Dayang Chem (Hangzhou) Co.,Ltd.
img heightAppearance:Light beige purple liquid Storage:Store in dry, dark and ventilated place. Package:according to the clients requirement Application:It is an important raw material and intermediate used in Organic Synthesis, Pharmaceuticals, Ag
Antimex Chemical Limied
ProName: o-Toluidine CasNo: 95-53-4 Molecular Formula: C7H9N Appearance: Light beige purple liquid Application: It is an important raw material and in... DeliveryTime: prompt PackAge: according to the clients requirement
Cas:95-53-4
Min.Order:1 Metric Ton
FOB Price: $2.0
Type:Lab/Research institutions
inquiryAecochem Corp.
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc. o-Toluidine Basic information Overview Toluidine Isomers Chemical and Physical Properties Synthesis Method Hazard Occasions Toxicity Transportation Storage
Cas:95-53-4
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
inquiryHangzhou Dingyan Chem Co., Ltd
Items Standard Result Appearance Light yellow to brown-red oily transparent liquid Light yellow, transparent liquid
Cas:95-53-4
Min.Order:1 Kilogram
FOB Price: $3.0 / 10.0
Type:Manufacturers
inquirySimagchem Corporation
Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Wuhan Fortuna Chemical Co.,Ltd
Unique advantages for o-Toluidine Cas 95-53-4 Guaranteed the purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Liquid Storage:2-8°C Package:1kg/foil bag, 25kg/drum or as you required
Cas:95-53-4
Min.Order:1 Kilogram
FOB Price: $55.0
Type:Trading Company
inquiryAlity Chemical Corporation
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Chemwill Asia Co., Ltd.
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Hebei yanxi chemical co.,LTD.
Hebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car
Henan Tianfu Chemical Co., Ltd.
Our company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:95-53-4
Min.Order:1 Kilogram
FOB Price: $1000.0
Type:Lab/Research institutions
inquiryHenan Sinotech Import&Export Corporation
CAS 95-53-4 Name o-Toluidine Appearance Light yellow liquid Application Used as intermediate of dye, pesticide, medicine and organic synthesi
Baoji Guokang Healthchem co.,ltd
Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:95-53-4
Min.Order:1 Kilogram
FOB Price: $12.0 / 20.0
Type:Trading Company
inquiryChangchun Artel lmport and Export trade company
Product Detail Minimum Order Qty. 10 Gram
Cas:95-53-4
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryHenan Wentao Chemical Product Co., Ltd.
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Hangzhou Keyingchem Co.,Ltd
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:95-53-4
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryHangzhou J&H Chemical Co., Ltd.
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:95-53-4
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryHangzhou Lingrui Chemical Co.,Ltd.
95-53-4Appearance:white powder Storage:keep cold Package:according to customers' requirements Application:Pharmaceutical intermediates 95-53-4 Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(FOB or CIF or CNF ect...)or according to
HANGZHOU YUNUO CHEMICAL CO.,LTD
Superior quality, moderate price & quick delivery. Appearance:Light beige purple liquid Storage:stored in a cool, dry and ventilated place to provent sun and rain Package:25kg/drum, or as per your request. Application:For medicine , pestici
Zibo Dorne chemical technology co. LTD
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:95-53-4
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou Huarong Pharm Co., Ltd.
Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
Hangzhou Zhongqi chem Co.,Ltd.
Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service an
Hunan chemfish Pharmaceutical co.,Ltd
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
SAGECHEM LIMITED
SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe
Beijing Greenchem Technology Co.,Ltd. ( Panjin Greenchem Technology Co.Ltd .)
Capability on chemical synthesis1. Beijing High-Tech Enterprises2. Strong R&D Team3. 8 years of experiences in R & D of high-tech Catalyst;4. 5000 production techniques, 69 items of national patents, and 360 kinds of products on sales;5. The producti
Kono Chem Co.,Ltd
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
GIHI CHEMICALS CO.,LIMITED
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
Henan Allgreen Chemical Co.,Ltd
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Jiangsu Glory Chemical Co., Ltd.
