Dayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantiti
Cas:111-26-2
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:111-26-2
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
inquiryProperties Hexylamine is a kind of water-white liquid with an amine-like odor. Flash point 85°F. Boiling point 132°F. Less dense than water and poorly soluble in swater. Hence floats on water. May be toxic by inhalation, ingestion or ski
high quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Henan Tianfu Chemical Co., Ltd. is located in Zhengzhou High-tech Development Zone with import and export license. We passed ISO 9001:2008 in 2009, and won "High-tech Enterprise" by provincial government in 2013.The objective of the com
Cas:111-26-2
Min.Order:1 Gram
FOB Price: $1000.0
Type:Lab/Research institutions
inquiryECNumber 203-851-8 BeilsteinRegistryNumber 1731298 Description Solubility:14 g/l (20°C). BP
Cas:111-26-2
Min.Order:5 Metric Ton
FOB Price: $1.0 / 2.0
Type:Other
inquiryHexylamine CAS:111-26-2 Specification properties hexylamine is a kind of water-white liquid with an amine-like odor. flash point 85°f. boiling point 132°f. less dense than water and poorly soluble in swater. hence floats on water. may be
Cas:111-26-2
Min.Order:1 Kilogram
FOB Price: $100.0 / 150.0
Type:Other
inquiryPrice, service, company and transport advantage: 1.place of origin china with super quality by reasonable price. 2.fast delivery by safe express way to all the country. 3.has a number of highly qualified engineers and experts to p
Cas:111-26-2
Min.Order:100 Gram
Negotiable
Type:Trading Company
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
We are leading fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...)
Cas:111-26-2
Min.Order:1 Kilogram
FOB Price: $5.0
Type:Lab/Research institutions
inquiry★.Best quality according to requirement ★.Competitive price in China market ★.Mature Technical support ★.Professional logistic support ★.Shortest delivery time . Appearance:Colorless liquid with ammonia flavor Storage:Store in dry, cool and ventilate
Cas:111-26-2
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates
stable supply&competitive price Storage:Available Package:25KG Or as client requirement Application:Important pharm intermediate Transportation:By air or By sea
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:111-26-2
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiryHexylamineAppearance:colourless liquid Storage:room temperature Package:as required Application:111-26-2 Transportation:by sea/ by express
Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi
Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home an
1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
Cas:111-26-2
Min.Order:10 Milligram
Negotiable
Type:Lab/Research institutions
inquiryHenan Sunlake Enterprise Corporation Our Advantages 1, Any inquiry about ch
Product Name Hexylamine Synonyms Hexylamine;1-Aminohexane CAS: 111-26-2 MF: - MW: - EINECS: - Produc
Cas:111-26-2
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryChangzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and fa
1. Factory steady offer directly; 2. More than 10 years of production and process improved experience; 3. Professional hazard chemical Logistics; 4. Reliable quality assurance 5. Punctual delivery time Appearance:A colorless clear liquid wi
