high purity of 99.5% above; stable supply with MTs stock material; Hangzhou Verychem Science And Technology Co. Ltd. was set up in year 2004, it’s a young but fast growing company. In the twelve years history, it invested two pharmaceutical
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Cas:496-15-1
Min.Order:0 Metric Ton
Negotiable
Type:Manufacturers
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Good quantity Indoline Basic information Product Name: Indoline Synonyms: 1-Azaindan;2,3-dihydro-1h-indol;Dihydroindole;2,3-DIHYDROINDOLE;2,3-DIHYDRO-1H-INDOLE HYDROCHLORIDE;2,3-DIHYDR
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Min.Order:1 Kilogram
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Product Name: Indoline Synonyms: 1-Azaindan;2,3-dihydro-1h-indol;Dihydroindole;2,3-DIHYDROINDOLE;2,3-DIHYDRO-1H-INDOLE HYDROCHLORIDE;2,3-DIHYDRO-1H-INDOLE;LABOTEST-BB LT01605668;INDOLINE CAS:
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superior quality Appearance:Clear colorless to slightly brown liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:An indole derivative used in
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A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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N-(benzyloxycarbonyl)indoline
1-indoline
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal; ethylenediamine In tetrahydrofuran at 20℃; under 760 Torr; for 1.5h; Hydrogenation; | 100% |
With boron trifluoride diethyl etherate; ethanethiol In chloroform for 14h; Ambient temperature; | 93% |
With tetrabutyl ammonium fluoride In tetrahydrofuran for 8h; Heating; | 22% |
Conditions | Yield |
---|---|
With hydrogen In water at 100℃; under 22502.3 Torr; for 10h; | 99% |
With tetrahydroxydiboron; palladium on activated carbon In 2,2,2-trifluoroethanol; water at 40℃; for 24h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Schlenk technique; | 99% |
With sodium cyanoborohydride; acetic acid at 20℃; for 10h; Cooling with ice; | 98% |
Conditions | Yield |
---|---|
With triethyl borane; Triethoxysilane; sodium hydroxide In hexane at 80℃; for 6h; Solvent; Reagent/catalyst; Inert atmosphere; Sealed tube; | A 97% B 2% |
Conditions | Yield |
---|---|
With sodium hydroxide | 96% |
indolin-1-yl(pyridin-2-yl)methanone
1-indoline
Conditions | Yield |
---|---|
With ammonium bromide; ethylenediamine at 50℃; for 5h; Microwave irradiation; Inert atmosphere; neat (no solvent); | 96% |
With ammonium bromide; ethylenediamine at 50℃; for 5h; Reagent/catalyst; Solvent; Microwave irradiation; | 96% |
With ammonium iodide; hydrazine hydrate In ethanol at 50℃; for 18h; Inert atmosphere; Sealed tube; | 85% |
With water; sodium hydroxide In tetrahydrofuran; methanol at 50℃; for 24h; | 83% |
With methanol; sodium hydroxide In tetrahydrofuran; water at 50℃; for 24h; |
1-indoline
Conditions | Yield |
---|---|
With potassium carbonate; mercaptoacetic acid In methanol at 0 - 25℃; Inert atmosphere; chemoselective reaction; | 96% |
1-indoline
Conditions | Yield |
---|---|
With potassium carbonate at 200℃; for 2h; Inert atmosphere; Sealed tube; | 96% |
2-(2-bromophenyl)ethanamine
1-indoline
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; palladium 10% on activated carbon; sodium t-butanolate In 1,3,5-trimethyl-benzene at 140℃; for 24h; Solvent; Temperature; Inert atmosphere; | 95% |
With 2-(2-methyl-1-oxopropyl)cyclohexanone; caesium carbonate; copper(l) iodide In N,N-dimethyl-formamide at 20℃; for 0.5h; | 92% |
