DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:609-72-3
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryProduct description: Product name N,N,2-Trimethylbenzenamine CAS number 609-72-3 Assay ≥99% Appearance Colorless transparent liquid Capacity 200mt/year Application Organic Sy
Cas:609-72-3
Min.Order:10 Gram
FOB Price: $12.0
Type:Lab/Research institutions
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Cas:609-72-3
Min.Order:1 Liter
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Cas:609-72-3
Min.Order:5 Kiloliter
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Type:Manufacturers
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Cas:609-72-3
Min.Order:10 Gram
FOB Price: $146.0 / 176.0
Type:Trading Company
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Cas:609-72-3
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Type:Trading Company
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Cas:609-72-3
Min.Order:1 Kilogram
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Cas:609-72-3
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Cas:609-72-3
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Cas:609-72-3
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The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Cas:609-72-3
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryProduct name: N,N-Dimethyl-O-Toluidine CAS No.:609-72-3 Molecule Formula:C9H13N Molecule Weight:135.21 Purity: 98.0% Package: 200kg/drum Description:Colorless to light yellow liquid Manufacture Standards:Enterprise Standard
Cas:609-72-3
Min.Order:1 Kilogram
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Type:Trading Company
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Cas:609-72-3
Min.Order:1 Kilogram
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Cas:609-72-3
Min.Order:1 Metric Ton
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Type:Other
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Cas:609-72-3
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
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Cas:609-72-3
Min.Order:1 Metric Ton
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Type:Trading Company
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Cas:609-72-3
Min.Order:1 Metric Ton
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Type:Trading Company
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Cas:609-72-3
Min.Order:1 Metric Ton
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Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
Cas:609-72-3
Min.Order:1 bottle
Negotiable
Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With phenylsilane; triphenylphosphine In tetrahydrofuran at 120℃; under 3750.38 Torr; for 24h; Autoclave; Green chemistry; | 99% |
With dimanganese decacarbonyl; phenylsilane; C29H33N2P In acetonitrile at 100℃; under 750.075 Torr; for 15h; | 85% |
With sodium tetrahydroborate In 1,4-dioxane at 100℃; under 7500.75 Torr; for 24h; Autoclave; Green chemistry; | 85% |
Conditions | Yield |
---|---|
With 0.72KNaX-BS zeolite at 150℃; for 1h; Reagent/catalyst; | 99% |
Conditions | Yield |
---|---|
With Zr(BH4)2Cl2(dabco)2; zirconium(IV) chloride In methanol; water at 20℃; for 0.1h; | 95% |
With N-methylpyrrolidine zinc borohydride; sulfuric acid In tetrahydrofuran; water at 0 - 10℃; for 0.25h; | 90% |
With sodium cyanoborohydride; acetic acid In tetrahydrofuran at 23 - 50℃; for 18h; Inert atmosphere; | 65% |
Conditions | Yield |
---|---|
