Dayang Chem (Hangzhou) Co.,Ltd.
As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:541-73-1
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquirySimagchem Corporation
Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:541-73-1
Min.Order:0 Metric Ton
Negotiable
Type:Manufacturers
inquiryHebei yanxi chemical co.,LTD.
Hebei yanxi chemical co., LTD is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low carb
Cas:541-73-1
Min.Order:1 Kilogram
FOB Price: $2.1 / 2.8
Type:Manufacturers
inquiryAlity Chemical Corporation
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Chemwill Asia Co., Ltd.
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:541-73-1
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryHenan Tianfu Chemical Co., Ltd.
TIANFUCHEM--541-73-1--1,3-Dichlorobenzene factory price Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business rel
Cas:541-73-1
Min.Order:1 Metric Ton
FOB Price: $2000.0
Type:Lab/Research institutions
inquiryJinan Finer Chemical Co., Ltd
Product Description Product website: http://www.finerchem.com Product Name 1,3-Dichlorobenzene CAS No. 541-73-1
Cas:541-73-1
Min.Order:1 Metric Ton
FOB Price: $12.0
Type:Lab/Research institutions
inquiryHenan Sinotech Import&Export Corporation
Product Name: 1,3-Dichlorobenzene Synonyms: 1,3-DICHLOROBENZENE;M-DICHLOROBENZENE;M-DICHLOROBENZENE 99;MDCB;1,3-dichlorbenzene;1,3-Dichlorbenzol;1,3-dichloro-benzen;Rcra waste number U071
Cas:541-73-1
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Other
inquiryHangzhou Keyingchem Co.,Ltd
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:541-73-1
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryHangzhou J&H Chemical Co., Ltd.
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
SHANGHAI T&W PHARMACEUTICAL CO., LTD.
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:541-73-1
Min.Order:4 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:541-73-1
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryHangzhou Lingrui Chemical Co.,Ltd.
1,3-Dichlorobenzene Storage:Shading, sealed, dry place. Package:according to customers' requirements Application:pharmaceutical intermediates raw material Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(FOB or CIF or CNF ect...)or
HANGZHOU YUNUO CHEMICAL CO.,LTD
Superior quality, moderate price & quick delivery. Appearance:colorless liquid Storage:stored in a cool, dry and ventilated place to provent sun and rain Package:25kg/drum, or as per your request. Application: Organic intermediates Transpor
Zibo Dorne chemical technology co. LTD
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:541-73-1
Min.Order:1 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co., Ltd.
1)quick response within 12 hours; 2)quality guarantee: all products are strictly tested by our qc, confirmed by qa and approved by third party lab in china, usa, canada, germany, uk, italy, france etc. 3) oem/odm available; 4) rea
Cas:541-73-1
Min.Order:1 Gram
FOB Price: $10.0
Type:Lab/Research institutions
inquiryHangzhou Huarong Pharm Co., Ltd.
Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
Hangzhou Zhongqi chem Co.,Ltd.
Qualified favorable price1,3-Dichlorobenzene 541-73-1 with reliable industry Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemi
Cas:541-73-1
Min.Order:1 Gram
Negotiable
Type:Other
inquiryHUNAN CHEMAPI BIOLOGICAL TECHNOLOGY CO.,LTD.
Hunan Kaimir Biotechnology Co., Ltd. is a professional technology company specializing in the research and production of raw materials and intermediates. In 2017, it was recognized as a high-tech enterprise and a small technological innovation giant
Hunan chemfish Pharmaceutical co.,Ltd
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
SAGECHEM LIMITED
SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe
Cas:541-73-1
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryBeijing Greenchem Technology Co.,Ltd. ( Panjin Greenchem Technology Co.Ltd .)
Capability on chemical synthesis1. Beijing High-Tech Enterprises2. Strong R&D Team3. 8 years of experiences in R & D of high-tech Catalyst;4. 5000 production techniques, 69 items of national patents, and 360 kinds of products on sales;5. The producti
Kono Chem Co.,Ltd
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
GIHI CHEMICALS CO.,LIMITED
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
JINHUA HUAYI CHEMICAL CO., LTD.
Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Hangzhou Dingyan Chem Co., Ltd
R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates
Wuhan Fortuna Chemical Co.,Ltd
1.High quality : the purity is 99% min . through multiple producing procedures. 2.Competitive price : low price because of our skilled production technolpgy ,save the production cost at most , and give big profit room to our customers453.Safe and fa
Henan Allgreen Chemical Co.,Ltd
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Aecochem Corp.
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Enke Pharma-tech Co.,Ltd. （Cangzhou, China ）
Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city?in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api,?intermediat
Synthetic route
-
-
541-73-1
1,3-Dichlorobenzene
| Conditions | Yield |
|---|---|
| With triethyl phosphate at 50 - 60℃; under 7.50075 - 22.5023 Torr; Product distribution / selectivity; | 99% |
-
-
95-94-3
1,2,4,5-tetrachlorobenzene
-
A
-
106-46-7
para-dichlorobenzene
-
B
-
95-50-1
1,2-dichloro-benzene
-
C
-
541-73-1
1,3-Dichlorobenzene
-
D
-
71-43-2
benzene
| Conditions | Yield |
|---|---|
| With potassium hydroxide; hydrogen; palladium on activated charcoal In water at 50℃; for 0.92h; Yields of byproduct given; | A n/a B n/a C n/a D 98% |
-
-
541-73-1
1,3-Dichlorobenzene
| Conditions | Yield |
|---|---|
| 98% |
| Conditions | Yield |
|---|---|
| With [Au(1,3-bis(2,6-diisopropylphenyl)-4,5-dihydroimidazol-2-ylidene)(O2CAd)] In toluene at 140℃; for 20h; | 93% |
| With silver(I) acetate; potassium carbonate In 1-methyl-pyrrolidin-2-one at 120℃; for 16h; Inert atmosphere; | 74% |
| With C38H53AuN2O2 at 120℃; |
-
-
19752-55-7
1-bromo-3,5-dichlorobenzene
-
-
541-73-1
1,3-Dichlorobenzene
| Conditions | Yield |
|---|---|
| With methanol; gold; hydrogen; caesium carbonate at 100℃; under 3800.26 Torr; for 72h; | 89% |
-
-
120-82-1
1,2,4-Trichlorobenzene
-
A
-
106-46-7
para-dichlorobenzene
-
B
-
95-50-1
1,2-dichloro-benzene
-
C
-
541-73-1
1,3-Dichlorobenzene
| Conditions | Yield |
|---|---|
| With radical anion of p,p'-di-tert-butylbiphenyl In tetrahydrofuran at -60℃; Product distribution; Rate constant; Mechanism; Irradiation; radical anion of naphthalene, different temperatures; | A 87.2% B 2.79% C 9.96% |
| With radical anion of p,p'-di-tert-butylbiphenyl In tetrahydrofuran at -70℃; Irradiation; | A 87.7% B 2.97% C 9.32% |
| With radical anion of p,p'-di-tert-butylbiphenyl In tetrahydrofuran at 45℃; Irradiation; | A 75.3% B 9.89% C 13.7% |
-
-
19230-28-5
1,3-dichloro-2-iodobenzene
-
-
541-73-1
1,3-Dichlorobenzene
| Conditions | Yield |
|---|---|
| With hydrogen; triethylamine In methanol; water at 120℃; under 22502.3 Torr; | 87% |
| With 2-(2-methoxyethoxy)ethyl alcohol; oxygen; sodium hydride In 1,4-dioxane at 20℃; for 18h; Schlenk technique; chemoselective reaction; | 73% |
| With sodium methylate In methanol; dimethyl sulfoxide at 50.1℃; Rate constant; | |
| With potassium cyanide; Pd(PPh2(C6H4-p-SO3K))2Cl2; zinc In n-heptane; water at 100℃; for 1h; Inert atmosphere; | 38 %Chromat. |