Conditions | Yield |
---|---|
With carbon monoxide; Au/TiO2-VS; water In ethanol at 25℃; under 3800.26 Torr; for 5.5h; Autoclave; chemoselective reaction; | 100% |
With trichlorosilane; N-ethyl-N,N-diisopropylamine In acetonitrile at 15℃; for 18h; | 100% |
With 5%-palladium/activated carbon; hydrogen In para-xylene; isopropyl alcohol at 25℃; under 760.051 Torr; Reagent/catalyst; Temperature; | 100% |
Conditions | Yield |
---|---|
With triethylamine alane In tetrahydrofuran for 0.5h; Ambient temperature; | 96.5% |
With hydrogen; aluminum oxide; silica gel; nickel In methanol; ammonia at 160℃; under 7600 Torr; for 1h; | 95% |
With palladium; hydrogen In ethanol at 50℃; under 3750.38 Torr; for 24h; Temperature; | 90% |
Conditions | Yield |
---|---|
With C25H19BrMnN2O2P; potassium tert-butylate; hydrogen In tetrahydrofuran at 130℃; under 22502.3 Torr; for 48h; Inert atmosphere; Glovebox; Autoclave; Green chemistry; | A 95% B 90% |
With [Ru(PtBuNNHtBu)H(CO)Cl]; potassium tert-butylate; hydrogen In tetrahydrofuran at 110℃; under 15001.5 Torr; for 24h; Autoclave; |
Conditions | Yield |
---|---|
With triethylamine alane In tetrahydrofuran for 48h; Ambient temperature; | 93% |
With hydrogen; hexarhodium hexadecacarbonyl; decacarbonyldirhenium(0) In 1,2-dimethoxyethane; diethylamine at 180℃; under 76000 Torr; for 8h; | 76% |
With sodium tetrahydroborate; methanesulfonic acid In dimethyl sulfoxide | 74% |
Conditions | Yield |
---|---|
With formiate d'ammonium; palladium on activated charcoal In methanol Ambient temperature; | 93% |
With formiate d'ammonium; palladium on activated charcoal In methanol Product distribution; Ambient temperature; | 93% |
With sodium tetrahydroborate; lithium chloride In tetrahydrofuran at 0 - 35℃; for 0.5h; | 90% |
Conditions | Yield |
---|---|
With hydrogen; aluminum oxide; carbon monoxide In cyclohexane at 120℃; under 152000 Torr; for 2.73333h; | A 91% B 9% |
With ammonium hydroxide; chloro(1,5-cyclooctadiene)rhodium(I) dimer; hydrogen at 100℃; under 20686.5 Torr; for 24h; Autoclave; Green chemistry; chemoselective reaction; |
Conditions | Yield |
---|---|
With ammonium formate In toluene at 80℃; for 4h; Reagent/catalyst; Inert atmosphere; chemoselective reaction; | 91% |
With ammonium hydroxide; ammonium acetate; hydrogen; [Ru(cod)Cl]2; trisodium tris(3-sulfophenyl)phosphine In toluene at 145℃; under 48754.9 Torr; for 10h; | 45 % Chromat. |
Multi-step reaction with 3 steps 1: 1,4-dioxane / 0.5 h / 60 °C / Inert atmosphere 2: copper(l) iodide; caesium carbonate / 1,4-dioxane / 3.5 h / 110 °C / Inert atmosphere 3: hydrazine hydrate / 1,4-dioxane / 110 °C / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
With hydrogen; Pt/Al2O3 In cyclohexane at 120℃; under 152000 Torr; for 2.66667h; | A 5.6% B 89% C 5.4% |
With hydrogen; aluminum oxide; nickel In cyclohexane at 120℃; under 152000 Torr; for 0.416667h; Product distribution; variation of temperature, time, catalyst; | A 57.5% B 41.3% C 1.2% |
hexylcarbamic acid tert-butyl ester
hexan-1-amine
Conditions | Yield |
---|---|
With nitric acid In dichloromethane at 0℃; for 1h; | 89% |
N-hexylphthalimide
hexan-1-amine
