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inquiryProduct Name: Diethylamine Synonyms: (C2H5)2NH;ai3-24215;detn;Diaethylamin;Diethamine CAS: 109-89-7 MF: C4H11N MW: 73.14 E
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Product Name: Diethylamine Synonyms: (C2H5)2NH;ai3-24215;detn;Diaethylamin;Diethamine;Diethylamin;Dietilamina;Dwuetyloamina CAS: 109-89-7 MF: C4H11…Appearance:Solid powder Storage:Sealed,light and oxygen resistant Package:aluminum foil bag,carton
Product Name:Diethylamine CAS: 109-89-7 MF: C4H11N MW: 73.14 EINECS: 203-716-3 mp -50 °C bp 55 °C(lit.) density 0.71 vap…
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Diethylamine CAS NO.109-89-7 Application:Diethylamine CAS NO.109-89-7
1-diethylamino-2,4-dinitronaphthalene
ethylamine
A
N-ethyl-2,4-dinitro-1-naphthylamine
B
diethylamine
Conditions | Yield |
---|---|
In water at 30℃; for 1h; | A 100% B n/a |
(N,N-diethylamino)tributyltin
2,5-diethynylthiophene
A
2,5-bis[(tributylstannyl)ethynyl]thiophene
B
diethylamine
Conditions | Yield |
---|---|
In neat (no solvent) stoich. amts., stirring (overnight, room temp., dry atmosphere), evapn. (vac.); | A 99% B n/a |
phenylphosphonic acid bis(N,N-diethylamide)
4-methoxy-aniline
A
phenyl N,N'-bis(p-methoxyphenyl)phosphorodiamidite
B
diethylamine
Conditions | Yield |
---|---|
for 12h; Heating; | A 26.3% B 98.5% |
Conditions | Yield |
---|---|
With aluminum (III) chloride; zinc borohydride In methanol at 60℃; for 10h; Reagent/catalyst; Temperature; Solvent; | A 95.7% B 98.1% |
trimethylsilyl diethylcarbamate
trimethylsilyl <2-(trimethylsiloxy)ethyl>carbamate
A
N,N'-bis-<β-(trimethylsiloxy)>ethylcarbodiimide
B
diethylamine
Conditions | Yield |
---|---|
A 66% B 98% |
4-methoxy-aniline
bis(diethylamino)phenylphosphine
A
N,N'-bis(p-methoxyphenyl)-P-phenylphosphonous diamide
B
diethylamine
Conditions | Yield |
---|---|
for 14h; Heating; | A 83.7% B 98% |
for 14h; Heating; | A 83.7% B 98% |
1-diethylamino-2,4-dinitronaphthalene
methylamine
A
1-(Methylamino)-2,4-dinitronaphthalene
B
diethylamine
Conditions | Yield |
---|---|
In water at 30℃; for 1h; | A 97% B n/a |
bis-(4-hydroxyphenyl)methane
bis(diethylamino)phenylphosphine
B
diethylamine
Conditions | Yield |
---|---|
In neat (no solvent) at 115 - 120℃; for 2h; | A 97% B n/a |
BPA
bis(diethylamino)phenylphosphine
A
4,4′-(propane-2,2-diyl)di(benzene-4,1-diyl) bis(N,N-diethyl-P-phenylphosphonamidite)
B
diethylamine
Conditions | Yield |
---|---|
In neat (no solvent) at 115 - 120℃; for 2h; | A 97% B n/a |
3-(trimethylsilyl)-1-(trimethylstannyl)propyne
Diethylamino-trimethyl-stannan
A
3-(trimethylsilyl)-1,3-bis(trimethylstannyl)propyne
B
3-(trimethylsilyl)-1,1-bis(trimethylstannyl)propadiene
C
(Trimethylsilyl)tris(trimethylstannyl)propadiene
D
diethylamine
Conditions | Yield |
---|---|
In neat (no solvent) heating (180-200°C, 1 h), continuous removal of HNEt2; distn.; elem. anal.; mixt. of propadiene/propyne bis(trimethylastannyl)-derivatives (90:10 %) not separated; | A n/a B n/a C n/a D 96% |