| With hydrogen; triethylamine In methanol; water at 120℃; under 22502.3 Torr; for 44h; Autoclave; | 87 %Chromat. |
| Conditions | Yield |
|---|---|
| With silver(I) acetate; potassium carbonate In 1-methyl-pyrrolidin-2-one at 120℃; for 16h; Inert atmosphere; | 76% |
| With acetamide at 225 - 235℃; | |
| With silver carbonate In dimethylsulfoxide-d6 at 120℃; for 16h; Sealed vessel; | 96 %Spectr. |
| With silver carbonate In 1,4-dioxane at 130℃; for 24h; |
-
-
95-94-3
1,2,4,5-tetrachlorobenzene
-
A
-
106-46-7
para-dichlorobenzene
-
B
-
108-90-7
chlorobenzene
-
C
-
95-50-1
1,2-dichloro-benzene
-
D
-
541-73-1
1,3-Dichlorobenzene
-
E
-
120-82-1
1,2,4-Trichlorobenzene
-
F
-
71-43-2
benzene
| Conditions | Yield |
|---|---|
| With potassium hydroxide; hydrogen; palladium on activated charcoal In water at 50℃; for 0.5h; Product distribution; Aliquat 336 and other phase-transfer catalysts, different multiphase systems, different time and solvents; | A n/a B 4% C n/a D n/a E 4% F 73% |
| With potassium hydroxide; sodium hypophosphite; cetyltributylphosphonium bromide; isobutyric Acid; palladium on activated charcoal In 2,2,4-trimethylpentane at 50℃; for 2h; Product distribution; varying conditions (solvent, aqueous phase, hydrogen source, phase-transfer agent, time), other aromatic halides, competitive hydrodehalogenations; | |
| With potassium hydroxide; hydrogen; palladium on activated charcoal In 2,2,4-trimethylpentane at 50℃; for 0.5h; Product distribution; add. of Aliquat 336, var. phase-transfer cat.; var. base: Ca(OH)2; add. of polyethylene glycol monomethyl ether; add of NaBO3*H2O or KF; var. solv. and time; | A n/a B 4 % Chromat. C n/a D n/a E 4 % Chromat. F 73 % Chromat. |
| Conditions | Yield |
|---|---|
| With phenylphosphorus tetrachloride at 160℃; | 71% |
-
-
1194-65-6
2,6-dichloro-benzonitrile
-
A
-
65231-41-6
2,6-Dichlorbenzophenonimin
-
B
-
541-73-1
1,3-Dichlorobenzene
| Conditions | Yield |
|---|---|
| In diethyl ether for 6h; Addition; Heating; | A 70% B 4% |
| Conditions | Yield |
|---|---|
| With hydrogen bromide; copper In acetonitrile at 20 - 25℃; for 0.25h; | A 70% B 15% |
-
-
541-73-1
1,3-Dichlorobenzene
| Conditions | Yield |
|---|---|
| With N-benzyl-N,N,N-triethylammonium chloride; copper In acetonitrile at 20℃; for 0.75h; Substitution; | 68% |
| Conditions | Yield |
|---|---|
| at 170℃; for 4h; Temperature; Inert atmosphere; | 64.7% |
| With aluminium trichloride at 160℃; | |
| With aluminum (III) chloride; lithium chloride In melt at 170℃; for 4h; Inert atmosphere; |
-
-
120-82-1
1,2,4-Trichlorobenzene
-
A
-
106-46-7
para-dichlorobenzene
-
B
-
108-90-7
chlorobenzene
-
C
-
95-50-1
1,2-dichloro-benzene
-
D
-
541-73-1
1,3-Dichlorobenzene
-
E
-
71-43-2
benzene
| Conditions | Yield |
|---|---|
| With hydrogen; palladium diacetate; sodium hydrogencarbonate In water at 25℃; under 760.051 Torr; | A n/a B 6% C n/a D n/a E 60% |
| With sodium tetrahydroborate In water; acetonitrile Quantum yield; Product distribution; Irradiation; effect of scavengers and quenchers; | A 37 % Chromat. B 18 % Chromat. C 2 % Chromat. D 43 % Chromat. E 1 % Chromat. |