Ortho Toluidine (OT) M. F. C7H9N M. W. 107Appearance:Yellowish to brown red transparent oily liquid Package:In 200KGS net weight iron drum; 16MT per 20’FCL
Zhuozhou Wenxi import and Export Co., Ltd
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:95-53-4
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquirySynthetic route
| Conditions | Yield |
|---|---|
| With hydrogen; palladium In methanol at 25℃; under 2327.2 Torr; for 1.5h; | 100% |
| With hydrogen; Pd in AV-17-8-Pd In ethanol at 40℃; | 100% |
| With hydrogen; Pd in AV-17-8-Pd In ethanol at 40℃; under 760 Torr; Rate constant; | 100% |
-
-
31656-92-5
1-azido-2-methyl-benzene
-
-
95-53-4
o-toluidine
| Conditions | Yield |
|---|---|
| With aluminum oxide; sodium formate; potassium hydroxide In neat (no solvent) for 1h; Milling; | 100% |
| With hydrogen; MCM-silylamine Pd(II) In methanol at 20℃; for 1h; Reduction; | 94% |
| With zinc(II) tetrahydroborate In 1,2-dimethoxyethane for 3h; Ambient temperature; | 90% |
| Conditions | Yield |
|---|---|
| With dichloro(dimethylglyoxime)(dimethylglyoximato)cobalt(III); (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; triethylamine In acetonitrile at -78℃; for 24h; Reagent/catalyst; Sealed tube; Inert atmosphere; Irradiation; | 100% |
| Multi-step reaction with 2 steps 1: hydrogen; nickel / 300 - 330 °C 2: hydrogen; reduced nickel / 200 °C View Scheme |
-
-
17512-73-1
2-methylphenylhydroxamic acid
-
-
95-53-4
o-toluidine
| Conditions | Yield |
|---|---|
| With potassium carbonate In dimethyl sulfoxide at 90℃; for 2h; Lossen rearrangement; | 99% |
| With potassium carbonate In dimethyl sulfoxide at 90℃; for 2h; Lossen Rearrangement; | 99% |
| Stage #1: 2-methylphenylhydroxamic acid With acetic anhydride; potassium carbonate In dimethyl sulfoxide at 50℃; for 2h; Lossen Rearrangement; Stage #2: With hydrogenchloride In water; dimethyl sulfoxide at 0℃; | 71% |
| Stage #1: 2-methylphenylhydroxamic acid With potassium carbonate In dimethyl sulfoxide at 90℃; for 3h; Lossen Rearrangement; Stage #2: With hydrogenchloride In water; dimethyl sulfoxide at 20℃; for 0.0833333h; |
| Conditions | Yield |
|---|---|
| With copper(I) oxide; ammonium hydroxide In 1-methyl-pyrrolidin-2-one at 80℃; for 20h; | 96% |
| With ammonium hydroxide In water at 20℃; for 9h; Green chemistry; | 92% |
| With ammonium hydroxide; L-2-O-methyl-chiro-inositol; copper(II) acetate monohydrate In 1-methyl-pyrrolidin-2-one at 110℃; for 12h; | 88% |
| Conditions | Yield |
|---|---|
| With ammonium acetate; zinc In methanol at 20℃; for 0.05h; | 95% |
| With formic acid; zinc In methanol at 20℃; for 0.1h; | 94% |
| With ammonium formate; nickel In methanol at 20℃; for 0.1h; | 94% |
| Conditions | Yield |
|---|---|
| With nickel; hydrazinium monoformate In methanol for 0.1h; Heating; | 94% |
| Conditions | Yield |
|---|---|
| With potassium phosphate; C29H55FeNOP2; hydrogen In tetrahydrofuran at 110℃; under 15001.5 Torr; for 3h; Catalytic behavior; | A n/a B 94% |