Conditions | Yield |
---|---|
With hydrazine hydrate In 1,4-dioxane at 110℃; Gabriel Amine Synthesis; Inert atmosphere; | 84% |
With potassium hydroxide; sodium hydroxide at 200 - 280℃; Yield given; |
Conditions | Yield |
---|---|
With indium(III) chloride; sodium tetrahydroborate In tetrahydrofuran at 25℃; for 4h; Inert atmosphere; | 76% |
hexanoic acid
A
hexane
B
hexan-1-amine
C
dihexylamine
D
Caproamide
E
N-(n-hexyl)hexanamide
Conditions | Yield |
---|---|
Stage #1: hexanoic acid With cyclopentyl methyl ether; ammonia at 200℃; under 4500.45 Torr; Sealed tube; Green chemistry; Stage #2: With cyclopentyl methyl ether; ammonia; hydrogen at 200℃; under 42004.2 Torr; for 6.5h; Cooling with ice; Green chemistry; | A n/a B 75% C 13% D n/a E 6% |
Conditions | Yield |
---|---|
With 5%-palladium/activated carbon; hydrogen In para-xylene; isopropyl alcohol at 25℃; under 760.051 Torr; for 4h; Reagent/catalyst; | A 26% B 72% |
With 5%-palladium/activated carbon; hydrogen In isopropyl alcohol at 20℃; under 750.075 Torr; for 2h; | A 6 %Spectr. B 94 %Spectr. |
hexylboronic acid
hexan-1-amine
Conditions | Yield |
---|---|
With N-Bromosuccinimide; CYANAMID; bis-[(trifluoroacetoxy)iodo]benzene In acetonitrile at 20℃; for 2h; chemoselective reaction; | 72% |
With N-Bromosuccinimide; N-methoxylamine hydrochloride; bis-[(trifluoroacetoxy)iodo]benzene In acetonitrile at 20℃; for 3h; | 65% |
1-hexyl-dimethylborane
hexan-1-amine
Conditions | Yield |
---|---|
With ammonium hydroxide; sodium hypochlorite In water 1.) 0 deg C, 5-10 min, 2.) 0 deg C -> room temperature; | 67% |
Conditions | Yield |
---|---|
With cobalt nanoparticles anchoring on nitrogen doped carbon, pyrolysis at 700 °C In acetonitrile at 110℃; under 750.075 Torr; for 5h; Inert atmosphere; chemoselective reaction; | A n/a B 59.2% |
Conditions | Yield |
---|---|
With ammonium hydroxide; sodium hypochlorite In diethyl ether at 25℃; for 0.5h; | A 38% B 56% |
Adipic acid
A
caprolactam
B
hexamethylene imine
C
6-(azepan-1-yl)hexan-1-amine
D
hexan-1-amine
E
1-pentanamine
Conditions | Yield |
---|---|
Stage #1: Adipic acid With cyclopentyl methyl ether; ammonia at 200℃; under 4500.45 Torr; Sealed tube; Green chemistry; Stage #2: With cyclopentyl methyl ether; ammonia; hydrogen at 200℃; under 42004.2 Torr; for 6.5h; Cooling with ice; Green chemistry; | A 39% B 53% C 4% D 2% E 2% |
Conditions | Yield |
---|---|
With sodium hydroxide; sodium persulfate; sodium chloride In water at 85 - 90℃; for 7h; | A 35% B 52% |
With sodium hydroxide; sodium persulfate; sodium chloride In water at 85 - 90℃; for 7h; | A 35% B 49% |
hexan-1-amine
Conditions | Yield |
---|---|
Stage #1: (n-C6H13)3ZnMgBr With O-Methylhydroxylamin In tetrahydrofuran at 20℃; for 3h; Amination; Stage #2: With ammonia; water; ammonium chloride at 20℃; for 2h; Hydrolysis; | 50% |
methanol
1-azidohexane
A
hexan-1-amine
B
N,N-dimethylhexylamine
C
N-methylhexan-1-amine hydrochloride
Conditions | Yield |
---|---|
Stage #1: methanol; 1-azidohexane With trans-RuCl(phenpyra-Me)(PPh3)2PF6; sodium hydroxide at 125℃; for 5h; Sealed tube; Inert atmosphere; Glovebox; Stage #2: With hydrogenchloride | A 10 %Chromat. B 12 %Chromat. C 42% |
tri-n-hexylamine
A
hexan-1-amine
B
dihexylamine
C
N-hexylidenehexan-1-amine
