DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:59-88-1
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inquiryItems Standard Result Appearance White or slightly reddish crystal slightly reddish crystal Assay
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Cas:59-88-1
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inquiryPhenylhydrazine hydrochloride Basic information Product Name: Phenylhydrazine hydrochloride Synonyms: PHENYLHYDRAZINE HCL;PHENYLHYDRAZINE HYDROCHLORIDE;PHENYLHYDRAZINIUM CHLORIDE;PHNEYLH
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:59-88-1
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiry1)quick response within 12 hours; 2)quality guarantee: all products are strictly tested by our qc, confirmed by qa and approved by third party lab in china, usa, canada, germany, uk, italy, france etc. 3) oem/odm available; 4) rea
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inquiryOur Adwantage: 1.We have stock so we can delivery quickly at the very day when receive the payment. 2.Best price, first class service, high successful delivery rate. A discount would be given when you make a large order. 3.High quality gua
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Cas:59-88-1
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Type:Trading Company
inquiryPhenylhydrazine hydrochloride CAS: 59-88-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organ
Cas:59-88-1
Min.Order:1 Gram
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:59-88-1
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryPacking: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Transportation:Express/Sea/Air Port:Ningbo/Shanghai/Qingd
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:59-88-1
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inquirySuperior quality Appearance:white to tan solid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application: selective mannosidase inhibitor Transportation:BY
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inquiryProduct name: Phenylhydrazine Hydrochloride CAS No.:59-88-1 Molecule Formula:C6H9ClN2 Molecule Weight:144.60 Purity: 99% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard TESTING IT
Cas:59-88-1
Min.Order:1 Kilogram
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inquiryHigh quality, competitive price, fast delivery and first-class service we possesses have won the trust and praise of customers. Standard: BP/USP/EP The purity is equal or greater than 99%. As a supplier, we can provide high-quality products. Cle
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inquiryPhenylhydrazine hydrochloride Chemical Properties Melting point 250-254 °C (dec.)(lit.) Boiling point 236.22°C (rough estimate) density 1.1672 (rough estimate) refractive index 1.5210 (estimate) storage temp. −20°
Cas:59-88-1
Min.Order:1 Gram
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:59-88-1
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Cas:59-88-1
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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inquiry1, High quality with competitive price:2, Fast and safe delivery3.Excellent pre-sales and after-sales service4. Well-trained and professional technologist and sales with rich experience in the field for 5-10 yearsAppearance:see detailed specification
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inquiryConditions | Yield |
---|---|
Stage #1: aniline With hydrogenchloride; sodium nitrite In water at 0℃; for 1h; Stage #2: With hydrogenchloride; tin(ll) chloride In water at 20℃; for 2h; | 98% |
Stage #1: aniline With hydrogenchloride In water for 0.166667h; Cooling with ice; Stage #2: With sodium nitrite In water for 1h; Cooling with ice; Stage #3: With hydrogenchloride; tin(ll) chloride In water for 3h; Cooling with ice; | 94.1% |