| With potassium hydroxide; hydrogen; palladium on activated charcoal In 2,2,4-trimethylpentane at 50℃; for 0.333333h; Product distribution; add. of Aliquat 336, var. cat.: Raney-Ni; var. temp.; | A 1 % Chromat. B 9 % Chromat. C 7 % Chromat. D 2 % Chromat. E 81 % Chromat. |
| Conditions | Yield |
|---|---|
| In methanol at 20 - 25℃; Dimerization; arylthiodediazoniation; hydrodediazoniation; | A 40% B n/a C 47% D 35% |
| Conditions | Yield |
|---|---|
| With aluminum (III) chloride; lithium chloride In melt at 170℃; for 4h; Catalytic behavior; Reagent/catalyst; Time; Autoclave; Inert atmosphere; | A n/a B 45% |
| With Zeolite β at 339.9℃; under 1 Torr; Mechanism; Thermodynamic data; Product distribution; activation energy; relative rate constants; different temperatures; | |
| ZSM-5 type zeolite at 399.9℃; under 26252.1 Torr; Product distribution; various catalysts; further temperatures; | |
| With aluminum (III) chloride; lithium chloride; sodium chloride at 150℃; for 16.5h; Reagent/catalyst; Temperature; |
-
-
292638-84-7
styrene
-
A
-
1725-76-4
(E,E)-1,3-distyrylbenzene
-
B
-
146736-38-1
1-phenyl-1-chloro-2-(3-chlorophenyl)ethane
-
D
-
541-73-1
1,3-Dichlorobenzene
| Conditions | Yield |
|---|---|
| With sodium chloride; copper dichloride In acetone at 5 - 50℃; | A 7% B 45% C n/a D n/a |
| Conditions | Yield |
|---|---|
| With sodium chloride; copper dichloride In acetone at 5 - 50℃; | A 39% B n/a C n/a |
-
-
81055-73-4
ethyl 2,6-dichlorobenzoate
-
-
541-73-1
1,3-Dichlorobenzene
| Conditions | Yield |
|---|---|
| With potassium fluoride; 18-crown-6 ether; tetraphenylphosphonium bromide at 210℃; for 3h; | 37% |
| Conditions | Yield |
|---|---|
| With sodium chloride; copper dichloride In acetone at 5 - 50℃; | A 36% B 5% C n/a |
-
-
107-13-1
acrylonitrile
-
A
-
18826-39-6
2-chloro-3-(3-chlorophenyl)propanenitrile
-
C
-
541-73-1
1,3-Dichlorobenzene
| Conditions | Yield |
|---|---|
| With sodium chloride; copper dichloride In acetone at 5 - 50℃; | A 32% B n/a C n/a |
| Conditions | Yield |
|---|---|
| With sodium chloride; copper dichloride In acetone at 5 - 50℃; | A 32% B 4% C n/a |
-
-
36997-05-4
2-methoxyacrylic acid ethyl ester
-
-
50-30-6
2,6-dichlorobenzoic acid
-
C
-
541-73-1
1,3-Dichlorobenzene
| Conditions | Yield |
|---|---|
| With palladium(II) trifluoroacetate; silver carbonate In 1,4-dioxane; dimethyl sulfoxide at 130℃; for 24h; Solvent; Sealed tube; Inert atmosphere; stereoselective reaction; | A 27% B n/a C n/a |
-
-
108-70-3
1,3,5-trichlorobenzene
-
-
67-63-0
isopropyl alcohol
-
A
-
67-64-1
acetone
-
B
-
541-73-1
1,3-Dichlorobenzene
-
C
-
71-43-2
benzene
| Conditions | Yield |
|---|---|
| With sodium hydroxide; 1,2-bis(diphenylphosphino)ethane nickel(II) chloride In water; toluene for 48h; Conversion of starting material; Alkaline conditions; Heating / reflux; | A n/a B 24% C 36 %Chromat. |
