Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:609-73-4
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:609-73-4
Min.Order:1 Kilogram
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inquiryProduct Description Product Name 1-Iodo-2-nitrobenzene CAS No. 609-73-4 Appearance
Cas:609-73-4
Min.Order:10 Gram
FOB Price: $20.0 / 30.0
Type:Lab/Research institutions
inquiryhigh quality Appearance:white powder Storage:Sealed, dry, microtherm , avoid light and smell Package:According to the demand of customer Application:Pharmaceutical intermediates Transportation:by air or by sea Port:shanghai
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:609-73-4
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inquiry1-Iodo-2-nitrobenzene Basic information Product Name: 1-Iodo-2-nitrobenzene Synonyms: 1-iodo-2-nitro-benzen;benzene,1-iodo-2-nitro-;o-Iodonitrobenzene;O-NITROIODOBENZ
Cas:609-73-4
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryProduct Name: 1-Iodo-2-nitrobenzene Synonyms: 1-iodo-2-nitro-benzen;benzene,1-iodo-2-nitro-;o-Iodonitrobenzene;O-NITROIODOBENZENE;2-NITRO IODO BENZENE;2-IODONITROBENZENE;1-IODO-2-NITROBENZENE;2-Iononitroben
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:609-73-4
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:609-73-4
Min.Order:4 Kilogram
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:609-73-4
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiry1)quick response within 12 hours; 2)quality guarantee: all products are strictly tested by our qc, confirmed by qa and approved by third party lab in china, usa, canada, germany, uk, italy, france etc. 3) oem/odm available; 4) rea
Cas:609-73-4
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
manufacture Application:The refence standard products, for lab use, also we could produce bigger quantity on yr requirement.
Superior quality, moderate price & quick delivery. Appearance:white crystalline powder Storage:Sealed in a cool ,dry and microtherm place , avoid light . Package:100g/bottle,1kg/bottle,25kg/drum or as per your request Application:It is an impo
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city?in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api,?intermediat
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
★.Best quality according to requirement ★.Competitive price in China market ★.Mature Technical support ★.Professional logistic support
Quality assurance, stable process and affordable priceAppearance:detailed see specifications Storage:enquiry Package:according to the clients requirement Application:Pharmaceutical intermediates Transportation:Normal Port:chengdu
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
Our mission is to provide high-quality and innovative products to our customers. By offering a broad range of products, custom synthesis and personalized services, Bide can help scientists speeding up their research in the chemical and pharmaceutical
1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
Cas:609-73-4
Min.Order:10 Milligram
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Type:Lab/Research institutions
inquiryKnown for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers.1) Standard:BP/USP/EP/Enterprise standard2) All Purity≥99%3) We are manufacturer and can provide high quality products with factory pric
Cas:609-73-4
