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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

1-Iodo-2-nitrobenzene Manufacturer/High quality/Best price/In stock

Cas:609-73-4

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 1-Iodo-2-Nitrobenzene

Cas:609-73-4

Min.Order:1 Kilogram

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Type:Manufacturers

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Jinan Finer Chemical Co., Ltd

Product Description Product Name 1-Iodo-2-nitrobenzene CAS No. 609-73-4 Appearance

1-Iodo-2-nitrobenzene

Cas:609-73-4

Min.Order:10 Gram

FOB Price: $20.0 / 30.0

Type:Lab/Research institutions

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Henan Allgreen Chemical Co.,Ltd

high quality Appearance:white powder Storage:Sealed, dry, microtherm , avoid light and smell Package:According to the demand of customer Application:Pharmaceutical intermediates Transportation:by air or by sea Port:shanghai

1-Iodo-2-nitrobenzene

Cas:609-73-4

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

o-Iodonitrobenzene

Cas:609-73-4

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

1-Iodo-2-nitrobenzene Basic information Product Name: 1-Iodo-2-nitrobenzene Synonyms: 1-iodo-2-nitro-benzen;benzene,1-iodo-2-nitro-;o-Iodonitrobenzene;O-NITROIODOBENZ

best offer 1-Iodo-2-nitrobenzene

Cas:609-73-4

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Sinotech Import&Export Corporation

Product Name: 1-Iodo-2-nitrobenzene Synonyms: 1-iodo-2-nitro-benzen;benzene,1-iodo-2-nitro-;o-Iodonitrobenzene;O-NITROIODOBENZENE;2-NITRO IODO BENZENE;2-IODONITROBENZENE;1-IODO-2-NITROBENZENE;2-Iononitroben

1-Iodo-2-nitrobenzene

Cas:609-73-4

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

1-Iodo-2-nitrobenzene

Cas:609-73-4

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

1-Iodo-2-nitrobenzene

Cas:609-73-4

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

1-Iodo-2-nitrobenzene

Cas:609-73-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality 1-Iodo-2-Nitrobenzene

Cas:609-73-4

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

1)quick response within 12 hours; 2)quality guarantee: all products are strictly tested by our qc, confirmed by qa and approved by third party lab in china, usa, canada, germany, uk, italy, france etc. 3) oem/odm available; 4) rea

609-73-4CAS NO.: 609-73-4

Cas:609-73-4

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

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Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

1-Iodo-2-nitrobenzene

Cas:609-73-4

Min.Order:0

Negotiable

Type:Manufacturers

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GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier

2-Iodonitrobenzene

Cas:609-73-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hangzhou Dingyan Chem Co., Ltd

manufacture Application:The refence standard products, for lab use, also we could produce bigger quantity on yr requirement.

1-iodo-2-nitrobenzene

Cas:609-73-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

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HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:white crystalline powder Storage:Sealed in a cool ,dry and microtherm place , avoid light . Package:100g/bottle,1kg/bottle,25kg/drum or as per your request Application:It is an impo

609-73-4 supplier in China

Cas:609-73-4

Min.Order:100 Gram

Negotiable

Type:Trading Company

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Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

1-Iodo-2-Nitrobenzene

Cas:609-73-4

Min.Order:0

Negotiable

Type:Manufacturers

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Enke Pharma-tech Co.,Ltd. (Cangzhou, China )

Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city?in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api,?intermediat

2-Iodonitrobenzene

Cas:609-73-4

Min.Order:0

Negotiable

Type:Manufacturers

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Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

1-Iodo-2-nitrobenzene

Cas:609-73-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hangzhou Ocean Chemical Co., Ltd.

★.Best quality according to requirement ★.Competitive price in China market ★.Mature Technical support ★.Professional logistic support

1-Iodo-2-nitrobenzene

Cas:609-73-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

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SAGECHEM LIMITED

609-73-4 Application:intermediate

Benzene, 1-iodo-2-nitro-

Cas:609-73-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

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AstaTech ( Chengdu) BioPharmaceutical Corp.