| With sodium hydroxide; nickel dihydroxide; 1,2-bis(diphenylphosphino)ethane nickel(II) chloride In water; toluene for 72h; Conversion of starting material; Alkaline conditions; Heating / reflux; | A n/a B 16% C 50 %Chromat. |
-
-
56-23-5
tetrachloromethane
-
-
937-14-4
3-chloro-benzenecarboperoxoic acid
-
A
-
67-72-1
hexachloroethane
-
B
-
541-73-1
1,3-Dichlorobenzene
| Conditions | Yield |
|---|---|
| With cyclohexane In 1,2-dichloro-ethane at 65℃; for 24h; Product distribution; Mechanism; | A 3.2% B 15.5% |
-
-
95-94-3
1,2,4,5-tetrachlorobenzene
-
A
-
106-46-7
para-dichlorobenzene
-
B
-
95-50-1
1,2-dichloro-benzene
-
C
-
541-73-1
1,3-Dichlorobenzene
-
D
-
120-82-1
1,2,4-Trichlorobenzene
| Conditions | Yield |
|---|---|
| With carbon dioxide; tetrabutylammomium bromide In N,N-dimethyl-formamide at -5 - 0℃; Dehalogenation; Electrochemical reaction; Further byproducts given; | A 9% B 1% C 2% D 8% |
| With [2,2]bipyridinyl; nickel dichloride; zinc In water; N,N-dimethyl-formamide at 80℃; for 6h; Title compound not separated from byproducts; | A 15.2 % Spectr. B 5.8 % Spectr. C 3.9 % Spectr. D 66.0 % Spectr. |
| Conditions | Yield |
|---|---|
| With chlorine at 220℃; Ausschluss von Wasser und Eisen; | |
| With tetrachloromethane at 260 - 310℃; | |
| With chlorine at 230 - 250℃; | |
| With chlorine at 230℃; Temperature; |
| Conditions | Yield |
|---|---|
| With tetrachloromethane; chlorine Photolysis; | |
| With iron(III) chloride; sodium chloride In acetonitrile for 10h; Irradiation; Green chemistry; regioselective reaction; |
| Conditions | Yield |
|---|---|
| With potassium hydroxide; PEG-6000 at 150℃; for 6h; | 100% |
| Conditions | Yield |
|---|---|
| With sodium hydroxide; ethanol; hydrogen; PdCl2-poly(N-vinyl-2-pyrrolidone); palladium dichloride at 65℃; under 760 Torr; for 2h; | 100% |
| With Ni[1,10-phenanthroline]2(PF6)2; water; zinc at 70℃; for 7h; Ionic liquid; | 46% |
| With Ni-Al clusters In tetrahydrofuran for 1.5h; Dehalogenation; reduction; hydrogenolysis; dechlorination; Heating; |
-
-
392-85-8
1-fluoro-2-trifluoromethylbenzene
-
-
541-73-1
1,3-Dichlorobenzene
-
-
917751-97-4
2,4-dichloro-1-[dichloro-(2-fluorophenyl)methyl]benzene
| Conditions | Yield |
|---|---|
| With aluminum (III) chloride In 1,2-dichloro-ethane at 0 - 5℃; for 3h; | 100% |
| With aluminium trichloride In 1,2-dichloro-ethane at 0℃; for 3h; Friedel-Crafts alkylation; | 92.4% |
| Conditions | Yield |
|---|---|
| With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II) In diethyl ether; hexane at 50℃; Kumada Cross-Coupling; Inert atmosphere; Schlenk technique; | 100% |
-
-
124-40-3
dimethyl amine
-
-
541-73-1
1,3-Dichlorobenzene
-
-
22440-93-3
N,N,N',N'-tetramethyl-m-phenylenediamine
| Conditions | Yield |
|---|---|
| With (R)-1-[(SP)-2-(dicyclohexylphosphino)ferrocenyl]ethyldi-tert-butylphosphine; palladium dichloride; lithium hexamethyldisilazane In tetrahydrofuran; 1,2-dimethoxyethane at 0 - 20℃; for 16h; Inert atmosphere; Glovebox; | 99.9% |
| With C8H11N*C33H50ClPPd; lithium hexamethyldisilazane In tetrahydrofuran at 0 - 20℃; Inert atmosphere; | 94% |
