Dayang Chem (Hangzhou) Co.,Ltd.
Dayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantiti
Cas:140-88-5
Min.Order:1 Metric Ton
FOB Price: $9.0
Type:Lab/Research institutions
inquirySimagchem Corporation
Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:140-88-5
Min.Order:0 Metric Ton
Negotiable
Type:Manufacturers
inquiryHebei yanxi chemical co.,LTD.
Hebei yanxi chemical co. LTD. has expanded a compositive entity from initially only as a small manufacturer. The company dedicated to the development, production and marketing of chemicals. After many years of efforts, we have established stable
Ality Chemical Corporation
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Chemwill Asia Co., Ltd.
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Henan Tianfu Chemical Co., Ltd.
Ethyl acrylate Basic information Product Name: Ethyl acrylate Synonyms: Acrylate d'ethyle;acrylated’ethyle;acrylated’ethyle(french);Acrylic acid, ethyl ester (inhibited);
Cas:140-88-5
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHenan Sinotech Import&Export Corporation
Product Name:Ethyl acrylate CAS No.:140-88-5 EINECS: 205-438-8 Molecular Formula: C5H8O2 Molecular Weight: 100.12 Appearance:Clear colorless liquid Appearance: Colorless Transparent Liquid Storage: Preserve in well-closed, light-resistant and
Changchun Artel lmport and Export trade company
Price, service, company and transport advantage: 1.place of origin china with super quality by reasonable price. 2. it's customers' right to choose the package (ems, dhl, fedex, ups); 3. it's custo
Hangzhou Fandachem Co.,Ltd
Hangzhou Fanda Chemical Co.,Ltd (FandaChem) , a China-based chemical company, specialize in exporting Ethyl Acrylate(EA) CAS：140-88-5, Please contact us by email freely. We are leading exporter in China. If you really need this cargo,
Cas:140-88-5
Min.Order:0 Metric Ton
Negotiable
Type:Other
inquiryHangzhou Keyingchem Co.,Ltd
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:140-88-5
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryHangzhou J&H Chemical Co., Ltd.
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Afine Chemicals Limited
Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
Zibo Hangyu Biotechnology Development Co., Ltd
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:140-88-5
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co., Ltd.
1)quick response within 12 hours; 2)quality guarantee: all products are strictly tested by our qc, confirmed by qa and approved by third party lab in china, usa, canada, germany, uk, italy, france etc. 3) oem/odm available; 4) rea
Cas:140-88-5
Min.Order:1 Kilogram
FOB Price: $4.0
Type:Lab/Research institutions
inquiryHunan chemfish Pharmaceutical co.,Ltd
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
HANGZHOU YUNUO CHEMICAL CO.,LTD
Superior quality, moderate price & quick delivery. Appearance:colorless transparent liquid Storage:stored in a cool, dry and ventilated place to provent sun and rain Package:25kg/drum, or as per your request. Application:Used for Pesticide
Hubei Vanz Pharm Co.,Ltd
ISO Factory/Good qualityAppearance:off white Storage:dry and cool place Package:10G/BAG; 1KG/BAG ;25KG/DRUM Application:Active pharaceutical ingredients Transportation:BY SEA,AIR,EXPRESS Port:SHANGHAI;BEIJING
Kono Chem Co.,Ltd
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Hangzhou Dingyan Chem Co., Ltd
R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates
Wuhan Fortuna Chemical Co.,Ltd
stable supply&competitive price Storage:Available Package:25KG Or as client requirement Application:Important pharm intermediate Transportation:By air or By sea
Henan Allgreen Chemical Co.,Ltd
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Aecochem Corp.
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Zhuozhou Wenxi import and Export Co., Ltd
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:140-88-5
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiryAntimex Chemical Limied
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Hunan Russell Chemicals Technology Co.,Ltd
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
Xiamen AmoyChem Co.,Ltd
Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi
Hubei Langyou International Trading Co., Ltd
CAS No.140-88-5 Ethyl acrylate Application:CAS No.140-88-5 Ethyl acrylate
Hunan Longxianng Runhui Trading Co.,Ltd
CAS No.140-88-5 Ethyl acrylateAppearance:Liquid Storage:Refrigerator Package:1KG -200KG Drum with pallet Application:Pharma intermediates Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airport) or
Cas:140-88-5
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryKoning Pharmchem Co., Ltd.