With potassium phosphate; N,N-diethylsalicylamide; copper (I) acetate In N,N-dimethyl-formamide at 35℃; for 12h; | 88% |
indole
1,4,4a,9a-tetrahydro-fluorene
A
1-indoline
B
9H-fluorene
Conditions | Yield |
---|---|
palladium on activated carbon at 250℃; for 2h; | A 90% B 95% |
C18H16N4O
A
1-indoline
B
1-benzyl-1H-[1,2,3]triazol-4-carboxylic acid
Conditions | Yield |
---|---|
With water; lithium hydroxide In tetrahydrofuran; methanol at 80℃; for 4h; Temperature; Time; | A 95% B 82% |
Conditions | Yield |
---|---|
With water; lithium hydroxide In tetrahydrofuran; methanol at 20℃; for 4h; | A n/a B 95% |
Conditions | Yield |
---|---|
Stage #1: 2-aminophenethyl alcohol With thionyl chloride In 1,2-dimethoxyethane at 20℃; Stage #2: In 1,2-dimethoxyethane; water at 60℃; Further stages.; | 94% |
With sodium hydroxide; benzenesulfonyl chloride | |
With zinc(II) chloride at 200℃; |
Conditions | Yield |
---|---|
With water; lithium hydroxide In tetrahydrofuran; methanol at 20℃; for 3.5h; | A 94% B n/a |
Conditions | Yield |
---|---|
In 5,5-dimethyl-1,3-cyclohexadiene; nitrogen; water | 93% |
1-benzenesulfonyl-2,3-dihydro-1H-indole
1-indoline
Conditions | Yield |
---|---|
With cesium fluoride supported on Celite at 120℃; for 2.5h; chemoselective reaction; | 91% |
Conditions | Yield |
---|---|
copper(I) chloride In benzene | 90.8% |
indole
1,2,3,4-tetrahydro-9H-fluorene
A
1-indoline
B
9H-fluorene
Conditions | Yield |
---|---|
A 90% B n/a |
1-(trifluoromethylsulfonyl)indoline
1-indoline
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In diethyl ether for 1h; Reflux; | 90% |
Conditions | Yield |
---|---|
With 5% Ru/MgO; hydrogen In tetrahydrofuran at 150℃; under 38002.6 Torr; for 0.4h; | A 10% B 90% |
With 6C53H32O8(4-)*13Zr(4+)*18O(2-)*8Co(2+)*8H(1-); hydrogen In tetrahydrofuran at 80℃; under 30003 Torr; for 66h; | A n/a B 84% |
With 6C53H32O8(4-)*13Zr(4+)*18O(2-)*8Co(2+)*8Cl(1-); hydrogen; sodium triethylborohydride In toluene at 80℃; under 30003 Torr; for 66h; | A n/a B 84% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; titanium tetrachloride In 1,2-dimethoxyethane for 14h; Ambient temperature; | 89% |
1-indoline
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid; methoxybenzene In dichloromethane at 0℃; desulfonation; | 88% |
1-indoline
Conditions | Yield |
---|---|
With sodium hydroxide In tetrahydrofuran; methanol at 100℃; for 24h; | 88% |
1-Acetyl-2,3-dihydro-1H-indole
1-indoline
Conditions | Yield |
---|---|
With sodium triethylborohydride In tetrahydrofuran at 80℃; for 12h; Inert atmosphere; Schlenk technique; Glovebox; Sealed tube; | 88% |
With sodium triethylborohydride In tetrahydrofuran at 80℃; for 6h; Inert atmosphere; Schlenk technique; High pressure; Sealed tube; | 88% |
2,3-dihydroindole-1-carboxylic acid methyl ester
1-indoline
Conditions | Yield |
---|---|
With 3-azapentane-1,5-diamine at 130℃; for 12h; Sealed tube; | 86% |
2-(2-chlorophenyl)ethanamine
1-indoline
Conditions | Yield |
---|---|
With 2-(2-methyl-1-oxopropyl)cyclohexanone; caesium carbonate; copper(l) iodide In N,N-dimethyl-formamide at 60℃; for 10h; | 85% |
With potassium phosphate; N,N-diethylsalicylamide; copper (I) acetate In N,N-dimethyl-formamide at 50℃; for 48h; | 78% |
With copper(l) iodide; N,N`-dimethylethylenediamine In dimethyl sulfoxide at 25℃; for 48h; Inert atmosphere; | 76% |