Stage #1: aniline With hydrogenchloride; sodium nitrite In water at 0 - 5℃; for 1h; Stage #2: With sodium sulfite In water at 80℃; for 2h; Stage #3: With hydrogenchloride In water at 100℃; for 2h; | 94% |
di-tert-butyl 1-phenylhydrazine-1,2-dicarboxylate
phenylhydrazine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In 1,4-dioxane; isopropyl alcohol for 0.25h; Heating; | 88% |
Conditions | Yield |
---|---|
Stage #1: iodobenzene With potassium phosphate; copper(l) iodide; N,N′-bis(2,6-dimethylphenyl)oxalamide; cetyltrimethylammonim bromide In water at 80℃; for 0.25h; Schlenk technique; Inert atmosphere; Sealed tube; Stage #2: With hydrazine hydrate In water at 80℃; Inert atmosphere; Schlenk technique; Sealed tube; Stage #3: With hydrogenchloride In water pH=3 - 4; Inert atmosphere; Schlenk technique; Sealed tube; | 87% |
Conditions | Yield |
---|---|
With chloroform at 60℃; | A 85% B 0.5 g |
Conditions | Yield |
---|---|
Stage #1: bromobenzene With potassium phosphate; copper(l) iodide; N,N′-bis(2,6-dimethylphenyl)oxalamide; cetyltrimethylammonim bromide In water at 80℃; for 0.25h; Schlenk technique; Inert atmosphere; Sealed tube; Stage #2: With hydrazine hydrate In water at 80℃; Inert atmosphere; Schlenk technique; Sealed tube; Stage #3: With hydrogenchloride In water pH=3 - 4; Inert atmosphere; Schlenk technique; Sealed tube; | 85% |
Stage #1: bromobenzene With potassium phosphate; N,N'-bis(2,5-dimethylpyrrol-1-yl)oxalamide; cetyltrimethylammonim bromide; copper(I) bromide In water at 110℃; for 0.166667h; Sealed tube; Inert atmosphere; Stage #2: With hydrazine hydrate In water at 110℃; for 1h; Sealed tube; Inert atmosphere; Stage #3: With hydrogenchloride In dichloromethane; water | 71% |
Multi-step reaction with 2 steps 1: bis(triphenylphosphine)nickel(II) chloride; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride; sodium t-butanolate / 1,4-dioxane / 5 h / 50 °C / Inert atmosphere 2: hydrogenchloride / water / 20 °C View Scheme |
phenylazobenzenethiosulfonate
phenylhydrazine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; sodium sulfite at 40 - 60℃; for 4h; | 79% |
Conditions | Yield |
---|---|
With hydrogenchloride In water at 20℃; | 56% |
but-2-ene-1,4-diylbis(triphenylphosphinium) dichloride
phenylhydrazine
A
C24H21N2P*ClH
B
triphenyl(4-phenylhydrazonobut-2-enyl)phosphonium chloride
D
phenylhydrazine hydrochloride
E
Triphenylphosphine oxide
Conditions | Yield |
---|---|
In chloroform at 55 - 57℃; for 10h; | A 19% B 46% C 7% D 0.37 g E 34% |
{Et4N}{oxomolybdenum(Cl)4(H2O)}
phenylhydrazine
B
phenylhydrazine hydrochloride
Conditions | Yield |
---|---|
In propan-1-ol addn. of org. compd. to suspn. of Mo-compd. in propanol, stirring (5 h, room temp.); filtn., standing (room temp., 48 h); elem. anal.; | A 39% B n/a |
Conditions | Yield |
---|---|
in der Waerme; |
ethanol
4-chloro-3-phenyl-1,2,3-λ5-oxadiazol-3-ium-5-olate
A
phenylhydrazine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride |
hydrogenchloride
1-phenylsemicarbazide
A
1-phenylurazole
B
phenylhydrazine hydrochloride
Conditions | Yield |
---|---|
at 120℃; schliesslich bei 140-150grad; |
hydrogenchloride
N-phenyl-N,N'-dibenzylhydrazine
A
phenylhydrazine hydrochloride
B
benzyl chloride
hydrogenchloride
1-benzylidene-3-formyl-2-phenyl-triazane
A
phenylhydrazine hydrochloride
B
benzaldehyde
Chloro<(1S)-7,7-dimethyl-2-oxobicyclo<2.2.1>hept-1-yl>sulfine
phenylhydrazine
A
phenylhydrazine hydrochloride
Conditions | Yield |
---|---|
