambient temperature; | 99% |
2,3-dibromo-3-phenyl propanal
(E)-3-phenylpropenal
Conditions | Yield |
---|---|
With 1,2-bis(diphenylphosphino)ethane nickel(II) chloride; tri-n-butyl-tin hydride In tetrahydrofuran for 0.5h; Ambient temperature; | 100% |
2-(trans-styryl)-3-ethyl-1,3-oxazolidine
(E)-3-phenylpropenal
Conditions | Yield |
---|---|
With diazomethane; copper(II) bis(trifluoromethanesulfonate) In diethyl ether; dichloromethane at 5 - 10℃; | 100% |
(2E)-3-phenyl-2-propen-1-ol
benzyl alcohol
A
(E)-3-phenylpropenal
B
benzaldehyde
Conditions | Yield |
---|---|
With potassium carbonate In toluene at 20℃; for 12h; | A 15% B 99% |
3-phenyl-propionaldehyde
(E)-3-phenylpropenal
Conditions | Yield |
---|---|
With oxygen; palladium diacetate; trifluoroacetic acid In dimethyl sulfoxide at 80℃; for 6h; Sealed tube; | 98% |
With 4-methyl-morpholine; bis(benzonitrile)palladium(II) dichloride; silver trifluoromethanesulfonate In tetrahydrofuran; dichloromethane for 12h; Ambient temperature; | 88% |
With 4-methyl-morpholine; bis(benzonitrile)palladium(II) dichloride; silver trifluoromethanesulfonate In tetrahydrofuran; dichloromethane for 12h; Product distribution; Ambient temperature; different aldehydes and reagent; | 88% |
Phenylpropargyl aldehyde
trisodium tris(3-sulfophenyl)phosphine
A
(E)-3-phenylpropenal
B
tris(natrium-m-sulfonatophenyl)phosphanoxid
Conditions | Yield |
---|---|
In water Ambient temperature; | A 98% B n/a |
trans-cinnamaldehyde diethylacetal
(E)-3-phenylpropenal
Conditions | Yield |
---|---|
With nitric acid; acetic anhydride at -50℃; | 98% |
With aluminum oxide; Oxone for 0.0266667h; Hydrolysis; Microwave irradiation; | 89% |
With tin(ll) chloride In dichloromethane for 1h; Ambient temperature; | 84% |
2-[(E)-2-phenylethenyl]-1,3-dioxolane
(E)-3-phenylpropenal
Conditions | Yield |
---|---|
With Ru(CH3CN)3(triphos)(OTf)2 (triphos = CH3C(CH2PPh2)3); acetone for 6h; Ambient temperature; | 98% |
With lithium chloride In water; dimethyl sulfoxide at 90℃; for 6h; | 96% |
With tin(ll) chloride In dichloromethane for 2h; Ambient temperature; other dioxolanes, other acetals and other pyran; | 95% |
(E)-1,1-diacetoxy-3-phenylprop-2-ene
(E)-3-phenylpropenal
Conditions | Yield |
---|---|
With Montmorillonite K10 In dichloromethane for 0.75h; Heating; | 98% |
With aminosulfonic acid In benzene for 0.25h; Heating; | 96% |
With N,N'-dibromo-N,N'-(1,2-ethanediyl)bis(p-toluenesulfonamide); water at 20℃; for 0.0666667h; solid-phase reaction; | 96% |
1-phenylprop-2-ynyl acetate
(E)-3-phenylpropenal
Conditions | Yield |
---|---|
With water; silver hexafluoroantimonate In tetrahydrofuran at 80℃; for 0.2h; Meyer-Schuster rearrangement; microwave irradiation; | 98% |
With toluene-4-sulfonic acid In 1,2-dichloro-ethane at 60℃; for 1h; Meyer-Schuster Rearrangement; stereoselective reaction; | 70% |
With methyl trifluoromethanesulfonate In 2,2,2-trifluoroethanol at 70℃; for 1h; | 65% |
(Z)-cinnamyl alcohol
(E)-3-phenylpropenal
