Simagchem Corporation
Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:121-69-7
Min.Order:0 Metric Ton
Negotiable
Type:Manufacturers
inquiryHebei yanxi chemical co.,LTD.
hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
Cas:121-69-7
Min.Order:1 Metric Ton
FOB Price: $1.0 / 3.0
Type:Manufacturers
inquiryWuhan Fortuna Chemical Co.,Ltd
Unique advantages for N,N-Dimethylaniline CAS 121-69-7 Guaranteed the purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Liquid Storage:0-6°C Package:180kg/drum Application:Intermediate Transpo
Cas:121-69-7
Min.Order:1 Kilogram
FOB Price: $1.0 / 60.0
Type:Trading Company
inquiryHefei TNJ chemical industry co.,ltd
1, Full experience of large numbers containers loading in main Chinese seaports 2, Packing with pallet as buyer's special request 3, Best service after shipment with e-mail 4, Cargoes together with container sales service available 5, R
Cas:121-69-7
Min.Order:1 Metric Ton
Negotiable
Type:Trading Company
inquiryAlity Chemical Corporation
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Dayang Chem (Hangzhou) Co.,Ltd.
Dayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantiti
Chemwill Asia Co., Ltd.
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:121-69-7
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryLIDE PHARMACEUTICALS LIMITED
Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:121-69-7
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHenan Tianfu Chemical Co., Ltd.
N,N-Dimethylaniline Basic information Product Name: N,N-Dimethylaniline Synonyms: Aniline, N,N-dimethyl-;Benzenamine,N,N-dimethyl-;Dimethylanilin;Dimethylaniline,N-N-dimethylphenylamine;
Cas:121-69-7
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryJinan Finer Chemical Co., Ltd
Product Description Product name N,N-Dimethylaniline CAS 121-69-7 Assay 99% Appearance Light Yellow Liq
Cas:121-69-7
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHubei Langyou International Trading Co., Ltd
1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:liquid Storage:Store in sealed containers at cool & dry pla
Cas:121-69-7
Min.Order:100 Gram
Negotiable
Type:Other
inquiryBaoji Guokang Healthchem co.,ltd
Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:121-69-7
Min.Order:1 Kilogram
FOB Price: $4.0 / 5.0
Type:Trading Company
inquiryChangchun Artel lmport and Export trade company
Price, service, company and transport advantage: 1.place of origin china with super quality by reasonable price. 2.fast delivery by safe express way to all the country. 3.has a number of highly qualified engineers and experts to p
Cas:121-69-7
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryHangzhou Keyingchem Co.,Ltd
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:121-69-7
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryHangzhou J&H Chemical Co., Ltd.
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:121-69-7
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryHangzhou Lingrui Chemical Co.,Ltd.
Factory supply N,N-Dimethylaniline CAS 121-69-7 with favorable priceAppearance:Yellow oily liquid Storage:0-6°C Package:according to customers' requirements Application:Pharmaceutical Intermediates Transportation:By air(EMS or EUB or FedEx or TNT ect
Cas:121-69-7
Min.Order:1 Gram
Negotiable
Type:Other
inquirySiwei Development Group Ltd.
Product name: N,N-Dimethyl Aniline CAS No.：121-69-7 Molecule Formula：C8H12N Molecule Weight：122.19 Purity: 99.0% Package: 190kg/drum Description：Colorless to light yellow oily liquid Manufacture Standards：Enterprise Standard
Cas:121-69-7
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryZibo Dorne chemical technology co. LTD
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:121-69-7
Min.Order:1 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryAntimex Chemical Limied
ProName: N,N-Dimethylaniline CasNo: 121-69-7 Molecular Formula: C8H11N Appearance: colorless to light yellow oily liquid Application: It is an important raw material and in... DeliveryTime: prompt PackAge: according to th
Cas:121-69-7
Min.Order:1 Metric Ton
FOB Price: $3.6
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co., Ltd.
We are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
Cas:121-69-7
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryHangzhou Fandachem Co.,Ltd
Hangzhou Fanda Chemical Co.,Ltd (FandaChem) , a China-based chemical company, specialize in exporting N,N-Dimethylaniline;PERGAQUICK A200 CAS: 121-69-7 , Please contact us by email freely. We are leading exporter in China. If you real
Cas:121-69-7
Min.Order:1 Metric Ton
Negotiable
Type:Other
inquiryHangzhou Zhongqi chem Co.,Ltd.
Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service an
Hunan chemfish Pharmaceutical co.,Ltd
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
HANGZHOU YUNUO CHEMICAL CO.,LTD
Superior quality, moderate price & quick delivery. Appearance:A yellow to brown colored oily liquid Storage:stored in a cool, dry and ventilated place to provent sun and rain Package:25kg/drum, or as per your request. Application:Used in or
Kono Chem Co.,Ltd
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
GIHI CHEMICALS CO.,LIMITED
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
JINHUA HUAYI CHEMICAL CO., LTD.
Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Cas:121-69-7
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou Dingyan Chem Co., Ltd
R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates
Henan Allgreen Chemical Co.,Ltd
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Synthetic route
| Conditions | Yield |
|---|---|
| With 4-methyl-morpholine; tetrahydroxydiboron; 5%-palladium/activated carbon In 1,2-dichloro-ethane at 50℃; for 3h; | 100% |
| With lithium aluminium tetrahydride; di-tert-butyl peroxide In tetrahydrofuran for 3h; Irradiation; | 93% |
| With isopropyl alcohol at 20℃; for 24h; UV-irradiation; chemoselective reaction; | 82% |
| Conditions | Yield |
|---|---|
| With 9-borabicyclo[3.3.1]nonane dimer; proazaphosphatrane In tetrahydrofuran-d8 at 90℃; under 750.075 Torr; for 0.166667h; Catalytic behavior; Time; Inert atmosphere; Schlenk technique; Sealed tube; chemoselective reaction; | 100% |
| With [Ru(Triphos)(TMM)]; hydrogen; bis(trifluoromethanesulfonyl)amide In tetrahydrofuran at 150℃; under 60006 Torr; for 10h; Temperature; Time; Reagent/catalyst; Pressure; Inert atmosphere; | 99% |
| With phenylsilane; triphenylphosphine In tetrahydrofuran at 120℃; under 3750.38 Torr; for 24h; Catalytic behavior; Reagent/catalyst; Autoclave; Green chemistry; | 99% |
-
-
171364-78-6
(4-(N,N-dimethylamino)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
-
-
121-69-7
N,N-dimethyl-aniline
| Conditions | Yield |
|---|---|
| With water In dimethylsulfoxide-d6 at 100℃; for 96h; | 100% |
-
-
121-69-7
N,N-dimethyl-aniline
| Conditions | Yield |
|---|---|
| With water In dimethylsulfoxide-d6 at 100℃; for 168h; | 100% |
-
-
124-38-9
carbon dioxide
-
-
1145-27-3
N,N’-dimethyl-N,N’-diphenylmethanediamine
-
-
121-69-7
N,N-dimethyl-aniline
| Conditions | Yield |
|---|---|
| With potassium tungstate; phenylsilane In acetonitrile at 70℃; for 12h; | 100% |
| Conditions | Yield |
|---|---|
| With ferric(III) bromide; 1,2,3,4,5-pentamethylcyclopentadiene; Pyroglutamic acid In 1,2,4-Trimethylbenzene at 200℃; for 36h; Inert atmosphere; | 99% |
| With tetrachloromethane; copper(ll) bromide at 180℃; for 6h; Reagent/catalyst; Temperature; Inert atmosphere; Sealed tube; | 99% |
| With 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine In 1,2,4-Trimethylbenzene at 200℃; for 36h; Inert atmosphere; | 97% |
| Conditions | Yield |
|---|---|
| With tris(pentafluorophenyl)borate In dibutyl ether at 100℃; for 8h; Inert atmosphere; Schlenk technique; | 99% |