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inquiry1. Subsidiary of Institute of Chemistry, Henan Academy of Sciences, national research platform;2. About 30 years’ experience in this field since 1983;3. An experienced R&D team consisting of Doctors and Masters;4. Various types of analytical instrume
Cas:609-73-4
Min.Order:0
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Type:Lab/Research institutions
inquiryBaynoe Chem is a technology innovation enterprise, specializing in searches, production,sale and service on OLED intermediates and fine chemical products. Baynoe Chem includes two R&D center(Suzhou), a production base(Gansu) and an internationa
Cas:609-73-4
Min.Order:1 Milligram
Negotiable
Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With potassium iodide In water at 25℃; for 0.0833333h; Solvent; Sandmeyer Reaction; | 99% |
With pyridine; iodine In acetonitrile at -30 - 25℃; for 2h; | 89% |
With iodine; potassium iodide In dimethyl sulfoxide at 15℃; |
2-nitrobenzenediazonium 4-methylbenzenesulfonate
o-nitroiodobenzene
Conditions | Yield |
---|---|
With potassium iodide In water at 20℃; for 0.166667h; | 97% |
With potassium iodide In water for 0.333333h; paste form; |
Conditions | Yield |
---|---|
With aluminum oxide; copper(l) iodide; potassium iodide In various solvent(s) at 150℃; Product distribution; other substances; | 95% |
With KI-CuI-alumina In various solvent(s) at 150℃; for 2h; | 86% |
o-nitroiodobenzene
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide In acetonitrile at 20℃; for 0.75h; Substitution; | 94% |
Conditions | Yield |
---|---|
With 1-iodo-3,5,5-trimethylhydantoin In tetrachloromethane for 24h; Concentration; Time; Solvent; Reagent/catalyst; Reflux; Irradiation; | 93% |
With N-iodo-succinimide; [4,4’-bis(1,1-dimethylethyl)-2,2’-bipyridine-N1,N1‘]bis [3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-N]phenyl-C]iridium(III) hexafluorophosphate; iodine; caesium carbonate In 1,2-dichloro-ethane at 50℃; for 36h; Inert atmosphere; Irradiation; Sealed tube; | 65% |
With copper(l) iodide; oxygen In dimethyl sulfoxide at 160℃; under 760.051 Torr; for 30h; Schlenk technique; Sealed tube; | 61% |
With 2.9-dimethyl-1,10-phenanthroline; oxygen; copper diacetate; silver sulfate; sodium iodide In dimethyl sulfoxide at 160℃; under 760.051 Torr; for 20h; Schlenk technique; | 39% |
Stage #1: ortho-nitrobenzoic acid With (tri-tert-butylphosphane)gold(I) chloride; silver(l) oxide In N,N-dimethyl-formamide at 100℃; for 2h; Inert atmosphere; Stage #2: With N-iodo-succinimide In N,N-dimethyl-formamide at 50℃; for 1h; Inert atmosphere; | 82 %Spectr. |
Conditions | Yield |
---|---|
With Nitrogen dioxide; sodium iodide In acetonitrile at -20℃; for 10h; | 92% |
Stage #1: 2-nitro-aniline With toluene-4-sulfonic acid In water at 20℃; Stage #2: With potassium iodide In water at 20℃; for 1.5h; | 91% |
Stage #1: 2-nitro-aniline With nicotinic acid sulfate; sodium nitrite In water at 20℃; for 0.333333h; Grinding; Stage #2: With sodium iodide In water at 20℃; | 88% |
Conditions | Yield |
---|---|
With sodium nitrite In acetonitrile at 80℃; for 9h; Sealed tube; | 90% |
With 1,10-Phenanthroline; oxygen; potassium iodide; copper(ll) bromide In N,N-dimethyl-formamide at 80℃; for 20h; | 86% |
With N-iodo-succinimide; potassium acetate In acetonitrile at 50℃; for 4h; | 52% |
Conditions | Yield |
---|---|
Stage #1: bis(trifluoromethanesulfonyl)amide With tert.-butylnitrite; acetic acid In ethanol Cooling with ice; Stage #2: 2-nitro-aniline With tetraethylammonium iodide In water at 20℃; | 82% |