Ethyl acrylate TOP1 supplier Storage:Store in dry, dark and ventilated plac... Package:according to the clients requirement Application:phama
Shanghai Send Pharmaceutical Technology Co., Ltd.
stock，low price，high quality，high purity，good sevice Application:R&D
Synthetic route
-
-
155201-03-9
ethyl 3-(trifluoromethanesulfonyl)propionate
-
A
-
2926-29-6
Langlois reagent
-
B
-
140-88-5
ethyl acrylate
| Conditions | Yield |
|---|---|
| With sodium methylate In methanol at 20℃; | A 100% B n/a |
| Conditions | Yield |
|---|---|
| With iron(III) sulfate; sulfuric acid for 3h; Heating; | 98% |
| In neat (no solvent) at 80℃; for 2.5h; | 89% |
| With sulfuric acid for 12h; Reflux; | 82% |
| Conditions | Yield |
|---|---|
| With diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; sodium carbonate In dimethyl sulfoxide at 20℃; for 1.5h; Inert atmosphere; Irradiation; | 95% |
| With ethanol; sulfuric acid; zinc | |
| With ethanol; zinc | |
| With diethyl ether; zinc | |
| With 2-methoxy-phenylamine In tetrahydrofuran at 20℃; stereospecific reaction; |
| Conditions | Yield |
|---|---|
| With P(MeNCH2CH2)3N In acetonitrile at 25℃; for 0.0833333h; | 92% |
| Multi-step reaction with 2 steps 1: 83 percent / dimethylformamide / 1.) 55 deg C, 60 h, 2.) room temperature, 6 h 2: 100 °C View Scheme | |
| With indole; dichloro bis(acetonitrile) palladium(II); potassium carbonate; norbornene In N,N-dimethyl acetamide; water Schlenk technique; Inert atmosphere; regioselective reaction; |
-
-
74-85-1
ethene
-
-
79-10-7
acrylic acid
-
A
-
60-29-7
diethyl ether
-
B
-
64-17-5
ethanol
-
C
-
140-88-5
ethyl acrylate
| Conditions | Yield |
|---|---|
| With water; cesium nitrate; tungstophosphoric acid; water; mixture of, dried, tabletted at 85.6 - 165℃; under 2250.23 Torr; Product distribution / selectivity; Gas phase; | A 3.5% B 4.3% C 91.8% |
| Conditions | Yield |
|---|---|
| In tetrahydrofuran N2 or Ar atmosphere; refluxing (3 h, ratio Rh-compd. org. compd. 1:10), cooling (room temp.); addn. of EtOH, washing (EtOH and pentane), drying (N2 stream); elem. anal.; | A 90% B 8-15 |
| In tetrahydrofuran N2 or Ar atmosphere; stirring (room temp., 24 h, ratio Rh-compd. org. compd. 1:10); addn. of EtOH, slow evapn., washing (EtOH and pentane), drying (N2 stream); elem. anal.; | A 90% B 8-15 |
| Conditions | Yield |
|---|---|
| In benzene Wittig reaction; Reflux; | 87% |
| In 1,4-dioxane at 50℃; for 16h; |
| Conditions | Yield |
|---|---|
| With potassium carbonate In water at 30℃; for 0.166667h; | 77% |
| With potassium carbonate In 1,4-dioxane at 70℃; for 5h; | 75% |
| Stage #1: diethoxyphosphoryl-acetic acid ethyl ester With sodium hydride In tetrahydrofuran; paraffin oil at 0 - 25℃; Horner-Wadsworth-Emmons Olefination; Inert atmosphere; Stage #2: formaldehyd In tetrahydrofuran; paraffin oil at 0 - 25℃; for 0.166667h; Horner-Wadsworth-Emmons Olefination; Inert atmosphere; | |
| Stage #1: diethoxyphosphoryl-acetic acid ethyl ester With sodium hydride In toluene at 0℃; Horner-Wadsworth-Emmons Olefination; Inert atmosphere; Schlenk technique; Stage #2: formaldehyd at 20℃; Horner-Wadsworth-Emmons Olefination; Inert atmosphere; Schlenk technique; | |