Stage #1: aniline hydrochloride With hydrogenchloride; sodium nitrite In water at 0 - 5℃; for 1h; Stage #2: With tin(ll) chloride for 2h; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) NaNO2, aq. HCl, 2.) NaHCO3 / 2.) -5 - -3 deg C 2: 79 percent / 1.) sodium sulfite, 2.) conc. aq. HCl / 4 h / 40 - 60 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 60 percent / tetrahydrofuran / 0.17 h / -78 °C 2: 88 percent / HCl / propan-2-ol; dioxane / 0.25 h / Heating View Scheme | |
With di-tert-butyl-diazodicarboxylate In tetrahydrofuran; cyclohexane |
sodium salt of phenyldiazosulfonic acid
phenylhydrazine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; platinum In water |
Nitrosophenylamine
phenylhydrazine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; tin(ll) chloride In water at 0℃; |
2-Hydroxy-cyclohexanon-2-carbonsaeureamid
phenylhydrazine hydrochloride
3a-Hydroxy-2-phenyl-3,3a,4,5,6,7-hexahydro-2H-indazol-3-on
Conditions | Yield |
---|---|
In water for 0.0333333h; Heating; | 100% |
phenylhydrazine hydrochloride
4-(2-tert-butoxycarbonyl-2-oxo-ethyl)-5-oxo-pyrrolidine-1,2-dicarboxylic acid di-tert-butyl ester
Conditions | Yield |
---|---|
With sodium acetate In methanol for 1h; Ambient temperature; | 100% |
4-oxocyclohexanecarboxylic acid
phenylhydrazine hydrochloride
2,3,4,9-tetrahydro-1H-carbazole-3-carboxylic acid
Conditions | Yield |
---|---|
With zinc(II) chloride In acetic acid at 70℃; for 20h; | 100% |
In ethanol for 3h; Heating / reflux; | 84% |
In ethanol for 3h; Reflux; | 84% |
Conditions | Yield |
---|---|
In dichloromethane (N2); stirring (-78°C, 0.08 h); warming to room temp., solvent removal (vac.), drying (vac., 0.5 h), pentane addn., stirring (0.2 h), filtn., washing (pentane), drying (vac.); | 100% |
2'-chloro-5'-nitroacetophenone
phenylhydrazine hydrochloride
2-(2-chloro-5-nitrophenyl)-1H-indole
Conditions | Yield |
---|---|
Stage #1: 2'-chloro-5'-nitroacetophenone; phenylhydrazine hydrochloride With acetic acid In ethanol at 80℃; Stage #2: at 120℃; Stage #3: With sodium hydroxide Cooling with ice; | 100% |
phenylhydrazine hydrochloride
chloroformic acid ethyl ester
ethyl phenylhydrazocarboxylate
Conditions | Yield |
---|---|
With pyridine In acetonitrile at 0 - 20℃; | 100% |
With pyridine In acetonitrile at 0℃; for 1.25h; | 90% |
2-methyl-3-(1-methyl-1H-pyrazol-4-yl)-3-oxopropanenitrile
phenylhydrazine hydrochloride
1′-4-dimethyl-1-phenyl-1H,1′H-[3,4′-bipyrazol]-5-amine
Conditions | Yield |
---|---|
In ethanol at 20℃; Reflux; | 100% |
In ethanol for 17h; Time; Reflux; | 100% |
In ethanol at 20℃; Reflux; | 100% |
2-methyl-3-(1-methyl-1H-pyrazol-4-yl)-3-oxopropanenitrile
phenylhydrazine hydrochloride
Conditions | Yield |
---|---|
In ethanol Reflux; | 100% |
phenylhydrazine hydrochloride
Conditions | Yield |
---|---|
In methanol for 0.5h; Reflux; | 100% |
2-(pentafluoroethyl)-3,4-dihydro-2H-pyrrole
phenylhydrazine hydrochloride
Conditions | Yield |
---|---|
In methanol for 0.5h; Reflux; | 100% |
7-(trifluoromethyl)-3,4,5,6-tetrahydro-2H-azepine
phenylhydrazine hydrochloride
Conditions | Yield |
---|---|
In methanol for 0.5h; Reflux; | 100% |
6-(trifluoromethyl)-2,3,4,5-tetrahydropyridine
phenylhydrazine hydrochloride
Conditions | Yield |
---|---|
In methanol for 0.5h; Reflux; | 100% |
acetamidine hydrochloride
phenylhydrazine hydrochloride
N-[(tert-butoxy)carbonyl]piperidine-4-carboxylic acid
Conditions | Yield |
---|---|
Stage #1: acetamidine hydrochloride; N-[(tert-butoxy)carbonyl]piperidine-4-carboxylic acid With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 2h; Stage #2: phenylhydrazine hydrochloride With acetic acid In N,N-dimethyl-formamide at 80℃; for 4h; | 100% |
phenylhydrazine hydrochloride
Conditions | Yield |
---|---|
Stage #1: phenylhydrazine hydrochloride With 1,8-diazabicyclo[5.4.0]undec-7-ene Stage #2: 1,1,1-trifluoro-4-(1-methoxynaphthalen-4-yl)but-3-yn-2-one for 24h; regioselective reaction; | 100% |