| With C24H38Cl2N3PRu; potassium tert-butylate; hydrogen In isopropyl alcohol at 110℃; under 30402 Torr; for 30h; Autoclave; Glovebox; |
| Conditions | Yield |
|---|---|
| With formic acid; zinc In methanol at 20℃; for 0.2h; | A 93% B 92% |
| With zinc; hydrazinium monoformate In methanol for 0.2h; Heating; | A n/a B 92% |
| With ammonium formate; magnesium In methanol at 20℃; for 0.25h; | A n/a B 90% |
| Conditions | Yield |
|---|---|
| With ammonium hydroxide In water at 20℃; for 9h; Green chemistry; | 93% |
| With ammonium hydroxide; caesium carbonate In acetonitrile for 8h; Reflux; Green chemistry; | 90% |
| With lithium amide; (CyPF-t-Bu)PdCl2 In 1,2-dimethoxyethane at 80℃; for 24h; | 81% |
-
-
101665-25-2
2-(2-trimethylsilylethyhyl)-1,2,3,4-tetrahydro-2-naphtol
-
-
95-53-4
o-toluidine
| Conditions | Yield |
|---|---|
| With sulfuric acid; mercury(II) oxide In tetrahydrofuran for 31h; Ambient temperature; | 92% |
-
-
61594-49-8
bis-(4-amino-3-methyl-phenyl)-diazene
-
A
-
95-53-4
o-toluidine
-
B
-
95-70-5
2-methyl-p-phenylenediamine
| Conditions | Yield |
|---|---|
| With ammonium acetate; zinc In methanol at 20℃; for 0.0833333h; | A n/a B 92% |
-
-
16419-60-6
2-Methylphenylboronic acid
-
-
95-53-4
o-toluidine
| Conditions | Yield |
|---|---|
| With potassium carbonate; ammonium hydroxide In methanol at 60℃; for 14h; | 92% |
| With sodium hydroxide; hydroxylamine-O-sulfonic acid In acetonitrile at 20℃; for 16h; | 87% |
| With N-Bromosuccinimide; CYANAMID; bis-[(trifluoroacetoxy)iodo]benzene In acetonitrile at 20℃; for 1h; chemoselective reaction; | 86% |
-
-
74965-31-4
N-(tert-butoxycarbonyl)-o-toluidine
-
-
95-53-4
o-toluidine
| Conditions | Yield |
|---|---|
| With 3-butyl-l-methyl-1H-imidazol-3-iumtrifloroacetate In 1,4-dioxane; water at 70 - 72℃; for 1h; | 92% |
-
-
88-72-2
1-methyl-2-nitrobenzene
-
A
-
95-53-4
o-toluidine
-
B
-
956-31-0, 51284-68-5, 116723-89-8
N,N'-Di-o-tolyl-diazene N-oxide
| Conditions | Yield |
|---|---|
| With ammonium chloride; zinc In water at 80℃; for 24h; Catalytic behavior; Inert atmosphere; | A 5% B 91% |
| With copper(l) iodide; sodium methylate In methanol; 5,5-dimethyl-1,3-cyclohexadiene at 120℃; for 12h; Inert atmosphere; | A 15% B n/a |
| With sodium tetrahydroborate In water at 50℃; for 1h; Catalytic behavior; Reagent/catalyst; chemoselective reaction; |
| Conditions | Yield |
|---|---|
| With hydrogen; trans-Pdpy2Cl2 In ethanol at 30℃; for 6h; Product distribution; Mechanism; Kinetics; further reagent, further catalyst, further reaction times; induction period of the reduction; | A 3.5% B 90% |
| With isopropyl alcohol; sodium hydroxide at 80℃; for 65h; Schlenk technique; Inert atmosphere; Green chemistry; |
| Conditions | Yield |
|---|---|
| With 40% potassium fluoride/alumina at 85℃; for 0.0666667h; Microwave irradiation; Neat (no solvent); | 90% |