Quality assurance, stable process and affordable priceAppearance:detailed see specifications Storage:enquiry Package:according to the clients requirement Application:Pharmaceutical intermediates Transportation:Normal Port:chengdu

1-Iodo-2-nitrobenzene

Cas:609-73-4

Min.Order:0

Negotiable

Type:Trading Company

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Hunan Russell Chemicals Technology Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

1-Iodo-2-nitrobenzene 609-73-4

Cas:609-73-4

Min.Order:0

Negotiable

Type:Trading Company

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Chemsigma International Co.,Ltd.

bulk?production Application:Pharmaceutical intermediates

2-iodonitrobenzene

Cas:609-73-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Bide Pharmatech Ltd

Our mission is to provide high-quality and innovative products to our customers. By offering a broad range of products, custom synthesis and personalized services, Bide can help scientists speeding up their research in the chemical and pharmaceutical

1-Iodo-2-nitrobenzene

Cas:609-73-4

Min.Order:0

Negotiable

Type:Other

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Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

1-Iodo-2-nitrobenzene

Cas:609-73-4

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

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HENAN SUNLAKE ENTERPRISE CORPORATION

1-Iodo-2-nitrobenzene

Cas:609-73-4

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Shaanxi Mingqi Chemical Co., Ltd

Known for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers.1) Standard:BP/USP/EP/Enterprise standard2) All Purity≥99%3) We are manufacturer and can provide high quality products with factory pric

Manufacturer Supply Top quality 1-Iodo-2-nitrobenzene

Cas:609-73-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Zhengzhou Kingorgchem Chemical Technology Co., Ltd.

1. Subsidiary of Institute of Chemistry, Henan Academy of Sciences, national research platform;2. About 30 years’ experience in this field since 1983;3. An experienced R&D team consisting of Doctors and Masters;4. Various types of analytical instrume

ISO 9001 National Research Platform CAS No. 609-73-4

Cas:609-73-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

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BAYNOE CHEM CO.,LTD

Baynoe Chem is a technology innovation enterprise, specializing in searches, production,sale and service on OLED intermediates and fine chemical products. Baynoe Chem includes two R&D center(Suzhou), a production base(Gansu) and an internationa

1-Iodo-2-nitrobenzene 99%

Cas:609-73-4

Min.Order:1 Milligram

Negotiable

Type:Lab/Research institutions

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Synthetic route

2-nitrobenzenediazonium tetrafluoroborate
365-33-3

2-nitrobenzenediazonium tetrafluoroborate

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

Conditions
ConditionsYield
With potassium iodide In water at 25℃; for 0.0833333h; Solvent; Sandmeyer Reaction;99%
With pyridine; iodine In acetonitrile at -30 - 25℃; for 2h;89%
With iodine; potassium iodide In dimethyl sulfoxide at 15℃;
2-nitrobenzenediazonium 4-methylbenzenesulfonate
1059625-66-9

2-nitrobenzenediazonium 4-methylbenzenesulfonate

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

Conditions
ConditionsYield
With potassium iodide In water at 20℃; for 0.166667h;97%
With potassium iodide In water for 0.333333h; paste form;
2-nitrophenyl bromide
577-19-5

2-nitrophenyl bromide

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

Conditions
ConditionsYield
With aluminum oxide; copper(l) iodide; potassium iodide In various solvent(s) at 150℃; Product distribution; other substances;95%
With KI-CuI-alumina In various solvent(s) at 150℃; for 2h;86%
2-nitrobenzenediazonium o-benzenedisulfonamide

2-nitrobenzenediazonium o-benzenedisulfonamide

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

Conditions
ConditionsYield
With tetra-(n-butyl)ammonium iodide In acetonitrile at 20℃; for 0.75h; Substitution;94%
ortho-nitrobenzoic acid
552-16-9