With hydrogen In toluene at 140℃; under 30003 Torr; for 3h; chemoselective reaction; | 94% |
2-methylchlorobenzene
N,N-dimethyl-formamide
N,N-dimethyl-o-toluidine
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel (0); 7,9-bis(2,6-diisopropylphenyl)-7H-acenaphtho[1,2-d]imidazol-9-ium chloride; potassium tert-butylate In water; toluene at 35℃; for 24h; Glovebox; Sealed tube; Inert atmosphere; | 90% |
Conditions | Yield |
---|---|
With copper(l) iodide; 6,7-dihydro-5H-quinolin-8-one oxime; potassium hydroxide In water at 65℃; for 24h; Inert atmosphere; | 89% |
Conditions | Yield |
---|---|
With sodium t-butanolate In tetrahydrofuran; toluene at 65℃; Buchwald-Hartwig amination; Inert atmosphere; Sealed vial; | 83% |
Conditions | Yield |
---|---|
With diphenylsilane; C21H41N3NiP2 In acetonitrile at 120℃; under 2052.14 Torr; for 24h; Autoclave; | 83% |
With hydrogen In hexane at 140℃; under 15001.5 - 45004.5 Torr; for 7h; Autoclave; Green chemistry; | 96 %Chromat. |
With diphenylsilane; caesium carbonate In acetonitrile at 80℃; | 14 %Spectr. |
Conditions | Yield |
---|---|
With C15H29IrN4(2+)*2I(1-) at 120℃; for 17h; Inert atmosphere; Schlenk technique; Sealed tube; | 82% |
With hydrogenchloride at 200 - 220℃; | |
With aluminum oxide at 350 - 400℃; | |
With aluminum oxide at 360℃; | |
With TiO2 supported nano-Pd(0.8) catalyst In water at 20℃; for 15h; Inert atmosphere; Irradiation; Green chemistry; | 87 %Chromat. |
Conditions | Yield |
---|---|
With palladium on activated charcoal; tetrabutylammomium bromide; water; sodium hydroxide; silicon at 100℃; for 6h; | 81% |
Conditions | Yield |
---|---|
Stage #1: o-toluidine With tetra-(n-butyl)ammonium iodide; potassium hydroxide In water; benzene at 20℃; for 0.166667h; Stage #2: methyl iodide In water; benzene at 90℃; for 24h; | 77% |
Behandeln des entstandenen Trimethyl-o-tolyl-ammonuimjodids mit Silberoxyd und Destillation; | |
With potassium fluoride at 180℃; |
Conditions | Yield |
---|---|
With sodium carbonate In water; dimethyl sulfoxide at 130℃; for 15h; Schlenk technique; Sealed tube; Green chemistry; | 70% |
2-methylphenyl bromide
N,N-dimethyl O-(2,4,6-trimethylphenyl-sulfonyl) hydroxylamine
N,N-dimethyl-o-toluidine
Conditions | Yield |
---|---|
With magnesium In tetrahydrofuran at 20℃; for 2h; | 60% |
methanol
o-toluidine
A
N,N-dimethyl-o-toluidine
B
N,2-dimethylaniline
Conditions | Yield |
---|---|
With copper(I) oxide; hydrogenchloride; titanium(IV) oxide In water for 6h; UV-irradiation; | A 6% B 58% |
With aluminum oxide at 350 - 400℃; |
methanol
1-methyl-2-nitrobenzene
A
N,N-dimethyl-o-toluidine
B
N,2-dimethylaniline
Conditions | Yield |
---|---|
With Cu-PMO (copper-doped porous metal oxide) for 6h; Supercritical conditions; | A 43% B 57% |
methanol
N-benzylidene-2-methylaniline
N,N-dimethyl-o-toluidine
Conditions | Yield |
---|---|
at 230℃; |
Conditions | Yield |
---|---|
at 120 - 130℃; |
o-tolylazanediyl-bis-acetic acid
N,N-dimethyl-o-toluidine
Conditions | Yield |
---|---|
With sulfuric acid; iron(II) sulfate |
phenyltrimethylammonium iodide
A
N,N-dimethyl-o-toluidine
B
Dimethyl-p-toluidine
Conditions | Yield |
---|---|
at 220 - 230℃; im Druckrohr; | |
at 220 - 230℃; |
phenyltrimethylammonium iodide
A
N,N-dimethyl-o-toluidine
B
N-methyl-2,6-dimethylaniline
C
N,N,2,6-tetramethylaniline
D
Dimethyl-p-toluidine
Conditions | Yield |
---|---|
at 220 - 230℃; im geschlossenen Rohr; |
Conditions | Yield |
---|---|
With sodium hydrogencarbonate | |
at 140℃; |
Conditions | Yield |
---|---|
With aluminum oxide at 350 - 400℃; |
N-allyl-N,N-dimethyl-o-toluidinium bromide
A
