Lonwin Industry group limited as a professional manufactor & exporter of chemical materials ,we totally haver more than 270 stuffs, we have been on this line for more than 9 years. Our chemical materials are exported to lot of countries and reg
Cas:108-42-9
Min.Order:100 Kilogram
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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:108-42-9
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:108-42-9
Min.Order:1 Metric Ton
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inquiryProduct description: Product name 3-Chloroaniline CAS number 108-42-9 Assay ≥99.5% Appearance Colorless to yellowish liquid Capacity 1000mt/year Application Dyes, pigments, p
Cas:108-42-9
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiry3-Chloroaniline CAS RN 108-42-9 EINECS 203-581-0 Molecular formula C6H6ClN Molecular weight 127.57334 Structural formula Ph
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:108-42-9
Min.Order:5 Kiloliter
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Type:Manufacturers
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so
Cas:108-42-9
Min.Order:1 Metric Ton
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Type:Lab/Research institutions
inquiryProduct Name: 3-Chloroaniline Synonyms: 3-Chlorobenzenamine; fast orange GC base; m-Chloroaniline; 3-chlorobenzeneamine; m-chloro aniline; 3-chloroaniline hydrochloride (1:1) Molecular Formula: C6H7Cl2N Molecular Weight: 164.0325 CA
Cas:108-42-9
Min.Order:5 Metric Ton
FOB Price: $1.0 / 2.0
Type:Other
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:108-42-9
Min.Order:0 Metric Ton
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Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
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Cas:108-42-9
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:108-42-9
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:108-42-9
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiry3-ChloroanilineAppearance:light or amber transparent oily liquid Storage:Kept in a cool, dry and ventilated place Package:according to customers' requirements Application:research chemicals antineoplastic drugs Transportation:By air(EMS or EUB or Fe
Superior quality, moderate price & quick delivery. Appearance:clear pale yellow to brown liquid Storage:Well-sealed and put in dry and cool conditions. Protected from direct sunlight or high temperature. Package:as per your request Applic
We are leading fine chemicals supplier in China and Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED intermediates (Flu
Cas:108-42-9
Min.Order:1 Kilogram
FOB Price: $9.0 / 10.0
Type:Lab/Research institutions
inquiryCAS:108-42-9 EINECS:203-581-0 MW:127.57 MF:C6H6ClN Melting point:−11-−9 °C(lit.) Boiling point:95-96 °C11 mm Hg(lit.) Appearance:colorless liquid Package:Aluminum bag Transportation:by sea/air/courier Port:Shanghai
Product name: 3-Chloroaniline CAS No.:108-42-9 Molecule Formula:C6H6ClN Molecule Weight:127.57 Purity: 98.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS
Cas:108-42-9
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryHangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
CHENGDU YANXI is a comprehensive manufacturer and an international distribution of products throughout the world. Specialized in Scrap metal, Chemical raw materials, Paper products and color industry. We aim to become leading position in global dis
Cas:108-42-9
Min.Order:1 Kilogram
FOB Price: $1.0 / 3.0
Type:Trading Company
inquiryLocated in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and h
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