ortho-nitrobenzoic acid

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

Conditions
ConditionsYield
With 1-iodo-3,5,5-trimethylhydantoin In tetrachloromethane for 24h; Concentration; Time; Solvent; Reagent/catalyst; Reflux; Irradiation;93%
With N-iodo-succinimide; [4,4’-bis(1,1-dimethylethyl)-2,2’-bipyridine-N1,N1‘]bis [3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-N]phenyl-C]iridium(III) hexafluorophosphate; iodine; caesium carbonate In 1,2-dichloro-ethane at 50℃; for 36h; Inert atmosphere; Irradiation; Sealed tube;65%
With copper(l) iodide; oxygen In dimethyl sulfoxide at 160℃; under 760.051 Torr; for 30h; Schlenk technique; Sealed tube;61%
With 2.9-dimethyl-1,10-phenanthroline; oxygen; copper diacetate; silver sulfate; sodium iodide In dimethyl sulfoxide at 160℃; under 760.051 Torr; for 20h; Schlenk technique;39%
Stage #1: ortho-nitrobenzoic acid With (tri-tert-butylphosphane)gold(I) chloride; silver(l) oxide In N,N-dimethyl-formamide at 100℃; for 2h; Inert atmosphere;
Stage #2: With N-iodo-succinimide In N,N-dimethyl-formamide at 50℃; for 1h; Inert atmosphere;
82 %Spectr.
2-nitro-aniline
88-74-4

2-nitro-aniline

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

Conditions
ConditionsYield
With Nitrogen dioxide; sodium iodide In acetonitrile at -20℃; for 10h;92%
Stage #1: 2-nitro-aniline With toluene-4-sulfonic acid In water at 20℃;
Stage #2: With potassium iodide In water at 20℃; for 1.5h;
91%
Stage #1: 2-nitro-aniline With nicotinic acid sulfate; sodium nitrite In water at 20℃; for 0.333333h; Grinding;
Stage #2: With sodium iodide In water at 20℃;
88%
2-nitrophenylboronic acid
5570-19-4

2-nitrophenylboronic acid

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

Conditions
ConditionsYield
With sodium nitrite In acetonitrile at 80℃; for 9h; Sealed tube;90%
With 1,10-Phenanthroline; oxygen; potassium iodide; copper(ll) bromide In N,N-dimethyl-formamide at 80℃; for 20h;86%
With N-iodo-succinimide; potassium acetate In acetonitrile at 50℃; for 4h;52%
bis(trifluoromethanesulfonyl)amide
82113-65-3

bis(trifluoromethanesulfonyl)amide

2-nitro-aniline
88-74-4

2-nitro-aniline

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

Conditions
ConditionsYield
Stage #1: bis(trifluoromethanesulfonyl)amide With tert.-butylnitrite; acetic acid In ethanol Cooling with ice;
Stage #2: 2-nitro-aniline With tetraethylammonium iodide In water at 20℃;
82%
o-nitro-iodosylbenzene
69180-53-6

o-nitro-iodosylbenzene

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

Conditions
ConditionsYield
In 1,2-dichloro-ethane at 60℃; for 8h;80%
1,2-Dinitrobenzene
528-29-0

1,2-Dinitrobenzene

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

Conditions
ConditionsYield
Stage #1: 1,2-Dinitrobenzene With perchloric acid; sulfuric acid; sodium nitrite In water; ethyl acetate Electrochemical reaction;
Stage #2: With copper; potassium iodide In water Electrochemical reaction;
74%
iodobenzene
591-50-4

iodobenzene

A

p-nitrobenzene iodide
636-98-6

p-nitrobenzene iodide

B

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

Conditions
ConditionsYield
With nitric acid at 50℃; for 3h;A 70.2%
B 29.2%
With trinitratooxovanadium(V) In dichloromethane for 0.333333h; Ambient temperature;A 63%
B 34%
With trinitratooxovanadium(V) In dichloromethane for 0.333333h; Ambient temperature;A 62%
B 35%
2-iodophenylamine
615-43-0

2-iodophenylamine

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

Conditions
ConditionsYield
With dihydrogen peroxide; potassium carbonate In water; acetonitrile at 20℃;65%
3,3-dimethyl-butan-2-one
75-97-8

3,3-dimethyl-butan-2-one

A

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

B

o-nitro-phenylpinacolone

o-nitro-phenylpinacolone

C

nitrobenzene
98-95-3

nitrobenzene

Conditions
ConditionsYield
With 3,3-dimethyl-butan-2-one; di-tert-butyl nitroxide; potassium tert-butylate In ammonia at -33℃; for 0.025h;A 55%
B 17 % Chromat.
C 19 % Chromat.
N-(2-nitrophenylazo)piperidine

