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This product is a nationally controlled contraband, and the Lookchem platform doesn't provide relevant sales information.

Synthetic route

ethanol
64-17-5

ethanol

diethyl ether
60-29-7

diethyl ether

Conditions
ConditionsYield
With reduced Sn/hydrotalcite catalyst at 250℃; under 25502.6 Torr; Catalytic behavior; Reagent/catalyst; Temperature; Pressure;99%
With SA5 at 199.84℃; Catalytic behavior; Reagent/catalyst; Temperature; Inert atmosphere;2.6%
With sulfuric acid at 130 - 140℃; Darstellung im grossen;
ethanol
64-17-5

ethanol

A

diethyl ether
60-29-7

diethyl ether

B

ethene
74-85-1

ethene

Conditions
ConditionsYield
With alumina at 449.84℃; Catalytic behavior; Reagent/catalyst; Temperature; Inert atmosphere; Overall yield = 100 %;A 0.1%
B 98.9%
C2I2O2Rh(1-)*C8H20N(1+); tetraethylammonium iodide; hydrogen iodide In water at 110℃; Product distribution / selectivity; Inert atmosphere; Autoclave;A 10%
B 50%
1-methyl-3-(propyl-3-sulfonyl)imidazolium trifluoromethanesulfonate; CF3O3S(1-)*CHF3O3S*C7H13N2O3S(1+) at 240 - 260℃; for 4h; Product distribution / selectivity;A n/a
B 12%
triethyloxonium tris(pentafluoroethyl)trifluorophosphate
945614-32-4

triethyloxonium tris(pentafluoroethyl)trifluorophosphate

1-ethyl-3-methyl-1H-imidazol-3-ium chloride
65039-09-0

1-ethyl-3-methyl-1H-imidazol-3-ium chloride

A

1-ethyl-3-methyl-imidazolium tris(pentafluoroethyl)trifluorophosphate
377739-43-0

1-ethyl-3-methyl-imidazolium tris(pentafluoroethyl)trifluorophosphate

B

diethyl ether
60-29-7

diethyl ether

C

chloroethane
75-00-3

chloroethane

Conditions
ConditionsYield
at 80℃; for 3h; Product distribution / selectivity;A 98.9%
B n/a
C n/a
...Expand
triethyloxonium tris(pentafluoroethyl)trifluorophosphate
945614-32-4

triethyloxonium tris(pentafluoroethyl)trifluorophosphate

N,N,N',N',N'',N''-hexamethylguanidinium chloride
30388-20-6

N,N,N',N',N'',N''-hexamethylguanidinium chloride

A

hexamethylguanidinium tris(pentafluoroethyl)trifluorophosphate

hexamethylguanidinium tris(pentafluoroethyl)trifluorophosphate

B

diethyl ether
60-29-7

diethyl ether

C

chloroethane
75-00-3

chloroethane

Conditions
ConditionsYield
at 80℃; for 3h;A 98.9%
B n/a
C n/a
...Expand
triethyloxonium tris(pentafluoroethyl)trifluorophosphate
945614-32-4

triethyloxonium tris(pentafluoroethyl)trifluorophosphate

1-ethyl-3-methylimidazolium hexafluorophosphate
155371-19-0

1-ethyl-3-methylimidazolium hexafluorophosphate

A

1-ethyl-3-methyl-imidazolium tris(pentafluoroethyl)trifluorophosphate
377739-43-0