Conditions | Yield |
---|---|
With dicarbonyl(chloro)(η5-pentaphenylcyclopentadienyl)ruthenium(II); ammonia In tert-Amyl alcohol at 170℃; for 23.5h; Inert atmosphere; Schlenk technique; Autoclave; | A 12% B 8% C 41.5% |
Conditions | Yield |
---|---|
Stage #1: di(n-hexyl)zinc; ( With O-Methylhydroxylamin In tetrahydrofuran at 20℃; for 3h; Amination; Stage #2: With ammonia; water; ammonium chloride at 20℃; for 2h; Hydrolysis; | 35% |
ammonium acetate
hexan-1-ol
A
1-hexene
B
hexan-1-amine
C
1-hexyl acetate
D
N-hexylacetamide
E
hexanal
Conditions | Yield |
---|---|
With water at 400℃; for 1h; Product distribution / selectivity; | A 29.4 %Chromat. B 1.9 %Chromat. C 4 %Chromat. D 30.8% E 1.3 %Chromat. |
With water at 380 - 420℃; for 0.05 - 1h; Product distribution / selectivity; | A 0.2 - 11.29 %Chromat. B 0.21 - 6.52 %Chromat. C 1.53 - 10.25 %Chromat. D 7.03 - 78.52 %Chromat. E 0.36 - 1.28 %Chromat. |
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In tetrahydrofuran | 30% |
N-(n-hexyl)hexanamide
A
hexan-1-amine
B
dihexylamine
C
hexan-1-ol
Conditions | Yield |
---|---|
With ruthenium(1,1,1-tris(di(3,5-dimethylphenyl)phosphinomethyl)ethane)(η4-trimethylenemethane); tris(pentafluorophenyl)borate; hydrogen In tetrahydrofuran at 160℃; under 75007.5 Torr; for 16h; | A 7.6% B 26.03% C 5.4% |
With aluminium(III) triflate; ruthenium(1,1,1-tris(di(3,5-dimethylphenyl)phosphinomethyl)ethane)(η4-trimethylenemethane); hydrogen In tetrahydrofuran at 160℃; under 75007.5 Torr; for 16h; | A 5.4% B 19.04% C 13.1% |
Conditions | Yield |
---|---|
With dicarbonyl(chloro)(η5-pentaphenylcyclopentadienyl)ruthenium(II); ammonia In tert-Amyl alcohol at 170℃; for 23.5h; Inert atmosphere; Schlenk technique; Autoclave; | A 8.5% B 25% C 11% |
Conditions | Yield |
---|---|
With Pd/C; hydrogen In ethanol at 130℃; for 24h; | 11% |
piperidine
1-Pentyl-1-hexylamine
A
1-pentylpiperidine
B
1-hexylpiperidine
C
hexan-1-amine
D
dihexylamine
E
1-pentanamine
F
Di-n-amylamine
Conditions | Yield |
---|---|
With hydrogen; sulphidized CoO-MoO3 at 300℃; under 45003.6 Torr; for 1h; Mechanism; Product distribution; | A 5.5% B 8.5% C 4% D 3% E 1% F 2.5% |
Conditions | Yield |
---|---|
at 20℃; for 2h; | 100% |
With ethanol; potassium carbonate | |
With aluminum oxide for 2h; Ambient temperature; |
Conditions | Yield |
---|---|
With potassium carbonate In dichloromethane; water at 5 - 20℃; for 4h; | 100% |
With potassium carbonate In dichloromethane; water at 4 - 20℃; for 4.5h; | 100% |
With potassium carbonate In dichloromethane; water at 0 - 20℃; for 6.5h; | 100% |
Conditions | Yield |
---|---|
100% | |
In tetrahydrofuran; diethyl ether at 0℃; for 3.5h; Inert atmosphere; | 80% |
With sodium carbonate In tetrahydrofuran at -20 - 0℃; |
Conditions | Yield |
---|---|
chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II) at 100℃; | 100% |
With tris(triphenylphosphine)ruthenium(II) chloride at 180℃; for 7h; | 88% |
With C53H41ClN3OP2Ru(1+)*F6P(1-); sodium methylate at 110℃; for 24h; Inert atmosphere; Glovebox; Schlenk technique; Sealed tube; Green chemistry; | 77% |
hexan-1-amine
trimethylsilyl cyanide
4,4'-[decane-1,10-diylbis(oxy)]dibenzaldehyde
(4-{10-[4-(Cyano-hexylamino-methyl)-phenoxy]-decyloxy}-phenyl)-hexylamino-acetonitrile
Conditions | Yield |