N-(2-nitrophenylazo)piperidine

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

Conditions
ConditionsYield
With zinc(II) iodide In acetonitrile at 20℃; for 2h;41%
iodobenzene
591-50-4

iodobenzene

nitromethane
75-52-5

nitromethane

nitro acetate
591-09-3

nitro acetate

A

p-nitrobenzene iodide
636-98-6

p-nitrobenzene iodide

B

m-iodonitrobenzene
645-00-1

m-iodonitrobenzene

C

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

2-nitro(dichloroiodo)benzene
827-28-1

2-nitro(dichloroiodo)benzene

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

Conditions
ConditionsYield
beim Umkrystallisieren;
With (dissociation) In acetic acid at 15 - 25℃; Kinetics;
3-nitro-4-iodoaniline
105752-04-3

3-nitro-4-iodoaniline

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

iodobenzene
591-50-4

iodobenzene

A

p-nitrobenzene iodide
636-98-6

p-nitrobenzene iodide

B

m-iodonitrobenzene
645-00-1

m-iodonitrobenzene

C

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

Conditions
ConditionsYield
With silver nitrate; boron trifluoride In acetonitrile at 25℃; for 10h; Product distribution; competitive nitration benzene, relative rate;A 80 % Chromat.
B 3 % Chromat.
C 17 % Chromat.
With nitro acetate; H-ZSM-11 In hexane at 30℃; Product distribution; different catalysts;
With Hβ zeolite; oxygen; dinitrogen tetraoxide In 1,2-dichloro-ethane at 0℃; for 48h; Nitration; Title compound not separated from byproducts.;
With nitric acid; acetic anhydride In tetrachloromethane
With nitrogen dioxide; oxygen; acetic anhydride at 35℃; under 3750.38 Torr; Autoclave;
(Dichloroiodo)benzene
932-72-9

(Dichloroiodo)benzene

A

p-nitrobenzene iodide
636-98-6

p-nitrobenzene iodide

B

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

Conditions
ConditionsYield
With nitronium tetrafluoborate; para-xylene In tetrachloromethane at 20℃; for 1h; Isomer distribution;
iodine
7553-56-2

iodine

1,2-Dinitrobenzene
528-29-0

1,2-Dinitrobenzene

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

Conditions
ConditionsYield
at 300℃;
aluminium trichloride
7446-70-0

aluminium trichloride

iodobenzene
591-50-4

iodobenzene

dinitrogen tetraoxide
10544-72-6

dinitrogen tetraoxide

A

p-nitrobenzene iodide
636-98-6

p-nitrobenzene iodide

B

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

Conditions
ConditionsYield
at 0 - 5℃;
iodobenzene
591-50-4

iodobenzene

diacetylnitric acid

diacetylnitric acid

A

p-nitrobenzene iodide
636-98-6

p-nitrobenzene iodide

B

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

iodobenzene
591-50-4

iodobenzene

nitric acid
7697-37-2

nitric acid

A

p-nitrobenzene iodide
636-98-6

p-nitrobenzene iodide

B

1-iodo-2,4-dinitrobenzene
709-49-9

1-iodo-2,4-dinitrobenzene

C

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

iodobenzene
591-50-4

iodobenzene

nitric acid
7697-37-2

nitric acid

A

p-nitrobenzene iodide
636-98-6

p-nitrobenzene iodide

B

m-iodonitrobenzene
645-00-1

m-iodonitrobenzene

C

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

iodosylbenzene
536-80-1

iodosylbenzene

nitric acid
7697-37-2

nitric acid

A

p-nitrobenzene iodide
636-98-6

p-nitrobenzene iodide

B

iodobenzene
591-50-4

iodobenzene

C

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

iodoxybenzene
696-33-3

iodoxybenzene

nitric acid
7697-37-2

nitric acid

A

p-nitrobenzene iodide
636-98-6

p-nitrobenzene iodide

B

iodobenzene
591-50-4

iodobenzene

C

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

o-iodosyl-nitrobenzene

o-iodosyl-nitrobenzene

A

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

B

2-nitro-1-iodylbenzene
16825-77-7

2-nitro-1-iodylbenzene

Conditions
ConditionsYield
With water
N-(2-nitro-phenyl)-N'-p-tolyl-triazene
76151-92-3