1-ethyl-3-methyl-imidazolium tris(pentafluoroethyl)trifluorophosphate

B

diethyl ether
60-29-7

diethyl ether

C

1-fluoroethane
353-36-6

1-fluoroethane

D

phosphorus pentafluoride
7647-19-0, 874483-74-6

phosphorus pentafluoride

Conditions
ConditionsYield
at 100℃; for 10h; Product distribution / selectivity;A 98.7%
B n/a
C n/a
D n/a
...Expand
triethyloxonium bis(trifluoromethylsulfonyl)imide
945614-34-6

triethyloxonium bis(trifluoromethylsulfonyl)imide

1-cyano-4-N,N-dimethylaminopyridinium bromide
59016-54-5

1-cyano-4-N,N-dimethylaminopyridinium bromide

A

ethyl bromide
74-96-4

ethyl bromide

B

diethyl ether
60-29-7

diethyl ether

C

1-cyano-4-dimethylaminopyridinium bis(trifluoromethylsulfonyl)imide
945614-38-0

1-cyano-4-dimethylaminopyridinium bis(trifluoromethylsulfonyl)imide

Conditions
ConditionsYield
at 60℃; for 5h;A n/a
B n/a
C 98.2%
...Expand
triethyloxonium bis(trifluoromethylsulfonyl)imide
945614-34-6

triethyloxonium bis(trifluoromethylsulfonyl)imide

1-ethyl-3-methyl-1H-imidazol-3-ium chloride
65039-09-0

1-ethyl-3-methyl-1H-imidazol-3-ium chloride

A

diethyl ether
60-29-7

diethyl ether

B

chloroethane
75-00-3

chloroethane

C

1-ethyl-3-methylimidazolium bis(trifluoromethylsulfonyl)imide
174899-82-2

1-ethyl-3-methylimidazolium bis(trifluoromethylsulfonyl)imide

Conditions
ConditionsYield
at 80℃; for 3h;A n/a
B n/a
C 97.9%
...Expand
Dimethylphenylsilane
766-77-8

Dimethylphenylsilane

paracetaldehyde
123-63-7

paracetaldehyde

A

diethyl ether
60-29-7

diethyl ether

B

1,1,3,3-tetramethyl-1,3-diphenyldisiloxane
56-33-7

1,1,3,3-tetramethyl-1,3-diphenyldisiloxane

Conditions
ConditionsYield
With (pentamethylcyclopentadienyl)Ge(II)+B(ArF)4- In dichloromethane-d2 at 50℃; Catalytic behavior; Reagent/catalyst;A n/a
B 97%
...Expand
ethyl acetate
141-78-6

ethyl acetate

A

diethyl ether
60-29-7

diethyl ether

B

ethoxytriethylsilane
597-67-1

ethoxytriethylsilane

Conditions
ConditionsYield
With triethylsilane; [CpW(CO)2(1,3-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene)]B(C6F5)4 at 23℃; for 26h; Conversion of starting material;A 5.9%
B 96.3%
bis(pentamethylcyclopentadienyl)ytterbium(diethyl ether)

bis(pentamethylcyclopentadienyl)ytterbium(diethyl ether)

tetraethyldiphosphine disulfide
3790-23-6

tetraethyldiphosphine disulfide

A

((CH3)5C5)2Yb(S2P(C2H5)2)
115018-02-5

((CH3)5C5)2Yb(S2P(C2H5)2)

B

diethyl ether
60-29-7

diethyl ether

C

1,1,2,2-tetraethyldiphosphane
3040-63-9

1,1,2,2-tetraethyldiphosphane

D

tetraethyldiphosphane monosulfide

tetraethyldiphosphane monosulfide

Conditions
ConditionsYield
In toluene stirring, 2 h, under N2; concn., cooling to -10°C; elem. anal.;A 96%
B n/a
C n/a
D n/a
...Expand
triethyloxonium tris(pentafluoroethyl)trifluorophosphate
945614-32-4

triethyloxonium tris(pentafluoroethyl)trifluorophosphate

1-decyl-3-methylimidazol-3-ium chloride

1-decyl-3-methylimidazol-3-ium chloride

A

diethyl ether
60-29-7

diethyl ether

B

chloroethane
75-00-3

chloroethane

C

1-decyl-3-methylimidazolium tris(pentafluoroethyl)trifluorophosphate
916807-26-6

1-decyl-3-methylimidazolium tris(pentafluoroethyl)trifluorophosphate

Conditions
ConditionsYield
at 80℃; for 3h;A n/a
B n/a
C 96%
...Expand
methyldiphenylsilane
776-76-1