| With phenyllithium In tetrahydrofuran at 20℃; for 24h; Inert atmosphere; |
| Conditions | Yield |
|---|---|
| With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 2.9-dimethyl-1,10-phenanthroline In 1,4-dioxane at 100℃; for 6h; Catalytic behavior; Reagent/catalyst; Inert atmosphere; Sealed tube; regioselective reaction; | 99% |
| With IrH3{κ3-P,O,P-[9,9-dimethyl-4,5-bis(diisopropylphosphino)xanthene]} In cyclohexene at 110℃; for 18h; Inert atmosphere; Glovebox; | 94% |
| With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 2,4,7-trimethyl-1,10-phenanthroline In tetrahydrofuran at 120℃; for 40h; Inert atmosphere; Sealed tube; | 66% |
| Conditions | Yield |
|---|---|
| With bromine; iron(III) chloride | 98.5% |
| With methanesulfonic acid; monobromoisocynaurate In diethyl ether for 6h; Heating; | 65% |
-
-
541-73-1
1,3-Dichlorobenzene
-
-
19230-28-5
1,3-dichloro-2-iodobenzene
| Conditions | Yield |
|---|---|
| Stage #1: 1,3-Dichlorobenzene With n-butyllithium In tetrahydrofuran; hexane at -75℃; for 2h; Stage #2: With iodine In tetrahydrofuran; hexane | 98% |
| Stage #1: 1,3-Dichlorobenzene With sodium; diisopropylamine; isoprene In tetrahydrofuran at -20℃; for 0.000138889h; Flow reactor; Stage #2: With iodine In tetrahydrofuran Temperature; Flow reactor; | 84% |
| Stage #1: 1,3-Dichlorobenzene With Li(2,2,6,6-tetramethylpiperidide)*Al(iBu)3 In tetrahydrofuran; hexane at -78℃; for 12h; Stage #2: With iodine In tetrahydrofuran; hexane at 0℃; for 1h; | 74% |
| Conditions | Yield |
|---|---|
| Stage #1: 9H-carbazole With methylmagnesium chloride In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene for 0.25h; Inert atmosphere; Schlenk technique; Stage #2: 1,3-Dichlorobenzene With [2,6-bis(2,4,6-triisopropylphenyl)phenyl(dicyclohexylphosphine)](allyl-η3)palladium(II) chloride; 2,6-bis(2,4,6-triisopropylphenyl)phenyl(dicyclohexylphosphine) In 5,5-dimethyl-1,3-cyclohexadiene at 145℃; for 3h; Reagent/catalyst; Temperature; Glovebox; Schlenk technique; Inert atmosphere; | 98% |
| Stage #1: 9H-carbazole With methylmagnesium chloride In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene at 5 - 20℃; for 0.166667h; Inert atmosphere; Stage #2: 1,3-Dichlorobenzene With PdCl(π-allyl)(cyclohexyl-(1-methyl-2,2-diphenylcyclopropylphophine)) In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene at 108 - 112℃; for 0.25h; Inert atmosphere; | 97% |
| With di-tert-butyl(2,2-diphenyl-1-methyl-1-cyclopropyl)phosphine; bis(η3-allyl-μ-chloropalladium(II)); methylmagnesium chloride In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene at 5℃; Buchwald-Hartwig Coupling; Inert atmosphere; Reflux; | 96.8% |
| Conditions | Yield |
|---|---|
| With aluminum (III) chloride at 40 - 55℃; | 97.9% |
| Stage #1: acetic anhydride; 1,3-Dichlorobenzene With aluminum (III) chloride at 40 - 55℃; under 637.564 Torr; Stage #2: With hydrogenchloride In water | 95% |
| With aluminum (III) chloride at 50℃; for 4h; Reagent/catalyst; Temperature; | 70.9% |