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; 5,6,9,10-tetrahydro-4H,8H-pyrido[3,2,1-ij][1,6]naphthyridine; oxygen; copper(I) bromide In acetonitrile at 20℃; for 16.5h; Schlenk technique; | 98% |
(E)-3-phenylpropenal
Conditions | Yield |
---|---|
With hydrogenchloride for 0.0416667h; Product distribution; Ambient temperature; pH = 4-6, regeneration of aldehyde; | 97.9% |
trans-3-phenylprop-2-enyl chloride
(E)-3-phenylpropenal
Conditions | Yield |
---|---|
With N-ethylmorpholine N-oxide In N,N-dimethyl-formamide r.t., 1 h, 50 deg C, 4 h; | 97% |
With sodium periodate In N,N-dimethyl-formamide at 150℃; for 0.916667h; | 84% |
With ethanol; hexamethylenetetramine | |
Multi-step reaction with 3 steps 1.1: sodium iodide / acetone / 1.5 h / 20 °C 2.1: sodium hydride / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere; Sealed tube 2.2: 6 h / 40 °C / Inert atmosphere 3.1: 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium tetrafluoroborate / dichloromethane; water / 45 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: sodium iodide / acetone / 1.5 h / 20 °C 2.1: sodium hydride / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere; Sealed tube 2.2: 6 h / 40 °C / Inert atmosphere 3.1: 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium tetrafluoroborate / dichloromethane; water / 45 °C View Scheme |
Conditions | Yield |
---|---|
With hydrogenchloride; aluminum isopropoxide In ethyl acetate; benzene | 97% |
allylbenzene
(E)-3-phenylpropenal
Conditions | Yield |
---|---|
With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium dichloride In 1,2-dichloro-ethane at 50℃; for 2h; stereoselective reaction; | 96% |
With water; oxygen; palladium diacetate In dimethyl sulfoxide at 100℃; under 760.051 Torr; for 24h; Reagent/catalyst; Solvent; Green chemistry; regioselective reaction; | 85% |
With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone In 1,2-dichloro-ethane at 60℃; for 10h; | 76% |
2-styryl-1,3-dithiane
(E)-3-phenylpropenal
Conditions | Yield |
---|---|
With silica gel; ferric nitrate In hexane at 50℃; for 0.166667h; | 96% |
With p-iodoxybenzoic acid In dimethyl sulfoxide at 25℃; for 0.75h; | 91% |
With Amberlite IR-120; palladium on activated charcoal In methanol for 36h; Heating; | 74% |
With Dimethoxymethane; oxalic acid In nitromethane at 60℃; for 25h; | 67% |
With Dess-Martin periodane In dichloromethane; water; acetonitrile at 20℃; for 1h; |
Dimethoxymethane
A
(E)-3-phenylpropenal
B
1-dodecylsulfanylmethylsulfanyldodecane
Conditions | Yield |
---|---|
With oxalic acid In nitromethane at 60℃; for 14h; | A 95% B 96% |
Conditions | Yield |
---|---|
Stage #1: tris(ethoxyvinyl)borane With diethylzinc In toluene at -78℃; for 0.333333h; Inert atmosphere; Stage #2: benzaldehyde In toluene at -78 - 20℃; for 14h; Inert atmosphere; Stage #3: With hydrogenchloride; water In diethyl ether; toluene at 0℃; pH=> 4; Inert atmosphere; | 96% |
1-Phenyl-2-propyn-1-ol
(E)-3-phenylpropenal
Conditions | Yield |
---|---|