| With [RuCl2(2-(diphenylphosphino)-N-((6-((diphenylphosphino)methyl)pyridin-2-yl)methyl)ethan-1-amine)]; potassium tert-butylate; hydrogen In tetrahydrofuran at 100℃; under 37503.8 Torr; for 20h; Catalytic behavior; Autoclave; chemoselective reaction; | 77% |
| With 2-[3,5-bis(trifluoromethyl)phenyl]-5,5-dimethyl-1,3,2-dioxaborinane; scandium tris(trifluoromethanesulfonate) In butan-1-ol for 40h; Reflux; Inert atmosphere; Schlenk technique; | 80 %Chromat. |
| Conditions | Yield |
|---|---|
| With copper(l) iodide In water at 200℃; for 2h; Autoclave; | 90% |
-
-
88-72-2
1-methyl-2-nitrobenzene
-
-
110-13-4
2,5-hexanedione
-
A
-
32570-09-5
2,5-dimethyl-1-o-tolyl-1H-pyrrole
-
B
-
95-53-4
o-toluidine
| Conditions | Yield |
|---|---|
| With formic acid for 12h; Autoclave; Inert atmosphere; Green chemistry; | A 90% B 9.9% |
-
-
88-72-2
1-methyl-2-nitrobenzene
-
A
-
584-90-7
2,2'-dimethylazobenzene
-
B
-
95-53-4
o-toluidine
-
C
-
956-31-0, 51284-68-5, 116723-89-8
N,N'-Di-o-tolyl-diazene N-oxide
| Conditions | Yield |
|---|---|
| With hydrazine hydrate; nickel(II) nitrate; zinc In tert-butyl alcohol for 0.666667h; Heating; | A 2 % Chromat. B 20% C 89% |
| With hydrazine hydrate; nickel(II) nitrate; zinc In ethanol for 5h; Heating; | A 6% B 28% C 20 % Chromat. |
| Conditions | Yield |
|---|---|
| With sodium azide; trifluoroacetic acid In hexane at 40℃; for 4h; Sealed tube; | 89% |
| With sodium azide; methanesulfonic acid; trifluoroacetic acid In hexane at 40℃; for 12h; | 89% |
| Conditions | Yield |
|---|---|
| With C28H30Cl5N3Pd; ammonia; lithium isopropoxide; sodium t-butanolate In 1,4-dioxane at 100℃; for 2h; Inert atmosphere; Schlenk technique; | A n/a B 88% |
| With lithium amide; (CyPF-t-Bu)PdCl2 In 1,2-dimethoxyethane at 80℃; for 24h; | A n/a B 70% |
| Stage #1: 2-methylchlorobenzene With lithium amide; [(CyPF-tBu)PdCl2] In 1,2-dimethoxyethane at 80℃; for 24h; Sealed vial; Stage #2: With hydrogenchloride In 1,2-dimethoxyethane; water at 20℃; for 0.0833333h; Stage #3: With sodium hydrogencarbonate In 1,2-dimethoxyethane; water Product distribution / selectivity; | A n/a B 70% |
| Conditions | Yield |
|---|---|
| With hydrogen In toluene at 160℃; under 45004.5 Torr; for 15h; Catalytic behavior; Autoclave; | A 89 %Chromat. B 88% |
| Conditions | Yield |
|---|---|
| Stage #1: 2-methylphenyl bromide With ammonia; sodium t-butanolate; [(CyPF-tBu)PdCl2] In 1,2-dimethoxyethane at 90℃; under 4137.29 - 10343.2 Torr; for 24h; Stage #2: With hydrogenchloride In 1,2-dimethoxyethane; water at 20℃; for 0.0833333h; Stage #3: In 1,2-dimethoxyethane; water Product distribution / selectivity; | A n/a B 86% |
| Stage #1: 2-methylphenyl bromide With lithium amide; [(CyPF-tBu)PdCl2] In 1,2-dimethoxyethane at 80℃; for 24h; Sealed vial; Stage #2: With hydrogenchloride In 1,2-dimethoxyethane; water at 20℃; for 0.0833333h; Stage #3: With sodium hydrogencarbonate In 1,2-dimethoxyethane; water Product distribution / selectivity; | A n/a B 86% |
| With bis(tri-ortho-tolylphosphine)palladium(0); (R)-(-)-1-[(S)-2-(dicyclohexylphosphino)ferrocenyl]ethyl-di-tert-butylphosphine; ammonia; sodium t-butanolate In 1,4-dioxane at 100℃; for 12h; Inert atmosphere; | A n/a B 71% |
