Luhan Pharmachem Co., Ltd. owns strong elite professional quality sales force, has the customer base from the US, Europe, Japan, Southeast Asia, Korea, Hong Kong, Taiwan and other countries and regions, the company operates in accordance with the mod
Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:936-59-4
Min.Order:0 Metric Ton
Negotiable
Type:Manufacturers
inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:936-59-4
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, intermedi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:936-59-4
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:936-59-4
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by email in time prod
Cas:936-59-4
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:936-59-4
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryProduct Name: 3-Chloropropiophenone CAS: 936-59-4 MF: C9H9ClO MW: 168.62 EINECS: 213-317-6 Mol File: 936-59-4.mol 3-Chloropropiophenone Structure 3-Chloropropiophenone Chemical Properties Melting point 48-50 °C(lit.) Boili
Cas:936-59-4
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:936-59-4
Min.Order:1 Kilogram
FOB Price: $42.0 / 46.0
Type:Trading Company
inquiry3-Chloropropiophenone CAS:936-59-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inter
Cas:936-59-4
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Product Name: 3-Chloropropiophenone Synonyms: 3-CHLORO-1-PHENYL-1-PROPANONE;3-CHLORO-1-OXO-1-PHENYLPROPANE;B-CHLOROPROPIOPHENONE;BETA-CHLOROPROPIOPHENONE;3-Chloropropiophenone98%;Chloropropiophenone, 98+%;beta-Chloropropiophenone,98+%;3-Chloropr
Cas:936-59-4
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryWe have two GMP facilities in Hubei Province and cooperative factories in Zhejiang Province We are concentrating on the R&D and technical service of APIs and pharmaceutical intermediates Appearance:white powder Storage:room temperature Pa
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Why Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu
Our Advantages Production: Advanced chemical equipment with years of experience.Staffs for producing various extract products. Quality Control:A complete set of Testing Professional and Analysis Equipment ensures the Quality Requirements and Speci
Cas:936-59-4
Min.Order:1 Kilogram
FOB Price: $150.0 / 180.0
Type:Trading Company
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:936-59-4
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryProduct Name:3-ChloropropiophenoneSynonyms:3-CHLORO-1-PHENYL-1-PROPANONE;3-CHLORO-1-OXO-1-PHENYLPROPANE;B-CHLOROPROPIOPHENONE;BETA-CHLOROPROPIOPHENONE;3-Chloropropiophenone98%;Chloropropiophenone, 98+%;beta-Chloropropiophenone,98+%;3-Chloro
Cas:936-59-4
Min.Order:1 Metric Ton
FOB Price: $20.0
Type:Lab/Research institutions
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:936-59-4
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryProduct name: 3-Chloropropiophenone CAS No.:936-59-4 Molecule Formula:C9H9ClO Molecule Weight:168.62 Purity: 99.0% Package: 25kg/drum Description: White or light yellow crystals powder Manufacture Standards:Enterprise Standard
Cas:936-59-4
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:936-59-4
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHigh quality, competitive price, fast delivery and first-class service we possesses have won the trust and praise of customers. Standard: BP/USP/EP The purity is equal or greater than 99%. As a supplier, we can provide high-quality products. Cle
Cas:936-59-4
Min.Order:1 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryLocated in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and h
