Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:86-74-8
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/291.html Product Name Carbazole CAS No. 86-74-8 Appearance
hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
Cas:86-74-8
Min.Order:1 Metric Ton
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inquiryhigh quality Good price Promptly delivery Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:OLED Intermediate Transportation:by air or by sea Por
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
TIANFUCHEM--86-74-8--Carbazole factory price Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business relationships
Cas:86-74-8
Min.Order:1 Metric Ton
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Type:Lab/Research institutions
inquiryAdvantage : LIDE PHARMACEUTICALS LIMITED is a professional chemicals and APIs leading manufacturer in China. Our core business line covers APIs, Intermediates, Herb extract, etc. We are specialized in chemical synthesis, process development of
Cas:86-74-8
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryProduct Name: Carbazole Synonyms: 9-Dibenzo-[b,d]-pyrrole;Diphenylenedimine;Diphenyleneimide;Diphenyleneimine;Diphenylenimide;Skf 20091;USAF ek-600;usafek-600 CAS: 86-74-8
1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:White Crystalline Powder Storage:Store in sealed conta
Cas:86-74-8
Min.Order:10 Gram
Negotiable
Type:Other
inquiry1. Best prices with satisfied quality; 2. It's clients' right to choose the package's Courier (EMS, DHL, FedEx, UPS); 3.It's clients' right to choose the packing way for his produccts from many recent effective packing ways;
Product Name: Carbazole Synonyms: 9-Dibenzo-[b,d]-pyrrole;Diphenylenedimine;Diphenyleneimide;Diphenyleneimine;Diphenylenimide;Skf 20091;USAF ek-600;usafek-600 CAS: 86-74-8 MF: C12H9N MW: 167.21 EINECS: 201-696-0 Product Categories: Intermedia
Cas:86-74-8
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Product quality: Our company have high quality product , and also the product we have good manufacture . First of all, this product is of fine quality. Every finish should be checked by quality inspection system.And every one should be also tr
Cas:86-74-8
Min.Order:1 Kilogram
FOB Price: $10.0 / 20.0
Type:Trading Company
inquiryProduct Name: Carbazole Synonyms: 9-Dibenzo-[b,d]-pyrrole;Diphenylenedimine;Diphenyleneimide;Diphenyleneimine;Diphenylenimide;Skf 20091;USAF ek-600;Carbazoletechn CAS: 86-74-8 MF: C12H9N MW: 167.21 EINECS: 201-696-0 Product Categories:
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:86-74-8
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquirySuperior quality, moderate price & quick delivery. Appearance:white crystal powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermed
Product name: Carbazole CAS No.:86-74-8 Molecule Formula:C12H9N Molecule Weight:167.21 Purity: 99.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard TESTING ITEMS
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:86-74-8
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryLocated in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service an
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:86-74-8
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiryConditions | Yield |
---|---|
With caesium carbonate In tetrahydrofuran; methanol for 24h; Reflux; | 100% |
Conditions | Yield |
---|---|
With water for 5h; Inert atmosphere; UV-irradiation; Sealed tube; chemoselective reaction; | 99% |
With dirhodium(II) tetrakis(perfluorobutyrate) In toluene at 60℃; for 16h; Reactivity; Reagent/catalyst; Solvent; Temperature; Molecular sieve; Inert atmosphere; | 98% |
With sulfur-modified Au-supported iron(0) nanoparticles In 1,4-dioxane at 110℃; for 12h; Inert atmosphere; | 93% |
9H-carbazole
Conditions | Yield |
---|---|
With potassium amide In ammonia at -33℃; for 3h; | 99% |
With potassium amide In ammonia at -33℃; for 3h; other N-(tert-butoxycarbonyl)-2-(chlorophenyl)anilines; | 99% |
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In methanol for 0.5h; Product distribution; Further Variations:; Solvents; reaction time; Heating; | 99% |
