As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:105-60-2
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:105-60-2
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inquiryProduct description: Product name 2-Oxohexamethylenimine CAS number 105-60-2 Assay ≥99% Appearance White crystalline powder Capacity 2000mt/year Application Resin, fiber, art
Cas:105-60-2
Min.Order:100 Gram
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Cas:105-60-2
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inquiryHebei yanxi chemical co., LTD is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low carb
Cas:105-60-2
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:105-60-2
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inquiryProduct Name: Caprolactam Synonyms: Benzyl Chloride (stabilized with εErlotinib-d10 HCl;2-OxohexamethyL;enimine;2-azacycloheptanone[qr];2-Azepanone;2H-Azepin-2-one, hexahydro-;2h-azepin-2-one,hexahydro-[qr] CAS: 105-60-2 MF: C6H11NO
Cas:105-60-2
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:105-60-2
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:105-60-2
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inquiryProduct name Caprolactam Appearance Powder CAS 105-60-2 Molecular Formula C6H11NO Molecular Weight 113.16 Einecs No 20
Cas:105-60-2
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Type:Other
inquiryAppearance:White Crystals or Flakes Storage:Store below +30°C. Package:25kg/drum Application:(1) The majority of caprolactam is used in the production of polycaprolactam, of which about 90% is used for the production of synthetic fibers, that is, K
Cas:105-60-2
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inquiryAmoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi
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Cas:105-60-2
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inquiryWe are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery
Cas:105-60-2
Min.Order:10 Gram
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Type:Trading Company
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:105-60-2
Min.Order:1 Kilogram
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Type:Trading Company
inquiryCaprolactam CAS:105-60-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates,
Cas:105-60-2
Min.Order:1 Gram
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Type:Lab/Research institutions
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Cas:105-60-2
Min.Order:1 Kilogram
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inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:105-60-2
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiry6-Caprolactam CAS: 105-60-2 Specification Product name 2-Oxohexamethylenimine CAS number 105-60-2 Assay ≥99% Appearance White crystalline powder Capacity 2000mt/year Applicatio
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:105-60-2
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Type:Lab/Research institutions
inquiryProduct Detail Minimum Order Qty. 10 Gram
Cas:105-60-2
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryProduct Description Product Name: Caprolactam CAS: 105-60-2 MF: C6H11NO MW: 113.16 EINECS: 203-313-2 Product Categories: Pharmaceutical Intermediates;Highly Purified Reagents;Other Categories;Zone Refined Products Mol File: 105-60-2.mol Melti