| With platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; 1,3-bis-(diphenylphosphino)propane; phenylsilane In dibutyl ether at 20℃; for 18h; Schlenk technique; Inert atmosphere; | 98% |
| With tetrabutyl ammonium fluoride; HSiPh3 In acetonitrile at 50℃; | 95% |
-
-
98-04-4
phenyltrimethylammonium iodide
-
-
93296-10-7
(4-(dimethylamino)phenyl)zinc(II) chloride
-
A
-
1137-79-7
N,N-dimethyl-4-biphenylamine
-
B
-
121-69-7
N,N-dimethyl-aniline
| Conditions | Yield |
|---|---|
| With bis(tricyclohexylphosphine)nickel(II) dichloride In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 90℃; for 8h; Negishi coupling reaction; Inert atmosphere; | A 99% B n/a |
| Conditions | Yield |
|---|---|
| With NHC-Pd(II)-Im; potassium tert-butylate at 20℃; for 6h; Inert atmosphere; | 99% |
| With bis(1,5-cyclooctadiene)nickel (0); 7,9-bis(2,6-diisopropylphenyl)-7H-acenaphtho[1,2-d]imidazol-9-ium chloride; potassium tert-butylate In water; toluene at 35℃; for 24h; Catalytic behavior; Reagent/catalyst; Glovebox; Sealed tube; Inert atmosphere; | 99 %Chromat. |
| Conditions | Yield |
|---|---|
| With C27H36Cl2N2Zn at 100℃; for 20h; | 99% |
| Conditions | Yield |
|---|---|
| With phenylsilane In dibutyl ether at 100℃; for 8h; Catalytic behavior; Solvent; Reagent/catalyst; Inert atmosphere; Schlenk technique; | 99% |
| With phenylsilane; copper diacetate In dibutyl ether at 80℃; for 8h; Catalytic behavior; Reagent/catalyst; Schlenk technique; Green chemistry; | 97% |
| With copper (II) carbonate hydroxide; phenylsilane; 1,4-di(diphenylphosphino)-butane In acetonitrile at 60℃; for 12h; | 74% |
| Conditions | Yield |
|---|---|
| With phenylsilane; triphenylphosphine In tetrahydrofuran at 120℃; under 3750.38 Torr; for 24h; Autoclave; Green chemistry; | 99% |
-
-
124-38-9
carbon dioxide
-
-
1145-27-3
N,N’-dimethyl-N,N’-diphenylmethanediamine
-
A
-
121-69-7
N,N-dimethyl-aniline
-
B
-
100-61-8
N-methylaniline
| Conditions | Yield |
|---|---|
| With diphenylsilane; cesium formate In acetonitrile at 50℃; under 750.075 Torr; Green chemistry; | A 99% B n/a |
| Conditions | Yield |
|---|---|
| With phenylboronic acid In dichloromethane at 20℃; for 0.0833333h; | 98% |
| With AFA In dichloromethane at 0 - 21℃; | 97% |
| With Amberlite IRA-400; borohydride form; copper(II) sulfate In methanol at 20℃; for 1h; Reduction; | 94% |
| Conditions | Yield |
|---|---|
| palladium at 120℃; for 20h; | A 98% B 98% |
| Conditions | Yield |
|---|---|
| With Raney-Ni at 169.84℃; under 22502.3 Torr; for 5h; Inert atmosphere; Autoclave; | 98% |
| With aluminum (III) chloride; water In acetonitrile at 20℃; Reagent/catalyst; Irradiation; | 88% |
| With TiO2 supported nano-Pd(0.8) catalyst In water at 20℃; for 15h; Inert atmosphere; Irradiation; Green chemistry; | 76 %Chromat. |
| With palladium 10% on activated carbon; potassium tert-butylate at 150℃; for 36h; |
| Conditions | Yield |
|---|---|
| With sodium carbonate In water; dimethyl sulfoxide at 130℃; for 15h; Schlenk technique; Sealed tube; Green chemistry; | 98% |
| With methanol; hydrogen at 79.84℃; under 9750.98 Torr; for 1.41667h; Autoclave; |
| Conditions | Yield |
|---|---|
| With disodium telluride In ethanol Heating; | 97% |
| With hydrogenchloride bei der Destillation; | |