methyldiphenylsilane

paracetaldehyde
123-63-7

paracetaldehyde

A

diethyl ether
60-29-7

diethyl ether

B

1,3-Dimethyl-1,1,3,3-tetraphenyldisiloxan
807-28-3

1,3-Dimethyl-1,1,3,3-tetraphenyldisiloxan

Conditions
ConditionsYield
With (pentamethylcyclopentadienyl)Ge(II)+B(ArF)4- In dichloromethane-d2 at 50℃; Catalytic behavior;A n/a
B 96%
...Expand
triethyloxonium tris(pentafluoroethyl)trifluorophosphate
945614-32-4

triethyloxonium tris(pentafluoroethyl)trifluorophosphate

trityl chloride
76-83-5

trityl chloride

A

diethyl ether
60-29-7

diethyl ether

B

chloroethane
75-00-3

chloroethane

C

tritylium tris(pentafluoroethyl)trifluorophosphate

tritylium tris(pentafluoroethyl)trifluorophosphate

Conditions
ConditionsYield
at 80℃; for 10h;A n/a
B n/a
C 93.6%
...Expand
triethyloxonium tris(pentafluoroethyl)trifluorophosphate
945614-32-4

triethyloxonium tris(pentafluoroethyl)trifluorophosphate

1-cyano-4-N,N-dimethylaminopyridinium bromide
59016-54-5

1-cyano-4-N,N-dimethylaminopyridinium bromide

A

ethyl bromide
74-96-4

ethyl bromide

B

diethyl ether
60-29-7

diethyl ether

C

1-cyano-4-dimethylaminopyridinium tris(pentafluoroethyl)trifluorophosphate
945614-37-9

1-cyano-4-dimethylaminopyridinium tris(pentafluoroethyl)trifluorophosphate

Conditions
ConditionsYield
at 60℃; for 5h;A n/a
B n/a
C 93.2%
...Expand
N-(n-hexyl)-N-methylpyrrolidinium chloride

N-(n-hexyl)-N-methylpyrrolidinium chloride

triethyloxonium tris(pentafluoroethyl)trifluorophosphate
945614-32-4

triethyloxonium tris(pentafluoroethyl)trifluorophosphate

A

diethyl ether
60-29-7

diethyl ether

B

chloroethane
75-00-3

chloroethane

C

1-hexyl-1-methylpyrrolidinium tris(pentafluoroethyl)trifluorophosphate
945614-40-4

1-hexyl-1-methylpyrrolidinium tris(pentafluoroethyl)trifluorophosphate

Conditions
ConditionsYield
at 80℃; for 3h;A n/a
B n/a
C 93%
...Expand
Diethyl carbonate
105-58-8

Diethyl carbonate

A

diethyl ether
60-29-7

diethyl ether

B

ethanol
64-17-5

ethanol

Conditions
ConditionsYield
With NaX faujasite at 180 - 240℃; for 6h;A 93%
B 5%
ethene
74-85-1