diethylammonium diethylcarbamate
diethylamine
Conditions | Yield |
---|---|
In methanol at 60 - 65℃; for 2h; | 95% |
phenylphosphonic acid bis(N,N-diethylamide)
aniline
A
triphenyl phosphite
B
N,N',N''-triphenylphosphorous triamide
C
phenyl N,N'-diphenylphosphorodiamidite
D
diphenyl phenylphosphoramidite
E
diethylamine
Conditions | Yield |
---|---|
for 17h; Product distribution; Heating; | A n/a B n/a C n/a D n/a E 94.5% |
4-[(diethylamino)methyl]-2,6-bis(1,1-dimethylethyl)phenol
phosphonic acid diethyl ester
A
diethyl 4-hydroxy-3,5-di-tert-butylbenzylphosphonate
B
diethylamine
Conditions | Yield |
---|---|
In toluene for 25h; Heating; | A 94% B n/a |
bis(diethylamino)phenylphosphine
4-bromo-aniline
A
N,N'-bis(p-bromophenyl)-P-phenylphosphonous diamide
B
diethylamine
Conditions | Yield |
---|---|
for 18.5h; Heating; | A 68.1% B 93.6% |
1,3-benzothiazol-2-ylhydrazine
bis(diethylamino)phenylphosphine
A
2-Hydrazono-3-(diethylaminophenylphosphino)-2,3-dihydro-1,3-benzothiazole
B
diethylamine
Conditions | Yield |
---|---|
at 110 - 115℃; under 5 - 10 Torr; for 1h; | A 92.3% B n/a |
bis(diethylamino)phenylphosphine
aniline
A
N,N'-triphenylphosphonous diamide
B
diethylamine
Conditions | Yield |
---|---|
for 20h; Heating; | A 72.2% B 92.1% |
bis(diethylamino)phenylphosphine
2-Chloroaniline
A
N,N'-bis(o-chlorophenyl)-P-phenylphosphonous diamide
B
diethylamine
Conditions | Yield |
---|---|
for 36h; Heating; | A 62.4% B 91.6% |
phenylphosphonic acid bis(N,N-diethylamide)
4-bromo-aniline
A
triphenyl phosphite
B
diethylamine
Conditions | Yield |
---|---|
for 22h; Product distribution; Heating; | A n/a B 91.4% C n/a D n/a E n/a |
Conditions | Yield |
---|---|
With hexaethylphosphoric triamide at 190℃; further reagent; | A 26.8% B 91.3% |
Conditions | Yield |
---|---|
With 4-Hydroxy-4-methyl-2-pentanone at 190℃; | A 26.8% B 91.3% |
O,O'-diethyl thiophosphonate
4-[(diethylamino)methyl]-2,6-bis(1,1-dimethylethyl)phenol
A
diethylamine
Conditions | Yield |
---|---|
In toluene for 25h; Heating; | A n/a B 90% |
ethylene glycol
A
1-thiopropane
B
1,4,6,9-tetraoxa-5λ5-phosphaspiro[4,4]nonane
C
diethylamine
Conditions | Yield |
---|---|
at 120 - 130℃; for 1h; | A n/a B 90% C n/a |
at 120 - 130℃; for 1h; Product distribution; | A n/a B 90% C n/a |
1-Bicyclo[2.2.1]hept-5-en-2-yl-butane-1,2-dione
N,N-diethyl-1,1,1-trimethylsilanamine
A
(Z)-1-Bicyclo[2.2.1]hept-5-en-2-yl-2-trimethylsilanyloxy-but-2-en-1-one
B
diethylamine
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid at 30 - 40℃; for 18h; | A 90% B n/a |
1-(3-Methyl-bicyclo[2.2.1]hept-5-en-2-yl)-butane-1,2-dione
N,N-diethyl-1,1,1-trimethylsilanamine
A
(Z)-1-(3-Methyl-bicyclo[2.2.1]hept-5-en-2-yl)-2-trimethylsilanyloxy-but-2-en-1-one
B
diethylamine
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid at 30 - 40℃; for 18h; | A 90% B n/a |
carbon monoxide