Packing: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Appearance:white powder/ Refer to COA Storage: 2-8°C Pack
Cas:105-60-2
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:105-60-2
Min.Order:100 Gram
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Type:Lab/Research institutions
inquirySuperior quality, moderate price & quick delivery. Appearance:White, crystalline solid or flakes Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:as per your request Application:to produce polyamide fibres,
Established in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
Conditions | Yield |
---|---|
With 1,3,5-trichloro-2,4,6-triazine In N,N-dimethyl-formamide at 20℃; for 3h; Beckmann rearrangement; | 100% |
With supercritical water; sulfuric acid at 374.84℃; under 300030 Torr; for 0.000202222h; | 99.5% |
With 1,3,5-trichloro-2,4,6-triazine at 60℃; for 2h; Beckmann rearrangement; | 99% |
1-[(2-oxazepan-1-yl)carbonyl]azepan-2-one
[1-(2-aminoethyl)-3-aminopropyl]trimethoxysilane
A
caprolactam
Conditions | Yield |
---|---|
In toluene at 75℃; for 3h; | A n/a B 100% |
3-(trimethoxysilyl)propan-1-amine
1-[(2-oxazepan-1-yl)carbonyl]azepan-2-one
A
caprolactam
Conditions | Yield |
---|---|
In toluene at 75℃; for 3h; | A n/a B 100% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide | 99.6% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide | 99.5% |
14,15-dioxa-7-aza-dispiro[5.1.5.2]pentadecane
A
caprolactam
B
11-cyanoundecanoic acid
C
cyclohexanone
Conditions | Yield |
---|---|
With cerium(IV) oxide; 2,2'-azobis(isobutyronitrile) at 50℃; for 12h; Reagent/catalyst; Temperature; Inert atmosphere; | A n/a B 99.2% C n/a |
Conditions | Yield |
---|---|
99.1% | |
99% | |
98.9% |
Conditions | Yield |
---|---|
zeolite F-9 In toluene for 20h; Heating; | 99.1% |
zeolite F-9 In toluene for 20h; Product distribution; Heating; other catalyst, other solvent; | 99.1% |
With di(n-butyl)tin oxide In xylene for 12h; Heating; | 95% |
methyl 6-oxohexanoate
A
caprolactam
C
6-aminocaproic amide
D
methyl 6-aminohexanoate hydrochloride
E
6-aminohexanoic acid
Conditions | Yield |
---|---|
Stage #1: methyl 6-oxohexanoate With ammonia In methanol; water at 35℃; under 22502.3 Torr; for 0.00416667h; Stage #2: With hydrogen; 5 % ruthenium on Al2O3 In methanol; water at 120℃; under 22502.3 Torr; for 22h; | A 99% B n/a C n/a D n/a E n/a |
A
caprolactam
B
pentamide
C
5-hexenoic acid
D
hexanoic acid
E
valeric acid
Conditions | Yield |
---|---|
at 300℃; under 9000.9 Torr; for 5h; | A 99% B n/a C n/a D n/a E n/a |
Stage #1: caprolactam; 6-aminocaproic acid; 6-aminocaproic amide; nylon-6-oligomers; water; mixture of at 220℃; under 5250.53 - 52505.3 Torr; for 0.5h; Stage #2: at 300℃; under 9000.9 - 90009 Torr; for 5h; | A 99% B n/a C n/a D n/a E n/a |
1-(4,5,6,7-tetrahydro-3H-azepin-2-yl)-hexahydro-2H-azepin-2-one
caprolactam
Conditions | Yield |
---|---|
With methanesulfonic acid; water In tert-butyl alcohol at 80℃; for 2h; | 98% |
Conditions | Yield |
---|---|
With sodium azide; methanesulfonic acid In 1,2-dimethoxyethane at -30 - 20℃; for 3h; | 96% |
With XY-zeolite; hydroxylamine hydrochloride for 0.0333333h; microwave irradiation; | 95% |
With sodium azide; sulfuric acid; silica gel at 60℃; for 0.583333h; Schmidt reaction; | 92% |
O-methylcaprolactim
naphthalene-2-carboxylate
A
caprolactam
B
methyl naphthalene-2-carboxylate
Conditions | Yield |
---|---|
at 80 - 85℃; for 16h; | A n/a B 96% |