| With ((+/-)-binap)Ni[P(OPh)3]2; ammonia; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate In 1,4-dioxane at 120℃; for 18h; Sealed tube; | A n/a B 66% |
-
-
70965-50-3
1-Amino-4,6-diphenyl-1,2-dihydropyridine-2-thione
-
A
-
84900-99-2
5,7-Diphenyl-2-o-tolyl-[1,3,4]thiadiazolo[3,2-a]pyridin-4-ylium; chloride
-
B
-
95-53-4
o-toluidine
| Conditions | Yield |
|---|---|
| In 1,4-dioxane for 4h; Ambient temperature; | A 85% B n/a |
-
A
-
58201-22-2
[1,2-bis(diphenylphosphino)ethane]tricarbonylruthenium
-
C
-
95-53-4
o-toluidine
| Conditions | Yield |
|---|---|
| With carbon monoxide; MeOH In not given byproducts: CO2; 25°C, 3 days; | A 40% B 50% C 85% |
| With carbon monoxide; MeOH In not given byproducts: CO2; 65°C,4 h; | A 40% B 50% C 85% |
| Conditions | Yield |
|---|---|
| With ammonium sulfate; C39H45FeNNiP2; sodium t-butanolate In 2-methyltetrahydrofuran at 100℃; for 7h; Reagent/catalyst; Solvent; Inert atmosphere; Glovebox; Autoclave; | 84% |
| With copper(I) oxide; ammonium hydroxide In 1-methyl-pyrrolidin-2-one at 110℃; for 15h; Microwave irradiation; | 83% |
| With C46H71Cl3N2Pd; ammonia; sodium t-butanolate In 1,4-dioxane at 100℃; for 2h; Inert atmosphere; Schlenk technique; | 75% |
-
-
133390-40-6
2-(o-aminobenzyl)-4-phenyl-6-methyl-1,2,3,4-tetrahydroisoquinoline dihydrochloride
-
A
-
133390-41-7
6-Methyl-4-phenyl-1,2,3,4-tetrahydro-isoquinoline; hydrochloride
-
B
-
95-53-4
o-toluidine
| Conditions | Yield |
|---|---|
| With hydrogen; palladium on activated charcoal In methanol; diethyl ether at 50℃; for 5h; Product distribution; other tetrahydroisoquinolines, other reagents; var. solvent, var. times and temp.; | A 84% B n/a |
| Conditions | Yield |
|---|---|
| Stage #1: ortho-methylbenzoic acid With trifluorormethanesulfonic acid; trimethylsilylazide In chloroform at 90℃; for 0.0566667h; Schmidt Reaction; Flow reactor; Stage #2: With water In methanol; chloroform at 20℃; Schmidt Reaction; Flow reactor; | 83% |
| With thionyl chloride; hydroxylamine-O-sulfonic acid 1) 1h, reflux, 2) toluene, 4h, reflux; Yield given. Multistep reaction; | |
| Multi-step reaction with 3 steps 1: phosphorus pentachloride / 120 °C 3: sodium hypobromite; water / >5 / man erhitzt nach Zufuegen von starker Natronlauge erst auf 75grad, dann zum Kochen View Scheme | |
| Multi-step reaction with 2 steps 1.1: 1,1'-carbonyldiimidazole / dimethyl sulfoxide / 1 h / 20 °C / Inert atmosphere 1.2: 18 h / 20 °C / Inert atmosphere 2.1: potassium carbonate / dimethyl sulfoxide / 3 h / 90 °C 2.2: 0.08 h / 20 °C View Scheme |
-
-
98-03-3
thiophene-2-carbaldehyde
-
-
95-53-4
o-toluidine
-
-
18209-98-8
(E)-(thien-2-yl)-N-(o-tolyl)methanimine
| Conditions | Yield |
|---|---|
| In toluene at 20℃; Inert atmosphere; Schlenk technique; Molecular sieve; | 100% |
| Conditions | Yield |
|---|---|
| In hexane for 16h; Reflux; | 100% |
| Conditions | Yield |