With trifluoroacetic acid; [Ru(η3-2-C3H4Me)(CO)(1,1'-(Ph2P)2-ferrocene)][SbF6] In tetrahydrofuran for 3.5h; Meyer-Schuster rearrangement; Heating; | 95% |
With [Re(κ3-P,N,S-Ph2PCH2P{=NP(=S)(OPh)2}Ph2)(CO)3]SbF6 at 80℃; for 0.25h; Catalytic behavior; Time; Meyer-Schuster Rearrangement; Inert atmosphere; Schlenk technique; | 93% |
With [Re(κ3-P,N,S-Ph2PCH2P{=NP(=S)(OPh)2}Ph2)(CO)3]SbF6 In tetrahydrofuran at 80℃; for 0.0833333h; Meyer-Schuster rearrangement; Microwave irradiation; Inert atmosphere; regioselective reaction; | 92% |
Conditions | Yield |
---|---|
With magnesium(II) perchlorate; water; methylene green In acetonitrile Irradiation; | A n/a B 95% |
With magnesium(II) perchlorate; water; methylene green In acetonitrile Mechanism; Irradiation; various dithio derivatives; | A n/a B 95% |
1-(tert-butyldimethylsilyloxy)-3-phenyl-2-propene
(E)-3-phenylpropenal
Conditions | Yield |
---|---|
With dioxochloro(trimethylsiloxy)chromate(VI) In dichloromethane for 1h; | 95% |
With quinolinium monofluorochromate(VI) In dichloromethane; N,N-dimethyl-formamide for 15h; Ambient temperature; | 66% |
(E)-2-(2-phenylethenyl)-1,3-dithiolane
(E)-3-phenylpropenal
Conditions | Yield |
---|---|
With silica gel; ferric nitrate In hexane at 50℃; for 0.166667h; | 95% |
With cerium(III) chloride; sodium iodide In acetonitrile for 3.5h; Heating; | 93% |
With iron(III) chloride; potassium iodide In methanol for 3h; Heating; | 90% |
With Oxone; potassium bromide In water; acetonitrile at 20℃; for 0.25h; | 78% |
With O-phenyl phosphorodichloridate; N,N-dimethyl-formamide; sodium iodide 1.) acetonitrile, few min, room temp., 2.) 5 h, room temp.; Yield given. Multistep reaction; |
2-styryl-1,3-oxathiolane
(E)-3-phenylpropenal
Conditions | Yield |
---|---|
With trimethylsilyl trifluoromethanesulfonate; nitrobenzaldehyde polymer In dichloromethane for 2h; Ambient temperature; | 95% |
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; β‐cyclodextrin In water; acetone at 20℃; for 0.333333h; | 90% |
With 4-nitrobenzaldehdye; trimethylsilyl trifluoromethanesulfonate In dichloromethane for 0.0833333h; Ambient temperature; | 75% |
(E)-3-phenylpropenal
Conditions | Yield |
---|---|
With triethylamine In dichloromethane | 95% |
Phenylpropargyl aldehyde
(E)-3-phenylpropenal
Conditions | Yield |
---|---|
With Pd3Pb/SiO2; RhSb/SiO2; hydrogen In tetrahydrofuran at 25℃; under 760.051 Torr; for 4.3h; | 94% |
With water; triphenylphosphine; benzoic acid In tetrahydrofuran at 65℃; for 24h; diastereoselective reaction; | 87% |
With palladium on activated charcoal; ethanol Hydrogenation; | |
With TPPMS (meta-monosulfonated triphenylphosphane, Na salt); water for 1h; | |
With hydrogen; silica gel In (2)H8-toluene at 100℃; under 3800.26 Torr; for 15h; diastereoselective reaction; | n/a |
Conditions | Yield |
---|---|
With p-CO2H-IBX In N,N-dimethyl-formamide at 55 - 60℃; for 4h; | A 5% B 94% |
2-styryl-1,3-dithiane-1-oxide
(E)-3-phenylpropenal
Conditions | Yield |
---|---|