| With potassium hydroxide | |
| Multi-step reaction with 2 steps 1: silver oxide 2: Erhitzen View Scheme |
-
-
110698-86-7
benzyl<2-(N,N-dimethylamino)phenyl>diphenylphosphonium bromide
-
A
-
2959-74-2
benzyldiphenylphosphine oxide
-
B
-
121-69-7
N,N-dimethyl-aniline
-
C
-
71-43-2
benzene
| Conditions | Yield |
|---|---|
| With potassium hydroxide In 1,4-dioxane; water at 37.7℃; relative rate constant; other o- and p-substituted phenyl phosphomium salts; other temperature; | A 96% B 96.5% C 3.5% |
| Conditions | Yield |
|---|---|
| With copper(l) iodide; 6,7-dihydro-5H-quinolin-8-one oxime; potassium hydroxide In water at 85℃; for 24h; Inert atmosphere; | 95% |
| With potassium hydroxide In N,N-dimethyl-formamide at 110℃; for 18h; Buchwald-Hartwig Coupling; | 73% |
| at 250 - 260℃; |
| Conditions | Yield |
|---|---|
| With potassium tert-butylate; N,N-dimethyl-formamide at 35℃; for 24h; Schlenk technique; Inert atmosphere; Irradiation; | 95% |
| With allyl-trimethyl-silane In cyclohexane Quantum yield; Further Variations:; Solvents; UV-irradiation; | |
| With [hmim][ClO4] for 16h; Irradiation; | 78 % Chromat. |
| In isopropyl alcohol for 4h; Irradiation; Inert atmosphere; | 99 %Chromat. |
| With triethanolamine; water In ethanol for 24h; Irradiation; Glovebox; | 90 %Chromat. |
| Conditions | Yield |
|---|---|
| With hydrogen In toluene at 140℃; under 30003 Torr; for 3h; chemoselective reaction; | 95% |
| With tetrakis(triphenylphosphine)platinum; phenylsilane; C30H51Cl3Mo3N6PPtS4(1+)*BF4(1-) In tetrahydrofuran at 70℃; under 760.051 Torr; Inert atmosphere; Schlenk technique; chemoselective reaction; | 91% |
| Conditions | Yield |
|---|---|
| With N-methylpyrrolidine zinc borohydride; sulfuric acid In tetrahydrofuran; water at 0 - 10℃; | 94% |
| With sodium cyanoborohydride for 2h; | 92% |
| With acetic acid; zinc In 1,4-dioxane at 30℃; for 0.5h; | 92% |
-
-
23145-45-1
(benzyl)di(methyl)(phenyl)ammonium bromide
-
-
121-69-7
N,N-dimethyl-aniline
| Conditions | Yield |
|---|---|
| With sodium hydrogen telluride In N,N-dimethyl-formamide at 40℃; for 4h; | 94% |
| With sodium hydrogen telluride In N,N-dimethyl-formamide at 40℃; for 4h; Mechanism; other phase transfer catalysts; |
-
A
-
13453-37-7
thallium(III) iodide
-
B
-
2923-17-3
lithium trifluoroacetate
-
C
-
121-69-7
N,N-dimethyl-aniline
| Conditions | Yield |
|---|---|
| In acetone -70°C, several hours, warming to room temp.; redn. of vol. (distn., vac., room temp.), pptn. on addn. of water, crystn. (overnight), dissolving (acetone), pptn. on pentane addn., crystn. (several days); | A 94% B n/a C n/a |
| Conditions | Yield |
|---|---|
| With [Ru(Triphos)(TMM)]; hydrogen; bis(trifluoromethanesulfonyl)amide In tetrahydrofuran at 150℃; under 60006 Torr; for 15h; Inert atmosphere; | 94% |
| With [RhCl{κ3-P,C,P′=C(NCH2PCy2)2C10H6}]; phenylsilane In toluene at 90℃; for 16h; Schlenk technique; | 93% |
| With hydrogen In hexane at 140℃; under 15001.5 - 60006 Torr; for 7h; Inert atmosphere; Autoclave; | 92% |
-
-
124-38-9
carbon dioxide
-
-
100-61-8
N-methylaniline
-
A
-
121-69-7
N,N-dimethyl-aniline
-
B
-
93-61-8
N-methyl-N-phenylformamide