ethene

acetic acid
64-19-7

acetic acid

A

diethyl ether
60-29-7

diethyl ether

B

ethanol
64-17-5

ethanol

C

ethyl acetate
141-78-6

ethyl acetate

Conditions
ConditionsYield
Stage #1: acetic acid With water at 92.4℃;
Stage #2: ethene; cesium nitrate; tungstophosphoric acid; water; mixture of, dried, tabletted at 92.4 - 194.4℃; under 6750.68 Torr; Product distribution / selectivity; Gas phase;		A 3.2%
B 3.6%
C 92.7%
With water; cesium nitrate; tungstophosphoric acid; water; mixture of, dried, tabletted at 92.4 - 165℃; under 6750.68 Torr; Product distribution / selectivity; Gas phase;A 3%
B 3.4%
C 91.5%
With water; lithium nitrate; silica; tungstophosphoric acid; water; mixture of, heated at 150 C at 102.2 - 165℃; under 6750.68 Torr; Product distribution / selectivity; Gas phase;A 2.2%
B 5%
C 90.1%
With water; lithium nitrate; silica; tungstosilicic acid; water; mixture of, heated at 150 C at 102.2 - 165℃; under 6750.68 Torr; Conversion of starting material; Gas phase;A 4.7%
B 7.6%
C 87.7%
...Expand
ethene
74-85-1

ethene

acrylic acid
79-10-7

acrylic acid

A

diethyl ether
60-29-7

diethyl ether

B

ethanol
64-17-5

ethanol

C

ethyl acrylate
140-88-5

ethyl acrylate

Conditions
ConditionsYield
With water; cesium nitrate; tungstophosphoric acid; water; mixture of, dried, tabletted at 85.6 - 165℃; under 2250.23 Torr; Product distribution / selectivity; Gas phase;A 3.5%
B 4.3%
C 91.8%
...Expand
ethanol
64-17-5

ethanol

1,3-bis(p-nitrophenyl)-2-thia-1,3-diazaallene
15148-19-3

1,3-bis(p-nitrophenyl)-2-thia-1,3-diazaallene

A

diethyl ether
60-29-7

diethyl ether

B

diethyl sulphite
623-81-4

diethyl sulphite

C

4-nitro-aniline
100-01-6

4-nitro-aniline

Conditions
ConditionsYield
With copper dichloride for 24h; Product distribution; Ambient temperature; other reagent;A 93.6 % Chromat.
B 70%
C 91%
...Expand
triethyloxonium tris(pentafluoroethyl)trifluorophosphate
945614-32-4

triethyloxonium tris(pentafluoroethyl)trifluorophosphate

1-ethyl-3-methylimidazolium tetrafluoroborate
143314-16-3

1-ethyl-3-methylimidazolium tetrafluoroborate

A

1-ethyl-3-methyl-imidazolium tris(pentafluoroethyl)trifluorophosphate
377739-43-0

1-ethyl-3-methyl-imidazolium tris(pentafluoroethyl)trifluorophosphate

B

diethyl ether
60-29-7

diethyl ether

C

1-fluoroethane
353-36-6

1-fluoroethane

D

boron trifluoride
7637-07-2

boron trifluoride

Conditions
ConditionsYield
at 100℃; for 10h; Product distribution / selectivity;A 90.3%
B n/a
C n/a
D n/a
...Expand
diethyl ether
60-29-7

diethyl ether

hexafluoro-3-oxatricyclo<3.2.0.02,4>hept-6-ene
74415-68-2

hexafluoro-3-oxatricyclo<3.2.0.02,4>hept-6-ene

A

1-fluoroethane
353-36-6

1-fluoroethane

B

pentafluoro-2-ethoxycyclohexa-2,5-dienone

pentafluoro-2-ethoxycyclohexa-2,5-dienone

Conditions
ConditionsYield
for 2160h; Ambient temperature;A 100%
B 75%
for 2160h; Yields of byproduct given;A n/a
B 21%
...Expand
diethyl ether
60-29-7

diethyl ether

A

1-fluoroethane
353-36-6

1-fluoroethane

B

pentafluoro-2-ethoxycyclohexa-2,5-dienone

pentafluoro-2-ethoxycyclohexa-2,5-dienone

Conditions
ConditionsYield
With hexafluoro-3-oxatricyclo<3.2.0.02,4>hept-6-ene for 2160h; Ambient temperature;A 100%
B 75%
diethyl ether
60-29-7