With sulfuric acid In methanol at 60℃; for 0.25h; | 97% |
With triethyl borane; sodium hydroxide In tert-butyl methyl ether at 80℃; for 6h; Inert atmosphere; Sealed tube; | 71% |
With sodium hydroxide; dipotassium hydrogenphosphate; potassium dihydrogenphosphate; D-glucose; Pseudomonas aeruginosa; magnesium sulfate; potassium nitrate; sodium chloride; calcium chloride In water for 72h; pH 7.0; | 70% |
Stage #1: 9-acetylcarbazole With Triethoxysilane; sodium triethylborohydride In tert-butyl methyl ether at 80℃; for 6h; Stage #2: With hydrogenchloride In tert-butyl methyl ether; water at 20℃; for 1h; chemoselective reaction; | 65% |
Conditions | Yield |
---|---|
With potassium carbonate; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride; N-heterocyclic carbene palladium In N,N-dimethyl acetamide at 130℃; | 99% |
With potassium tert-butylate; ammonia for 1h; UV-irradiation; | 93% |
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol for 4h; Reflux; | 98% |
With sodium hydride In N,N-dimethyl acetamide at 60℃; for 3h; Inert atmosphere; | 98% |
With tetrabutyl ammonium fluoride In tetrahydrofuran for 4h; Reflux; | 96% |
Conditions | Yield |
---|---|
With 1,10-Phenanthroline; carbon monoxide; palladium diacetate In N,N-dimethyl-formamide at 140℃; under 3102.89 Torr; for 16h; | 97% |
With triphenylphosphine for 0.0333333h; Cadogan reaction; Microwave irradiation; | 96% |
With triphenylphosphine In 1,2-dichloro-benzene at 180℃; for 21h; | 91% |
9-benzoyl-9H-carbazole
9H-carbazole
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In methanol for 0.5h; Product distribution; Further Variations:; Solvents; reaction time; Heating; | 97% |
Conditions | Yield |
---|---|
With copper(II) choride dihydrate In dimethyl sulfoxide at 100℃; for 7h; | 96% |
With ethene; palladium 10% on activated carbon In acetonitrile at 100℃; for 96h; Sealed tube; | 92% |
With vanadium(V) oxide; acetic acid at 118℃; for 24h; Time; Inert atmosphere; | 83% |
9H-carbazole
Conditions | Yield |
---|---|
With manganese(IV) oxide; copper diacetate; acetic acid In N,N-dimethyl-formamide at 170℃; for 0.666667h; Kinetics; Temperature; Reagent/catalyst; Microwave irradiation; Sealed tube; | 96% |
Conditions | Yield |
---|---|
With hydrogen; triethylamine In ethanol; water at 140℃; under 37503.8 Torr; for 110h; Autoclave; | 96% |
With triethylamine In acetonitrile at 20℃; for 15h; Irradiation; Inert atmosphere; | 77% |
Conditions | Yield |
---|---|
Stage #1: 1-azido-2-iodo-benzene; phenylboronic acid With potassium carbonate In 1,4-dioxane at 110℃; for 8h; Inert atmosphere; Stage #2: In 1,4-dioxane; water Inert atmosphere; Reflux; | 96% |
Conditions | Yield |
---|---|
With air; potassium carbonate; Trimethylacetic acid; palladium diacetate at 110℃; for 14h; | 95% |
With oxygen; palladium diacetate In acetic acid at 80℃; under 760.051 Torr; for 24h; | 91% |
With copper diacetate; palladium diacetate In N,N-dimethyl-formamide at 130℃; for 1h; Sealed tube; Microwave irradiation; | 84% |
Conditions | Yield |
---|---|
With sodium; lithium In tetrahydrofuran for 24h; Heating; | 95% |
C18H22BNO2
9H-carbazole
Conditions | Yield |
---|---|
With copper diacetate; potassium carbonate In toluene at 110℃; for 1h; Reagent/catalyst; Temperature; Solvent; | 95% |
9H-carbazole
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 1h; Wavelength; Temperature; Solvent; Inert atmosphere; Irradiation; | 95% |
Conditions | Yield |
---|---|
In toluene at 60℃; for 16h; Molecular sieve; | A 88.3% B 94.1% |
Conditions | Yield |
---|---|
With boron trifluoride In benzene for 0.166667h; Ambient temperature; | A 3% B 94% |
9H-carbazole
Conditions | Yield |
---|---|
With water at 20℃; for 1h; | 94% |
2-bromodiphenylamine
9H-carbazole
Conditions | Yield |
---|---|
With palladium diacetate; potassium carbonate; tricyclohexylphosphine tetrafluoroborate In N,N-dimethyl acetamide at 130℃; | 94% |
With potassium tert-butylate; ammonia for 0.5h; UV-irradiation; | 93% |