Cyclohexanone oxime
A
caprolactam
B
cyclohexenone
C
cyclohexanone
Conditions | Yield |
---|---|
Hβ zeolite In various solvent(s) at 349.9℃; under 750.06 Torr; Title compound not separated from byproducts; | A 95.9% B 0.8% C 0.7% |
With Mg-Al-borate-pillared layerd double hydroxides at 340℃; for 4h; Product distribution; Further Variations:; Reagents; Beckmann rearrangement; vapor-phase; | |
With WOx/SBA-15 (10 wt.percent W) In methanol at 350℃; for 3h; Beckmann rearrangement; Inert atmosphere; Flow reactor; |
Conditions | Yield |
---|---|
With Vanadium(IV)-verbindung | 95% |
tert-butyl 2-oxoazepane-1-carboxylate
caprolactam
Conditions | Yield |
---|---|
With copper(II) bis(trifluoromethanesulfonate) In dichloromethane at 50℃; for 18h; Sealed tube; | 95% |
With silica gel; ytterbium(III) triflate In neat (no solvent) at 40℃; for 3h; Yield given; |
Cyclohexanone oxime
A
caprolactam
B
hex-5-enenitrile
C
cyclohexanone
Conditions | Yield |
---|---|
silica-boria catalyst at 250℃; | A 93% B n/a C n/a |
silica-boria at 250℃; Product distribution; Effect of silica-boria catalyst.; | |
With benzene; boria-hydroxyapatite at 300℃; Product distribution; further catalysts; | |
potassium phosphate at 350℃; Product distribution; study of activity and selectivity of various phosphate catalysts in the Beckmann rearrangement; other temperatures; other catalysts; | |
With calcined hierarchical silicalite-1 octahedra comprising highly-branched and orthogonally-stacked nanoplates catalyst In ethanol at 349.84℃; Beckmann Rearrangement; Inert atmosphere; |
caprolactam
Conditions | Yield |
---|---|
In water; toluene at 370℃; under 96759.7 Torr; for 1h; Autoclave; Supercritical conditions; | 93% |
With C2F6NO4S2(1-)*C11H20N3(1+) In PP13; TFSA at 300℃; | 80% |
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride In neat (no solvent) at 70℃; for 15h; Temperature; Solvent; Time; | A 7% B 92% |
With acetylhydroxamic acid; sulfuric acid In acetonitrile at 80℃; under 1292.9 Torr; for 0.166667h; Microwave irradiation; | A 83% B 4% |
With hydroxylamine hydrochloride In acetonitrile at 100℃; for 3h; Temperature; | A 72% B 23% |
N-(benzyloxycarbonyl)-2-oxo-azepane
caprolactam
Conditions | Yield |
---|---|
Stage #1: N-(benzyloxycarbonyl)-2-oxo-azepane With diethylaluminium chloride In hexane; dichloromethane at -78℃; for 0.166667h; Stage #2: With methyl-phenyl-thioether In hexane; dichloromethane at 0℃; for 1h; | 92% |
1-[(2-oxazepan-1-yl)carbonyl]azepan-2-one
dopamine hydrochloride
A
caprolactam
Conditions | Yield |
---|---|
With triethylamine In chloroform at 20 - 90℃; for 48h; | A n/a B 92% |
O-methylcaprolactim
benzoic acid
A
caprolactam
B
benzoic acid methyl ester
Conditions | Yield |
---|---|
at 80 - 85℃; for 16h; | A n/a B 91% |
Cyclohexanone oxime
A
caprolactam
B
hexanenitrile
C
hex-5-enenitrile
D
cyclohexanone
Conditions | Yield |
---|---|
With boron(III) phosphate In benzene at 300℃; under 750.06 Torr; for 2.66667h; Product distribution; Further Variations:; Catalysts; Solvents; Beckmann rearrangement; | A 90.4% B n/a C n/a D n/a |
Hβ(10)500 In benzene at 300℃; Product distribution; Further Variations:; Catalysts; Solvents; Temperatures; |
C12H21N3
1-amino-5-cyanopentane
A
caprolactam
B
ethyl 6-aminohexanoate
Conditions | Yield |
---|---|
With water; titanium(IV) oxide In ethanol at 230℃; under 60006 Torr; | A 90% B n/a |
Conditions | Yield |
---|---|