With copper(l) iodide; potassium carbonate; L-proline In dimethyl sulfoxide at 70℃; for 45h; | 71% |
With sodium hydride; tert-butyl alcohol; 1,3-bis[2,6-bis(1-methylethyl)phenyl]-1,3-dihydro-2H-imidazol-2-ylidene monohydrochloride; palladium diacetate In 1,4-dioxane for 4h; |
(R)-indoline-carboxylic acid
1-indoline
Conditions | Yield |
---|---|
In dimethyl sulfoxide for 2h; UV-irradiation; | 85% |
In d7-N,N-dimethylformamide Thermodynamic data; |
1-indoline
chloroacetyl chloride
2-Chloro-1-(2,3-dihydro-1H-1-indolyl)-1-ethanone
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 3h; | 100% |
With N,N-dimethyl acetamide at 0℃; for 0.0833333h; Green chemistry; | 89% |
In acetone at 0 - 20℃; for 1h; | 63% |
1-indoline
benzenesulfonyl chloride
1-benzenesulfonyl-2,3-dihydro-1H-indole
Conditions | Yield |
---|---|
With triethylamine In 1,2-dichloro-ethane at 0 - 20℃; for 1h; | 100% |
With potassium trimethylsilonate In water at 20℃; for 0.5h; Concentration; Inert atmosphere; | 97% |
With dmap; triethylamine In dichloromethane at 0 - 20℃; | 96% |
Conditions | Yield |
---|---|
100% |
Conditions | Yield |
---|---|
With pyridine for 18h; | 100% |
Conditions | Yield |
---|---|
Heating; | 100% |
With pyridine at 120℃; for 4h; Inert atmosphere; Schlenk technique; | 97% |
With pyridine at 120℃; for 4h; Inert atmosphere; Schlenk technique; | 97% |
Conditions | Yield |
---|---|
With sodium bicarbonate In water; toluene | 100% |
Stage #1: 1-indoline With sodium hydrogencarbonate In water at 90℃; Stage #2: benzyl chloride In water at 90℃; | 99% |
With cesium fluoride In acetonitrile for 48h; Heating; | 98% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane 1.) 0 deg C, 10 min, 2.) RT, 1 h; | 100% |
In tetrahydrofuran for 2h; Heating; | 63% |
Conditions | Yield |
---|---|
Stage #1: 1-indoline; benzonitrile With aluminum (III) chloride; water; boron trichloride In dichloromethane; toluene at 110℃; Stage #2: With hydrogenchloride; water In dichloromethane; toluene at 80℃; for 1h; | 100% |
Stage #1: 1-indoline; benzonitrile With aluminum (III) chloride; boron trichloride In dichloromethane; toluene at 0 - 110℃; Stage #2: With hydrogenchloride; water at 80℃; for 1h; | 100% |
With aluminum (III) chloride; boron trichloride In toluene Friedel-Crafts Acylation; Inert atmosphere; Reflux; | 84% |
Conditions | Yield |
---|---|
In acetone at 70℃; for 3h; | 100% |
In acetone at 70℃; for 3h; Inert atmosphere; Sealed tube; | 99% |
In acetone for 1h; Reflux; | 73% |
1-indoline
trifluoroacetic anhydride
2,2,2-trifluoro-1-(indolin-1-yl)ethan-1-one
Conditions | Yield |
---|---|
With triethylamine In dichloromethane | 100% |
In dichloromethane at 0℃; for 1h; Inert atmosphere; | 100% |
In benzene at 0 - 5℃; | 96% |
Conditions | Yield |
---|---|
tris(triphenylphosphine)ruthenium(II) chloride In toluene for 6h; Rate constant; Mechanism; Heating; | 100% |
With C21H32Cl4N2Ru In toluene for 6h; Reagent/catalyst; Heating; | 100% |
With tert.-butylhydroperoxide; iron(III) chloride; C42H40Cu2N8 In water; acetonitrile at 60℃; for 16h; | 100% |
Conditions | Yield |
---|---|
Stage #1: 1-indoline With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 1h; Inert atmosphere; Stage #2: benzyl bromide In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; | 100% |
With n-butyllithium In tetrahydrofuran; hexane at -78 - 20℃; for 1.25h; | 99% |
Stage #1: 1-indoline With sodium hydrogencarbonate In water at 90 - 95℃; Stage #2: benzyl bromide In water at 90 - 95℃; for 5h; | 93% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; sulfinylation; | 100% |