o-nitro-iodosylbenzene
o-nitroiodobenzene
Conditions | Yield |
---|---|
In 1,2-dichloro-ethane at 60℃; for 8h; | 80% |
Conditions | Yield |
---|---|
Stage #1: 1,2-Dinitrobenzene With perchloric acid; sulfuric acid; sodium nitrite In water; ethyl acetate Electrochemical reaction; Stage #2: With copper; potassium iodide In water Electrochemical reaction; | 74% |
Conditions | Yield |
---|---|
With nitric acid at 50℃; for 3h; | A 70.2% B 29.2% |
With trinitratooxovanadium(V) In dichloromethane for 0.333333h; Ambient temperature; | A 63% B 34% |
With trinitratooxovanadium(V) In dichloromethane for 0.333333h; Ambient temperature; | A 62% B 35% |
Conditions | Yield |
---|---|
With dihydrogen peroxide; potassium carbonate In water; acetonitrile at 20℃; | 65% |
Conditions | Yield |
---|---|
With 3,3-dimethyl-butan-2-one; di-tert-butyl nitroxide; potassium tert-butylate In ammonia at -33℃; for 0.025h; | A 55% B 17 % Chromat. C 19 % Chromat. |
o-nitroiodobenzene
Conditions | Yield |
---|---|
With zinc(II) iodide In acetonitrile at 20℃; for 2h; | 41% |
iodobenzene
nitromethane
nitro acetate
A
p-nitrobenzene iodide
B
m-iodonitrobenzene
C
o-nitroiodobenzene
Conditions | Yield |
---|---|
beim Umkrystallisieren; | |
With (dissociation) In acetic acid at 15 - 25℃; Kinetics; |
3-nitro-4-iodoaniline
o-nitroiodobenzene
iodobenzene
A
p-nitrobenzene iodide
B
m-iodonitrobenzene
C
o-nitroiodobenzene
Conditions | Yield |
---|---|
With silver nitrate; boron trifluoride In acetonitrile at 25℃; for 10h; Product distribution; competitive nitration benzene, relative rate; | A 80 % Chromat. B 3 % Chromat. C 17 % Chromat. |
With nitro acetate; H-ZSM-11 In hexane at 30℃; Product distribution; different catalysts; | |
With Hβ zeolite; oxygen; dinitrogen tetraoxide In 1,2-dichloro-ethane at 0℃; for 48h; Nitration; Title compound not separated from byproducts.; | |
With nitric acid; acetic anhydride In tetrachloromethane | |
With nitrogen dioxide; oxygen; acetic anhydride at 35℃; under 3750.38 Torr; Autoclave; |
Conditions | Yield |
---|---|
With nitronium tetrafluoborate; para-xylene In tetrachloromethane at 20℃; for 1h; Isomer distribution; |
Conditions | Yield |
---|---|
at 300℃; |
aluminium trichloride
iodobenzene
dinitrogen tetraoxide
A
p-nitrobenzene iodide
B
o-nitroiodobenzene
Conditions | Yield |
---|---|
at 0 - 5℃; |
iodobenzene
nitric acid
A
p-nitrobenzene iodide
B
1-iodo-2,4-dinitrobenzene
C
o-nitroiodobenzene
iodobenzene
nitric acid
A
p-nitrobenzene iodide
B
m-iodonitrobenzene
C
o-nitroiodobenzene
iodosylbenzene
nitric acid
A
p-nitrobenzene iodide
B
iodobenzene
C
o-nitroiodobenzene
iodoxybenzene
nitric acid
A
p-nitrobenzene iodide
B
iodobenzene
C
o-nitroiodobenzene
A
o-nitroiodobenzene
B
2-nitro-1-iodylbenzene
Conditions | Yield |
---|---|
With water |
N-(2-nitro-phenyl)-N'-p-tolyl-triazene
A
4-tolyl iodide
B
o-nitroiodobenzene
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate; sodium iodide In acetonitrile at 40℃; for 2h; |
Conditions | Yield |
---|---|
With potassium hydroxide In N,N-dimethyl-formamide at 135℃; for 2h; Sonogashira Cross-Coupling; Inert atmosphere; | 100% |
With tetrakis(acetonitrile)copper(I) perchlorate; 2,5-bis(2-(diphenylphosphino)5-methoxyphenyl)-1,3,4-oxadiazole; potassium carbonate In 1,4-dioxane Catalytic behavior; Reagent/catalyst; Sonogashira Cross-Coupling; Reflux; Inert atmosphere; Schlenk technique; | 99% |