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
We are a large company integrating the production and sales of chemical and pharmaceutical intermediates. Appearance:Off-White to Pale Yellow Package:1kg Application:Pharmaceutical intermediate
Cas:936-59-4
Min.Order:1 box
Negotiable
Type:Other
inquiryGOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
Superior quality, moderate price & quick delivery. Appearance:white crystalline powder Storage:stored in a cool, dry and ventilated place to provent sun and rain Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical
Conditions | Yield |
---|---|
With aluminum (III) chloride In dichloromethane at 0 - 20℃; Inert atmosphere; | 100% |
aluminium trichloride; nitromethane In carbon disulfide for 2h; Product distribution; Mechanism; Ambient temperature; further Friedel-Crafts catalysts, further arenes, further haloacid chlorides; variation of temperature and time; | 88% |
aluminium trichloride; nitromethane In carbon disulfide for 2h; Ambient temperature; | 88% |
Conditions | Yield |
---|---|
With Oxone; potassium bromide In dichloromethane; water at 20℃; for 24h; visible light irradiation; | 97% |
3-chloro-1-phenyl-propan-1-ol
3-chloropropiophenone
Conditions | Yield |
---|---|
With dihydrogen peroxide; acetic acid; sodium bromide In water at 60℃; for 2h; Inert atmosphere; | 93% |
With dipotassium peroxodisulfate; V2O5/TiO2 In water; acetonitrile at 80℃; Sealed tube; Green chemistry; | 88% |
With oxone; C18H17IN2O7PolS(1-)*Na(1+); tetra(n-butyl)ammonium hydrogensulfate In acetonitrile at 70℃; for 18h; Reagent/catalyst; Solvent; Sealed tube; Green chemistry; | 84% |
With sodium dichromate; sulfuric acid |
Conditions | Yield |
---|---|
With iron(II) acetylacetonate; Triethoxysilane In tert-butyl alcohol at 20℃; for 24h; regioselective reaction; | 90% |
With tris(1-phenylbutane-1,3-dionato)iron(III); phenylsilane In ethanol at 20℃; for 6.5h; Reagent/catalyst; Wacker Oxidation; | 81% |
With iron(III) chloride; tetraphenylsilane In tert-butyl alcohol at 80℃; for 24h; | 90 %Chromat. |
Conditions | Yield |
---|---|
With Triphenylphosphine oxide In dichloromethane at 20℃; for 2h; | 88% |
With hydrogenchloride; diethyl ether |
1-phenylcyclopropan-1-ol
3-chloropropiophenone
Conditions | Yield |
---|---|
With manganese(II) triflate; tetrabutylammonium acetate; acetic acid; magnesium chloride In acetonitrile at 25℃; for 3.5h; Inert atmosphere; Electrochemical reaction; Sealed tube; | 54% |
Conditions | Yield |
---|---|
51% |
diethyl ether
ethyl 3-chloropropanoate
A
3-chloropropiophenone
B
3,3-diphenylallyl chloride
ethyl 3-chloropropanoate
A
3-chloropropiophenone
B
3,3-diphenylallyl chloride
Conditions | Yield |
---|---|
With diethyl ether Destillation des nach Hydrolyse erhaltenen Reaktionsprodukts unter vermindertem Druck; |
Conditions | Yield |
---|---|
With ethyl bromide; aluminium trichloride anschliessendes Einleiten von Aethylen; |
Conditions | Yield |
---|---|
With aluminium trichloride; benzene |
hydrogenchloride
acetic acid
1-phenyl-propan-1-one
A
3-chloropropiophenone
Conditions | Yield |
---|---|
an Graphit-Anoden.Electrolysis; |
Conditions | Yield |
---|---|
With aluminium trichloride |
Conditions | Yield |
---|---|
With potassium chloride In N,N-dimethyl-formamide for 8h; Ambient temperature; | A 28 % Turnov. B 25 % Turnov. C 25 % Turnov. D n/a |
3-chloro-1-phenyl-propan-1-ol
A
3-chloropropiophenone
B
(1R)-3-chloro-1-phenylpropanol
Conditions | Yield |
---|---|
With Sphingomonas paucimobilis NCIMB 8195 In water; N,N-dimethyl-formamide for 120h; | A 21 % Chromat. B 79 % Chromat. |
formaldehyd