N-(2-nitro-phenyl)-N'-p-tolyl-triazene

A

4-tolyl iodide
624-31-7

4-tolyl iodide

B

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

Conditions
ConditionsYield
With boron trifluoride diethyl etherate; sodium iodide In acetonitrile at 40℃; for 2h;
o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

phenylacetylene
536-74-3

phenylacetylene

1-nitro-2-phenylethynyl-benzene
35010-17-4

1-nitro-2-phenylethynyl-benzene

Conditions
ConditionsYield
With potassium hydroxide In N,N-dimethyl-formamide at 135℃; for 2h; Sonogashira Cross-Coupling; Inert atmosphere;100%
With tetrakis(acetonitrile)copper(I) perchlorate; 2,5-bis(2-(diphenylphosphino)5-methoxyphenyl)-1,3,4-oxadiazole; potassium carbonate In 1,4-dioxane Catalytic behavior; Reagent/catalyst; Sonogashira Cross-Coupling; Reflux; Inert atmosphere; Schlenk technique;99%
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tributyl-amine; potassium carbonate In water; N,N-dimethyl-formamide at 20℃; for 1h; Mechanism; Product distribution; various bases and solvents;98%
n-octyne
629-05-0

n-octyne

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

1-nitro-2-(oct-1-yn-1-yl)benzene

1-nitro-2-(oct-1-yn-1-yl)benzene

Conditions
ConditionsYield
With copper(l) iodide; C27H34Cl2N4Pd; potassium carbonate; triphenylphosphine In ethanol at 60℃; for 13h; Solvent; Reagent/catalyst; Time; Sonogashira Cross-Coupling;100%
With triethylamine; zinc dibromide; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 23℃;89%
Stage #1: o-nitroiodobenzene With bis(triphenylphosphine)palladium(II) chloride; triethylamine at 20℃; for 0.166667h;
Stage #2: n-octyne With copper(l) iodide at 20℃; for 6h;
o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

dichloromethylphenylsilane
149-74-6

dichloromethylphenylsilane

2-nitrobiphenyl
86-00-0

2-nitrobiphenyl

Conditions
ConditionsYield
With potassium hydroxide; palladium on activated charcoal In water Heating;100%
5-formylfurane-2-boronic acid
27329-70-0

5-formylfurane-2-boronic acid

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

5-(2-nitrophenyl)-2-furaldehyde
20000-96-8

5-(2-nitrophenyl)-2-furaldehyde

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; sodium carbonate In 1,2-dimethoxyethane; ethanol; water at 50℃; for 3h; Suzuki reaction;100%
With bis-triphenylphosphine-palladium(II) chloride; sodium carbonate In water; acetonitrile at 80℃; for 3h; Suzuki Coupling;
4-(benzoyloxy)morpholine
5765-65-1

4-(benzoyloxy)morpholine

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

N-(2-nitrophenyl)morpholine
5320-98-9

N-(2-nitrophenyl)morpholine

Conditions
ConditionsYield
Stage #1: o-nitroiodobenzene With isopropylmagnesium bromide In tetrahydrofuran at -35℃; for 0.166667h;
Stage #2: With zinc(II) chloride In tetrahydrofuran at -35℃; for 0.166667h;
Stage #3: 4-(benzoyloxy)morpholine With copper (I) trifluoromethane sulfonate benzene In tetrahydrofuran at 20℃; for 1h;
100%
Stage #1: o-nitroiodobenzene With phenylmagnesium bromide In tetrahydrofuran at -35℃; for 0.166667h;
Stage #2: With zinc(II) chloride In tetrahydrofuran at -35℃; for 0.166667h;
Stage #3: 4-(benzoyloxy)morpholine; copper (I) trifluoromethane sulfonate benzene In tetrahydrofuran at 25℃; for 1h;
o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

hexamethyldistannane
661-69-8

hexamethyldistannane

trimethyl-(2-nitro-phenyl)-stannane
76074-18-5

trimethyl-(2-nitro-phenyl)-stannane

Conditions
ConditionsYield
dichloro bis(acetonitrile) palladium(II) In N,N-dimethyl-formamide byproducts: (CH3)3SnI; Me6Sn2, o-NO2C6H4I dissolved in DMF in a flask, catalyst added with stirring, reacted for 5 min at 20°C; water added, extracted with ether, extracts filtered, washed with water, dried with Na2SO4, chromy.(silica gel, hexane/ether 2:1);100%
tetrakis(triphenylphosphine) palladium(0)66%
o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

