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Cas:625-36-5
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inquiryProduct Description Product Name 3-Chloropropionyl chloride CAS No. 625-36-5 Appearan
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiry3-Chloropropionyl chloride Basic information Product Name: 3-Chloropropionyl chloride Synonyms: 3-Chloropropanoyl chloride;3-chloro-propanoylchlorid;beta-Chloropropanoyl chloride;beta-Ch
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inquiryProduct name: 3-Chloropropionyl chloride CAS : 625-36-5 Appearance: Colorless transparent liquid Content: 99% Appearance:Colorless transparent liquid?? Storage:Preserve in well-closed, light-resistant and airtight containers. Package:25kg/drum App
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Min.Order:1 Gram
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiry625-36-5 99%Appearance:white powder Storage:keep cold Package:according to customers' requirements Application:Pharmaceutical intermediates 625-36-5 Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(FOB or CIF or CNF ect...)or accord
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inquiryProduct name: 3-Chloropropionyl Chloride CAS No.:625-36-5 Molecule Formula:C3H4Cl2O Molecule Weight:126.97 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS
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Min.Order:1 Kilogram
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inquiryConditions | Yield |
---|---|
With bis(trichloromethyl) carbonate In toluene at 25℃; for 8h; Reagent/catalyst; Temperature; | 98.5% |
With thionyl chloride | 63% |
With phosphorus trichloride |
Conditions | Yield |
---|---|
With bis(trichloromethyl) carbonate; N,N-dimethylpiperidine-4-carboxamide hydrochloride at 25℃; for 10h; Reagent/catalyst; Large scale; | 98% |
With phosphorus pentachloride In benzene at 20℃; for 10h; Chlorination; | 87% |
With tetrachloromethane; sulfuryl dichloride | |
With tetrachloromethane; phosphorus pentachloride | |
With thionyl chloride |
Conditions | Yield |
---|---|
With thionyl chloride In N,N-dimethyl-formamide at 80℃; under 2068.65 Torr; for 0.416667h; Reagent/catalyst; Pressure; | A 4% B 94% |
With trichlorophosphate In N,N-dimethyl-formamide at 80℃; for 0.00833333h; Reagent/catalyst; Temperature; | A 91% B 6% |
With thionyl chloride; N,N-dimethyl-formamide In neat (no solvent) at 60℃; for 0.0166667h; Catalytic behavior; Reagent/catalyst; Temperature; Time; Flow reactor; |
Conditions | Yield |
---|---|
With thionyl chloride In N,N-dimethyl-formamide at 60℃; for 0.0166667h; Reagent/catalyst; | A 7% B 82% C 11% |
Conditions | Yield |
---|---|
With phosgene; N,N-dimethyl-formamide at 70℃; for 10h; | 80% |
With N,N-dimethyl-formamide | |
With phosgene In N,N-dimethyl-formamide at 70℃; for 40h; | |
With phosgene In N,N-dimethyl-formamide at 70℃; for 40h; | 200 g |
With thionyl chloride In N,N-dimethyl-formamide at 80℃; for 0.416667h; Concentration; Reagent/catalyst; |
methyldichlorophosphane
acrylic acid
A
2-methyl-2,5-dioxo-1,2-oxaphospholane
B
2-chloropropionyl chloride
Conditions | Yield |
---|---|
In paraffin | A n/a B 76% |
A n/a B 76% |
3-(chloro-methyl-phosphinoyl)-butyryl chloride
acrylic acid
B
2-chloropropionyl chloride