---|---|
In dichloromethane for 120h; | 100% |
Conditions | Yield |
---|---|
triphenylantimony(V) diacetate In pyridine at 100℃; for 10h; | 100% |
With silica In toluene for 8h; Dean-Stark; Reflux; Green chemistry; | 99% |
tetraphosphorus decasulfide; triphenyl antimony oxide In benzene at 40℃; for 5h; | 90% |
With HOBt-6-carboxamidomethyl polystyrene; dicyclohexyl-carbodiimide 1.) CH2Cl2, 25 deg C, 2.) CH2Cl2, 25 deg C, 4 h; Yield given. Multistep reaction; | |
With Sc(OTf)3 immobilized onto mesoporous at 80℃; for 24h; Product distribution; Further Variations:; Reagents; |
hexan-1-amine
N,N-dimethyl-formamide dimethyl acetal
N2-n-hexyl-N1,N1-dimethylformamidine
Conditions | Yield |
---|---|
at 60℃; | 100% |
Conditions | Yield |
---|---|
at 40℃; for 1h; lipase SP 382 (from Candida sp.); | 100% |
Conditions | Yield |
---|---|
With Zr6O4(OH)4(BDC-NH2)5.7([LIr]BF4)0.3 at 80℃; for 24h; Catalytic behavior; Autoclave; Green chemistry; | 100% |
dihydridotetrakis(triphenylphosphine)ruthenium In neat (no solvent) at 180℃; for 6h; | 52 % Chromat. |
Conditions | Yield |
---|---|
With 2-(2-methyl-1-oxopropyl)cyclohexanone; caesium carbonate; copper(l) iodide In N,N-dimethyl-formamide at 25℃; for 1.5h; | 100% |
With caesium carbonate; copper(I) bromide In dimethyl sulfoxide at 55℃; for 24h; Ullmann coupling; | 87% |
With tetra(n-butyl)ammonium hydroxide; copper(l) chloride In water at 80℃; for 24h; Inert atmosphere; | 86% |
hexan-1-amine
2-chloro-3-methyl-1-oxa-3-aza-2-phosphacyclopentane 2-oxide
Hexyl-(3-methyl-2-oxo-2λ5-[1,3,2]oxazaphospholidin-2-yl)-amine
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 17h; Ambient temperature; | 100% |
hexan-1-amine
2-(bromomethyl)-7-(benzyloxy)chroman
(7-Benzyloxy-chroman-2-ylmethyl)-hexyl-amine
Conditions | Yield |
---|---|
at 100℃; for 2h; | 100% |
Conditions | Yield |
---|---|
With 2-(2-methyl-1-oxopropyl)cyclohexanone; caesium carbonate; copper(l) iodide In N,N-dimethyl-formamide at 25℃; for 1.16667h; | 100% |
With copper(l) iodide; 1-(5,6,7,8-tetrahydroquinolin-8-yl)ethan-1-one; caesium carbonate In N,N-dimethyl-formamide at 25℃; for 10h; Ullmann condensation; Inert atmosphere; | 97% |
With caesium carbonate; copper(I) bromide In dimethyl sulfoxide at 55℃; for 24h; Ullmann coupling; | 91% |
Conditions | Yield |
---|---|
Stage #1: 3,3-Dimethylbut-1-yne; carbon monoxide With quinoline; tri(2-furyl)germane; tris(2,4-di-tert-butylphenyl)phosphite; bis(η3-allyl-μ-chloropalladium(II)) In toluene at 20℃; under 760.051 Torr; for 5.5h; Stage #2: hexan-1-amine; dmap In toluene at 70℃; for 6h; Further stages.; | 100% |
Conditions | Yield |
---|---|
With 4 A molecular sieve; zinc(II) chloride at -20℃; for 48h; | 100% |
hexan-1-amine
N-(benzyloxycarbonyl)-L-serine
((S)-1-Hexylcarbamoyl-2-hydroxy-ethyl)-carbamic acid benzyl ester
Conditions | Yield |
---|---|
With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide In N,N-dimethyl-formamide | 100% |
Conditions | Yield |
---|---|
With 2-(2-methyl-1-oxopropyl)cyclohexanone; caesium carbonate; copper(l) iodide In N,N-dimethyl-formamide at 25℃; for 1.83333h; | 100% |
With copper(l) iodide; 1-(5,6,7,8-tetrahydroquinolin-8-yl)ethan-1-one; caesium carbonate In N,N-dimethyl-formamide at 25℃; for 12h; Ullmann condensation; Inert atmosphere; | 97% |