With rubidium carbonate; tri(cyclohexylmethyl)acetic acid; palladium dichloride at 60℃; for 24h; Inert atmosphere; Schlenk technique; | 74% |
With 6-methoxy quinoline; palladium diacetate; potassium carbonate In 1-methyl-pyrrolidin-2-one at 135℃; for 48h; Sealed tube; | 50% |
With sodium carbonate; palladium diacetate In N,N-dimethyl-formamide for 15h; Cyclization; Heating; | 41% |
Conditions | Yield |
---|---|
With 4-tert-Butylcatechol In chloroform; water at 20℃; for 18h; | 94% |
9-benzyl-9H-carbazole
9H-carbazole
Conditions | Yield |
---|---|
With potassium tert-butylate; oxygen; dimethyl sulfoxide at 25℃; for 0.166667h; | 93% |
With aluminium trichloride In various solvent(s) for 3h; Ambient temperature; | 85% |
With aluminium trichloride; methoxybenzene | 85% |
1-diphenylmethyl-4-<2-(9-carbazolyl)ethyl>pyridinium bromide
9H-carbazole
Conditions | Yield |
---|---|
With 2,3,5-trimethyl-pyridine In ethanol for 29h; Heating; | 93% |
With sodium In pyridine; acetonitrile for 4.5h; Heating; | 78% |
1-(9H-carbazol-9-yl)-2,2-dimethylpropan-1-one
9H-carbazole
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran at 40 - 45℃; | 93% |
With n-butyllithium; diisopropylamine In tetrahydrofuran; hexanes at -78 - 45℃; for 2h; Inert atmosphere; | 93% |
Conditions | Yield |
---|---|
With ammonium hydroxide; 10 wt% Pd(OH)2 on carbon; sodium formate; trifluoroacetic acid In m-xylene at 140℃; for 24h; Reagent/catalyst; Temperature; Inert atmosphere; | 92% |
With ammonium hydroxide; ammonium sulfite monohydrate at 200℃; for 288h; Autoclave; | 12% |
With ammonia; water at 260℃; |
Conditions | Yield |
---|---|
With dimethylsulfide at 155℃; | A 92% B 6% |
With aluminium trichloride In dichloromethane Ambient temperature; | A 83% B 2% |
With aluminium trichloride In dichloromethane Ambient temperature; | A 83% B n/a |
With tetrabutylammonium tricarbonylnitrosylferrate In 1,2-dichloro-ethane at 100℃; for 16h; Inert atmosphere; Schlenk technique; |
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate at 60℃; | A 3% B 92% |
trans-9-(2-Acetoxyvinyl)carbazole
9H-carbazole
Conditions | Yield |
---|---|
With hydrogenchloride In 1,4-dioxane at 20℃; for 27h; | 92% |
A
tetrakis(triphenylphosphine) palladium(0)
B
9H-carbazole
Conditions | Yield |
---|---|
1 h, room temp.; | A n/a B 92% |
Conditions | Yield |
---|---|
Stage #1: 9H-carbazole With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 0.5h; Stage #2: methyl iodide In N,N-dimethyl-formamide | 100% |
With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; | 96% |
With sodium hydroxide In N,N-dimethyl-formamide at 2℃; for 4h; | 95% |
Conditions | Yield |
---|---|
100% | |
98.1% | |
93.1% | |
With sodium amide; toluene und Erwaermen des Reaktionsgemisches mit Aethylbromid; | |
Multi-step reaction with 2 steps 1: potassium hydroxide; decalin / 170 °C 2: nickel; methanol / 80 °C / 11032.6 Torr / Hydrogenation View Scheme |
Conditions | Yield |
---|---|
With potassium hydroxide In tetrahydrofuran for 48h; Heating; | 100% |
With potassium hydroxide; PEG-400-Et2 In water; benzene at 30℃; for 3h; | 97% |
With tetrabutylammomium bromide; potassium carbonate for 0.0666667h; Irradiation; | 95% |
Conditions | Yield |
---|---|
Stage #1: 9H-carbazole With potassium hydroxide In dimethyl sulfoxide at 50℃; for 0.5h; Stage #2: allyl bromide In dimethyl sulfoxide for 0.25h; | 100% |
Stage #1: 9H-carbazole With potassium hydroxide In dimethyl sulfoxide at 20℃; for 0.333333h; Stage #2: allyl bromide In dimethyl sulfoxide at 35℃; for 0.5h; Solvent; Sonication; | 98% |
With caesium carbonate In N,N-dimethyl-formamide at 26℃; for 8h; | 97% |
Conditions | Yield |
---|---|
With trifluoroacetic acid Heating; | 100% |
9H-carbazole
N-chlorocarbazole
Conditions | Yield |
---|---|
With sodium hypochlorite In dichloromethane for 48h; | 100% |
With sodium hypochlorite In dichloromethane; water for 48h; Yield given; |
Conditions | Yield |
---|---|
With dmap In acetonitrile for 1.75h; | 100% |
Stage #1: 9H-carbazole With hydrogenchloride In water at -5 - 0℃; for 0.5h; Stage #2: di-tert-butyl dicarbonate In water at -5 - 0℃; for 1h; | 91.2% |