2-iodophenylamine
615-43-0

2-iodophenylamine

Conditions
ConditionsYield
With hydrogenchloride; iron In water; N,N-dimethyl-formamide for 2h; Reflux;99.2%
With sodium tetrahydroborate; cyclohexanediamine-Pd-β-cyclodextrin In water at 20℃; for 3h; Sealed tube;98%
With hexacarbonyl molybdenum In ethanol for 24h; Heating;96%
1-hepten-3-ol
4938-52-7

1-hepten-3-ol

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

1-(2-nitrophenyl)-3-heptanone
159617-00-2

1-(2-nitrophenyl)-3-heptanone

Conditions
ConditionsYield
With tetrabutyl-ammonium chloride; palladium diacetate; sodium hydrogencarbonate In N,N-dimethyl-formamide at 50℃; for 7h;99%
o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

trimethylsilylacetylene
1066-54-2

trimethylsilylacetylene

trimethyl((2-nitrophenyl)ethynyl)silane
75867-47-9

trimethyl((2-nitrophenyl)ethynyl)silane

Conditions
ConditionsYield
With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; triethylamine In tetrahydrofuran Sonogashira Cross-Coupling; Inert atmosphere;99%
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine In N,N-dimethyl-formamide at 50℃; for 2h; Sonogashira reaction;94%
With copper(l) iodide; triethylamine In N,N-dimethyl-formamide at 50℃; for 6h; Sonogashira coupling;91%
pent-1-yn-5-ol
5390-04-5

pent-1-yn-5-ol

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

2-(5-hydroxy-1-pentynyl)nitrobenzene
442155-83-1

2-(5-hydroxy-1-pentynyl)nitrobenzene

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; Sonogashira coupling;99%
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; for 14h; Sonogashira coupling;92%
With copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride at 25℃; for 16h; Sonogashira cross-coupling;91%
Stage #1: pent-1-yn-5-ol; o-nitroiodobenzene With bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine In N,N-dimethyl-formamide for 0.5h; Sonogashira coupling; Inert atmosphere;
Stage #2: With copper(l) iodide In N,N-dimethyl-formamide at 20℃; for 5.16667h; Sonogashira coupling; Inert atmosphere;
83%
5-hexyl-1-ol
928-90-5

5-hexyl-1-ol

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

2-(6-hydroxy-1-hexynyl)nitrobenzene
442155-84-2

2-(6-hydroxy-1-hexynyl)nitrobenzene

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; Sonogashira coupling;99%
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; for 13h; Sonogashira coupling;99%
Stage #1: 5-hexyl-1-ol; o-nitroiodobenzene With bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine In N,N-dimethyl-formamide for 0.5h; Sonogashira coupling; Inert atmosphere;
Stage #2: With copper(l) iodide In N,N-dimethyl-formamide at 20℃; for 5.16667h; Sonogashira coupling; Inert atmosphere;
71%
o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

p-Chlorothiophenol
106-54-7

p-Chlorothiophenol

4-chlorophenyl 2-nitrophenyl sulfide
6764-10-9

4-chlorophenyl 2-nitrophenyl sulfide

Conditions
ConditionsYield
With potassium phosphate; copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline In butan-1-ol at 120℃; for 2h; Microwave irradiation;99%
With potassium hydroxide; copper(l) iodide; sarcosine In 1,4-dioxane at 100℃; for 24h;33%
o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

phenylboronic acid
98-80-6

phenylboronic acid

2-nitrobiphenyl
86-00-0

2-nitrobiphenyl

Conditions
ConditionsYield
With potassium carbonate; palladium diacetate In methanol; water at 20℃; for 1.5h; Suzuki cross-coupling;99%
With potassium phosphate In water; N,N-dimethyl-formamide at 100℃; for 0.5h; Suzuki-Miyaura reaction;99%
With potassium phosphate; tetrakis(triphenylphosphine) palladium(0) In ethanol for 6h; Reflux; Inert atmosphere;99%
o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