phenylhydrazine hydrochloride
pivaloyl chloride
N’-phenyl-N-pivaloylhydrazine
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 0.0833333h; | 99.6% |
Conditions | Yield |
---|---|
With acetic acid at 90 - 120℃; for 1h; Temperature; | 99% |
With L-(+)-tartaric acid-urea melt at 70℃; for 0.25h; Fischer Indole Synthesis; | 97% |
With 1-(3-sulfopropyl)pyridinium p-toluenesulfonate In water at 100℃; for 0.166667h; | 96% |
Conditions | Yield |
---|---|
With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃; | 99% |
Conditions | Yield |
---|---|
With acetic acid at 20℃; | 99% |
phenylhydrazine hydrochloride
2-Methylcyclohexanone
4a-methyl-2,3,4,4a-tetrahydro-1H-carbazole
Conditions | Yield |
---|---|
With L-(+)-tartaric acid-urea melt at 70℃; for 0.5h; Fischer Indole Synthesis; | 99% |
With acetic acid for 2h; Reflux; | 65% |
With acetic acid at 120℃; for 14h; Inert atmosphere; Schlenk technique; | |
In acetic acid for 2h; Inert atmosphere; Reflux; | 12.5 g |
phenylhydrazine hydrochloride
1-benzyl-4-(5-(4-methoxyphenyl)-1-phenyl-4,5-dihydro-1H-pyrazol-3-yl)-5-methyl-1H-1,2,3-triazole
Conditions | Yield |
---|---|
In water for 1h; Solvent; Reflux; Green chemistry; | 99% |
phenylhydrazine hydrochloride
1-benzyl-4-(5-(4-fluorophenyl)-1-phenyl-4,5-dihydro-1H-pyrazol-3-yl)-5-methyl-1H-1,2,3-triazole
Conditions | Yield |
---|---|
In water for 1.5h; Solvent; Reflux; Green chemistry; | 99% |
Conditions | Yield |
---|---|
With sodium acetate In water | 99% |
phenylhydrazine hydrochloride
4-(4-chlorophenyl)-1,1,1-trifluorobut-3-yn-2-one
5-(4-chlorophenyl)-1-phenyl-3-(trifluoromethyl)-1H-pyrazole
Conditions | Yield |
---|---|
Stage #1: phenylhydrazine hydrochloride With 1,8-diazabicyclo[5.4.0]undec-7-ene Stage #2: 4-(4-chlorophenyl)-1,1,1-trifluorobut-3-yn-2-one for 24h; regioselective reaction; | 99% |
phenylhydrazine hydrochloride
1-phenyl-3-(trifluoromethyl)-5-(4-bromophenyl)-1H-pyrazole
Conditions | Yield |
---|---|
Stage #1: phenylhydrazine hydrochloride With 1,8-diazabicyclo[5.4.0]undec-7-ene Stage #2: 4-(4-bromophenyl)-1,1,1-trifluorobut-3-yn-2-one for 24h; regioselective reaction; | 99% |
phenylhydrazine hydrochloride
Conditions | Yield |
---|---|
Stage #1: phenylhydrazine hydrochloride With 1,8-diazabicyclo[5.4.0]undec-7-ene Stage #2: 1,1,1-trifluoro-4-(2,3-dihydrobenzo[b][1,4]dioxin-7-yl)but-3-yn-2-one for 24h; regioselective reaction; | 99% |
Conditions | Yield |
---|---|
In water at 20℃; Fischer indole synthesis; | 98% |
With acetic acid Heating; further reagent; |
phenylhydrazine hydrochloride
Norhydromorphone hydrochloride
Conditions | Yield |
---|---|
In acetic acid at 90℃; for 16h; | 98% |
phenylhydrazine hydrochloride
noroxymorphone
Conditions | Yield |
---|---|
With hydrogenchloride for 16h; Heating; | 98% |
With hydrogenchloride In methanol Reflux; |
ethyl 2-(1H-indol-3-yl)-2-oxoacetate
phenylhydrazine hydrochloride
2-phenylpyrazolo[3,4-c]quinolin-4(5H)-one
Conditions | Yield |
---|---|
With acetic acid In ethanol at 140℃; for 0.05h; microwave irradiation; | 98% |
With acetic acid In ethanol at 140℃; for 0.05h; Microwave irradiation; | 98% |
With acetic acid In ethanol for 3h; Heating; | 72% |
phenylhydrazine hydrochloride
cycloheptanone
5,6,7,8,9,10-hexahydrocyclohept[b]indole
Conditions | Yield |
---|---|
With L-(+)-tartaric acid-urea melt at 70℃; for 1h; Fischer Indole Synthesis; | 98% |
With 1-(3-sulfopropyl)pyridinium p-toluenesulfonate In water at 100℃; for 0.166667h; | 93% |
With 1,3-bis(3-sulfopropyl)-1H-imidazol-3-ium trifluoromethanesulfonate In water at 100℃; for 0.25h; Fischer Indole Synthesis; Microwave irradiation; Green chemistry; | 91% |
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