With hydrogenchloride In water; acetonitrile at 20℃; for 12h; | 94% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 0 - 20℃; for 16h; | 100% |
In diethyl ether at 0 - 20℃; for 8h; | 39% |
With diethyl ether |
(E)-3-phenylpropenal
3-Phenyl-1-propanol
Conditions | Yield |
---|---|
With sodium aluminum tetrahydride In tetrahydrofuran at 0℃; for 0.0833333h; | 100% |
With baker's yeast; D-glucose; resin XAD 1180 In water at 28℃; for 24h; | 100% |
With (7,8-benzoquinolinato)hydrido(aqua)bis(triphenylphosphine)iridium(III) tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; hydrogen; N-ethyl-N,N-diisopropylamine In toluene at 80℃; under 760.051 Torr; for 4h; | 98% |
(E)-3-phenylpropenal
(E)-3-phenylacrylic acid
Conditions | Yield |
---|---|
With cobalt(II) 2,9,16,23-phthalocyanine tetrasulfonic acid In water; acetonitrile at 20℃; under 760.051 Torr; for 150h; UV-irradiation; | 100% |
With oxygen; potassium carbonate; 1,3-bis(mesityl)imidazolium chloride In water; N,N-dimethyl-formamide at 25℃; for 16h; | 99% |
With sodium chlorite; sodium dihydrogenphosphate; dihydrogen peroxide In toluene at 10℃; for 1h; Product distribution; var. solvents; other reaction partners; other aldehydes; | 95% |
(E)-3-phenylpropenal
(2E)-3-phenyl-2-propen-1-ol
Conditions | Yield |
---|---|
With sodium aluminum tetrahydride In tetrahydrofuran at 0℃; for 0.0833333h; | 100% |
With Zn(BH4)2(Ph3P)2 In tetrahydrofuran for 0.4h; Reduction; Heating; | 100% |
With borohydride Ultra resin In methanol at 20℃; for 4h; | 100% |
(E)-3-phenylpropenal
ethyl acetoacetate
2-oxo-6-phenyl-cyclohex-3-enecarboxylic acid ethyl ester
Conditions | Yield |
---|---|
In ethanol | 100% |
With ethanol; sodium ethanolate at -10℃; |
(E)-3-phenylpropenal
phenylacetylene
(1E)-1,5-diphenylpent-1-en-4-yn-3-ol
Conditions | Yield |
---|---|
Stage #1: phenylacetylene With ethylmagnesium bromide In tetrahydrofuran at 50℃; for 1h; Stage #2: (E)-3-phenylpropenal In tetrahydrofuran at 23 - 25℃; for 3h; Further stages.; | 100% |
Stage #1: phenylacetylene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.166667h; Stage #2: (E)-3-phenylpropenal In tetrahydrofuran; hexane at -78℃; for 1h; Further stages.; | 97% |
Stage #1: phenylacetylene With n-butyllithium In tetrahydrofuran; pentane at -78℃; Stage #2: (E)-3-phenylpropenal In tetrahydrofuran; pentane at -78℃; | 89% |
(E)-3-phenylpropenal
ethyl 2-cyanoacetate
(2E,4E)-2-cyano-5-phenyl-2,4-pentadienoic acid ethyl ester
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane In neat liquid at 20℃; for 0.25h; Knoevenagel Condensation; Green chemistry; | 100% |
With zinc(II) chloride at 100℃; for 1.5h; | 92% |
With 1-methyl-piperazine at 25 - 30℃; for 0.166667h; Knoevenagel condensation; | 91% |
(E)-3-phenylpropenal
2-Methoxypropene
[(E)-5-Methoxy-3-(1-methoxy-1-methyl-ethoxy)-hexa-1,5-dienyl]-benzene
Conditions | Yield |
---|---|
With tris(6,6,7,7,8,8,8-heptafluoro-2,2-dimethyl-3,5-octanedionato)ytterbium; acetic acid In dichloromethane for 18h; Ambient temperature; | 100% |