| Stage #1: diethoxyphosphoryl-acetic acid ethyl ester With sodium hydride In tetrahydrofuran at 20 - 40℃; for 1h; Stage #2: formaldehyd In tetrahydrofuran at 40℃; for 5h; |
-
-
3553-93-3
1-(trimethylsilyl)piperidin-2-one
-
-
535-11-5, 41978-69-2
Ethyl 2-bromopropionate
-
A
-
675-20-7
piperidin-2-one
-
B
-
2857-97-8
trimethylsilyl bromide
-
D
-
140-88-5
ethyl acrylate
| Conditions | Yield |
|---|---|
| at 155 - 180℃; for 3h; Yields of byproduct given; | A n/a B n/a C 73% D n/a |
| Conditions | Yield |
|---|---|
| With oxygen; tetraethylammonium perchlorate In N,N-dimethyl-formamide at 20℃; electroreduction at -1.1 V; | A 70% B 20 % Chromat. |
| With oxygen In N,N-dimethyl-formamide at 20℃; Product distribution; electrolysis of the oxygen saturated solution at -1,1 V; 0.1 M TEAP; further esters; | A 70% B 20 % Chromat. |
-
-
535-11-5, 41978-69-2
Ethyl 2-bromopropionate
-
-
3553-94-4
1-trimethylsilanyl-azepan-2-one
-
A
-
105-60-2
caprolactam
-
B
-
2857-97-8
trimethylsilyl bromide
-
D
-
140-88-5
ethyl acrylate
| Conditions | Yield |
|---|---|
| at 150 - 185℃; for 3h; Yields of byproduct given; | A n/a B n/a C 65% D n/a |
-
-
1291-32-3
zirconocene dichloride
-
-
5459-35-8
2-bromo-acrylic acid ethyl ester
-
-
928-49-4
hex-3-yne
-
A
-
1219618-63-9
ethyl 2,3,4,5-tetraethylbenzoate
-
B
-
140-88-5
ethyl acrylate
| Conditions | Yield |
|---|---|
| Stage #1: zirconocene dichloride With n-butyllithium In tetrahydrofuran at -78℃; Inert atmosphere; Stage #2: hex-3-yne In tetrahydrofuran at 20℃; Inert atmosphere; Stage #3: 2-bromo-acrylic acid ethyl ester Further stages; | A 63% B n/a |
| Conditions | Yield |
|---|---|
| C-200 (barium hydroxide) In tetrahydrofuran; water for 0.166667h; Ambient temperature; sonication; | 57% |
-
-
1291-32-3
zirconocene dichloride
-
-
5459-35-8
2-bromo-acrylic acid ethyl ester
-
-
1942-45-6
4-Octyne
-
A
-
1219618-70-8
ethyl 2,3,4,5-tetrapropylbenzoate
-
B
-
140-88-5
ethyl acrylate
| Conditions | Yield |
|---|---|
| Stage #1: zirconocene dichloride With n-butyllithium In tetrahydrofuran at -78℃; Inert atmosphere; Stage #2: 4-Octyne In tetrahydrofuran at 20℃; Inert atmosphere; Stage #3: 2-bromo-acrylic acid ethyl ester Further stages; | A 57% B n/a |
| Conditions | Yield |
|---|---|
| With ethanol; sulfuric acid; copper at 220℃; Product distribution / selectivity; | A 50% B 50 %Chromat. |
| With ethanol; NaH2PO4-silica at 250 - 275℃; Product distribution / selectivity; | A 21% B 14 - 49 %Chromat. |
-
A
-
19006-76-9
2-ethylthiopyridine
-
B
-
89407-42-1
(propionate d'ethyle-3)(pyridyl-2) sulfure
-
C
-
140-88-5
ethyl acrylate
| Conditions | Yield |
|---|---|
| at 220℃; under 1 Torr; | A 13% B 16% C 43% |
| at 220℃; under 1 Torr; Product distribution; other conditions, other substrates; | A 13% B 16% C 43% |
| Conditions | Yield |
|---|---|
| With bis(acetylacetonate)nickel(II); sodium acetylacetonate In tetrahydrofuran at 220℃; under 1500.15 - 35253.5 Torr; for 1h; Autoclave; | 42.1% |
| With copper(ll) bromide; nickel dibromide In tetrahydrofuran at 240℃; under 3750.38 Torr; | |