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tributyl-amine; potassium carbonate In water; N,N-dimethyl-formamide at 20℃; for 1h; Mechanism; Product distribution; various bases and solvents; | 98% |
Conditions | Yield |
---|---|
With copper(l) iodide; C27H34Cl2N4Pd; potassium carbonate; triphenylphosphine In ethanol at 60℃; for 13h; Solvent; Reagent/catalyst; Time; Sonogashira Cross-Coupling; | 100% |
With triethylamine; zinc dibromide; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 23℃; | 89% |
Stage #1: o-nitroiodobenzene With bis(triphenylphosphine)palladium(II) chloride; triethylamine at 20℃; for 0.166667h; Stage #2: n-octyne With copper(l) iodide at 20℃; for 6h; |
Conditions | Yield |
---|---|
With potassium hydroxide; palladium on activated charcoal In water Heating; | 100% |
5-formylfurane-2-boronic acid
o-nitroiodobenzene
5-(2-nitrophenyl)-2-furaldehyde
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; sodium carbonate In 1,2-dimethoxyethane; ethanol; water at 50℃; for 3h; Suzuki reaction; | 100% |
With bis-triphenylphosphine-palladium(II) chloride; sodium carbonate In water; acetonitrile at 80℃; for 3h; Suzuki Coupling; |
4-(benzoyloxy)morpholine
o-nitroiodobenzene
N-(2-nitrophenyl)morpholine
Conditions | Yield |
---|---|
Stage #1: o-nitroiodobenzene With isopropylmagnesium bromide In tetrahydrofuran at -35℃; for 0.166667h; Stage #2: With zinc(II) chloride In tetrahydrofuran at -35℃; for 0.166667h; Stage #3: 4-(benzoyloxy)morpholine With copper (I) trifluoromethane sulfonate benzene In tetrahydrofuran at 20℃; for 1h; | 100% |
Stage #1: o-nitroiodobenzene With phenylmagnesium bromide In tetrahydrofuran at -35℃; for 0.166667h; Stage #2: With zinc(II) chloride In tetrahydrofuran at -35℃; for 0.166667h; Stage #3: 4-(benzoyloxy)morpholine; copper (I) trifluoromethane sulfonate benzene In tetrahydrofuran at 25℃; for 1h; |
o-nitroiodobenzene
hexamethyldistannane
trimethyl-(2-nitro-phenyl)-stannane
Conditions | Yield |
---|---|
dichloro bis(acetonitrile) palladium(II) In N,N-dimethyl-formamide byproducts: (CH3)3SnI; Me6Sn2, o-NO2C6H4I dissolved in DMF in a flask, catalyst added with stirring, reacted for 5 min at 20°C; water added, extracted with ether, extracts filtered, washed with water, dried with Na2SO4, chromy.(silica gel, hexane/ether 2:1); | 100% |
tetrakis(triphenylphosphine) palladium(0) | 66% |
Conditions | Yield |
---|---|
With hydrogenchloride; iron In water; N,N-dimethyl-formamide for 2h; Reflux; | 99.2% |
With sodium tetrahydroborate; cyclohexanediamine-Pd-β-cyclodextrin In water at 20℃; for 3h; Sealed tube; | 98% |
With hexacarbonyl molybdenum In ethanol for 24h; Heating; | 96% |
Conditions | Yield |
---|---|
With tetrabutyl-ammonium chloride; palladium diacetate; sodium hydrogencarbonate In N,N-dimethyl-formamide at 50℃; for 7h; | 99% |
o-nitroiodobenzene
trimethylsilylacetylene
trimethyl((2-nitrophenyl)ethynyl)silane
Conditions | Yield |
---|---|
With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; triethylamine In tetrahydrofuran Sonogashira Cross-Coupling; Inert atmosphere; | 99% |
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine In N,N-dimethyl-formamide at 50℃; for 2h; Sonogashira reaction; | 94% |
With copper(l) iodide; triethylamine In N,N-dimethyl-formamide at 50℃; for 6h; Sonogashira coupling; | 91% |
pent-1-yn-5-ol
o-nitroiodobenzene
2-(5-hydroxy-1-pentynyl)nitrobenzene
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; Sonogashira coupling; | 99% |