|---|---|
| With aluminum oxide for 5h; Milling; | 100% |
| sodium hydrogen sulfate; silica gel at 52 - 54℃; for 0.0152778h; microwave irradiation; | 92% |
| With 4 A molecular sieve In benzene at 20℃; for 23h; | 76% |
| Conditions | Yield |
|---|---|
| In ethanol at 80℃; for 2h; Inert atmosphere; | 100% |
| In ethanol at 20℃; for 0.166667h; | 82% |
| In methanol for 5h; Reflux; | 78% |
-
-
124-63-0
methanesulfonyl chloride
-
-
95-53-4
o-toluidine
-
-
7022-17-5
2-methyl-N-methanesulfonyl benzenamine
| Conditions | Yield |
|---|---|
| With pyridine In dichloromethane at 0 - 20℃; for 1 - 1.25h; Product distribution / selectivity; | 100% |
| β‐cyclodextrin In water; acetone at 20℃; for 0.666667h; | 90% |
| With pyridine In dichloromethane at 20℃; for 3h; | 76% |
| Conditions | Yield |
|---|---|
| With pyridine In chloroform at 20℃; for 24h; | 100% |
| With sodium carbonate In water pH=9 - 10; | 99% |
| With potassium carbonate In dichloromethane; water at 0℃; for 1h; | 98% |
| Conditions | Yield |
|---|---|
| With pyridine In dichloromethane at 20℃; for 3h; | 100% |
| 86% | |
| With pyridine for 4h; Heating; | 81% |
| Conditions | Yield |
|---|---|
| In acetonitrile at 25℃; | 100% |
-
-
3507-26-4
2-chloro-6-methylbenzo[d]thiazole
-
-
95-53-4
o-toluidine
-
-
78073-02-6
2-o-tolylimino-6-methylbenzothiazoline
| Conditions | Yield |
|---|---|
| at 120 - 140℃; for 2h; | 100% |
-
-
24424-99-5
di-tert-butyl dicarbonate
-
-
95-53-4
o-toluidine
-
-
74965-31-4
N-(tert-butoxycarbonyl)-o-toluidine
| Conditions | Yield |
|---|---|
| copper(II) bis(tetrafluoroborate) at 30 - 33℃; for 0.5h; | 100% |
| With lanthanum(III) nitrate at 20℃; for 0.0333333h; | 100% |
| With sulfonic acid-functionalized ordered nanoporous Na+-montmorillonite at 20℃; for 0.25h; Neat (no solvent); | 97% |
-
-
95-53-4
o-toluidine
| Conditions | Yield |
|---|---|
| With acetic acid for 0.166667h; | 100% |
| Conditions | Yield |
|---|---|
| With triethylamine In 1,4-dioxane at 0℃; | 100% |
| With triethylamine at 20℃; Glovebox; | 100% |
| In tetrahydrofuran at 0 - 20℃; for 1h; | 98% |
-
-
59565-09-2
2-(vinyloxy)ethyl isothiocyanate
-
-
95-53-4
o-toluidine
| Conditions | Yield |
|---|---|
| at 40℃; | 100% |
| Conditions | Yield |
|---|---|
| Stage #1: Isovaleronitrile; o-toluidine With boron trichloride In toluene at 20℃; for 1h; Addition; Stage #2: With aluminium trichloride In acetonitrile for 5h; Rearrangement; Heating; Stage #3: With hydrogenchloride In acetonitrile for 2.5h; Hydrolysis; Heating; | 100% |
-
-
95-53-4
o-toluidine
| Conditions | Yield |
|---|---|
| Stage #1: trifluoromethyl dihydro-1,4-dioxin-3-carbonyl chloride With pyridine; polystyrene-bound 4-hydroxy-3-nitrobenzophenone In dichloromethane at 20℃; for 24h; Acylation; Stage #2: o-toluidine With triethylamine In acetonitrile for 5h; Acylation; Heating; | 100% |
| Conditions | Yield |
|---|---|
| With 18-crown-6 ether; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; palladium diacetate In tetrahydrofuran at 68℃; for 3h; | 100% |