Conditions | Yield |
---|---|
A n/a B 70% |
2-methyl-2,5-dioxo-1,2-oxaphospholane
2-chloropropionyl chloride
Conditions | Yield |
---|---|
70% |
Conditions | Yield |
---|---|
With aluminium trichloride; toluene | |
With carbon disulfide at -5 - -4℃; |
propionyl chloride
A
2-chloropropionyl chloride
B
2-chloropropionyl chloride
Conditions | Yield |
---|---|
With chlorine at 0 - 5℃; Irradiation.unter UV-Bestrahlung; | |
With sulfuryl dichloride; dibenzoyl peroxide | |
With sulfuryl dichloride; dibenzoyl peroxide |
Conditions | Yield |
---|---|
With chlorine at 0 - 5℃; Irradiation.UV-Bestrahlung; | |
With sulfuryl dichloride; dibenzoyl peroxide |
Conditions | Yield |
---|---|
(i) PdCl2, benzene, (ii) /BRN= 3587209/; Multistep reaction; |
Conditions | Yield |
---|---|
(i) aq. HCl, (ii) SOCl2; Multistep reaction; |
β-Propiolactone
phosphorus pentachloride
2-chloropropionyl chloride
Conditions | Yield |
---|---|
Chlorierung unter Belichtung; |
propionyl chloride
chlorine
A
2-chloropropionyl chloride
B
2-chloropropionyl chloride
Conditions | Yield |
---|---|
at 0 - 5℃; UV-Bestrahlung.Irradiation; |
sulfuryl dichloride
propionyl chloride
dibenzoyl peroxide
A
2-chloropropionyl chloride
B
2-chloropropionyl chloride
Conditions | Yield |
---|---|
With tetrachloromethane; chlorine |
phosgene
aluminium trichloride
ethene
toluene
2-chloropropionyl chloride
Conditions | Yield |
---|---|
at 35 - 40℃; |
Conditions | Yield |
---|---|
at -7 - -2℃; |
1,2,3,4-tetrahydroisoquinoline
2-chloropropionyl chloride
1,2,6,7-tetrahydropyrido<3,2,1-i,j>quinolin-3(5H)-one
Conditions | Yield |
---|---|
Stage #1: 1,2,3,4-tetrahydroisoquinoline; 2-chloropropionyl chloride In acetone for 1h; Inert atmosphere; Reflux; Stage #2: With aluminum (III) chloride; sodium chloride at 150℃; for 1h; Inert atmosphere; | 100% |
Stage #1: 1,2,3,4-tetrahydroisoquinoline; 2-chloropropionyl chloride In acetone for 1h; Reflux; Stage #2: With aluminum (III) chloride; sodium chloride at 150℃; for 0.5h; | 88% |
With acetone Erhitzen des Reaktionsprodukts mit Aluminiumchlorid; | |
With aluminium trichloride 1.) acetone, reflux, 2 h, 2.) heating; Multistep reaction; |
p-toluidine
2-chloropropionyl chloride
3-chloro-N-(4-methylphenyl)propionamide
Conditions | Yield |
---|---|
In acetone for 1h; Acylation; Heating; | 100% |
In water; acetone for 6h; Reflux; | 100% |
With potassium carbonate In acetone at 0℃; for 1h; Condensation; | 95% |
4-chloro-aniline
2-chloropropionyl chloride
3-chloro-N-(4-chlorophenyl)propanamide
Conditions | Yield |
---|---|
In acetone for 1h; Acylation; Heating; | 100% |
In acetone for 2h; Reflux; | 85% |
Stage #1: 4-chloro-aniline With sodium acetate; acetic acid In water at 5℃; Stage #2: 2-chloropropionyl chloride at 0 - 20℃; | 70% |
phenethylamine
2-chloropropionyl chloride
3-chloro-N-(4-phenylethyl)propanamide
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In chloroform; water at 20℃; for 1h; | 100% |
With sodium hydroxide |
4-nitro-aniline
2-chloropropionyl chloride
3-chloro-N-(4-nitrophenyl)propanamide
Conditions | Yield |
---|---|
at 0 - 50℃; Neat (no solvent); | 100% |
at 20 - 50℃; | 100% |
at 50℃; for 16h; | 97% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; for 2h; | 100% |
With potassium carbonate In acetone at 0℃; for 1h; Condensation; | 98% |