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; for 14h; Sonogashira coupling; | 92% |
With copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride at 25℃; for 16h; Sonogashira cross-coupling; | 91% |
Stage #1: pent-1-yn-5-ol; o-nitroiodobenzene With bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine In N,N-dimethyl-formamide for 0.5h; Sonogashira coupling; Inert atmosphere; Stage #2: With copper(l) iodide In N,N-dimethyl-formamide at 20℃; for 5.16667h; Sonogashira coupling; Inert atmosphere; | 83% |
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; Sonogashira coupling; | 99% |
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; for 13h; Sonogashira coupling; | 99% |
Stage #1: 5-hexyl-1-ol; o-nitroiodobenzene With bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine In N,N-dimethyl-formamide for 0.5h; Sonogashira coupling; Inert atmosphere; Stage #2: With copper(l) iodide In N,N-dimethyl-formamide at 20℃; for 5.16667h; Sonogashira coupling; Inert atmosphere; | 71% |
o-nitroiodobenzene
p-Chlorothiophenol
4-chlorophenyl 2-nitrophenyl sulfide
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline In butan-1-ol at 120℃; for 2h; Microwave irradiation; | 99% |
With potassium hydroxide; copper(l) iodide; sarcosine In 1,4-dioxane at 100℃; for 24h; | 33% |
Conditions | Yield |
---|---|
With potassium carbonate; palladium diacetate In methanol; water at 20℃; for 1.5h; Suzuki cross-coupling; | 99% |
With potassium phosphate In water; N,N-dimethyl-formamide at 100℃; for 0.5h; Suzuki-Miyaura reaction; | 99% |
With potassium phosphate; tetrakis(triphenylphosphine) palladium(0) In ethanol for 6h; Reflux; Inert atmosphere; | 99% |
o-nitroiodobenzene
2-Methylphenylboronic acid
2-methyl-2'-nitro-1,1'-biphenyl
Conditions | Yield |
---|---|
With potassium carbonate; palladium diacetate In methanol; water at 50℃; for 24h; Suzuki cross-coupling; | 99% |
With C43H54N2S; palladium diacetate; potassium carbonate In water; isopropyl alcohol at 100℃; for 11h; Suzuki-Miyaura coupling reaction; Aerobic condition; Sealed tube; | 96% |
1-cyano-2-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)naphthalene
o-nitroiodobenzene
Conditions | Yield |
---|---|
With potassium carbonate; tetrakis(triphenylphosphine) palladium(0) In ethanol; toluene at 100℃; for 6h; | 99% |
Conditions | Yield |
---|---|
With sodium phenoxide; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; tris(dibenzylideneacetone)dipalladium (0) In 1,4-dioxane at 80℃; for 2h; | 99% |
o-nitroiodobenzene
4-methoxyphenylacetylen
1-(4-methoxyphenyl)-2-(2-nitrophenyl)acetylene
Conditions | Yield |
---|---|
With tetrakis(acetonitrile)copper(I) perchlorate; 2,5-bis(2-(diphenylphosphino)5-methoxyphenyl)-1,3,4-oxadiazole; potassium carbonate In 1,4-dioxane Catalytic behavior; Reagent/catalyst; Sonogashira Cross-Coupling; Reflux; Inert atmosphere; Schlenk technique; | 99% |
With potassium phosphate In water; isopropyl alcohol at 80℃; for 20h; Sonogashira Cross-Coupling; Sealed tube; | 85% |
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine In N,N-dimethyl-formamide at 20℃; for 6h; Sonogashira coupling; Inert atmosphere; | 78% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 25℃; for 4h; Inert atmosphere; | 99% |
With potassium carbonate In N,N-dimethyl-formamide at 152℃; for 18h; | 87% |