With 3-chloro-benzenecarboperoxoic acid In dichloromethane for 2h; Ambient temperature; | 89% |
With eosin; oxygen In N,N-dimethyl-formamide at 20℃; for 10h; Irradiation; Green chemistry; | 87% |
With manganese(IV) oxide In chloroform Ambient temperature; | 85% |
caprolactam
Conditions | Yield |
---|---|
In cyclohexane for 1h; Irradiation; | 89% |
In cyclohexane at 0℃; for 3.5h; Schmidt Reaction; Inert atmosphere; UV-irradiation; | 83% |
N-benzyl-2-azetidinone
7-Methylsulfanyl-2,3,4,5-tetrahydro-1H-azepine
A
caprolactam
B
N-benzyl 3-methylthiopropionamide
Conditions | Yield |
---|---|
at 140℃; for 72h; sealed tube; | A 88.5% B 59.8% |
N-hydroxysuccinimide ester of 6-{[(benzyloxy)carbonyl]amino}hexanoic acid
caprolactam
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethyl acetate | 88% |
2-aminocaprolactam
caprolactam
Conditions | Yield |
---|---|
With potassium hydroxide; hydroxylamine-O-sulfonic acid In water at 0 - 95℃; for 0.333333h; pH=11; Temperature; pH-value; Flow reactor; | 88% |
With potassium hydroxide; hydroxylamine-O-sulfonic acid In water at -5 - 75℃; for 4h; Product distribution / selectivity; | 75% |
With hydrogen sulfide; hydrogen; Ru-S/C (8 molpercent) In tetrahydrofuran at 250℃; under 5171.62 Torr; for 8h; Product distribution / selectivity; | 42% |
caprolactam
α-chlorooxohexamethylenimine
Conditions | Yield |
---|---|
With sodium hypochlorite; acetic acid; tert-butyl alcohol In toluene at 0℃; for 2h; | 100% |
With sodium hypochlorite; acetic acid; tert-butyl alcohol In toluene at -5 - 0℃; for 2h; | 100% |
With trichloroisocyanuric acid In dichloromethane at 20℃; for 1h; | 99% |
caprolactam
N-nitroso-6-caprolactam
Conditions | Yield |
---|---|
With sodium acetate; Nitrogen dioxide In dichloromethane at -20℃; | 100% |
With sodium acetate; dinitrogen tetraoxide In dichloromethane at -10℃; for 1h; | 100% |
With hydrogenchloride; water; sodium nitrite | |
With mixture of gaseous nitrogen oxides; acetic acid | |
With pyridine; nitrosonium tetrafluoroborate In acetonitrile |
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran for 4h; 0 deg C to 25 deg C; | 100% |
Stage #1: caprolactam With sodium hydride In tetrahydrofuran at 0℃; for 0.5h; Inert atmosphere; Stage #2: benzyl bromide In tetrahydrofuran at 0 - 20℃; Inert atmosphere; | 98% |
With sodium hydride In tetrahydrofuran; paraffin 1.) 0 deg C to room temperature, 2 h, 2.) room temperature, 2 h; | 96% |
caprolactam
ethyl acrylate
3-(2-Oxo-azepan-1-yl)-propionic acid ethyl ester
Conditions | Yield |
---|---|
With sodium hydroxide In tetrahydrofuran Michael addition reaction; | 100% |
With tetraethoxy orthosilicate; cesium fluoride In neat (no solvent) at 25℃; for 1h; | 89% |
Conditions | Yield |
---|---|
Stage #1: caprolactam With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Inert atmosphere; Stage #2: benzyl chloroformate In tetrahydrofuran at 20℃; for 10h; | 100% |
With n-butyllithium In tetrahydrofuran at -78℃; for 0.333333h; | 88% |
Stage #1: caprolactam With n-butyllithium In tetrahydrofuran at -78℃; for 0.5h; Inert atmosphere; Stage #2: benzyl chloroformate In tetrahydrofuran at -78 - 20℃; Inert atmosphere; | 52% |
With sodium hydride 1.) THF, 2.) THF, from 0 to 25 deg C, 75 min; Yield given. Multistep reaction; |
caprolactam
(isocyanatomethyl)methoxydimethylsilane
Conditions | Yield |
---|---|
In 1,4-dioxane for 4h; Heating / reflux; | 100% |
Conditions | Yield |