diethyl ether

trifluoroacetyl triflate
68602-57-3

trifluoroacetyl triflate

A

ethyl trifluoroacetate,
383-63-1

ethyl trifluoroacetate,

B

trifluoromethanesulfonic acid ethyl ester
425-75-2

trifluoromethanesulfonic acid ethyl ester

Conditions
ConditionsYield
at 0℃;A 100%
B 100%
...Expand
diethyl ether
60-29-7

diethyl ether

2,3-bis(dimethylsilyl)-1,1,4,4-tetramethyl-1,4-disila-1,4-dihydronaphthalene

2,3-bis(dimethylsilyl)-1,1,4,4-tetramethyl-1,4-disila-1,4-dihydronaphthalene

[2,3-bis(dimethylsilyl)-1,1,4,4-tetramethyl-1,4-disila-1,4-dihydronaphthalenato]bis[(diethyl ether)lithium(I)]

[2,3-bis(dimethylsilyl)-1,1,4,4-tetramethyl-1,4-disila-1,4-dihydronaphthalenato]bis[(diethyl ether)lithium(I)]

Conditions
ConditionsYield
With lithium at 20℃; for 20h; Reduction;100%
diethyl ether
60-29-7

diethyl ether

2,3,6,7-tetrakis(dimethylsilyl)-1,1,4,4,5,5,8,8-octamethyl-1,4,5,8-tetrasila-1,4,5,8-tetrahydroanthracene

2,3,6,7-tetrakis(dimethylsilyl)-1,1,4,4,5,5,8,8-octamethyl-1,4,5,8-tetrasila-1,4,5,8-tetrahydroanthracene

[2,3,6,7-tetrakis(dimethylsilyl)-1,1,4,4,5,5,8,8-octamethyl-1,4,5,8-tetrasila-1,4,5,8-tetrahydroanthracenato]tetrakis[(diethyl ether)lithium(I)]

[2,3,6,7-tetrakis(dimethylsilyl)-1,1,4,4,5,5,8,8-octamethyl-1,4,5,8-tetrasila-1,4,5,8-tetrahydroanthracenato]tetrakis[(diethyl ether)lithium(I)]

Conditions
ConditionsYield
With lithium at 20℃; for 20h; Reduction;100%
diethyl ether
60-29-7

diethyl ether

2-(trifluoromethyl)phenol
444-30-4

2-(trifluoromethyl)phenol

1,4-bis(bromomethyl)-2,5-dibromobenzene
35335-16-1

1,4-bis(bromomethyl)-2,5-dibromobenzene

1,4-dibromo-2,5-bis(2-trifluoromethylphenoxymethyl)benzene
474330-25-1

1,4-dibromo-2,5-bis(2-trifluoromethylphenoxymethyl)benzene

Conditions
ConditionsYield
With sodium hydroxide; potassium carbonate In dichloromethane; acetone100%
...Expand
4-[[[4-[4-(ethyloxycarbonyl)-1-piperazinyl]phenyl]amino]carbonyl]-1-t-butyloxycarbonyl-piperidine
193902-67-9

4-[[[4-[4-(ethyloxycarbonyl)-1-piperazinyl]phenyl]amino]carbonyl]-1-t-butyloxycarbonyl-piperidine

diethyl ether
60-29-7

diethyl ether

4-[[[4-[4-(ethyloxycarbonyl)-1-piperazinyl]phenyl]amino]carbonyl]piperidine
193902-68-0

4-[[[4-[4-(ethyloxycarbonyl)-1-piperazinyl]phenyl]amino]carbonyl]piperidine

Conditions
ConditionsYield
In 1,4-dioxane; hydrogenchloride100%
diethyl ether
60-29-7

diethyl ether

phenol
108-95-2

phenol

2-phenoxytetrahydropyran
4203-50-3

2-phenoxytetrahydropyran

Conditions
ConditionsYield
With hydrogenchloride In 3,4-dihydro-2H-pyran100%
oxalyl dichloride
79-37-8

oxalyl dichloride

diethyl ether
60-29-7

diethyl ether

3,3-diphenylpropan-1-ol
20017-67-8

3,3-diphenylpropan-1-ol

3,3-diphenylpropanal
4279-81-6

3,3-diphenylpropanal

Conditions
ConditionsYield
With dimethyl sulfoxide; triethylamine In dichloromethane100%
...Expand
2-(2-ethyl-benzofuran-3-yl)-propionic acid
63606-55-3