benzenenesulfenyl dimethylamine
A
N,N'-diethylurea
B
N,N,N',N'-tetraethyloxamide
C
diethylamine
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0) In pyridine at 80℃; under 14701.2 Torr; for 10h; Carbonylation; | A n/a B 1.4 % Spectr. C 3 % Spectr. D 90% |
2-hydrazino-6-methylbenzothiazole
bis(diethylamino)phenylphosphine
A
C18H23N4PS
B
diethylamine
Conditions | Yield |
---|---|
at 110 - 115℃; under 5 - 10 Torr; for 1h; | A 89.7% B n/a |
Conditions | Yield |
---|---|
With carbon monoxide; hexarhodium hexadecacarbonyl In 2-ethoxy-ethanol; water at 40℃; under 12160 Torr; for 5h; | 89% |
With N,N,N'N'-tetramethyl-1,3-propanediamine; carbon monoxide; water; hexarhodium hexadecacarbonyl In 2-ethoxy-ethanol at 40℃; under 6080 Torr; for 5h; | 93 % Chromat. |
With N,N,N'N'-tetramethyl-1,3-propanediamine; carbon monoxide; water; hexarhodium hexadecacarbonyl In 2-ethoxy-ethanol at 40℃; under 6080 Torr; for 5h; Product distribution; Mechanism; (CH3)2NC3H6NH-substituted polystyrene instead of TMPDA; analogous reaction of other hydroxylamines; | 93 % Chromat. |
(2-hydroxyethyl)urea
N,N-diethyl-1,1,1-trimethylsilanamine
A
diethylamine
B
N-<2-(trimethylsiloxy)ethyl>-N'-(trimethylsilyl)urea
Conditions | Yield |
---|---|
With ammonium sulfate at 120℃; for 1h; | A 82% B 89% |
bis(diethylamino)phenylphosphine
(4-chloro-1,3-benzothiazol-2-yl)hydrazine
A
C17H20ClN4PS
B
diethylamine
Conditions | Yield |
---|---|
at 110 - 115℃; under 5 - 10 Torr; for 1h; | A 88.5% B n/a |
1-butanethiol
dibutyl diethylphosphoramidodithioite
A
merphos
B
diethylamine
Conditions | Yield |
---|---|
for 0.5h; Ambient temperature; | A 88% B 77% |
1,3-propanesultone
diethylamine
3-(diethylamino)propane-1-sulfonic acid
Conditions | Yield |
---|---|
In dichloromethane at 10℃; for 1h; Product distribution / selectivity; | 100% |
In dichloromethane Inert atmosphere; | 53% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 6h; | 100% |
With sodium carbonate In tert-butyl methyl ether; water at 15 - 25℃; for 1h; Schotten-Baumann Reaction; Inert atmosphere; | 98.7% |
In toluene at 50℃; | 90% |
Conditions | Yield |
---|---|
With copper diacetate In water at 20℃; for 12h; aza-Michael addition; | 100% |
copper diacetate In water at 20℃; for 15h; aza-type Michael addition; | 100% |
at 0℃; Inert atmosphere; | 99% |
2-bromobenzoic acid chloride
diethylamine
2-bromo-N,N-diethylbenzamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 0.5h; Inert atmosphere; | 100% |
In dichloromethane at 0 - 20℃; Schlenk technique; | 99% |
In dichloromethane at 0 - 20℃; for 0.5h; | 95% |
formaldehyd
4-acetaminophenol
diethylamine
N-{3-[(diethylamino)methyl]-4-hydroxyphenyl}acetamide
Conditions | Yield |
---|---|
In ethanol at 80℃; for 1.5h; Microwave irradiation; | 100% |
In ethanol for 12h; Heating; | 80% |
In ethanol at 80℃; for 1h; Microwave irradiation; | 77% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 14h; Inert atmosphere; | 100% |