Capability on chemical synthesis 1. Beijing High-Tech Enterprises 2. Strong R&D Team 3. 8 years of experiences in R & D of high-tech Catalyst; 4. 5000 production techniques, 69 items of national patents, and 360 kinds of products on sal
ISO/factory/goodqualityAppearance:off white Storage:Dry,cool place Package:drum Application:active pharmaceutical ingredients Transportation:by air/sea/express Port:shenzhen/shanghai
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Conditions | Yield |
---|---|
With 2 weight% platinum on carbon; ethanol at 100℃; under 7500.75 Torr; for 8h; Autoclave; | 100% |
With hydrogen In ethanol at 20℃; under 7500.75 Torr; for 8h; Catalytic behavior; Sealed tube; | 100% |
With hydrazine hydrate In ethanol; water at 80℃; for 1h; chemoselective reaction; | 100% |
Conditions | Yield |
---|---|
100% |
Conditions | Yield |
---|---|
100% |
Conditions | Yield |
---|---|
With hydrogenchloride; potassium iodide | 98.2% |
Conditions | Yield |
---|---|
With samarium diiodide In tetrahydrofuran for 2h; Ambient temperature; | 98% |
Stage #1: 1-azido-3-chlorobenzene With hydrazine hydrate for 0.166667h; Inert atmosphere; Stage #2: for 10h; Irradiation; chemoselective reaction; | 90% |
With zinc(II) tetrahydroborate In 1,2-dimethoxyethane for 3.5h; Ambient temperature; | 89% |
Conditions | Yield |
---|---|
A 97.9% B n/a |
2,3-dichloroaniline
1,2-dichloro-benzene
m,p-dichloroaniline
3-chloro-aniline
Conditions | Yield |
---|---|
With HI; hydrogen iodide | 96.5% |
Conditions | Yield |
---|---|
With hydrogen; palladium/charcoal In tantalum; water; toluene | 96% |
Conditions | Yield |
---|---|
With copper(I) oxide; ammonium hydroxide; C17H14N2O3; potassium hydroxide In ethanol at 60℃; for 24h; Schlenk technique; Inert atmosphere; | 96% |
With ammonium hydroxide; potassium phosphate; 1-(5,6,7,8-tetrahydroquinolin-8-yl)-2-methylpropan-1-one; copper(I) bromide In dimethyl sulfoxide at 25℃; for 24h; Inert atmosphere; Sealed tube; | 90% |
With copper(l) iodide; tetra(n-butyl)ammonium hydroxide; ammonia In water at 25℃; for 24h; Inert atmosphere; Sealed tube; chemoselective reaction; | 89% |
Conditions | Yield |
---|---|
With copper(I) oxide; ammonium hydroxide In 1-methyl-pyrrolidin-2-one at 80℃; for 15h; | 93% |
With ammonium hydroxide; potassium phosphate; 1-(5,6,7,8-tetrahydroquinolin-8-yl)-2-methylpropan-1-one; copper(I) bromide In dimethyl sulfoxide at 110℃; for 24h; Inert atmosphere; Sealed tube; | 93% |
With ammonium hydroxide; copper(l) iodide; 2,2-[μ-(N,N'-piperazindiyl)dimethyl]-bis(4,6-di-tert-butyl-phenol) In water at 120℃; for 12h; | 85% |
3-chloro-aniline
Conditions | Yield |
---|---|
With indium; ammonium chloride In ethanol for 2.5h; Heating; | 86% |
(3-chlorophenyl)magnesium bromide
3-chloro-aniline
Conditions | Yield |
---|---|
Stage #1: (3-chlorophenyl)magnesium bromide With zinc(II) chloride In tetrahydrofuran at -3 - 20℃; Inert atmosphere; Stage #2: With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; dimethylsulfide; acetone oxime-o-p-benzenesulfonic ester; copper(ll) bromide In tetrahydrofuran at 20℃; for 1.5h; Inert atmosphere; Stage #3: With hydrogenchloride; water In tetrahydrofuran at 20℃; for 4h; Inert atmosphere; | 85% |
Multi-step reaction with 3 steps 1: tetrahydrofuran / -3 - 20 °C / Inert atmosphere 2: copper(l) cyanide / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere 3: hydrogenchloride / water; tetrahydrofuran / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: tetrahydrofuran / -5 - 20 °C / Inert atmosphere 2.1: acetone O-(2,4,6-trimethylphenylsulfonyl)oxime; triphenylphosphine / tetrahydrofuran / 0.08 h / 20 °C / Inert atmosphere 2.2: 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: tetrahydrofuran / 0.17 h / 10 °C / Inert atmosphere 2: copper(l) cyanide / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere 3: water; hydrogenchloride / 24 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: tetrahydrofuran / 0.17 h / 10 °C / Inert atmosphere 2: copper(l) cyanide / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere 3: water; hydrogenchloride / 24 h / 20 °C / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