2-(2-ethyl-benzofuran-3-yl)-propionic acid

diethyl ether
60-29-7

diethyl ether

2-(2-ethyl-benzofuran-3-yl)-propionamide
63606-56-4

2-(2-ethyl-benzofuran-3-yl)-propionamide

Conditions
ConditionsYield
In thionyl chloride100%
diethyl ether
60-29-7

diethyl ether

N,N-dimethyl-o-toluidine
609-72-3

N,N-dimethyl-o-toluidine

2-(dimethylamino)benzyllithium
64308-58-3

2-(dimethylamino)benzyllithium

Conditions
ConditionsYield
With n-butyllithium In hexane100%
With n-butyllithium In hexane
diethyl ether
60-29-7

diethyl ether

trans-dichloro(ethylene)(2,4,6-trimethylpyridine)platinum
52341-13-6, 12264-20-9

trans-dichloro(ethylene)(2,4,6-trimethylpyridine)platinum

trans-dichloro(diethyl ether)(2,4,6-trimethylpyridine)platinum(II)
91068-18-7

trans-dichloro(diethyl ether)(2,4,6-trimethylpyridine)platinum(II)

Conditions
ConditionsYield
In diethyl ether byproducts: ethylene; Irradiation (UV/VIS);100%
In diethyl ether Irradiation (UV/VIS); the Pt-complex dissolved in Et2O was introduced into a muffshaped Schlenk tube surrounding a 125-W medium-pressure mercury lamp, Philips HPK 125, irradn. for 15 min at room temp., λ<310 nm was eliminated by Pyrex filter; the solvent was removed under reduced pressure at -30°C, the solid was recrystd. at -30°C in pentane-CH2Cl2;95%
diethyl ether
60-29-7

diethyl ether

dimethylgallium tetrahydroborate

dimethylgallium tetrahydroborate

(CH3)2GaBH4(CH3CH2)2O
326903-59-7

(CH3)2GaBH4(CH3CH2)2O

Conditions
ConditionsYield
In diethyl ether (high vac. line); condensing gallium complex in an ampoule with Et2O, warming to room temp. over a period of 30 min; fractionation, collection in a trap at -30°C;100%
diethyl ether
60-29-7

diethyl ether

[(C5H4N)C(CH3)(CH2N(C6H2(CH3)3))2]Zr(CH3)2
293764-40-6

[(C5H4N)C(CH3)(CH2N(C6H2(CH3)3))2]Zr(CH3)2

methyllithium
917-54-4

methyllithium

[C5H4NC(CH3)(CH2NC6H2(CH3)3)2]Zr(methyl)3[Li*diethyl ether]
486413-21-2

[C5H4NC(CH3)(CH2NC6H2(CH3)3)2]Zr(methyl)3[Li*diethyl ether]

Conditions
ConditionsYield
In diethyl ether N2; addn. of methyllithium as 4.4 M ether soln. to ether suspn. of Zr complex at -30° C, stirring at room temp. for 10 min; filtration through Celite, drying the filtrate in vac.; elem. anal.;100%
...Expand
diethyl ether
60-29-7

diethyl ether

bis[bis(pentamethylcyclopentadienyl)(μ-hydride)yttrium]

bis[bis(pentamethylcyclopentadienyl)(μ-hydride)yttrium]

benzene-d6
1076-43-3

benzene-d6

A

((CH3)5C5)2Y(OC2H5)
165269-59-0

((CH3)5C5)2Y(OC2H5)