| Conditions | Yield |
|---|---|
| With phenylsilane In N,N-dimethyl acetamide at 60℃; for 4h; Time; Sealed tube; | A 94% B 8% |
| With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 110℃; under 760.051 Torr; for 48h; Mechanism; Solvent; Reagent/catalyst; Schlenk technique; | A 92% B 8% |
| With phenylsilane; C23H23O2P In acetonitrile at 100℃; under 15001.5 Torr; for 24h; | A 8% B 91% |
-
-
28611-39-4
4-(dimethylamino)benzene-boronic acid
-
-
121-69-7
N,N-dimethyl-aniline
| Conditions | Yield |
|---|---|
| With water In dimethyl sulfoxide at 100℃; for 2h; Reagent/catalyst; Solvent; Enzymatic reaction; | 94% |
| Multi-step reaction with 2 steps 1: dimethyl sulfoxide / toluene / 0.5 h / 120 °C / Dean-Stark 2: water / dimethylsulfoxide-d6 / 168 h / 100 °C View Scheme | |
| Multi-step reaction with 2 steps 1: N,N-dimethyl-formamide / 1 h / 120 °C / Molecular sieve; Inert atmosphere 2: water / dimethylsulfoxide-d6 / 168 h / 100 °C View Scheme | |
| Multi-step reaction with 2 steps 1: toluene / 1 h / 20 °C / Inert atmosphere 2: water / dimethylsulfoxide-d6 / 96 h / 100 °C View Scheme |
| Conditions | Yield |
|---|---|
| With sodium tetrahydroborate In 2,2,2-trifluoroethanol for 1.1h; Reflux; | 93% |
| Stage #1: formaldehyd; N-methylaniline With hydrogenchloride In methanol at 20℃; Stage #2: With N-methylpiperidine zinc borohydride In methanol at 20℃; for 0.25h; | 88% |
| With N-methylpyrrolidine zinc borohydride; sulfuric acid In tetrahydrofuran; water at 0 - 10℃; for 0.333333h; | 88% |
| Conditions | Yield |
|---|---|
| With 4a-FlEt-OOH In 1,4-dioxane at 30℃; Rate constant; | 100% |
| With oxygen; ruthenium trichloride In 1,2-dichloro-ethane at 20℃; under 760 Torr; for 8h; | 98% |
| With dihydrogen peroxide In acetonitrile at 80℃; under 760.051 Torr; for 4h; | 98% |
| Conditions | Yield |
|---|---|
| With bis(trimethylsilyl)sulphate at 170℃; for 5h; | 100% |
| Stage #1: N,N-dimethyl-aniline With bis(trimethylsilyl)sulphate at 170℃; for 4h; Stage #2: With water | 96% |
| With bis(trimethylsilyl)sulphate at 170℃; for 4h; | 85% |
| Conditions | Yield |
|---|---|
| With bismuth(III) nitrate; sulfuric acid; silica gel at 25℃; for 0.0333333h; | 100% |
| With sodium nitrate In neat (no solvent) at 20℃; for 0.05h; Green chemistry; | 98% |
| With 2-chloro-1-methyl-pyridinium iodide; water; silica gel; sodium nitrite In hexane at 20℃; for 0.75h; regioselective reaction; | 85% |
| Conditions | Yield |
|---|---|
| In methanol for 2h; Ambient temperature; | 100% |
-
-
129075-92-9
(4-Benzotriazol-1-ylmethyl-phenyl)-diethyl-amine
-
-
121-69-7
N,N-dimethyl-aniline
-
-
129075-94-1
C19H26N2
| Conditions | Yield |
|---|---|
| In acetic acid for 3h; Heating; | 100% |
-
-
98-88-4
benzoyl chloride
-
-
121-69-7
N,N-dimethyl-aniline
-
-
4931-66-2, 54571-66-3, 64700-65-8
methyl 5-oxopyrrolidine-2-carboxylate
-
-
1934-92-5
N-methyl-N-phenyl-benzamide
| Conditions | Yield |
|---|---|
| Product distribution; | 100% |
-
-
121-69-7
N,N-dimethyl-aniline
-
-
515145-68-3
bis(2-amino-4-nitrophenyl) ether
| Conditions | Yield |
|---|---|
| Stage #1: bis(2-amino-4-nitrophenyl) ether With hydrogenchloride; sodium nitrite at 0 - 5℃; for 1h; Stage #2: N,N-dimethyl-aniline With hydrogenchloride In acetate buffer pH=5; | 100% |