With hydrogenchloride In water | 84.1% |
Conditions | Yield |
---|---|
With dihydridocarbonyl(1,1,1-tris(diphenylphosphinomethyl)ethane)ruthenium(II) complex; boron trifluoride diethyl etherate; hydrogen; toluene-4-sulfonic acid In tetrahydrofuran at 120℃; under 38002.6 Torr; for 16h; Glovebox; Autoclave; Inert atmosphere; | A 84% B n/a |
With [bis(2-methylallyl)cycloocta-1,5-diene]ruthenium(II); formic acid; bis(trifluoromethanesulfonyl)amide; triethylamine; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine] In dibutyl ether at 130℃; for 24h; | A n/a B 76% |
With C18H32ClIrO2P2; tris(pentafluorophenyl)borate; hydrogen; sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate In toluene at 120℃; under 38002.6 Torr; for 24h; Overall yield = 84 %; Overall yield = 87 %Chromat.; chemoselective reaction; |
2-(trimethylsilyl)-5-chloronitrobenzene
3-chloro-aniline
Conditions | Yield |
---|---|
With hydrogenchloride; tin for 15h; Heating; | 83% |
Conditions | Yield |
---|---|
With methanol; oxalyl dichloride at 20℃; for 2h; | 83% |
3-Chloronitrobenzene
A
aniline
B
3-chloro-aniline
C
3,3'-dichloroazobenzene
D
3,3'-dichloroazoxybenzene
Conditions | Yield |
---|---|
With bis(acetylacetonato)palladium(II); phosphorus; hydrogen In N,N-dimethyl-formamide; benzene at 50℃; under 1520.1 Torr; for 1.75h; Catalytic behavior; Time; chemoselective reaction; | A 9.4% B 81.4% C n/a D n/a |
Conditions | Yield |
---|---|
With Rh/Al2O3; hydrogen In water; toluene at 80℃; under 30003 Torr; for 24h; Reagent/catalyst; | A 17% B 81% |
With isopropyl alcohol; sodium hydroxide for 12h; Inert atmosphere; Reflux; chemoselective reaction; | A n/a B 76% |
With hydrogen; nickel-chromium catalyst In isopropyl alcohol at 49.9℃; under 760 Torr; |
Conditions | Yield |
---|---|
With sodium hydroxide; benzyltrimethylazanium tribroman-2-uide In water for 2h; Ambient temperature; | 79% |
Conditions | Yield |
---|---|
Stage #1: 3-chlorobenzoate With trifluorormethanesulfonic acid; trimethylsilylazide In chloroform at 90℃; for 0.055h; Schmidt Reaction; Flow reactor; Stage #2: With water In methanol; chloroform at 20℃; Schmidt Reaction; Flow reactor; | 79% |
With thionyl chloride; hydroxylamine-O-sulfonic acid 1) 1h, reflux, 2) toluene, 2h, reflux; Yield given. Multistep reaction; |
3-Chloronitrobenzene
A
3-chloro-aniline
B
3,3'-dichloroazobenzene
C
3,3'-dichloroazoxybenzene
Conditions | Yield |
---|---|
With hydrazine hydrate; nickel(II) nitrate; zinc In tert-butyl alcohol for 0.333333h; Heating; | A 5% B 6 % Chromat. C 78% |
With hydrazine hydrate; nickel(II) nitrate; zinc In ethanol for 3h; Heating; | A 15 % Chromat. B 12% C 43% |
indole
2-phenyl-1,2,3,4-tetrahydroisoquinoline
3-Chloronitrobenzene
B
3-chloro-aniline
Conditions | Yield |
---|---|
With Co(dmgH)2Cl2; Eosin Y In water; acetonitrile at 20℃; for 48h; Inert atmosphere; Irradiation; Sealed tube; | A 78% B 90 %Spectr. |
Conditions | Yield |
---|---|
With methanesulfonic acid; trimethylsilylazide In tetrachloromethane at 80℃; for 4h; | 76% |
3-chlorophenylboronic acid
3-chloro-aniline
Conditions | Yield |
---|---|
With copper(I) oxide; ammonium hydroxide; air In methanol at 20℃; for 18h; | 74% |
With copper(I) oxide; ammonium hydroxide; oxygen; sodium hydroxide In water at 25℃; for 15h; | 70% |
Conditions | Yield |
---|---|
With tributylgermanium hydride; thiophenol In toluene for 0.5h; Heating; | A 7% B 5% C 73% |
3-chloro-aniline
Conditions | Yield |
---|---|