acetophenone
A
3-chloropropiophenone
B
1-phenyl-3-chloro-2-(chloromethyl)-1-propanone
C
4-chloromethylacetophenone
D
Phenyl vinyl ketone
Conditions | Yield |
---|---|
With hydrogenchloride for 2h; Heating; Further byproducts. Title compound not separated from byproducts.; |
Conditions | Yield |
---|---|
With hydrogenchloride; ammonium nitrate; iodine; oxygen In water; acetonitrile at 60℃; for 24h; Green chemistry; regioselective reaction; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: titanium(IV) isopropylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere; Sealed tube 2: acetic acid; manganese(II) triflate; magnesium chloride; tetrabutylammonium acetate / acetonitrile / 3.5 h / 25 °C / Inert atmosphere; Electrochemical reaction; Sealed tube View Scheme |
1,2,3,4-tetrahydroisoquinoline
3-chloropropiophenone
3-(3,4-dihydro-1H-isoquinolin-2-yl)-1-phenylpropanone
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 20℃; for 16h; | 100% |
6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline
3-chloropropiophenone
3-(6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl)-1-phenyl-propan-1-one
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 20℃; | 100% |
3-chloropropiophenone
(S)-1-(p-chlorophenyl)ethylamine
3-[(S)-1-(4-chloro-phenyl)-ethylamino]-1-phenyl-propan-1-one
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; | 100% |
With triethylamine In tetrahydrofuran at 20℃; |
Conditions | Yield |
---|---|
With triethylamine In chloroform at 20℃; for 18.0833h; Inert atmosphere; | 99% |
With triethylamine In chloroform at 0 - 30℃; for 18h; | 99% |
With triethylamine In chloroform for 18h; | 99% |
3-chloropropiophenone
(1R)-3-chloro-1-phenylpropanol
Conditions | Yield |
---|---|
With borane; S-oxaborolidine In tetrahydrofuran at 0℃; for 0.833333h; | 99% |
With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; C22H32N4O4S2; water; sodium formate at 40℃; for 0.25h; Air atmosphere; optical yield given as %ee; enantioselective reaction; | 99% |
With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; (1R,2R)-9H-fluorene-2,7-disulfonic acid bis-[(2-amino-cyclohexyl)amide]; sodium formate In water at 40℃; for 0.25h; optical yield given as %ee; enantioselective reaction; | 99% |
3-chloropropiophenone
4-tert-butylphenylboronic acid
3-(4-(tert-butyl)phenyl)-1-phenylpropan-1-one
Conditions | Yield |
---|---|
With potassium phosphate; Wilkinson's catalyst; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In 1,4-dioxane at 80℃; under 750.075 Torr; for 30h; Inert atmosphere; | 99% |
Thien-3-ylboronic acid
3-chloropropiophenone
1-phenyl-3-(thiophen-3-yl)propan-1-one
Conditions | Yield |
---|---|
With potassium phosphate; Wilkinson's catalyst; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In 1,4-dioxane at 60℃; under 750.075 Torr; for 20h; Inert atmosphere; | 99% |
3-chloropropiophenone
3-(benzyl(methyl)amino)-1-phenylpropan-1-one
Conditions | Yield |
---|---|
98% |
3-chloropropiophenone
m-tolylboronic acid
1-phenyl-3-(3-methylphenyl)-1-propananone
Conditions | Yield |
---|---|
With potassium phosphate; Wilkinson's catalyst; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In 1,4-dioxane at 60℃; under 750.075 Torr; for 20h; Inert atmosphere; | 98% |
3-chloropropiophenone
1-Naphthylboronic acid
3-(naphthalen-1-yl)-1-phenylpropan-1-one
Conditions | Yield |
---|---|
With potassium phosphate; Wilkinson's catalyst; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In 1,4-dioxane at 60℃; under 750.075 Torr; for 20h; Inert atmosphere; | 98% |
α-naphthol
3-chloropropiophenone
N,N-dimethylamino-3-(naphthyl-1-oxy)-1-phenylprop-1-amine
Conditions | Yield |
---|---|