| Conditions | Yield |
|---|---|
| With ammonium formate; palladium on activated charcoal In methanol; water at 20℃; | 100% |
-
-
5950-87-8
2,4-dinitrophenyl 2,4,6-trinitrophenyl ether
-
-
95-53-4
o-toluidine
-
-
7616-99-1
picryl-o-tolyl-amine
| Conditions | Yield |
|---|---|
| In acetonitrile at 25℃; | 100% |
| In acetonitrile at 25℃; Equilibrium constant; Kinetics; Further Variations:; title comp. concentration; |
| Conditions | Yield |
|---|---|
| With potassium carbonate In tetrahydrofuran for 24h; Reflux; | 100% |
| With sodium acetate In ethanol at 85 - 90℃; | 99% |
| With silica gel at 20℃; for 0.133333h; microwave irradiation; |
| Conditions | Yield |
|---|---|
| In methanol at 20℃; for 24h; | 100% |
| With toluene-4-sulfonic acid In diethyl ether at 20℃; Molecular sieve; Inert atmosphere; | 100% |
| With 4 A molecular sieve In benzene at 20℃; for 22h; | 76% |
-
-
31739-56-7
2-(1H-pyrrol-1-yl)benzaldehyde
-
-
95-53-4
o-toluidine
| Conditions | Yield |
|---|---|
| at 20℃; | 100% |
-
-
103-83-3
N,N'-dimethylbenzylamine
-
-
3375-31-3
palladium diacetate
-
-
95-53-4
o-toluidine
-
-
93916-94-0
bisacetato-N,N-dimethylbenzylamine-o-toluidinepalladium(II)
| Conditions | Yield |
|---|---|
| In dichloromethane o-toluidine in CH2Cl2 was added dropwise to Pd acetate in CH2Cl2, stirring for 5 min, Me2NCH2C6H5 in CH2Cl2 was added, stirring for 10 min; evapn., stirring with light petroleum, filtration; elem. anal.; | 100% |
| Conditions | Yield |
|---|---|
| In benzene-d6 air and H2O free atmosphere, NMR tube; room temp. (1 week); detd. by (1)H NMR spectroscopy; | 100% |
-
-
591-50-4
iodobenzene
-
-
201230-82-2
carbon monoxide
-
-
95-53-4
o-toluidine
-
-
584-70-3
N-benzoyl-2-methylaniline
| Conditions | Yield |
|---|---|
| With triethylamine In N,N-dimethyl-formamide at 100℃; under 750.075 Torr; for 8h; Schlenk technique; Inert atmosphere; | 100% |
| With palladium diacetate; triethylamine In water at 100℃; under 5171.62 Torr; for 8h; Autoclave; | 92% |
| With 1%Pd/SiO2; potassium carbonate In neat (no solvent) at 80℃; for 24h; Sealed tube; Green chemistry; | 99 %Spectr. |
| Conditions | Yield |
|---|---|
| In acetonitrile at 25℃; Kinetics; Concentration; | 100% |
-
-
10242-31-6
1-(4-nitrophenoxy)-2,4,6-trinitrobenzene
-
-
95-53-4
o-toluidine
-
-
7616-99-1
picryl-o-tolyl-amine
| Conditions | Yield |
|---|---|
| In acetonitrile at 25℃; Kinetics; Concentration; | 100% |
-
-
10242-30-5
2-nitrophenyl 2,4,6-trinitrophenyl ether
-
-
95-53-4
o-toluidine
-
-
7616-99-1
picryl-o-tolyl-amine
| Conditions | Yield |
|---|---|
| In acetonitrile at 25℃; Kinetics; Concentration; | 100% |
Related products
Downstream Products
Hot Products
T, 
N, 
FAbout|Contact|Cas|Product Name|Molecular|Country|Encyclopedia
Message|New Cas|MSDS|Service|Advertisement|CAS DataBase|Article Data|Manufacturers | Chemical Catalog
©2008 LookChem.com,License: ICP
NO.:Zhejiang16009103
complaints:service@lookchem.com Desktop View