With potassium hydroxide In dimethyl sulfoxide at 140℃; for 6h; Green chemistry; | 71% |
Conditions | Yield |
---|---|
With copper(ll) sulfate pentahydrate; potassium phosphate tribasic heptahydrate; water; Sucrose In water at 90℃; for 15h; Catalytic behavior; Green chemistry; | 70% |
1-(3-Chlor-anilino)-3-(3-chlor-phenylimino)-propen
A
β-(m-Chloranilino)acrolein
B
3-chloro-aniline
Conditions | Yield |
---|---|
With water; sodium acetate; acetic acid In ethanol at 70℃; for 32.5h; | A 52% B 68% |
chloroformic acid ethyl ester
3-chloro-aniline
(3-chlorophenyl) carbamic acid ethyl ester
Conditions | Yield |
---|---|
With pyridine at 0℃; for 1h; | 100% |
With sodium carbonate; benzene | |
With potassium carbonate In 1,4-dioxane for 2h; Heating; | |
With pyridine at 0 - 20℃; |
chloroacetyl chloride
3-chloro-aniline
2-chloro-N-(3-chlorophenyl)acetamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 25℃; | 100% |
With triethylamine In dichloromethane at 0 - 25℃; | 100% |
In tetrahydrofuran at 20℃; for 18h; | 100% |
3-chloro-aniline
diethyl 2-ethoxymethylenemalonate
2-(3-chlorophenylamino)methylenemalonic acid diethyl ester
Conditions | Yield |
---|---|
In toluene at 110℃; for 24h; | 100% |
In neat (no solvent) at 120℃; for 0.75h; | 98% |
In ethanol for 3h; Reflux; | 91% |
3,4-dimethoxy-benzaldehyde
3-chloro-aniline
(3-Chloro-phenyl)-[1-(3,4-dimethoxy-phenyl)-meth-(E)-ylidene]-amine
Conditions | Yield |
---|---|
In toluene Heating; | 100% |
2-isothiocyanatobenzylpyridinium bromide
3-chloro-aniline
1-{2-[3-(3-Chloro-phenyl)-thioureido]-benzyl}-pyridinium; bromide
Conditions | Yield |
---|---|
In methanol for 5h; | 100% |
3-chloro-aniline
Conditions | Yield |
---|---|
Stage #1: trifluoromethyl dihydro-1,4-dioxin-3-carbonyl chloride With pyridine; polystyrene-bound 4-hydroxy-3-nitrobenzophenone In dichloromethane at 20℃; for 24h; Condensation; Stage #2: 3-chloro-aniline With triethylamine In acetonitrile for 14h; Condensation; Heating; | 100% |
Conditions | Yield |
---|---|
With C15H29IrN4(2+)*2I(1-) at 120℃; for 17h; Inert atmosphere; Schlenk technique; Sealed tube; | 100% |
With tetrachloromethane; copper(ll) bromide at 180℃; for 6h; Inert atmosphere; Sealed tube; | 99% |
With sulfuric acid at 200℃; for 16h; | 77% |
With TiO2 supported nano-Pd(0.3) catalyst In water at 20℃; for 5h; Inert atmosphere; Irradiation; Green chemistry; | 65 %Chromat. |
With zinc oxide-supported iridium catalyst at 150℃; under 3750.38 Torr; for 5h; Inert atmosphere; | 99 %Chromat. |
Conditions | Yield |
---|---|
In isopropyl alcohol at 100℃; for 1h; | 100% |
With triethylamine In butan-1-ol at 100℃; | |
Stage #1: 1,4-dichlorophthalazine; 3-chloro-aniline In ethanol for 0.5h; Reflux; Stage #2: With sodium hydroxide In ethanol; water at 20℃; |
di-tert-butyl dicarbonate
3-chloro-aniline
t-butyl 3-chlorophenylcarbamate
Conditions | Yield |
---|---|
In methanol at 100℃; for 6h; | 100% |
Stage #1: 3-chloro-aniline With triethylamine In tetrahydrofuran; water at 20℃; for 0.0833333h; Stage #2: di-tert-butyl dicarbonate In tetrahydrofuran; water at 0 - 20℃; for 6h; | 100% |
With 1,1'-hexane-1,6-diylbis(3-methylpyridinium)tetrachlorocobaltate(II) In neat (no solvent) at 20℃; for 1h; | 97% |
Conditions | Yield |
---|---|
With tris(dibenzylideneacetone)dipalladium (0); 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate In toluene at 90 - 110℃; for 11h; Buchwald-Hartwig reaction; | 100% |
With pectin-stabilized copper nanoparticles In dimethyl sulfoxide at 110℃; for 2h; | 82% |
Conditions | Yield |
---|---|
With tert.-butylnitrite; trimethylsilylazide In acetonitrile at 0 - 20℃; for 1h; | 100% |
Stage #1: 3-chloro-aniline With hydrogenchloride; sodium nitrite In ethyl acetate at 0℃; for 0.5h; Stage #2: With sodium azide In ethyl acetate at 20℃; for 2h; | 91% |