With tris(6,6,7,7,8,8,8-heptafluoro-2,2-dimethyl-3,5-octanedionato)ytterbium; silica gel; acetic acid at 25℃; | 83% |
With silica gel; acetic acid; tris(6,6,7,7,8,8,8-heptafluoro-2,2-dimethyl-3,5-octanedionato)ytterbium In dichloromethane at 25℃; Addition; | 83% |
(E)-3-phenylpropenal
trimethylsilyl cyanide
(E)-4-phenyl-2-(trimethylsiloxy)but-3-enenitrile
Conditions | Yield |
---|---|
With zinc(II) iodide In dichloromethane at 20℃; for 2h; Addition; | 100% |
With 1-methoxy-2-methyl-1-(trimethylsiloxy)propene at 19℃; for 36h; | 99% |
With tin-tungsten mixed oxide, Sn/W molar ratio = 2, calcined at 800 °C In 1,2-dichloro-ethane at 22 - 23℃; for 1h; Inert atmosphere; | 99% |
(E)-3-phenylpropenal
2-propylidene malonic acid dimethyl ester
2-[(2E,4E)-2-Methyl-5-phenyl-penta-2,4-dien-(E)-ylidene]-malonic acid monomethyl ester
Conditions | Yield |
---|---|
N-benzyl-trimethylammonium hydroxide In methanol for 24h; Ambient temperature; | 100% |
(E)-3-phenylpropenal
sodium 6-aminohexanoate
Conditions | Yield |
---|---|
In di-isopropyl ether; water for 0.0416667h; Product distribution; Ambient temperature; separation of aldehyde; | 100% |
(E)-3-phenylpropenal
cinnamic nitrile
Conditions | Yield |
---|---|
With trimethylsilylacetylene; zinc(II) chloride In chloroform for 4h; Ambient temperature; | 100% |
With 1-methyl-pyrrolidin-2-one; hydroxylamine hydrochloride at 100℃; for 0.25h; Condensation; microwave irradiation; | 100% |
With hydroxylamine hydrochloride In 1-methyl-pyrrolidin-2-one at 100℃; for 0.0833333h; | 100% |
(E)-3-phenylpropenal
cinnamaldehyde oxime
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride | 100% |
With hydroxylamine hydrochloride; sodium hydroxide In methanol; water at 20℃; for 0.5h; | 90% |
With hydroxylamine hydrochloride; triethylamine In dichloromethane at 25℃; Inert atmosphere; | 85% |
(E)-3-phenylpropenal
4-methoxy-aniline
(E)-4-methoxy-N-((E)-3-phenylallylidene)aniline
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane for 4h; Ambient temperature; | 100% |
With magnesium sulfate In ethyl acetate for 1h; Ambient temperature; | 100% |
In neat (no solvent) for 0.25h; | 100% |
Conditions | Yield |
---|---|
With magnesium sulfate In ethyl acetate at 20℃; Inert atmosphere; | 100% |
Ambient temperature; | 98% |
In toluene for 3.5h; Reflux; | 90% |
(E)-3-phenylpropenal
chloro-trimethyl-silane
phenyllithium
(E)-1,3-diphenyl-1-trimethylsilyloxy-2-propene
Conditions | Yield |
---|---|
Stage #1: (E)-3-phenylpropenal; phenyllithium In tetrahydrofuran at -78℃; for 0.25h; Stage #2: chloro-trimethyl-silane In tetrahydrofuran Further stages.; | 100% |
1) THF, -20 deg C, 15 min; 2) THF, RT, 12 h; Yield given. Multistep reaction; |
(E)-3-phenylpropenal
orthoformic acid triethyl ester
trans-cinnamaldehyde diethylacetal
Conditions | Yield |
---|---|
With lithium tetrafluoroborate In ethanol at 40℃; for 2h; | 100% |
With N-Bromosuccinimide In ethanol at 20℃; for 0.5h; Inert atmosphere; | 97% |
aminosulfonic acid at 25℃; for 2h; | 92% |