With potassium carbonate In water; acetone at 0℃; for 1h; | 98% |
naphthalene
2-chloropropionyl chloride
3-chloro-1-(naphthalen-2-yl)propan-1-one
Conditions | Yield |
---|---|
With aluminum (III) chloride In dichloromethane at 20℃; Cooling with ice; | 100% |
With carbon disulfide; aluminium trichloride | |
With aluminium trichloride In nitrobenzene 1.) 5 h, room temp., 2.) 30 min, 40-45 deg C; | |
Stage #1: naphthalene; 2-chloropropionyl chloride With aluminum (III) chloride In nitrobenzene at 0℃; Stage #2: With hydrogenchloride In nitrobenzene |
5-chloro-2-phenylsulfanyl-aniline
2-chloropropionyl chloride
N-(3-chloropropyl)-5-chloro-2-phenylthiophenylamine
Conditions | Yield |
---|---|
With pyridine In diethyl ether at 0℃; for 0.333333h; | 100% |
Conditions | Yield |
---|---|
With aluminum (III) chloride In dichloromethane at 0 - 20℃; Inert atmosphere; | 100% |
aluminium trichloride; nitromethane In carbon disulfide for 2h; Product distribution; Mechanism; Ambient temperature; further Friedel-Crafts catalysts, further arenes, further haloacid chlorides; variation of temperature and time; | 88% |
aluminium trichloride; nitromethane In carbon disulfide for 2h; Ambient temperature; | 88% |
thiophene
2-chloropropionyl chloride
3-chloro-1-(2-thienyl)propan-1-one
Conditions | Yield |
---|---|
Stage #1: 2-chloropropionyl chloride With aluminum (III) chloride In dichloromethane at -5℃; for 0.166667h; Friedel Crafts Acylation; Stage #2: thiophene In dichloromethane at -5℃; for 1h; Friedel Crafts Acylation; | 100% |
Stage #1: 2-chloropropionyl chloride With aluminum (III) chloride In dichloromethane at 20℃; for 0.25h; Stage #2: thiophene In dichloromethane at 0 - 20℃; for 4h; | 99% |
Stage #1: 2-chloropropionyl chloride With aluminum (III) chloride In dichloromethane at 20℃; for 0.25h; Stage #2: thiophene In dichloromethane at 0 - 20℃; for 4h; | 99% |
Conditions | Yield |
---|---|
In acetone at 70℃; for 3h; | 100% |
In acetone at 70℃; for 3h; Inert atmosphere; Sealed tube; | 99% |
In acetone for 1h; Reflux; | 73% |
methyl 3-amino-2-[[(2'-cyanobiphenyl-4-yl)methyl]amino]benzoate
2-chloropropionyl chloride
methyl 2-(2-chloroethyl)-1-[(2'-cyanobiphenyl-4-yl)methyl]benzimidazole-7-carboxylate
Conditions | Yield |
---|---|
In dichloromethane for 2h; Ambient temperature; | 100% |
With hydrogenchloride In methanol; CH2 Cl2 -H2 O; dichloromethane |
Conditions | Yield |
---|---|
In benzene for 1h; Ambient temperature; | 100% |
trans-1,2,3,4-tetrahydro-7-methoxy-1-naphthylamine
2-chloropropionyl chloride
Conditions | Yield |
---|---|
With sodium hydroxide In dichloromethane | 100% |
2-chloropropionyl chloride
2-(3-methoxyphenyl)-1-ethanamine
3-chloro-N-[2-(3-methoxyphenyl)ethyl]propionamide
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In chloroform; water at 20℃; for 1h; | 100% |
1,4-dihydro-4-(3-aminophenyl)-2,6-dimethyl-3,5-pyridinedicarboxylic acid,dimethyl ester
2-chloropropionyl chloride
Conditions | Yield |
---|---|
In tetrahydrofuran; ethyl acetate | 100% |
In tetrahydrofuran; ethyl acetate | 100% |
In tetrahydrofuran; ethyl acetate | 100% |
Conditions | Yield |
---|---|
With hydrogenchloride In acetone | 100% |
2-chloropropionyl chloride
C3H4ClN3O
Conditions | Yield |
---|---|