| Stage #1: acetic anhydride With aluminum (III) chloride In 1,2-dichloro-benzene for 0.333333h; Stage #2: 1,3-Dichlorobenzene With hydrogenchloride In water; 1,2-dichloro-benzene Cooling with ice; | 55.46% |
| With hydrogenchloride; aluminum (III) chloride; calcium chloride In water for 0.833333h; | 55.46% |
| Conditions | Yield |
|---|---|
| With sulfuric acid; nitric acid at 10 - 15℃; for 3h; Temperature; | 97.2% |
| With sulfuric acid; nitric acid at 60℃; for 1h; | 95.4% |
| With nitric acid; acetic anhydride In tetrachloromethane | 65.3% |
-
-
108-30-5
succinic acid anhydride
-
-
541-73-1
1,3-Dichlorobenzene
-
-
58457-57-1
4-(2,4-dichlorophenyl)-4-oxobutanoic acid
| Conditions | Yield |
|---|---|
| With aluminium trichloride at 80℃; for 1h; | 96% |
| With aluminium trichloride |
| Conditions | Yield |
|---|---|
| at 60℃; for 4h; Ionic liquid; Green chemistry; | 96% |
| at 60℃; for 4h; Temperature; Ionic liquid; | 96% |
| With aluminium trichloride |
| Conditions | Yield |
|---|---|
| Stage #1: carbon dioxide With AuOH(1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene); potassium hydroxide In tetrahydrofuran at 20℃; under 1125.11 Torr; for 0.25h; Stage #2: 1,3-Dichlorobenzene In tetrahydrofuran at 20℃; under 1125.11 Torr; for 12h; Stage #3: With hydrogenchloride In tetrahydrofuran; water regioselective reaction; | 96% |
| With n-butyllithium In tetrahydrofuran; hexane for 0.75h; cooling; | 95% |
| Stage #1: 1,3-Dichlorobenzene With n-butyllithium In tetrahydrofuran at -75℃; for 2h; Stage #2: carbon dioxide In tetrahydrofuran | 95% |
| Stage #1: 1,3-Dichlorobenzene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.75h; Inert atmosphere; Stage #2: carbon dioxide In tetrahydrofuran; hexane at -78℃; for 0.166667h; Inert atmosphere; | 437 mg |
| Conditions | Yield |
|---|---|
| Stage #1: 1,3-Dichlorobenzene With n-butyllithium Stage #2: With zinc(II) chloride In tetrahydrofuran; hexane at 0 - 20℃; Stage #3: ortho-methylphenyl iodide With tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 20℃; for 10h; Negishi coupling reaction; Inert atmosphere; Reflux; | 96% |
| Conditions | Yield |
|---|---|
| With Ni(N,N'-bis(diphenylphosphino)-1,3-benzenediamine(-1H))Cl In tetrahydrofuran at 40℃; for 18h; Kumada Cross-Coupling; Schlenk technique; Inert atmosphere; | 95.7% |
| Conditions | Yield |
|---|---|
| Stage #1: 1,3-Dichlorobenzene With sodium; diisopropylamine; isoprene In tetrahydrofuran at -20℃; for 0.000138889h; Flow reactor; Stage #2: benzaldehyde In tetrahydrofuran Flow reactor; | 95% |
| With n-butyllithium 1.) hexane,THF, -65 to -70 deg C, 45 min, 2.) THF, -70 deg C, 45 min; Yield given. Multistep reaction; |
-
-
73183-34-3
bis(pinacol)diborane
-
-
541-73-1
1,3-Dichlorobenzene
-
-
68716-51-8
2-(3,5-dichlorophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
| Conditions | Yield |
|---|---|
| Stage #1: bis(pinacol)diborane With C24H28ClIrN2O In n-heptane; isopropyl alcohol at 75℃; for 1h; Sealed tube; Inert atmosphere; Stage #2: 1,3-Dichlorobenzene In n-heptane; isopropyl alcohol Sealed tube; Inert atmosphere; | 95% |