| Conditions | Yield |
|---|---|
| In benzene at 23℃; for 48h; | 100% |
| Conditions | Yield |
|---|---|
| In toluene Product distribution / selectivity; | 100% |
| In neat (no solvent) addn. of diborane to amine at liquid N2 temp., keeping at -111°C, -78°C and 0°C consecutively, stirring at 0°C for 4-6 h (vacuum line); cooling to -78°C, removal of B2H6 by distn.; | |
| In neat (no solvent) at 0°C;; | |
| In neat (no solvent) at room temp.;; |
-
-
113860-02-9
[Cp*Ru(CH3CN)3]OTf
-
-
121-69-7
N,N-dimethyl-aniline
| Conditions | Yield |
|---|---|
| In tetrahydrofuran byproducts: CH3CN; under N2; addn. of Ru-complex to N,N-dimethylaniline and THF (benzene-free), mixt. stirred (30°C); addn. of hexane, solid filtered, washed twice (hexane), dried (vac.), elem. anal.; | 100% |
-
-
258519-28-7
[((CH3)3CC(NC(CH3)3)2)GaCH3](1+)*[B(C6F5)4](1-)=[((CH3)3CC(NC(CH3)3)2)GaCH3][B(C6F5)4]
-
-
121-69-7
N,N-dimethyl-aniline
-
-
258519-32-3
[((CH3)3CC(NC(CH3)3)2)Ga(CH3)(N(CH3)2C6H5)](1+)*[B(C6F5)4](1-)=[((CH3)3CC(NC(CH3)3)2)Ga(CH3)(N(CH3)2C6H5)][B(C6F5)4]
| Conditions | Yield |
|---|---|
| In further solvent(s) under N2; in C6D5Cl, 23°C, 10 min; not isolated; NMR; | 100% |
| Conditions | Yield |
|---|---|
| With C47H45Cl2N5Ru2(2+)*2F6P(1-); dihydrogen peroxide; acetic acid In methanol at 60℃; for 8h; Reagent/catalyst; Solvent; Temperature; Inert atmosphere; | 100% |
| With dihydrogen peroxide; acetic acid In water at 20℃; for 0.416667h; Reagent/catalyst; Solvent; | 98% |
| With C22H26N2O5U; dihydrogen peroxide; acetic acid In methanol at 20℃; for 8h; Catalytic behavior; Reagent/catalyst; Solvent; Irradiation; | 97% |
-
-
1493-13-6
trifluorormethanesulfonic acid
-
-
121-69-7
N,N-dimethyl-aniline
-
-
142279-32-1
N,N-dimethylphenylammonium trifluoromethanesulfonate
| Conditions | Yield |
|---|---|
| In hexane at 20℃; for 1h; | 100% |
-
-
121-69-7
N,N-dimethyl-aniline
-
-
33454-16-9
3-iodo-N,N-dimethylaniline
| Conditions | Yield |
|---|---|
| Stage #1: N,N-dimethyl-aniline With (TMEDA)Na(TMP)(t-Bu)Zn(t-Bu) In hexane at 20℃; Inert atmosphere; Stage #2: With iodine Inert atmosphere; | 100% |
-
-
121-69-7
N,N-dimethyl-aniline
-
-
199620-14-9, 13007-92-6
chromium(0) hexacarbonyl
-
-
124916-48-9, 14122-95-3, 12109-10-3
(N,N-dimethylaniline)tricarbonylchromium
| Conditions | Yield |
|---|---|
| In decalin byproducts: CO; 3.5:1 mixture of arene and Cr(CO)6 in solvent purged for 20 min with Ar, evacuated for 20 min, mixture refluxed, cooled to 20°C, cooled to -18°C under argon, reaction time 5.5 h; filtered off, dissolved in benzene, filtered through Kieselguhr, concentrated, light petroleum added, crystn. at -18°C, complexes eluted with benzene/ethyl acetate, elem. anal., NMR; | 99.5% |
| In neat (no solvent) boiling;; | 91% |
| In neat (no solvent) boiling;; | 91% |
| Conditions | Yield |
|---|---|
| With aluminum (III) chloride; sodium pyrophosphate; hydrazine hydrate; pyrographite; ammonium hydroxide; 1-butyl-3-methylimidazolium chloride; sodium hydroxide at 130℃; for 0.0222222h; Reagent/catalyst; Temperature; | 99.4% |