With sodium azide | 100% |
6-amino-4-((3-chloro-4-(pyridin-2-ylmethoxy)phenyl)amino)-7-ethoxyquinoline-3-carbonitrile
2-chloropropionyl chloride
3-chloro-N-(4-(3-chloro-4-(pyridin-2-ylmethoxy)anilino)-3-cyano-7-ethoxyquinolin-6-yl)propanamide
Conditions | Yield |
---|---|
at 50℃; for 16h; | 100% |
at 50℃; | 99% |
3-aminoisoxazole
2-chloropropionyl chloride
3-chloro-N-(isoxazol-3-yl)propanamide
Conditions | Yield |
---|---|
Stage #1: 3-aminoisoxazole With sodium hydride In tetrahydrofuran; mineral oil for 6h; Inert atmosphere; Stage #2: 2-chloropropionyl chloride In tetrahydrofuran; mineral oil at 20℃; Inert atmosphere; | 100% |
2-chloropropionyl chloride
Conditions | Yield |
---|---|
In tetrahydrofuran; water at 25℃; for 2h; | 100% |
3-bromo-4-fluorophenol
2-chloropropionyl chloride
Conditions | Yield |
---|---|
With aluminum (III) chloride In dichloromethane at -50 - 20℃; | 100% |
With aluminum (III) chloride In dichloromethane at -50 - 20℃; | 71% |
Conditions | Yield |
---|---|
Reflux; | 100% |
N,O-dimethylhydroxylamine*hydrochloride
2-chloropropionyl chloride
3-chloro-N-methoxy-N-methylpropanamide
Conditions | Yield |
---|---|
With potassium carbonate In diethyl ether; water at 0 - 20℃; Inert atmosphere; | 99.9% |
With potassium carbonate In diethyl ether; water at 0 - 20℃; Inert atmosphere; | 92% |
With potassium carbonate In tetrahydrofuran; water at 0 - 20℃; Inert atmosphere; |
tert-butylamine
2-chloropropionyl chloride
N-tert-butyl-2-(chloromethyl)acetamide
Conditions | Yield |
---|---|
With sodium hydroxide In dichloromethane; water at -20 - 20℃; for 2h; | 99% |
With sodium hydroxide; 1,2-dichloro-ethane |
o-xylene
2-chloropropionyl chloride
3-chloro-1-(3,4-dimethyl-phenyl)-propan-1-one
Conditions | Yield |
---|---|
With aluminum (III) chloride; nitromethane at 19 - 22℃; under 760.051 Torr; Friedel Crafts acylation; Inert atmosphere; | 99% |
With aluminum (III) chloride In dichloromethane at 0 - 20℃; Friedel-Crafts acylation; Inert atmosphere; | 98% |
With aluminum (III) chloride In dichloromethane at 25℃; for 3h; | 96% |
Conditions | Yield |
---|---|
In benzene for 1h; Heating; | 99% |
Conditions | Yield |
---|---|
Stage #1: 2-chloropropionyl chloride With aluminum (III) chloride In dichloromethane at 20℃; for 0.25h; Stage #2: hexylbenzene In dichloromethane at 20℃; for 24h; | 99% |
With aluminium trichloride In pentane at 20℃; for 1h; | 67% |
4-bromo-m-xylene
2-chloropropionyl chloride
4-bromo-1-(3'-chloro-1'-oxopropyl)-2,5-dimethylbenzene
Conditions | Yield |
---|---|
Stage #1: 2-chloropropionyl chloride With aluminum (III) chloride In dichloromethane for 0.25h; Schlenk technique; Inert atmosphere; Stage #2: 4-bromo-m-xylene In dichloromethane at 20℃; for 20h; Inert atmosphere; | 99% |
With aluminium trichloride In dichloromethane at 50℃; for 3h; Addition; | 87% |
With aluminum (III) chloride In carbon disulfide at 0℃; for 1h; Reflux; | 61% |
With aluminium trichloride In carbon disulfide at 20℃; for 16h; |
1-bromo-2,4-dimethylbenzene
2-chloropropionyl chloride
1-(5-bromo-2,4-dimethylphenyl)-3-chloropropan-1-one
Conditions | Yield |
---|---|
With aluminium trichloride In carbon disulfide for 0.5h; Friedel-Crafts reaction; Heating; | 99% |
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