Stage #1: 3-chloro-aniline With hydrogenchloride In water; ethyl acetate at 0℃; for 0.166667h; Stage #2: With sodium nitrite In water; ethyl acetate for 0.5h; Stage #3: With sodium azide In water; ethyl acetate for 0.5h; | 88% |
2-Bromoacetyl bromide
3-chloro-aniline
2-bromo-N-(3-chlorophenyl)acetamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; for 1.25h; Inert atmosphere; | 100% |
With triethylamine In dichloromethane at 0℃; for 1.25h; Inert atmosphere; | 100% |
With triethylamine at 0℃; for 1h; Inert atmosphere; | 100% |
3-chloro-aniline
trifluoroacetic anhydride
N-(3-chlorophenyl)-2,2,2-trifluoro-acetamide
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 0 - 20℃; for 0.75h; | 100% |
With triethylamine In dichloromethane at 0 - 25℃; for 12h; Inert atmosphere; | 91% |
With triethylamine In dichloromethane at -78 - 26℃; for 1h; | 2.29 g |
trimethylsilyl cyanide
N-tert-butyloxycarbonylpiperidin-4-one
3-chloro-aniline
Conditions | Yield |
---|---|
In acetic acid at 0℃; | 100% |
In acetic acid at 0 - 20℃; |
3-chloro-aniline
2-chloro-5-methoxyquinoline
Conditions | Yield |
---|---|
In neat (no solvent) at 160℃; | 100% |
In neat (no solvent) at 160℃; |
Conditions | Yield |
---|---|
With triethylamine In acetone at 90℃; for 3h; Inert atmosphere; | 100% |
3-chloro-aniline
2,4,6-tribromo-3-chloroaniline
Conditions | Yield |
---|---|
With hydrogenchloride; dihydrogen peroxide; sodium bromide In water at 15℃; for 2h; | 99.8% |
With bromine In tetrachloromethane at 20 - 40℃; | 91% |
With methanol; P-benzyltriphenylphosphonium tribromide; sodium hydrogencarbonate In dichloromethane for 0.166667h; Ambient temperature; | 86% |
Camphorsulfonyl chloride
3-chloro-aniline
(1S)-2-oxo-bornane-10-sulfonic acid-(3-chloro-anilide)
Conditions | Yield |
---|---|
With dmap In acetonitrile at 0℃; for 1h; Inert atmosphere; | 99% |
3-chloro-aniline
3-chloro-4-iodoaniline
Conditions | Yield |
---|---|
With sodium hydrogencarbonate; N,N,N-trimethylbenzenemethanaminium dichloroiodate In methanol; dichloromethane at 20℃; for 0.416667h; | 99% |
With tetramethylammonium dibromoiodate(I) at 20℃; for 0.116667h; | 97% |
With iodine at 30℃; for 12h; Green chemistry; | 95% |
Conditions | Yield |
---|---|
With hydrogen; triethylamine In water at 120 - 140℃; under 22502.3 - 37503.8 Torr; | 99% |
With lithium at 230℃; Zersetzen der Reaktionsprodukte mit Wasser; | |
With potassium fluoride; polymethylhydrosiloxane; palladium diacetate In tetrahydrofuran at 20℃; for 0.75h; | 94 % Spectr. |
Conditions | Yield |
---|---|
With potassium carbonate In water; acetone at 20℃; | 99% |
With ammonia; N,N-dimethyl-aniline In benzene |
3-chloro-aniline
ortho-chlorobenzoic acid
N-(3-chlorophenyl)anthranilic acid
Conditions | Yield |
---|---|
With copper(I) oxide; copper; potassium carbonate In 2-ethoxy-ethanol at 130℃; for 24h; | 99% |
With pyridine; copper; potassium carbonate In water for 1h; Heating; | 60% |
With copper; potassium carbonate for 5h; Heating; | 44% |
Conditions | Yield |
---|---|
In toluene Heating; | 99% |
Conditions | Yield |
---|---|
Stage #1: 3-chloro-aniline With boron trifluoride diethyl etherate In acetonitrile Cooling with ice; Stage #2: With isopentyl nitrite In acetonitrile at 0℃; for 0.5h; | 99% |
With tetrafluoroboric acid; sodium nitrite In water Diazotization; | 95% |
Stage #1: 3-chloro-aniline With hydrogenchloride; sodium nitrite In water for 0.166667h; Cooling with ice; Stage #2: With sodium tetrafluoroborate for 0.5h; Cooling with ice; | 74% |
6-chlorouracil
3-chloro-aniline
6-(3-chlorophenylamino)pyrimidine-2,4(1H,3H)-dione
Conditions | Yield |
---|---|
at 170℃; for 0.333333h; | 99% |
for 2h; Reflux; | 95% |
In melt at 180 - 200℃; |
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