N,N-dimethyl-o-toluidine
B
N-allyl-N-methyl-o-toluidine
C
4-allyl-2-methyl-N,N-dimethylaniline
D
3-allyl-2-dimethylaminotoluene
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water; glycerol at 140℃; Product distribution; Mechanism; rearrangaments of anilinium compounds between var. conditions; | A 25 % Chromat. B 5 % Chromat. C 1 % Chromat. D 18 % Chromat. |
With sodium hydrogencarbonate In water; glycerol at 140℃; | A 25 % Chromat. B 5 % Chromat. C 1 % Chromat. D 18 % Chromat. |
methyl benzyl(phenyl)phosphinate
o-toluidine
A
N,N-dimethyl-o-toluidine
B
(±)-benzyl(phenyl)phosphinic acid
C
N,2-dimethylaniline
Conditions | Yield |
---|---|
With hydrogenchloride 1.) 200-210 deg C, 10 min, 2.) dichloromethane; Yield given. Multistep reaction. Yields of byproduct given; |
(N,N-dimethylaniline)tricarbonylchromium
methyl iodide
A
N,N-dimethyl-m-toluidine
B
N,N-dimethyl-o-toluidine
C
Dimethyl-p-toluidine
Conditions | Yield |
---|---|
Yield given. Multistep reaction; |
methanol
aniline
A
N,N-dimethyl-o-toluidine
B
N-methyl-p-toluidine
C
N,N-dimethyl-aniline
D
N-methylaniline
E
N,2-dimethylaniline
F
Dimethyl-p-toluidine
Conditions | Yield |
---|---|
With monoaluminum phosphate at 425℃; Product distribution; other catalyst, var. temp., var.molar ratio of educts; | A 7.0 % Chromat. B 8.5 % Chromat. C 18.3 % Chromat. D 31.2 % Chromat. E 5.1 % Chromat. F 10.0 % Chromat. |
Conditions | Yield |
---|---|
With n-butyllithium In hexane | 100% |
With n-butyllithium In hexane |
trimethylsilyl cyanide
N,N-dimethyl-o-toluidine
N-methyl-N-(2-methylphenyl)aminoacetonitrile
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; [(bpy)AuCl2]Cl In methanol; decane at 20℃; for 5h; regioselective reaction; | 95% |
With amine functionalized Zr(IV) metal-organic framework (UiO-66-NH2) through covalent hooking of EOSIN-Y In methanol at 20℃; for 4h; | 84% |
With tert.-butylhydroperoxide; iron(II) chloride In methanol; decane at 20℃; Inert atmosphere; | 76% |
N,N-dimethyl-o-toluidine
2-methyl-4-bromo-N,N-dimethylaniline
Conditions | Yield |
---|---|
With N-Bromosuccinimide; ammonium acetate In acetonitrile at 20℃; for 0.166667h; | 92% |
With bromine; acetic acid | |
Multi-step reaction with 2 steps 1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 23 °C / Inert atmosphere 2.1: dibromo sulfoxide / tetrahydrofuran / 4 h / -78 °C / Inert atmosphere 2.2: 0.75 h / -78 - 23 °C / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; | 91% |
In diethyl ether at 0 - 20℃; | 67% |
In dichloromethane at 20℃; for 4h; | |
In dichloromethane at 20℃; Inert atmosphere; |
Dimethyldisulphide
N,N-dimethyl-o-toluidine
2-[(methylthio)methyl]-N,N-dimethylbenzenamine
Conditions | Yield |
---|---|
Stage #1: N,N-dimethyl-o-toluidine With n-butyllithium In diethyl ether at 20 - 35℃; Stage #2: Dimethyldisulphide In diethyl ether at 0 - 20℃; | 90% |
Conditions | Yield |
---|---|
With dihydrogen peroxide In acetonitrile at 80℃; under 760.051 Torr; for 4.5h; | 89% |
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 23℃; for 1h; Inert atmosphere; | 68% |
With peracetic acid | |
With dihydrogen peroxide |
Conditions | Yield |
---|---|
With (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile; sodium acetate In N,N-dimethyl-formamide at 20℃; for 16h; Irradiation; Inert atmosphere; diastereoselective reaction; | 89% |
Conditions | Yield |
---|---|
With C32H53N2OScSi2; N,N'-dimethylaniliniumtetrakis(pentafluorophenyl)borate In toluene at 80℃; for 12h; Inert atmosphere; | 89% |
N,N-dimethyl-o-toluidine
1-methyl-4,6-diphenyl-2(1H)-pyrimidinone