| With 2-Picolinic acid In tetrahydrofuran at 210℃; under 1500.15 - 37503.8 Torr; for 0.5h; Autoclave; Inert atmosphere; | |
| With 8-hydroxy-quinoline-2-carboxylic acid; triethylaluminum; nickel(II) acetate tetrahydrate; triphenylphosphine In tetrahydrofuran at 60℃; under 10501.1 - 12001.2 Torr; for 1h; Autoclave; Inert atmosphere; |
-
-
14468-90-7
N-trimethylsilyl-pyrrolidin-2-one
-
-
535-11-5, 41978-69-2
Ethyl 2-bromopropionate
-
A
-
616-45-5
2-pyrrolidinon
-
B
-
70717-55-4
ethyl 2-(2-oxo-1-pyrrolidinyl)propanoate
-
C
-
2857-97-8
trimethylsilyl bromide
-
D
-
140-88-5
ethyl acrylate
| Conditions | Yield |
|---|---|
| at 170 - 200℃; for 3h; Yields of byproduct given; | A n/a B 37% C n/a D n/a |
| Conditions | Yield |
|---|---|
| Hoveyda-Grubbs catalyst second generation In dichloromethane at 40℃; under 562.556 Torr; for 24h; Product distribution / selectivity; Inert atmosphere; | A 19% B 28% |
| With Hoveyda-Grubbs catalyst second generation at 25℃; under 13187.6 Torr; for 21h; Catalytic behavior; Reagent/catalyst; | A n/a B 6.2% |
-
-
1291-32-3
zirconocene dichloride
-
-
5459-35-8
2-bromo-acrylic acid ethyl ester
-
-
501-65-5
diphenyl acetylene
-
A
-
96676-89-0
ethyl-5',6'-diphenyl-[1,1':2',1''-terphenyl]-3'-carboxylate
-
B
-
140-88-5
ethyl acrylate
| Conditions | Yield |
|---|---|
| Stage #1: zirconocene dichloride With n-butyllithium In tetrahydrofuran at -78℃; Inert atmosphere; Stage #2: diphenyl acetylene In tetrahydrofuran at 20℃; Inert atmosphere; Stage #3: 2-bromo-acrylic acid ethyl ester Further stages; | A 26% B n/a |
-
-
106-98-9
1-butylene
-
-
103-36-6
ethyl 3-phenyl-2-propenoate
-
A
-
292638-84-7
styrene
-
B
-
140-88-5
ethyl acrylate
| Conditions | Yield |
|---|---|
| Hoveyda-Grubbs catalyst second generation In dichloromethane at 40℃; under 750.075 Torr; for 24h; Inert atmosphere; | A 8% B 8% |
| Conditions | Yield |
|---|---|
| Hoveyda-Grubbs catalyst second generation at 60℃; under 7757.43 Torr; for 4h; Conversion of starting material; | A 4% B 7% |
| Conditions | Yield |
|---|---|
| [1,3-bis(2-methylphenyl)-2-(imidazolidene)dichloro(phenylmethylene)(tricyclohexylphosphine)]ruthenium (II) at 60℃; under 7757.43 Torr; for 4h; Conversion of starting material; | 1% |
| dichloro(tricyclohexylphosphino)(benzylidene)(1,3-dimesityl-4,5-dihydroimidazol-2-ylidene)ruthenium(III) at 60℃; under 7757.43 Torr; for 4h; Conversion of starting material; | 1% |
| [1,3-bis(2,4,6-trimethylphenyl)-2-(imidazolidene)dichloro(3-methyl-2-butenylidene)(tricyclohexylphosphine)]ruthenium (II) at 60℃; under 7757.43 Torr; for 16h; Conversion of starting material; | 1% |
-
-
64-18-6
formic acid
-
-
590-29-4
potassium formate
-
-
86931-46-6
1-(2-carbethoxyethyl)pyridinium bromide
-
A
-
110-86-1
pyridine
-
B
-
140-88-5
ethyl acrylate
-
-
97-64-3, 2676-33-7
ethyl 2-hydroxypropionate
-
-
140-88-5
ethyl acrylate
| Conditions | Yield |
|---|---|
| at 450℃; ueber einen aus Natriumdihydrogenphosphat und Graphit hergestellten Katalysator; | |
| Multi-step reaction with 2 steps 1: pyridine; diethyl ether; SOCl2 / -10 °C 2: 390 - 420 °C View Scheme | |