With copper(l) iodide; 1-tetralone oxime; potassium hydroxide In water at 25℃; for 36h; Sealed tube; Inert atmosphere; Green chemistry; | 94% |
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane for 48h; | 100% |
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane Heating; | 100% |
Conditions | Yield |
---|---|
With 2-(2-methyl-1-oxopropyl)cyclohexanone; caesium carbonate; copper(l) iodide In N,N-dimethyl-formamide at 25℃; for 0.833333h; | 100% |
With copper(l) iodide; 1-tetralone oxime; potassium hydroxide In water at 25℃; for 18h; Sealed tube; Inert atmosphere; Green chemistry; | 92% |
With copper(l) iodide; 1-(5,6,7,8-tetrahydroquinolin-8-yl)ethan-1-one; caesium carbonate In N,N-dimethyl-formamide at 25℃; for 12h; Ullmann condensation; Inert atmosphere; | 91% |
Conditions | Yield |
---|---|
With 2-(2-methyl-1-oxopropyl)cyclohexanone; caesium carbonate; copper(l) iodide In N,N-dimethyl-formamide at 25℃; for 0.666667h; | 100% |
With copper(l) iodide; 1-(5,6,7,8-tetrahydroquinolin-8-yl)ethan-1-one; caesium carbonate In N,N-dimethyl-formamide at 25℃; for 10h; Ullmann condensation; Inert atmosphere; | 95% |
With copper(l) iodide; 1-tetralone oxime; potassium hydroxide In water at 25℃; for 18h; Sealed tube; Inert atmosphere; Green chemistry; | 95% |
Conditions | Yield |
---|---|
With erbium(III) triflate In dichloromethane at 20℃; for 2h; | 100% |
S,S-dimethyl dithiocarbonate
hexan-1-amine
S-methyl N-hexylthiocarbamate
Conditions | Yield |
---|---|
In water at 20 - 25℃; for 2h; | 100% |
hexan-1-amine
Conditions | Yield |
---|---|
In not given heating to 100°C for 2 days; centrifugation; filtration; washing (ethanol, acetone); drying in vac. for 1 h; chem. anal.; TGA; electron diffraction; | 100% |
In not given stirring for 6 days at 50°C; centrifugation; filtration; washing (ethanol, acetone); drying in vac. for 1 h; chem. anal.; TGA; electron diffraction; |
Conditions | Yield |
---|---|
In methanol at 20℃; | 100% |
Conditions | Yield |
---|---|
With cyclooctadiene ruthenium(II) dichloride; potassium tert-butylate; 1,3-diisopropyl-1H-imidazol-3-ium chloride; tricyclopentylphosphonium tetrafluoroborate In toluene for 24h; Inert atmosphere; Reflux; | 100% |
With dichloro(1,5-cyclooctadiene)ruthenium(II); potassium tert-butylate; 1,3-diisopropyl-1H-imidazol-3-ium chloride; tricyclopentylphosphonium tetrafluoroborate In toluene at 110℃; for 24h; Inert atmosphere; | 100% |
With pyridine; [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; sodium hydride; 1,3-di(propan-2-yl)-1H-imidazol-3-ium bromide In toluene for 36h; Inert atmosphere; Reflux; | 98% |
Conditions | Yield |
---|---|
With Zr6O4(OH)4(BDC-NH2)5.7([LIr]BF4)0.3 at 120℃; for 0.5h; Catalytic behavior; Temperature; Microwave irradiation; Green chemistry; | 100% |
With lithium hydroxide In neat (no solvent) at 120℃; for 24h; Inert atmosphere; | 94% |
With palladium nanoparticles embedded in the solid matrix of tetrabutylammonium bromide synthetized in supercritical carbon dioxide at 140℃; Sealed tube; Inert atmosphere; Green chemistry; | 88% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; for 1h; | 100% |
In N,N-dimethyl-formamide at 20℃; for 1h; |
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