3-Methyl-4-[(methyl-o-tolyl-amino)-methyl]-4,6-diphenyl-3,4-dihydro-1H-pyrimidin-2-one
Conditions | Yield |
---|---|
In benzene for 15h; Ambient temperature; Irradiation; | 88% |
Conditions | Yield |
---|---|
With oxygen In tetrahydrofuran at 20℃; for 4h; Irradiation; chemoselective reaction; | 87% |
With oxygen; Nitrogen dioxide; trifluoroacetic acid In acetonitrile at 15℃; for 3h; | 49% |
Conditions | Yield |
---|---|
Stage #1: N,N-dimethyl-o-toluidine With n-butyllithium In tetrahydrofuran at -30℃; for 10h; Inert atmosphere; Stage #2: N,N'-bis(2,6-diisopropylphenyl)carbodiimide In tetrahydrofuran at -30 - 20℃; Inert atmosphere; | 87% |
chloro-trimethyl-silane
N,N-dimethyl-o-toluidine
2-(dimethylamino)-α-(trimethylsilyl)toluene
Conditions | Yield |
---|---|
Stage #1: N,N-dimethyl-o-toluidine With 2,2,6,6-tetramethyl-piperidine; n-butyllithium; potassium tert-butylate In hexane; n-heptane at 0℃; for 0.25h; Inert atmosphere; Stage #2: chloro-trimethyl-silane In hexane; n-heptane at 0℃; for 1h; Inert atmosphere; | 86% |
Stage #1: N,N-dimethyl-o-toluidine With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.0833333h; Inert atmosphere; Stage #2: With 2,2,6,6-tetramethyl-piperidine; potassium tert-butylate In tetrahydrofuran; hexane at -78℃; for 0.25h; Inert atmosphere; Stage #3: chloro-trimethyl-silane In tetrahydrofuran at -78 - 20℃; Inert atmosphere; | 84% |
Stage #1: N,N-dimethyl-o-toluidine With n-butyllithium In tetrahydrofuran at -78℃; for 0.0833333h; Stage #2: With 2,2,6,6-tetramethyl-piperidine; potassium tert-butylate In tetrahydrofuran at -78℃; for 0.25h; Stage #3: chloro-trimethyl-silane In tetrahydrofuran at -78℃; for 0.5h; regioselective reaction; |
Conditions | Yield |
---|---|
With N-hydroxyphthalimide In acetonitrile at 20℃; for 12h; Irradiation; Inert atmosphere; | 86% |
N,N-dimethyl-o-toluidine
chloro-diphenylphosphine
2-{(diphenylphosphino)methyl}-N,N-dimethylaniline
Conditions | Yield |
---|---|
Stage #1: N,N-dimethyl-o-toluidine With n-butyllithium; N,N,N,N,-tetramethylethylenediamine In hexane at 20℃; for 3h; Stage #2: chloro-diphenylphosphine In diethyl ether; hexane at -4 - 20℃; for 2h; | 85% |
N,N-dimethyl-o-toluidine
(2-deuteriomethylphenyl)dimethylamine
Conditions | Yield |
---|---|
Stage #1: N,N-dimethyl-o-toluidine With 2,2,6,6-tetramethyl-piperidine; n-butyllithium; potassium tert-butylate In tetrahydrofuran; hexane at -78℃; Inert atmosphere; Stage #2: With d(4)-methanol In tetrahydrofuran; hexane Inert atmosphere; regioselective reaction; | 83% |
N,N-dimethyl-o-toluidine
benzyl bromide
N,N-dimethyl-2-phenethylaniline
Conditions | Yield |
---|---|
Stage #1: N,N-dimethyl-o-toluidine With 2,2,6,6-tetramethyl-piperidine; n-butyllithium; potassium tert-butylate In hexane; n-heptane at 0℃; for 0.25h; Inert atmosphere; Stage #2: benzyl bromide In hexane; n-heptane at 0℃; for 1h; Inert atmosphere; | 83% |
benzoyl cyanide
N,N-dimethyl-o-toluidine
N-methyl-N-(2-methylphenyl)aminoacetonitrile
Conditions | Yield |
---|---|
With ferrous(II) sulfate heptahydrate; oxygen In methanol for 14h; Reflux; | 83% |
Conditions | Yield |
---|---|
With tert-butylammonium hexafluorophosphate(V) at 20℃; for 4h; Electrochemical reaction; | 83% |
Conditions | Yield |
---|---|
With lithium hexamethyldisilazane In tetrahydrofuran; toluene at 110℃; for 16h; Inert atmosphere; | 82% |
Conditions | Yield |
---|---|
With titanium tetrachloride In dichloromethane at 0 - 25℃; for 8h; N-dealkylation; | 81% |
Multi-step reaction with 2 steps 2: bei der Verseifung View Scheme |