| Multi-step reaction with 2 steps 1: concentrated H2SO4 / bei der Destillation 2: quartz / 450 °C View Scheme |
| Conditions | Yield |
|---|---|
| With iron(II) sulfate at 140℃; |
| Conditions | Yield |
|---|---|
| With pyrographite at 250℃; | |
| With sulfuric acid; hydroquinone |
| Conditions | Yield |
|---|---|
| With ethanol; tetracarbonyl nickel at 190℃; |
| Conditions | Yield |
|---|---|
| cobalt(II) acetate In water at 20℃; for 15h; aza-type Michael addition; | 100% |
| ammonium cerium(IV) nitrate for 0.333333h; aza-Michael addition; ultrasonication; | 100% |
| With ammonium cerium(IV) nitrate In water at 20℃; for 12h; aza-Michael addition; | 99% |
-
-
75-31-0
isopropylamine
-
-
140-88-5
ethyl acrylate
-
-
16217-22-4
3-isopropylaminopropionic acid ethyl ester
| Conditions | Yield |
|---|---|
| In tetrahydrofuran; ethanol at 0 - 20℃; for 16h; | 100% |
| In ethanol at 0 - 20℃; for 24h; | 100% |
| With poly(ethylene glycol) 2000; ruthenium trichloride at 50℃; for 8h; aza-Michael addition; | 91% |
| Conditions | Yield |
|---|---|
| With copper diacetate In water at 20℃; for 12h; aza-Michael addition; | 100% |
| iron(III) chloride In dichloromethane at 25℃; for 42h; Product distribution; various catalysts and further amines with various Michael acceptors; | 96% |
| iron(III) chloride In dichloromethane at 25℃; for 42h; | 96% |
| Conditions | Yield |
|---|---|
| In ethanol at 20℃; for 2h; Michael addition; | 100% |
| With poly(ethylene glycol) 2000; ruthenium trichloride at 50℃; for 8h; aza-Michael addition; | 96% |
| Stage #1: N-butylamine With cerous nitrate for 4h; Reflux; Stage #2: ethyl acrylate for 8h; Time; | 93.8% |
| Conditions | Yield |
|---|---|
| In acetonitrile electrolysis (0.01-0.1 N Et4NBr or Bu4NBr, Pt cathode, Mg anode); | 100% |
| With dibenzoyl peroxide at 240℃; |
| Conditions | Yield |
|---|---|
| With bromine In acetone for 0.5h; Reflux; | 100% |
| With bromine In tetrachloromethane at 0 - 60℃; for 2h; | 99% |
| With bromine In dichloromethane at 0 - 20℃; for 4.33333h; Inert atmosphere; | 95% |
-
-
140-88-5
ethyl acrylate
-
-
71962-74-8
Ethyl nipecotate
-
-
128200-19-1
ethyl 1-[2-(ethoxycarbonyl)ethyl]-3-piperidinecarboxylate
| Conditions | Yield |
|---|---|
| at 55℃; | 100% |
| In toluene at 18 - 52℃; for 12.9167 - 13.1667h; | 100% |
| In toluene at 18 - 52℃; for 12.9167 - 13.1667h; Product distribution / selectivity; | 97.6% |
| Conditions | Yield |
|---|---|
| iron(III) chloride In water at 20℃; for 15h; aza-type Michael addition; | 100% |
-
-
14318-66-2
3-methoxy-N-methylaniline
-
-
140-88-5
ethyl acrylate
-
-
7280-98-0
3-(N-Methyl-N-m-methoxyphenylamino)-propionsaeure-aethylester
| Conditions | Yield |
|---|---|
| at 60℃; for 2h; | 100% |
| In acetic acid |
| Conditions | Yield |
|---|---|
| With hydroxylamine; triphenylphosphine In acetonitrile at 20℃; for 0.25h; Michael addition; | 100% |
| With hydroxylamine hydrochloride; sodium hydroxide In methanol for 0.25h; Inert atmosphere; | 72% |
| With hydroxylamine In methanol | |
| With hydroxylamine hydrochloride; ammonia In ethanol at 20℃; for 15h; |
-
-
675-20-7
piperidin-2-one
-
-
140-88-5
ethyl acrylate
-
-
88948-40-7