(E)-3-phenylpropenal
ethyl iodoacetae
(E)-ethyl 3-hydroxy-5-phenylpent-4-enoate
Conditions | Yield |
---|---|
With indium iodide In tetrahydrofuran for 17h; Ambient temperature; | 100% |
With manganese; copper(l) iodide; trifluoroacetic acid In acetonitrile at 20℃; for 12h; Reformatsky Reaction; Schlenk technique; Inert atmosphere; | 93% |
With indium In tetrahydrofuran for 1.5h; Ambient temperature; | 89% |
(E)-3-phenylpropenal
benzylamine
(E,E)-4-aza-1,5-diphenylpenta-1,3-diene
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane for 0.5h; Heating; | 100% |
With aluminum oxide for 12h; | 100% |
In diethyl ether at 25℃; | 94% |
(E)-3-phenylpropenal
benzylamine
N-((E)-3-phenylallylidene)benzylamine
Conditions | Yield |
---|---|
With 4 A molecular sieve In benzene for 2h; Ambient temperature; | 100% |
In toluene at 23℃; for 36h; Molecular sieve; Inert atmosphere; | 85% |
With 4 A molecular sieve In dichloromethane at 0℃; for 12h; |
(E)-3-phenylpropenal
malononitrile
(E)-2-(3-phenylallylidene)malononitrile
Conditions | Yield |
---|---|
With aluminum oxide Inert atmosphere; Neat (no solvent); | 100% |
With 1,4-diaza-bicyclo[2.2.2]octane In water at 20℃; for 0.0833333h; Knoevenagel Condensation; Green chemistry; | 100% |
With fluorapatite at 20℃; for 1.5h; Knoevenagel condensation; | 98% |
(E)-3-phenylpropenal
Methyltriphenylphosphonium bromide
(E)-1-Phenyl-1,3-butadiene
Conditions | Yield |
---|---|
Stage #1: Methyltriphenylphosphonium bromide With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 0.25h; Inert atmosphere; Stage #2: (E)-3-phenylpropenal In tetrahydrofuran; hexane at 0 - 20℃; Inert atmosphere; | 100% |
Stage #1: Methyltriphenylphosphonium bromide With n-butyllithium In tetrahydrofuran; cyclohexane at 0℃; for 0.25h; Stage #2: (E)-3-phenylpropenal In tetrahydrofuran; cyclohexane at 0 - 20℃; for 2h; Wittig olefination; | 96% |
Stage #1: Methyltriphenylphosphonium bromide In tetrahydrofuran; hexane at 0℃; for 0.25h; Inert atmosphere; Stage #2: (E)-3-phenylpropenal In tetrahydrofuran; hexane at 0 - 20℃; for 10h; Inert atmosphere; | 96% |
(E)-3-phenylpropenal
allyltributylstanane
(E)-1-phenyl-1,5-hexadien-3-ol
Conditions | Yield |
---|---|
With maleic acid at 20℃; for 2h; | 100% |
(S)-Tol-BINAP*AgNO3 In ethanol; water at -40℃; for 20h; Alkylation; | 98% |
With tin(ll) chloride In acetonitrile for 1h; | 97% |
(E)-3-phenylpropenal
5-Trimethylsilanyl-4-trimethylsilanylmethyl-pent-3-enylamine
[(E)-3-Phenyl-prop-2-en-(E)-ylidene]-(5-trimethylsilanyl-4-trimethylsilanylmethyl-pent-3-enyl)-amine
Conditions | Yield |
---|---|
With 4 A molecular sieve In tetrahydrofuran Ambient temperature; | 100% |
(E)-3-phenylpropenal
N,N'-diacetylpiperazin-2,5-dione
Conditions | Yield |
---|---|
With potassium In toluene for 0.0333333h; Irradiation; | 100% |
(E)-3-phenylpropenal
hexa-2,4-dienyl bromide
Conditions | Yield |
---|---|
With indium In N,N-dimethyl-formamide at 0℃; for 3h; | 100% |
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