With triethylamine In dichloromethane at 0 - 20℃; for 14h; Inert atmosphere; | 100% |
With diethyl ether; triethylamine | |
With benzene |
fumaryl dichloride
diethylamine
N1,N1,N4,N4-tetraethylfumaramide
Conditions | Yield |
---|---|
In diethyl ether at 0 - 20℃; Inert atmosphere; | 100% |
With diethyl ether |
Conditions | Yield |
---|---|
With copper diacetate In water at 20℃; for 12h; aza-Michael addition; | 100% |
iron(III) chloride In water at 20℃; for 15h; aza-type Michael addition; | 100% |
1-butyl-3-methylimidazolium Tetrafluoroborate In water at 20℃; for 7h; aza-Michael reaction; | 97% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 100% |
With benzene | |
With diethyl ether | |
In benzene | |
With sodium carbonate In benzene at 0 - 5℃; |
Conditions | Yield |
---|---|
In dichloromethane; water at 5℃; Temperature; Solvent; | 100% |
With triethylamine In dichloromethane at 0℃; | 99% |
With triethylamine In 1,2-dichloro-ethane at 10 - 20℃; for 3h; Cooling with ice; | 95% |
formaldehyd
diethylamine
phenylacetylene
diethyl-(3-phenyl-prop-2-ynyl)-amine
Conditions | Yield |
---|---|
With copper dichloride at 80℃; under 150.015 Torr; for 3h; Mannich reaction; | 100% |
With silver nitrate at 105℃; for 0.133333h; microwave irradiation; | 99% |
copper(l) iodide In water; dimethyl sulfoxide at 30℃; for 10h; | 98% |
Conditions | Yield |
---|---|
In ethanol; water at 60℃; for 6h; | 100% |
In acetonitrile at 25℃; for 2h; Solvent; | 85% |
With ethanol | |
With sodium carbonate In acetone for 5h; Substitution; Heating; | |
In acetonitrile at 25℃; Kinetics; Solvent; |
diethylamine
hydrocinnamic acid chloride
N,N-diethyl-3-phenylpropanamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 14h; Inert atmosphere; | 100% |
With triethylamine In dichloromethane at 0 - 20℃; for 14h; Inert atmosphere; | 96% |
Conditions | Yield |
---|---|
With copper diacetate In water at 20℃; for 12h; aza-Michael addition; | 100% |
iron(III) chloride In dichloromethane at 25℃; for 42h; Product distribution; various catalysts and further amines with various Michael acceptors; | 96% |
iron(III) chloride In dichloromethane at 25℃; for 42h; | 96% |
Conditions | Yield |
---|---|
With phosphorus trichloride In diethyl ether at -78 - 20℃; for 2h; | 100% |
With phosphorus trichloride In diethyl ether at -78 - 20℃; Inert atmosphere; | 100% |
With phosphorus trichloride In diethyl ether at -78 - 20℃; for 2h; | 100% |
Conditions | Yield |
---|---|
With [NO(1+)*18-crown-6*H(NO3)2(1-)] In dichloromethane at 20℃; for 0.0833333h; | 100% |
With magnesium hydrogen sulfate; silica gel; sodium nitrite In dichloromethane at 20℃; for 1h; Nitrosation; | 98% |
With aluminium trichloride; silica gel; sodium nitrite In dichloromethane at 20℃; for 0.5h; Nitrosation; | 98% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 0℃; Inert atmosphere; | 100% |
In tetrahydrofuran at 0℃; for 0.0833333h; Inert atmosphere; | 100% |