1-indoline
4-(bromomethyl)benzene-1-sulfonyl chloride
Conditions | Yield |
---|---|
With triethylamine In diethyl ether at 20℃; for 3h; Substitution; | 100% |
1-indoline
4-chloro-2,6-dimethoxypyrimidine-5-carboxaldehyde
5-formyl-4-(N-indolinyl)-2,6-dimethoxypyrimidine
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 0.25h; Substitution; | 100% |
Conditions | Yield |
---|---|
In acetic acid at 90℃; for 3h; | 100% |
With sodium hydrogencarbonate In dichloromethane | 100% |
With sodium hydrogencarbonate In dichloromethane at 20℃; for 2h; | 100% |
1-indoline
N-tert-butyloxycarbonylpiperidin-4-one
tert-butyl 4-(indolin-1-yl) piperidine-1-carboxylate
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride; acetic acid In 1,2-dichloro-ethane at 0 - 65℃; for 65h; Product distribution / selectivity; | 100% |
With sodium tris(acetoxy)borohydride; acetic acid at 0 - 25℃; for 1h; Product distribution / selectivity; | 100% |
Stage #1: 1-indoline; N-tert-butyloxycarbonylpiperidin-4-one With acetic acid In 1,2-dichloro-ethane at 0℃; for 0.166667h; Stage #2: With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 10 - 20℃; for 65h; Product distribution / selectivity; | 100% |
1-indoline
D-Glucose
1-(β-D-glucopyranosyl)indoline
Conditions | Yield |
---|---|
In ethanol; water for 26h; Reflux; | 100% |
In ethanol; water for 26h; Reflux; | 100% |
In ethanol; water for 24h; Heating; | 95% |
In ethanol; water for 24h; | 95% |
In ethanol Reflux; |
1-indoline
Allyl chloroformate
2,3-dihydroindole-1-carboxylic acid allyl ester
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 20℃; for 1h; | 100% |
1-indoline
2-Nitrobenzenesulfonyl chloride
1-((2-nitrophenyl)sulfonyl)indoline
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; | 100% |
Stage #1: 1-indoline; 2-Nitrobenzenesulfonyl chloride at 20℃; Stage #2: With sodium hydroxide for 0.666667h; | 72% |
With pyridine; dmap; triethylamine at 0 - 110℃; for 27.5h; Inert atmosphere; | 57% |
1-indoline
Piperonylic acid
1-[(1,3-benzodioxol-5-yl)carbonyl]-2,3-dihydroindole
Conditions | Yield |
---|---|
With dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane for 2h; Inert atmosphere; | 100% |
With PS-triphenylphosphane; iodine; N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 2h; |
1-indoline
3-fluorobenzene-1-sulfonyl chloride
1-((3-fluorophenyl)sulfonyl)indoline
Conditions | Yield |
---|---|
With pyridine at 20℃; | 100% |
In pyridine at 20℃; for 20h; |
1-indoline
3-methylphenylsulfonyl chloride
1-(m-tolylsulfonyl)indoline
Conditions | Yield |
---|---|
With pyridine at 20℃; | 100% |
Conditions | Yield |
---|---|
With pyridine at 20℃; | 100% |
1-indoline
4-Fluorobenzenesulfonyl chloride
1-((4-fluorophenyl)sulfonyl)indoline
Conditions | Yield |
---|---|
With pyridine at 20℃; | 100% |
1-indoline
6-deoxy-L-galactose
1-(β-L-fucopyranosyl)indoline
Conditions | Yield |
---|---|
In ethanol; water for 20h; Reflux; | 100% |
1-indoline
3,4-dichlorobenzoyl chloride
(3,4-dichlorophenyl)(indolin-1-yl)methanone
Conditions | Yield |
---|---|
With triethylamine In acetonitrile at 0 - 20℃; for 1h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 18℃; for 0.0833333h; Solvent; Green chemistry; | 100% |
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile Reflux; | 100% |
With potassium carbonate In acetonitrile Reflux; |
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