B

((CH3)5C5)2Y(D)((C2H5)2O)

((CH3)5C5)2Y(D)((C2H5)2O)

Conditions
ConditionsYield
In diethyl ether; benzene-d6 byproducts: ethane; N2-atmosphere; room temp. (20 min);A 100%
B n/a
...Expand
diethyl ether
60-29-7

diethyl ether

[La(η5-C5(CH3)5)H]2
98720-39-9

[La(η5-C5(CH3)5)H]2

((CH3)5C5)2La(OC2H5)(O(C2H5)2)
165269-60-3

((CH3)5C5)2La(OC2H5)(O(C2H5)2)

Conditions
ConditionsYield
In benzene-d6 byproducts: ethane; N2-atmosphere; room temp. (10 min); evapn. (vac.);100%
diethyl ether
60-29-7

diethyl ether

supersilylgallium dichloride, dimer

supersilylgallium dichloride, dimer

supersilylgallium dichloride-diethyl ether (1/1)

supersilylgallium dichloride-diethyl ether (1/1)

Conditions
ConditionsYield
In dichloromethane (inert conditions); removal of volatiles (vac.);100%
lithium aluminium tetrahydride
16853-85-3

lithium aluminium tetrahydride

diethyl ether
60-29-7

diethyl ether

Gallium trichloride
13450-90-3

Gallium trichloride

gallane etherate

gallane etherate

Conditions
ConditionsYield
In diethyl ether (N2), GaCl3 in Et2O added dropwise to soln. of LiAlH4 in Et2O at 0°C, stirred at 0°C for 2 h; stored overnight at -20°C, filtered cold, evapd. at -78°C;100%
...Expand
diethyl ether
60-29-7

diethyl ether

C20H30O6

C20H30O6

A

(1S,3aR,5S,5'S,6R,6a'R)-2,2'-dimethyl-5'-(2-methyl-1,3-dioxolan-4-yl)dihydro-3a'H-3-oxaspiro[bicyclo[3.2.0.]heptane-6,6'-furo[2,3-d][1,3]dioxole]
1244773-04-3

(1S,3aR,5S,5'S,6R,6a'R)-2,2'-dimethyl-5'-(2-methyl-1,3-dioxolan-4-yl)dihydro-3a'H-3-oxaspiro[bicyclo[3.2.0.]heptane-6,6'-furo[2,3-d][1,3]dioxole]

B

cyclohexanone
108-94-1

cyclohexanone

Conditions
ConditionsYield
With copper(II) bis(trifluoromethanesulfonate); benzene Inert atmosphere; Irradiation;A 65%
B 100%
...Expand
diethyl ether
60-29-7

diethyl ether

bis(trimethylsilyl)-trifluoromethylsulfonium tetrakis(pentafluorophenyl)borate
1235436-62-0

bis(trimethylsilyl)-trifluoromethylsulfonium tetrakis(pentafluorophenyl)borate

diethyl(trimethylsilyl)oxonium tetrakis(pentafluorophenyl)borate

diethyl(trimethylsilyl)oxonium tetrakis(pentafluorophenyl)borate

Conditions
ConditionsYield
react. bis(trimethylsilyl)-trifluoromethylsulfonium tetrakis(pentafluorophenyl)borate with Et2O;100%
methyl magnesium iodide
917-64-6

methyl magnesium iodide

benzophenone
119-61-9

benzophenone

diethyl ether
60-29-7

diethyl ether

C18H23IMgO2

C18H23IMgO2

Conditions
ConditionsYield
at 20℃; for 12h;100%
...Expand
methyl magnesium iodide
917-64-6

methyl magnesium iodide

diethyl ether
60-29-7

diethyl ether

acetophenone
98-86-2

acetophenone

C13H21IMgO2

C13H21IMgO2

Conditions
ConditionsYield
at 20℃; for 12h;100%
...Expand
diethyl ether
60-29-7

diethyl ether

Cp*Ru(μ-SnC4Et4)2RuCp*

Cp*Ru(μ-SnC4Et4)2RuCp*

lithium
7439-93-2

lithium

[Li(Et2O)]2[Cp*Ru(μ-SnC4Et4)2RuCp*]