| With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine In tert-butyl methyl ether at 80℃; for 1h; Microwave irradiation; | 94% |
| With [Ir(OMe)(1,5-cyclooctadiene)]2; C88H164N2 In n-heptane at 25℃; for 18h; Inert atmosphere; | 84% |
-
-
25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane
-
-
541-73-1
1,3-Dichlorobenzene
-
-
68716-51-8
2-(3,5-dichlorophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
| Conditions | Yield |
|---|---|
| With IrH2(Bpin){κ3-P,O,P-[9,9-dimethyl-4,5-bis(diisopropylphosphino)xanthene]}; cyclohexene at 110℃; for 18h; Inert atmosphere; Glovebox; | 95% |
| With iridium-bipyridine periodic mesoporous organosilica In cyclohexane at 80℃; for 12h; Inert atmosphere; Schlenk technique; | 94% |
| With 4,4'-di-tert-butyl-2,2'-bipyridine; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer In hexane at 25℃; for 8h; | 86% |
-
-
541-73-1
1,3-Dichlorobenzene
| Conditions | Yield |
|---|---|
| In tetrahydrofuran at 0℃; for 1h; Inert atmosphere; Schlenk technique; regioselective reaction; | 95% |
-
-
31600-86-9
2-methoxyphenyllithium
-
-
541-73-1
1,3-Dichlorobenzene
-
-
103068-14-0
2,2”-dimethoxy-1,1’:3’,1”-terphenyl
| Conditions | Yield |
|---|---|
| In diethyl ether for 15h; Ambient temperature; | 94% |
-
-
61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
-
-
541-73-1
1,3-Dichlorobenzene
-
-
69807-92-7
2-(2,6-dichlorophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
| Conditions | Yield |
|---|---|
| With bis(2,2,6,6-tetramethylpiperidin-1-yl)magnesium-bis(lithium chloride) complex In tetrahydrofuran at 0 - 25℃; for 2h; Inert atmosphere; Schlenk technique; | 94% |
-
-
15529-90-5
(triethylphosphine)chlorogold(I)
-
-
541-73-1
1,3-Dichlorobenzene
| Conditions | Yield |
|---|---|
| With sodium t-butanolate In N,N-dimethyl-formamide at 50℃; for 15h; | 94% |
| With potassium tert-butylate In neat (no solvent) for 1.5h; Reagent/catalyst; Time; Milling; | 92% |
| Conditions | Yield |
|---|---|
| With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; tert-butylethylene; 3,4,7,8-Tetramethyl-o-phenanthrolin In cyclohexane at 100℃; for 4h; Time; Inert atmosphere; Sealed tube; chemoselective reaction; | 94% |
| Conditions | Yield |
|---|---|
| With aluminum (III) chloride at 30℃; for 3h; Friedel-Crafts Acylation; | 93.1% |
| With aluminum (III) chloride In dichloromethane at 20℃; | 90% |
| With aluminum (III) chloride In dichloromethane for 3h; Reflux; | 86% |
-
-
13139-86-1
4-methoxyphenyl magnesium bromide
-
-
541-73-1
1,3-Dichlorobenzene
-
-
1568-74-7
4,4’’-dimethoxy-1,1′:3′,1’’-terphenyl
| Conditions | Yield |
|---|---|
| With C20H23BrN4Ni In tetrahydrofuran at 25℃; for 24h; Kumada Cross-Coupling; Inert atmosphere; | 93% |
| Stage #1: 1,3-Dichlorobenzene With Ni(PPh3)(1,3-di-tert-butylimidazol-2-ylidene)Br2 In tetrahydrofuran at 0℃; for 0.0333333h; Inert atmosphere; Schlenk technique; Stage #2: 4-methoxyphenyl magnesium bromide In tetrahydrofuran at 0 - 25℃; for 5h; Inert atmosphere; Schlenk technique; | 79% |
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