| With acetic acid; β-naphthol In ethanol at 20℃; for 12h; Mannich type Friedel-Crafts reaction; | 90% |
| With acetic acid In water | 82% |
-
-
121-69-7
N,N-dimethyl-aniline
-
A
-
14503-46-9
2-dimethylamino-benzenesulfonic acid
-
B
-
121-58-4
p-N,N-dimethylaminobenzenesulfonic acid
| Conditions | Yield |
|---|---|
| With chlorosulfonic acid In 1,2-dichloro-benzene at 50℃; for 1h; Product distribution; Kinetics; Mechanism; E(activ), oth. temperatures; | A 0.6% B 99.4% |
| With sulfur trioxide In 1,2-dichloro-ethane at 5℃; Rate constant; Thermodynamic data; Product distribution; oth. temperature, E(activ.), var. ratios of reactants; | |
| With sulfuric acid In 1,2-dichloro-benzene at 180℃; Kinetics; Thermodynamic data; Equilibrium constant; variation of molar ratio and temperature, Ea, ΔGo, ΔHo, ΔSo; | |
| With sulfuric acid In 1,2-dichloro-benzene at 24.9℃; Thermodynamic data; Mechanism; Activation Free Energy, Enthalpy, Entropy of sulfonation and desulfonation; |
-
-
121-69-7
N,N-dimethyl-aniline
-
-
1588-83-6
4-amino-3-nitrobenzoic acid
-
-
392300-99-1
4'-dimethylamino-2-nitroazobenzene-4-carboxylic acid
| Conditions | Yield |
|---|---|
| Stage #1: 4-amino-3-nitrobenzoic acid With hydrogenchloride; sodium nitrite In water; acetic acid at 15 - 20℃; for 0.25h; Stage #2: N,N-dimethyl-aniline In water; acetic acid at 0 - 5℃; | 99.4% |
-
-
670-54-2
ethenetetracarbonitrile
-
-
121-69-7
N,N-dimethyl-aniline
-
-
6673-15-0
2-(4-dimethylaminophenyl)ethylene-1,1,2-tricarbonitrile
| Conditions | Yield |
|---|---|
| In N,N-dimethyl-formamide at 20 - 25℃; for 0.0833333h; Sonication; | 99% |
| In N,N-dimethyl-formamide at 50 - 60℃; for 0.5h; | 95% |
| With choline chloride; urea at 35℃; for 0.0833333h; Reagent/catalyst; Solvent; Green chemistry; | 89% |
| With N,N-dimethyl-formamide | |
| In N,N-dimethyl-formamide |
-
-
556-56-9
allyl iodid
-
-
121-69-7
N,N-dimethyl-aniline
-
-
73680-59-8
N-allyl-N,N-dimethylbenzenaminium iodide
| Conditions | Yield |
|---|---|
| at 30℃; | 99% |
| Conditions | Yield |
|---|---|
| With methanol; tetraethylammonium chloride; bromine In dichloromethane at 35℃; other substituted anilines: regioselectivity of bromination; | 99% |
| With methanol; tetraethylammonium chloride; bromine In dichloromethane at 35℃; | 99% |
| With hexabromocyclopenta-1,3-diene; triethylamine In acetonitrile for 24h; Ambient temperature; | 99% |
| Conditions | Yield |
|---|---|
| With iodine at 30℃; for 12h; Green chemistry; | 99% |
| With tetrafluoroboric acid; [bis(pyridine)iodine]+ tetrafluoroborate In diethyl ether; dichloromethane for 0.1h; Ambient temperature; | 98% |
| With iodine In 1,4-dioxane; pyridine at 0 - 20℃; | 98% |
-
-
121-69-7
N,N-dimethyl-aniline
-
-
35462-54-5
N,N-Dimethylaniline hydroiodide
| Conditions | Yield |
|---|---|
| With hydrogen iodide In 1,4-dioxane; water at 0 - 20℃; for 12h; | 99% |
| With hydrogen iodide |
Related products
Raw Materials
Downstream Products
Hot Products
T,
NAbout|Contact|Cas|Product Name|Molecular|Country|Encyclopedia
Message|New Cas|MSDS|Service|Advertisement|CAS DataBase|Article Data|Manufacturers | Chemical Catalog
©2008 LookChem.com,License: ICP
NO.:Zhejiang16009103
complaints:service@lookchem.com Desktop View