1-(2-ethoxycarbonylethyl)-2-piperidinone
| Conditions | Yield |
|---|---|
| With sodium hydroxide In tetrahydrofuran Michael addition reaction; | 100% |
| With tetraethoxy orthosilicate; cesium fluoride In neat (no solvent) at 25℃; for 0.166667h; Product distribution; Mechanism; variation of reaction time and amount of CsF; further α,β-unsaturated esters; further amides; presence of different solvents; | 98% |
| With tetraethoxy orthosilicate; cesium fluoride In neat (no solvent) at 25℃; for 0.166667h; | 98% |
-
-
105-60-2
caprolactam
-
-
140-88-5
ethyl acrylate
-
-
88948-41-8
3-(2-Oxo-azepan-1-yl)-propionic acid ethyl ester
| Conditions | Yield |
|---|---|
| With sodium hydroxide In tetrahydrofuran Michael addition reaction; | 100% |
| With tetraethoxy orthosilicate; cesium fluoride In neat (no solvent) at 25℃; for 1h; | 89% |
-
-
623-73-4
diazoacetic acid ethyl ester
-
-
140-88-5
ethyl acrylate
-
-
82706-83-0
diethyl Δ2-pyrazoline-3,5-dicarboxylate
| Conditions | Yield |
|---|---|
| at 22℃; for 5h; | 100% |
| In pyridine at 60℃; for 3h; | 99% |
| With water at 20℃; for 3h; Green chemistry; | 99% |
-
-
61-54-1
tryptamine
-
-
140-88-5
ethyl acrylate
-
-
14487-98-0
3-<<2-(1H-indol-3-yl)ethyl>amino>propanoic acid ethyl ester
| Conditions | Yield |
|---|---|
| In ethanol for 1h; Reflux; | 100% |
| In ethanol at 0℃; for 24h; | 83% |
| In tetrahydrofuran at 20℃; for 12h; | 83% |
| In ethanol at 0 - 20℃; | 80% |
| In ethanol |
-
-
75-07-0
acetaldehyde
-
-
140-88-5
ethyl acrylate
-
-
98837-34-4, 130196-00-8, 19362-99-3
ethyl 3-hydroxy-2-methylenebutanoate
| Conditions | Yield |
|---|---|
| With 1,4-diaza-bicyclo[2.2.2]octane at 20℃; for 216h; | 100% |
| With 1,4-diaza-bicyclo[2.2.2]octane at 25℃; for 168h; | 94% |
| 1,4-diaza-bicyclo[2.2.2]octane for 168h; Ambient temperature; | 90% |
| Conditions | Yield |
|---|---|
| triethylamine Ambient temperature; | 100% |
| In acetonitrile electrolysis (0.01-0.1 N Et4NBr or Bu4NBr, Pt cathode, Mg anode); | 100% |
| perchloric acid; silica gel In dichloromethane at 20℃; for 0.166667h; thia-Michael addition; | 95% |
-
-
60-24-2
2-hydroxyethanethiol
-
-
140-88-5
ethyl acrylate
-
-
77475-66-2
ethyl 3-((2-hydroxyethyl)thio)propionate
| Conditions | Yield |
|---|---|
| In acetonitrile electrolysis (0.01-0.1 N Et4NBr or Bu4NBr, Pt cathode, Mg anode); | 100% |
| With triethylamine In methanol; acetone at 0 - 20℃; for 16h; Product distribution / selectivity; | 100% |
| With C15H22N4O4 In neat (no solvent) for 1h; Michael Addition; Irradiation; | 100 %Spectr. |
| Conditions | Yield |
|---|---|
| With potassium phosphate; tetrabutylammomium bromide; [PdCl{[η5-C5H5)]Fe[(η5-C5H3)C(CH3)=NC12H25]}]2 In N,N-dimethyl-formamide at 140℃; for 12h; Heck coupling; | 100% |
| With {4-[di(2-hydroxyethyl)amino]butyl}tri(n-butyl)ammonium bromide; palladium diacetate at 100℃; for 6h; Heck reaction; Inert atmosphere; stereoselective reaction; | 99% |
| With C37H38BrClFeN3Pd; potassium acetate In N,N-dimethyl acetamide at 150℃; for 12h; Heck reaction; Inert atmosphere; regioselective reaction; | 97% |
| Conditions | Yield |
|---|---|