[Li(Et2O)]2[Cp*Ru(μ-SnC4Et4)2RuCp*]

Conditions
ConditionsYield
at 20℃; for 1h; Inert atmosphere;100%
...Expand
diethyl ether
60-29-7

diethyl ether

Ce(decafluorodiphenylamide)3

Ce(decafluorodiphenylamide)3

Ce(decafluorodiphenylamide)3(diethyl ether)2
1445605-48-0

Ce(decafluorodiphenylamide)3(diethyl ether)2

Conditions
ConditionsYield
for 0.5h; Inert atmosphere;100%
chloro(1,5-cyclooctadiene)rhodium(I) dimer

chloro(1,5-cyclooctadiene)rhodium(I) dimer

diethyl ether
60-29-7

diethyl ether

(R,Rb)-[1,1'-binaphthalene]-2,2'-diyl(2'-methoxy-[1,1'-binaphthalen]-2-yl)phosphonite
1365891-80-0, 1365891-81-1

(R,Rb)-[1,1'-binaphthalene]-2,2'-diyl(2'-methoxy-[1,1'-binaphthalen]-2-yl)phosphonite

[RhCl((R,R)-C41H27O3P)(η4-cod)]*(C2H5)2O
1436385-41-9

[RhCl((R,R)-C41H27O3P)(η4-cod)]*(C2H5)2O

Conditions
ConditionsYield
In dichloromethane for 0.5h; Inert atmosphere; Schlenk technique;100%
...Expand
diethyl ether
60-29-7

diethyl ether

bis(3,5-di-tert-butyl-2-phenol)amine trilithium salt

bis(3,5-di-tert-butyl-2-phenol)amine trilithium salt

tantalum pentachloride
7721-01-9

tantalum pentachloride

(bis(3,5-di-tert-butyl-2-phenol)amine-3H)TaCl2(Et2O)

(bis(3,5-di-tert-butyl-2-phenol)amine-3H)TaCl2(Et2O)

Conditions
ConditionsYield
In toluene Inert atmosphere; Glovebox;100%
...Expand
morpholine
110-91-8

morpholine

diethyl ether
60-29-7

diethyl ether

N-ethylmorpholine;
100-74-3

N-ethylmorpholine;

Conditions
ConditionsYield
With alumina at 270℃; under 760.051 Torr; Inert atmosphere; Gas phase; Green chemistry;100%
diethyl ether
60-29-7

diethyl ether

Mo2[μ-κ2-PhB(N-2,6-iPr2C6H3)2]2

Mo2[μ-κ2-PhB(N-2,6-iPr2C6H3)2]2

[(tetrahydrofuran)2K18-C-6]2[Mo2{μ-κ2-PhB(2,6-iPr2C6H3)2}2]

[(tetrahydrofuran)2K18-C-6]2[Mo2{μ-κ2-PhB(2,6-iPr2C6H3)2}2]

[(Et2O)K18-C-6][Mo2{μ-κ2-PhB(N-2,6-iPr2C6H3)2}2]

[(Et2O)K18-C-6][Mo2{μ-κ2-PhB(N-2,6-iPr2C6H3)2}2]

Conditions
ConditionsYield
at -35 - 20℃; Inert atmosphere;100%
...Expand
diethyl ether
60-29-7

diethyl ether

ethylene dibromide
106-93-4

ethylene dibromide

magnesium bromide diethyl etherate
29858-07-9

magnesium bromide diethyl etherate

Conditions
ConditionsYield
With magnesium Heating;100%

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Raw Materials

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