With triethylamine In methanol; toluene at 0℃; for 2h; | 95% |
diethylamine
dimethyl acetylenedicarboxylate
dimethyl (2E)-2-(diethylamino)but-2-enedioate
Conditions | Yield |
---|---|
In water at 20℃; for 2h; Michael-type addition; | 100% |
In diethyl ether |
Conditions | Yield |
---|---|
In acetonitrile at 30℃; under 6750540 Torr; for 96h; | 100% |
Stage #1: diethylamine With diisobutylaluminium hydride In tetrahydrofuran; toluene Stage #2: 4-butanolide In tetrahydrofuran at 45℃; for 2h; | 72% |
carbon monoxide
benzyl bromide
diethylamine
S-benzyl N,N-diethylthiolcarbamate
Conditions | Yield |
---|---|
With sulfur; selenium In tetrahydrofuran 1.) 30 deg C; 2.) rt.; | 100% |
With n-butyllithium; sulfur 1.) THF/hexane, from -78 deg C to -20 deg C; 2.) - 78 deg C; 3.) 20 deg C, 1 atm, 2 h; Yield given. Multistep reaction; | |
Yield given. Multistep reaction; |
7-chloro-1,3-dimethyl-6-azalumazine
diethylamine
7-(diethylamino)-1,3-dimethyl-6-azalumazine
Conditions | Yield |
---|---|
In dichloromethane for 2.5h; | 100% |
formaldehyd
N-(3-sec-Butyl-4-hydroxy-phenyl)-acetamide
diethylamine
N-(3-sec-Butyl-5-diethylaminomethyl-4-hydroxy-phenyl)-acetamide
Conditions | Yield |
---|---|
In ethanol for 48h; Heating; | 100% |
formaldehyd
N-(6-Hydroxy-2',5'-dimethoxy-biphenyl-3-yl)-acetamide
diethylamine
N-(5-Diethylaminomethyl-6-hydroxy-2',5'-dimethoxy-biphenyl-3-yl)-acetamide
Conditions | Yield |
---|---|
In ethanol; water Heating; | 100% |
formaldehyd
N-(6-Hydroxy-2'-trifluoromethyl-biphenyl-3-yl)-acetamide
diethylamine
N-(5-Diethylaminomethyl-6-hydroxy-2'-trifluoromethyl-biphenyl-3-yl)-acetamide
Conditions | Yield |
---|---|
In ethanol; water Heating; | 100% |
formaldehyd
3a,3b,4,4a,7a,8,8b-octahydro-4,8-ethenopyrrolo<3',4':3,4>cyclobut<1,2-f>isoindole-1,3,5,7<2H,6H>tetrone
diethylamine
C24H34N4O4
Conditions | Yield |
---|---|
In water; N,N-dimethyl-formamide at 70℃; for 6h; | 100% |
ethylene glycol diacrylate
diethylamine
1,10-bis-diethylamino-4,7-dioxa-3,8-dioxodecane
Conditions | Yield |
---|---|
In diethyl ether for 18h; Ambient temperature; | 100% |
Diethylamino-(chlormethyl)-chlorphosphin
diethylamine
P-(Chloromethyl)-N,N,N',N'-tetraethylphosphonous diamide
Conditions | Yield |
---|---|
In diethyl ether | 100% |
o-formylbenzonitrile
diethylamine
3-Diethylamino-2,3-dihydro-isoindol-1-one
Conditions | Yield |
---|---|
at 40℃; for 1h; | 100% |
(E)-4-Ethoxy-1,1,1-trifluoro-3-buten-2-one
diethylamine
β-(N,N-diethylamino)vinyltrifluoromethylketone
Conditions | Yield |
---|---|
In acetonitrile Ambient temperature; | 100% |
In cyclohexane at 19.9℃; Rate constant; other solvents; ΔG(excit.), ΔH(excit.), ΔS(excit.); | |
In cyclohexane at 19.9℃; Yield given; |
4-bromo-4-methyl-1-phenyl-pent-1-yn-3-one
diethylamine
(Z)-4-Bromo-1-diethylamino-4-methyl-1-phenyl-pent-1-en-3-one
Conditions | Yield |
---|---|
In hexane Ambient temperature; | 100% |
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