With sodium hydroxide In N,N-dimethyl-formamide at 60 - 65℃; for 5h; Reagent/catalyst; Temperature; | 97.7% |
3-chloropropiophenone
3-chloro-1-phenyl-propan-1-ol
Conditions | Yield |
---|---|
With sodium tetrahydroborate In tetrahydrofuran at 20℃; for 2h; | 97% |
With sodium tetrahydroborate In methanol at 20℃; for 24h; Inert atmosphere; | 95% |
With sodium tetrahydroborate; ethanol In tetrahydrofuran at -10 - -5℃; for 0.333333h; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
With water; ammonium chloride; zinc In tetrahydrofuran Reflux; | 97% |
With water; ammonium chloride; zinc In tetrahydrofuran Inert atmosphere; | 97% |
With ammonium chloride; zinc In tetrahydrofuran; water for 1h; Reflux; | 97% |
Conditions | Yield |
---|---|
With potassium phosphate; Wilkinson's catalyst; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In 1,4-dioxane at 60℃; under 750.075 Torr; for 20h; Reagent/catalyst; Solvent; Temperature; Concentration; Inert atmosphere; | 97% |
3-chloropropiophenone
4-fluoroboronic acid
1-phenyl-3-(4-fluorophenyl)-1-propananone
Conditions | Yield |
---|---|
With potassium phosphate; Wilkinson's catalyst; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In 1,4-dioxane at 60℃; under 750.075 Torr; for 20h; Inert atmosphere; | 97% |
α-naphthol
3-chloropropiophenone
3-(naphthalen-1-yloxy)-1-phenylpropan-1-one
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; N-benzyl-N,N,N-triethylammonium chloride In dichloromethane; water at 20℃; for 42h; Temperature; Solvent; Large scale; | 97% |
Stage #1: α-naphthol With potassium hydroxide In N,N-dimethyl-formamide at 0℃; for 2h; Inert atmosphere; Stage #2: 3-chloropropiophenone In N,N-dimethyl-formamide at 50℃; for 30h; Reagent/catalyst; Temperature; Inert atmosphere; | 73.52% |
3-chloropropiophenone
tert-butylamine
3-(tert-butylamino)-1-phenylpropan-1-one
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 20℃; | 96% |
3-chloropropiophenone
2-Allyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
1-chloro-3-phenyl-5-hexen-3-ol
Conditions | Yield |
---|---|
With ethanol; diethylzinc In tetrahydrofuran at 20℃; for 2h; Inert atmosphere; | 96% |
3-chloropropiophenone
(4-(2-hydroxyethoxy)phenyl)(phenyl)methanone
ospemifene
Conditions | Yield |
---|---|
With titanium tetrachloride; zinc In 2-methyltetrahydrofuran at 15 - 50℃; Product distribution / selectivity; | 96% |
With titanium tetrachloride; zinc In 2-methyltetrahydrofuran at -10 - 80℃; for 5.5h; Inert atmosphere; | |
With titanium tetrachloride; zinc In tetrahydrofuran McMurry Reaction; Reflux; | |
With titanium tetrachloride; zinc In tetrahydrofuran for 6h; McMurry Reaction; Reflux; Inert atmosphere; |
3-chloropropiophenone
B-allenyl-1,3,2-dioxaborolane
(S)-(+)-1-chloro-3-phenylhex-5-yn-3-ol
Conditions | Yield |
---|---|
Stage #1: B-allenyl-1,3,2-dioxaborolane With (S)-3,3'-dibromo-1,1'-bi-2-naphthol at 20℃; for 0.0833333h; Inert atmosphere; Neat (no solvent); Stage #2: 3-chloropropiophenone at 72℃; for 0.75h; Inert atmosphere; Neat (no solvent); Microwave irradiation; optical yield given as %ee; enantioselective reaction; | 96% |
3-chloropropiophenone
2-Methylphenylboronic acid
1-phenyl-3-(2-methylphenyl)-1-propananone
Conditions | Yield |
---|---|
With potassium phosphate; Wilkinson's catalyst; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In 1,4-dioxane at 60℃; under 750.075 Torr; for 20h; Inert atmosphere; | 96% |
3-chloropropiophenone
4-trifluoromethylphenylboronic acid
Conditions | Yield |
---|---|
With potassium phosphate; Wilkinson's catalyst; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In 1,4-dioxane at 60℃; under 750.075 Torr; for 20h; Inert atmosphere; | 96% |