| With tetrabutylammomium bromide; potassium acetate; Pd(0)-ferrocenyl In N,N-dimethyl-formamide at 60℃; for 2.5h; | 100% |
| With palladium nanoparticles on graphene; triethylamine In N,N-dimethyl-formamide at 120 - 125℃; for 2h; Heck Reaction; | 100% |
| With triethylamine; silica aerogel nanocomposite; palladium In acetonitrile for 8h; Mizoroki-Heck reaction; Heating; | 99% |
| Conditions | Yield |
|---|---|
| In acetonitrile electrolysis (0.01-0.1 N Et4NBr or Bu4NBr, Pt cathode, Mg anode); | 100% |
-
-
38512-35-5
1-(1-diazo-2,2,2-trifluoroethyl)-4-methylbenzene
-
-
140-88-5
ethyl acrylate
-
-
136603-49-1
3-carbethoxy-5-trifluoromethyl-5-(p-tolyl)-2-pyrazoline
| Conditions | Yield |
|---|---|
| at 20 - 25℃; for 0.083h; | 100% |
| Conditions | Yield |
|---|---|
| With hydrogen; triethylamine; di(rhodium)tetracarbonyl dichloride; 1,4-di(diphenylphosphino)-butane at 25℃; under 15001.2 Torr; for 12h; Product distribution; other ligands: phosphanobornadiene; | 100% |
| With hydrogen; triethylamine; di(rhodium)tetracarbonyl dichloride; 1,4-di(diphenylphosphino)-butane at 25℃; under 15001.2 Torr; for 12h; | 100% |
| With hydrogen; [Rh(acac)(CO)2]-fluoropolymer ligand In carbon dioxide at 80℃; for 1h; | |
| With hydrogen; C23H22NO5Rh In water; toluene at 85℃; under 30003 Torr; for 8h; Catalytic behavior; Autoclave; chemoselective reaction; |
-
-
138356-10-2
BD 1060
-
-
140-88-5
ethyl acrylate
-
-
141044-90-8
N-<2-(3,4-dichlorophenyl)-1-ethyl>-N-<1-(ethoxypropionyl)>-2-(1-pyrrolidinyl)ethylamine
| Conditions | Yield |
|---|---|
| In toluene for 72h; Heating; | 100% |
-
-
140-88-5
ethyl acrylate
-
-
4439-02-5
3,4-methylenedioxyphenylacetonitrile
-
-
76934-80-0
4-Benzo[1,3]dioxol-5-yl-4-cyano-heptanedioic acid diethyl ester
| Conditions | Yield |
|---|---|
| With N-benzyl-trimethylammonium hydroxide In acetonitrile | 100% |
-
-
140-88-5
ethyl acrylate
| Conditions | Yield |
|---|---|
| In ethanol Heating; | 100% |
-
-
126570-60-3
4-(8-Chloro-5,11-dihydro[1]benzoxepino[4,3-b]pyridin-11-ylidene)piperidine
-
-
140-88-5
ethyl acrylate
| Conditions | Yield |
|---|---|
| In ethanol Heating; | 100% |
-
-
140-88-5
ethyl acrylate
| Conditions | Yield |
|---|---|
| In ethanol Heating; | 100% |
-
-
161522-66-3
8-Fluoro-5-piperidin-4-ylidene-5,11-dihydro-10-oxa-1-aza-dibenzo[a,d]cycloheptene
-
-
140-88-5
ethyl acrylate
| Conditions | Yield |
|---|---|
| In ethanol Heating; | 100% |
-
-
140-88-5
ethyl acrylate
| Conditions | Yield |
|---|---|
| In ethanol Heating; | 100% |
| Conditions | Yield |
|---|---|
| With silver(I) acetate; palladium diacetate; acetic acid at 110℃; for 6h; Inert atmosphere; | 100% |
| With dipalladium(II)(1,1'-di-t-butyl-3,3'-(1,2-ethanediyl)bisimidazolium)dipyridinetetradichloride; tetrabutylammomium bromide; sodium acetate In N,N-dimethyl acetamide at 120℃; for 18h; Heck Reaction; Inert atmosphere; | 95% |
| With silver(I) acetate; palladium diacetate; acetic acid at 110℃; for 6h; Heck reaction; | 94% |
| With bis-triphenylphosphine-palladium(II) chloride; triethylamine In acetonitrile at 140℃; under 7500600 Torr; for 4h; | 76% |
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