2-Methylphenylboronic acid
16419-60-6

2-Methylphenylboronic acid

2-methyl-2'-nitro-1,1'-biphenyl
67992-12-5

2-methyl-2'-nitro-1,1'-biphenyl

Conditions
ConditionsYield
With potassium carbonate; palladium diacetate In methanol; water at 50℃; for 24h; Suzuki cross-coupling;99%
With C43H54N2S; palladium diacetate; potassium carbonate In water; isopropyl alcohol at 100℃; for 11h; Suzuki-Miyaura coupling reaction; Aerobic condition; Sealed tube;96%
1-cyano-2-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)naphthalene
918630-49-6

1-cyano-2-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)naphthalene

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

2-(2-nitrophenyl)naphthalene-1-carbonitrile

2-(2-nitrophenyl)naphthalene-1-carbonitrile

Conditions
ConditionsYield
With potassium carbonate; tetrakis(triphenylphosphine) palladium(0) In ethanol; toluene at 100℃; for 6h;99%
2-Aminopyrazine
5049-61-6

2-Aminopyrazine

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

N-(2-nitrophenyl)pyrazin-2-amine

N-(2-nitrophenyl)pyrazin-2-amine

Conditions
ConditionsYield
With sodium phenoxide; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; tris(dibenzylideneacetone)dipalladium (0) In 1,4-dioxane at 80℃; for 2h;99%
o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

4-methoxyphenylacetylen
768-60-5

4-methoxyphenylacetylen

1-(4-methoxyphenyl)-2-(2-nitrophenyl)acetylene
121387-01-7

1-(4-methoxyphenyl)-2-(2-nitrophenyl)acetylene

Conditions
ConditionsYield
With tetrakis(acetonitrile)copper(I) perchlorate; 2,5-bis(2-(diphenylphosphino)5-methoxyphenyl)-1,3,4-oxadiazole; potassium carbonate In 1,4-dioxane Catalytic behavior; Reagent/catalyst; Sonogashira Cross-Coupling; Reflux; Inert atmosphere; Schlenk technique;99%
With potassium phosphate In water; isopropyl alcohol at 80℃; for 20h; Sonogashira Cross-Coupling; Sealed tube;85%
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine In N,N-dimethyl-formamide at 20℃; for 6h; Sonogashira coupling; Inert atmosphere;78%
1H-imidazole
288-32-4

1H-imidazole

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

1-(2-nitrophenyl)-1H-imidazole
23309-16-2

1-(2-nitrophenyl)-1H-imidazole

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 25℃; for 4h; Inert atmosphere;99%
With potassium carbonate In N,N-dimethyl-formamide at 152℃; for 18h;87%
With 8-Hydroxyquinoline-N-oxide; caesium carbonate; copper(I) bromide In dimethyl sulfoxide at 65℃; for 60h; Ullmann coupling; Inert atmosphere; chemoselective reaction;84%
o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

cyclohexylamine
108-91-8

cyclohexylamine

N-cyclohexyl-2-nitroaniline
6373-71-3

N-cyclohexyl-2-nitroaniline

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 25℃; for 1h; Inert atmosphere;99%
With 2Na(1+)*CuC6H4(NCHC6H3OO3S)2(2-)=CuC6H4(NCHC6H3ONaO3S)2; sodium hydroxide In water at 120℃; for 15h;90%
With rac-BINAP; palladium diacetate; caesium carbonate In toluene at 115℃; for 18h; Inert atmosphere;80%
o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

1-pentanamine
110-58-7

1-pentanamine

2-nitro-N-pentylaniline
91430-23-8

2-nitro-N-pentylaniline

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 25℃; for 2h; Inert atmosphere;99%
o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

benzylamine
100-46-9

benzylamine

N-benzyl-2-nitroaniline
5729-06-6

N-benzyl-2-nitroaniline

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 25℃; for 2h; Inert atmosphere;99%
o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