---|---|
at 90℃; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With sodium hydroxide In water; toluene | 99.6% |
With sodium hydroxide In toluene | 95% |
With sodium hydroxide; tetrabutylammomium bromide; potassium carbonate In cyclohexane | 92.8% |
Conditions | Yield |
---|---|
With dodecatungstosilic acid; water at 75℃; for 6h; Reagent/catalyst; Large scale; | 99.4% |
With water; sodium hydroxide at 120℃; under 1500.15 Torr; for 11h; Temperature; Pressure; Time; | 98.5% |
Stage #1: caprolactam With acetic acid In water; acetone at 120℃; for 12h; Stage #2: With ethylamine at 15℃; for 12h; Reagent/catalyst; Temperature; Solvent; | 88.1% |
Conditions | Yield |
---|---|
With pyridin-1-ium-1-yl[pyridin-1-ium-1-yl(sulfido)phosphinothioyl]sulfanyl-sulfido-thioxo-phosphane In acetonitrile for 0.5h; Reflux; | 99% |
With Lawessons reagent In tetrahydrofuran at 20℃; for 0.0833333h; | 98% |
With 2,4-{[3-[(CH2)5C8F17]-4-MeO-phenyl]}2-P2S2 2,4-disulfide In tetrahydrofuran for 2h; | 96% |
Conditions | Yield |
---|---|
With manganese(IV) oxide; ammonia at 200℃; under 9750.98 Torr; Reagent/catalyst; Temperature; Pressure; | 99% |
With ammonia; silica gel; copper at 360℃; |
Conditions | Yield |
---|---|
Stage #1: caprolactam With sodium hydride In tetrahydrofuran Stage #2: allyl bromide In tetrahydrofuran | 99% |
With sodium hydride In tetrahydrofuran at 20℃; | 92% |
With potassium hydroxide 1.) toluene, 80 deg C to 90 deg C, 45 min, 2.) toluene; Yield given. Multistep reaction; |
caprolactam
2-(ethylthio)acetyl chloride
1-ethylsulfenylacetylazepan-2-one
Conditions | Yield |
---|---|
In benzene for 12h; Heating; | 99% |
In benzene |
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; N,N`-dimethylethylenediamine In 1,4-dioxane at 110℃; for 24h; Inert atmosphere; | 99% |
With potassium phosphate; copper(l) iodide; glycine In 1,4-dioxane at 100℃; for 24h; Goldberg reaction; | 92% |
With pyridine; [Cu2(pda)3(ReO4)2]2*2H2O; caesium carbonate at 170℃; for 3h; Inert atmosphere; | 87% |
Conditions | Yield |
---|---|
With dmap; ruthenium trichloride; tributylphosphine; water; potassium carbonate In toluene at 100℃; for 15h; optical yield given as %de; | 99% |
With [bis(2-methylallyl)cycloocta-1,5-diene]ruthenium(II); 1,4-bis(dicyclohexylphosphino)butane; ytterbium(III) triflate In chlorobenzene at 60℃; for 16h; Inert atmosphere; optical yield given as %de; | 32% |
Conditions | Yield |
---|---|
Stage #1: caprolactam With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Stage #2: benzyl chloroformate In tetrahydrofuran; hexane at -78 - 20℃; for 2h; | 99% |
caprolactam
6-nitrohexanoic acid
Conditions | Yield |
---|---|
With methyltrifluoromethyldioxirane In water at 0℃; for 2h; | 99% |
With methyltrifluoromethyldioxirane; trifluoroacetic acid In acetone at 0℃; for 3h; | 99% |
Conditions | Yield |
---|---|
With bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In toluene at 100℃; under 30003 Torr; for 20h; Autoclave; | A 99% B n/a |
Conditions | Yield |
---|---|
With bis(2-(diphenylphosphanyl)-1H-pyrrol-1-yl)methane; palladium(II) acetylacetonate; toluene-4-sulfonic acid In toluene at 100℃; under 30003 Torr; for 12h; Autoclave; regioselective reaction; | 99% |
caprolactam
hexahydro-azepin-2-one; hydrogenphosphate
Conditions | Yield |
---|---|
With phosphoric acid In water at 20℃; for 12.5h; | 98.6% |
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