With 8-Hydroxyquinoline-N-oxide; caesium carbonate; copper(I) bromide In dimethyl sulfoxide at 65℃; for 60h; Ullmann coupling; Inert atmosphere; chemoselective reaction; | 84% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 25℃; for 1h; Inert atmosphere; | 99% |
With 2Na(1+)*CuC6H4(NCHC6H3OO3S)2(2-)=CuC6H4(NCHC6H3ONaO3S)2; sodium hydroxide In water at 120℃; for 15h; | 90% |
With rac-BINAP; palladium diacetate; caesium carbonate In toluene at 115℃; for 18h; Inert atmosphere; | 80% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 25℃; for 2h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 25℃; for 2h; Inert atmosphere; | 99% |
o-nitroiodobenzene
4-methoxyphenylboronic acid
4'-methoxy-2-nitrobiphenyl
Conditions | Yield |
---|---|
With potassium carbonate In ethanol at 80℃; for 0.5h; Catalytic behavior; Reagent/catalyst; Suzuki-Miyaura Coupling; | 99% |
With C43H54N2S; palladium diacetate; potassium carbonate In water; isopropyl alcohol at 100℃; for 6h; Suzuki-Miyaura coupling reaction; Aerobic condition; Sealed tube; | 94% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,2-dimethoxyethane; water for 18h; Inert atmosphere; Reflux; | 88% |
(4-Nitrophenyl)acetylene
o-nitroiodobenzene
2,4'-dinitrophenylacetylene
Conditions | Yield |
---|---|
With tetrakis(acetonitrile)copper(I) perchlorate; 2,5-bis(2-(diphenylphosphino)5-methoxyphenyl)-1,3,4-oxadiazole; potassium carbonate In 1,4-dioxane Catalytic behavior; Reagent/catalyst; Sonogashira Cross-Coupling; Reflux; Inert atmosphere; Schlenk technique; | 99% |
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine In N,N-dimethyl-formamide at 20℃; for 6h; Sonogashira coupling; Inert atmosphere; | 65% |
4-Methoxybenzenethiol
o-nitroiodobenzene
4-methoxyphenyl-2-nitrophenylsulfide
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline In butan-1-ol at 120℃; for 2h; Microwave irradiation; | 99% |
2,4-dichlorobenzenethiol
o-nitroiodobenzene
2,4-dichlorophenyl 2-nitrophenyl sulfide
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline In butan-1-ol at 120℃; for 2h; Microwave irradiation; | 99% |
o-nitroiodobenzene
4-Chlorophenylboronic acid
4'-chloro-2-nitrobiphenyl
Conditions | Yield |
---|---|
With sodium methylate In 1,4-dioxane at 100℃; for 25h; Suzuki-Miyaura Coupling; Schlenk technique; | 99% |
With C30H24N3OPPd; potassium carbonate In tetrahydrofuran; N,N-dimethyl-formamide for 1h; Suzuki Coupling; Reflux; | 80% |
With sodium methylate In 1,4-dioxane at 100℃; for 24h; Inert atmosphere; |
o-nitroiodobenzene
isobutyraldehyde
(R/S)-1-(2-nitrophenyl)-2-methyl-1-propanol
Conditions | Yield |
---|---|
Stage #1: o-nitroiodobenzene With phenylmagnesium chloride In tetrahydrofuran at -40℃; for 0.0833333h; Inert atmosphere; Stage #2: isobutyraldehyde In tetrahydrofuran at 20℃; | 99% |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate In water; N,N-dimethyl-formamide at 150℃; for 0.25h; Suzuki-Miyaura Coupling; Microwave irradiation; | 99% |
With tetrakis(triphenylphosphine) palladium(0) In water; N,N-dimethyl-formamide at 90℃; for 12h; | 88.6% |
With tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate In water; N,N-dimethyl-formamide | |
With tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate In water; N,N-dimethyl-formamide for 12h; Reflux; |
2-(2-amino-4-methoxyphenyl)propan-2-ol
o-nitroiodobenzene
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; SPhos Pd G2; caesium carbonate In toluene for 18h; Reflux; | 99% |
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