4-methoxyphenylboronic acid
5720-07-0

4-methoxyphenylboronic acid

4'-methoxy-2-nitrobiphenyl
20013-55-2

4'-methoxy-2-nitrobiphenyl

Conditions
ConditionsYield
With potassium carbonate In ethanol at 80℃; for 0.5h; Catalytic behavior; Reagent/catalyst; Suzuki-Miyaura Coupling;99%
With C43H54N2S; palladium diacetate; potassium carbonate In water; isopropyl alcohol at 100℃; for 6h; Suzuki-Miyaura coupling reaction; Aerobic condition; Sealed tube;94%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,2-dimethoxyethane; water for 18h; Inert atmosphere; Reflux;88%
(4-Nitrophenyl)acetylene
937-31-5

(4-Nitrophenyl)acetylene

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

2,4'-dinitrophenylacetylene
408321-17-5

2,4'-dinitrophenylacetylene

Conditions
ConditionsYield
With tetrakis(acetonitrile)copper(I) perchlorate; 2,5-bis(2-(diphenylphosphino)5-methoxyphenyl)-1,3,4-oxadiazole; potassium carbonate In 1,4-dioxane Catalytic behavior; Reagent/catalyst; Sonogashira Cross-Coupling; Reflux; Inert atmosphere; Schlenk technique;99%
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine In N,N-dimethyl-formamide at 20℃; for 6h; Sonogashira coupling; Inert atmosphere;65%
4-Methoxybenzenethiol
696-63-9

4-Methoxybenzenethiol

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

4-methoxyphenyl-2-nitrophenylsulfide
3169-69-5

4-methoxyphenyl-2-nitrophenylsulfide

Conditions
ConditionsYield
With potassium phosphate; copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline In butan-1-ol at 120℃; for 2h; Microwave irradiation;99%
2,4-dichlorobenzenethiol
1122-41-4

2,4-dichlorobenzenethiol

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

2,4-dichlorophenyl 2-nitrophenyl sulfide
187845-78-9

2,4-dichlorophenyl 2-nitrophenyl sulfide

Conditions
ConditionsYield
With potassium phosphate; copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline In butan-1-ol at 120℃; for 2h; Microwave irradiation;99%
o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

4-Chlorophenylboronic acid
1679-18-1

4-Chlorophenylboronic acid

4'-chloro-2-nitrobiphenyl
6271-80-3

4'-chloro-2-nitrobiphenyl

Conditions
ConditionsYield
With sodium methylate In 1,4-dioxane at 100℃; for 25h; Suzuki-Miyaura Coupling; Schlenk technique;99%
With C30H24N3OPPd; potassium carbonate In tetrahydrofuran; N,N-dimethyl-formamide for 1h; Suzuki Coupling; Reflux;80%
With sodium methylate In 1,4-dioxane at 100℃; for 24h; Inert atmosphere;
o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

isobutyraldehyde
78-84-2

isobutyraldehyde

(R/S)-1-(2-nitrophenyl)-2-methyl-1-propanol
93420-32-7

(R/S)-1-(2-nitrophenyl)-2-methyl-1-propanol

Conditions
ConditionsYield
Stage #1: o-nitroiodobenzene With phenylmagnesium chloride In tetrahydrofuran at -40℃; for 0.0833333h; Inert atmosphere;
Stage #2: isobutyraldehyde In tetrahydrofuran at 20℃;
99%
Thien-3-ylboronic acid
6165-69-1

Thien-3-ylboronic acid

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

3-(2-nitrophenyl)thiophene
96919-48-1

3-(2-nitrophenyl)thiophene

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate In water; N,N-dimethyl-formamide at 150℃; for 0.25h; Suzuki-Miyaura Coupling; Microwave irradiation;99%
With tetrakis(triphenylphosphine) palladium(0) In water; N,N-dimethyl-formamide at 90℃; for 12h;88.6%
With tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate In water; N,N-dimethyl-formamide
With tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate In water; N,N-dimethyl-formamide for 12h; Reflux;
2-(2-amino-4-methoxyphenyl)propan-2-ol
1050514-19-6

2-(2-amino-4-methoxyphenyl)propan-2-ol

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

2-(4-methoxy-2-((2-nitrophenyl)amino)phenyl)propan-2-ol

2-(4-methoxy-2-((2-nitrophenyl)amino)phenyl)propan-2-ol

Conditions
ConditionsYield
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; SPhos Pd G2; caesium carbonate In toluene for 18h; Reflux;99%

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