Conditions | Yield |
---|---|
With formic acid; C30H31ClN2O2RuS; triethylamine at 60℃; for 1.5h; Inert atmosphere; enantioselective reaction; | 96% |
Multi-step reaction with 2 steps 1: sodium carbonate / water / 72 h / 28 °C / pH 9 2: yeast strain Rhodotorula glutinis H93 / Microbiological reaction View Scheme | |
Multi-step reaction with 2 steps 1: triethylamine / chloroform / Inert atmosphere 2: [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; Boc-L-alanine(2S)-hydroxypropylamide; lithium chloride; potassium tert-butylate / tetrahydrofuran; ethanol / 40 °C / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
With titanium tetrachloride; zinc In tetrahydrofuran at 0 - 20℃; for 5h; McMurry Reaction; Inert atmosphere; Reflux; | 96% |
With titanium tetrachloride; zinc In tetrahydrofuran for 2.5h; McMurry Reaction; Inert atmosphere; Reflux; | 70% |
With titanium tetrachloride; zinc In tetrahydrofuran McMurry Reaction; |
3-chloropropiophenone
triethyl phosphite
diethyl (3-oxo-3-phenylpropyl)phosphonate
Conditions | Yield |
---|---|
for 6h; Heating; | 95% |
With aluminum oxide for 0.0833333h; Arbuzov rearrangement; microwave irradiation; | 90% |
at 85 - 100℃; Kinetics; Thermodynamic data; Mechanism; Ea, ΔH(excit.), ΔS(excit.), ΔG(excit.); other substituted 3-chloropropiophenones; other solvents; | |
With diethylene glycol dimethyl ether |
3-chloropropiophenone
Conditions | Yield |
---|---|
With sodium tetrahydroborate; dimethyl sulfate; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole In tetrahydrofuran at 0℃; for 1.5h; Inert atmosphere; enantioselective reaction; | 95% |
2-[(1,3,2-dioxaborolan-2-yloxy)diphenylmethyl]pyrrolidine Product distribution / selectivity; | 86% |
3-chloropropiophenone
B-allyl-1,3,2-dioxaborinane
Conditions | Yield |
---|---|
With (S)-3,3'-dibromo-1,1'-bi-2-naphthol; tert-butyl alcohol at 20℃; for 24h; Inert atmosphere; enantioselective reaction; | 95% |
3-chloropropiophenone
3-Chloro-2-methylpropene
1-chloro-5-methyl-3-phenylhex-5-en-3-ol
Conditions | Yield |
---|---|
Stage #1: 3-Chloro-2-methylpropene With diisobutylaluminium hydride; magnesium In tetrahydrofuran; hexane at 20 - 30℃; for 2h; Inert atmosphere; Stage #2: With cerium(III) chloride In tetrahydrofuran; hexane at -10℃; for 0.5h; Inert atmosphere; Stage #3: 3-chloropropiophenone | 95% |
Stage #1: 3-Chloro-2-methylpropene With diisobutylaluminium hydride; magnesium at 20 - 30℃; for 2h; Inert atmosphere; Stage #2: 3-chloropropiophenone With cerium(III) chloride In tetrahydrofuran; hexane at -10 - 0℃; for 1h; Stage #3: With hydrogenchloride In tetrahydrofuran; hexane; water at 30℃; | 95% |
Stage #1: 3-Chloro-2-methylpropene With diisobutylaluminium hydride; magnesium In tetrahydrofuran; hexane at 20 - 30℃; Inert atmosphere; Stage #2: With cerium(III) chloride In tetrahydrofuran; hexane at -10 - 20℃; Inert atmosphere; Stage #3: 3-chloropropiophenone | |
Stage #1: 3-Chloro-2-methylpropene With diisobutylaluminium hydride; magnesium In tetrahydrofuran; hexane at 20 - 30℃; Inert atmosphere; Stage #2: With cerium(III) chloride In tetrahydrofuran; hexane at -10 - 20℃; Inert atmosphere; Stage #3: 3-chloropropiophenone In tetrahydrofuran; hexane at -10 - 0℃; | |
Stage #1: 3-Chloro-2-methylpropene With diisobutylaluminium hydride; magnesium In tetrahydrofuran; hexane at 20 - 30℃; for 2h; Inert atmosphere; Stage #2: 3-chloropropiophenone With cerium(III) chloride In tetrahydrofuran; hexane at 0℃; for 0.5h; Inert atmosphere; Stage #3: With hydrogenchloride; water In tetrahydrofuran; hexane at 30℃; |
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