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; sodium hydroxide In toluene at 120℃; | 100% |
With sodium hydroxide; triethylamine hydrochloride In water; dimethyl sulfoxide at 80℃; for 8h; | 97.4% |
With tetrabutylammomium bromide; sodium hydroxide In water; toluene for 24h; Inert atmosphere; Reflux; | 96% |
Di-tert-butyl acetylenedicarboxylate
9H-carbazole
d t-butyl 2-(carbazol-9-yl)-2-butene-1,4-dicarboxylate
Conditions | Yield |
---|---|
With 1-methyl-1H-imidazole In dichloromethane at 20℃; for 4h; optical yield given as %de; | 100% |
9H-carbazole
acetylenedicarboxylic acid diethyl ester
diethyl 2-(carbazol-9-yl)-2-butene-1,4-dicarboxylate
Conditions | Yield |
---|---|
With 1-methyl-1H-imidazole In dichloromethane at 20℃; for 4h; optical yield given as %de; | 100% |
9H-carbazole
bis(5-bromomethyl-1,3-phenylene)-32-crown-10
bis[5-(N-carbazylmethyl)-1,3-phenylene]-32-crown-10
Conditions | Yield |
---|---|
Stage #1: 9H-carbazole With sodium hydride In tetrahydrofuran at 20℃; for 1h; Inert atmosphere; Reflux; Stage #2: bis(5-bromomethyl-1,3-phenylene)-32-crown-10 In tetrahydrofuran at 20℃; for 24.5h; Inert atmosphere; Reflux; | 100% |
Conditions | Yield |
---|---|
Stage #1: 9H-carbazole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃; Stage #2: C18H10FNO3 In N,N-dimethyl-formamide; mineral oil at 20℃; for 3h; | 100% |
9H-carbazole
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; sodium hydroxide In water; toluene for 48h; Reflux; | 100% |
9H-carbazole
Ethyl 2-bromopropionate
ethyl 2-(9H-carbazol-9-yl)propanoate
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide; paraffin oil at 20℃; for 3h; Inert atmosphere; | 100% |
Stage #1: 9H-carbazole With sodium hydride In N,N-dimethyl-formamide at 0℃; Schlenk technique; Inert atmosphere; Stage #2: Ethyl 2-bromopropionate In N,N-dimethyl-formamide at 0 - 20℃; Schlenk technique; Inert atmosphere; |
9H-carbazole
Conditions | Yield |
---|---|
With sodium t-butanolate In tetrahydrofuran at 20℃; Inert atmosphere; Glovebox; Darkness; | 100% |
9H-carbazole
2'-aminobiphenyl-2,3-diol
Conditions | Yield |
---|---|
With Escherichia coli JM109 In dimethyl sulfoxide at 30℃; for 18h; L-medium; Enzymatic reaction; | 99.1% |
Conditions | Yield |
---|---|
Stage #1: 9H-carbazole With methylmagnesium chloride In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene at 5 - 20℃; for 0.166667h; Inert atmosphere; Stage #2: 2-Chloroquinoline With PdCl(π-allyl)(cyclohexyl-(1-methyl-2,2-diphenylcyclopropylphophine)) In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene at 108 - 112℃; for 0.25h; Inert atmosphere; | 99% |
With [(1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene)Ni(styrene)2]; lithium tert-butoxide In 1,4-dioxane at 110℃; for 2h; Inert atmosphere; | 94% |
With iodine; copper; potassium carbonate |
Conditions | Yield |
---|---|
With copper(l) iodide; 1,10-Phenanthroline; potassium hydroxide In 1,2-dimethoxyethane; water at 95℃; for 20h; Catalytic behavior; Solvent; Schlenk technique; Inert atmosphere; Sealed tube; | 99% |
With Cu(HOC6H3(O)CHNCH2CH2NCHC6H3(O)OH); sodium hydroxide at 120℃; for 8h; | 90% |
With copper(l) iodide; cesium fluoride; N,N`-dimethylethylenediamine In tetrahydrofuran at 25℃; for 18 - 24h; Inert atmosphere; | 88% |
Conditions | Yield |
---|---|
With copper(l) iodide; 1,10-Phenanthroline; potassium hydroxide In 1,2-dimethoxyethane; water at 95℃; for 20h; Catalytic behavior; Solvent; Schlenk technique; Inert atmosphere; Sealed tube; | 99% |
With copper; potassium carbonate In N,N-dimethyl-formamide at 130℃; for 42h; Inert atmosphere; | 96% |
With copper(I) oxide; 2,2,6,6-tetramethylheptane-3,5-dione; potassium hydroxide In N,N-dimethyl-formamide at 110℃; for 24h; Inert atmosphere; Schlenk technique; | 95% |
Conditions | Yield |
---|---|
Stage #1: 9H-carbazole With potassium hydroxide In dimethyl sulfoxide at 20℃; for 0.333333h; Stage #2: ethyl bromide In dimethyl sulfoxide at 35℃; for 0.05h; Solvent; Sonication; | 99% |
With sodium hydroxide In N,N-dimethyl-formamide at 20℃; for 0.666667h; Cooling with ice; | 95% |
With potassium hydroxide; PEG-400-Et2 In water; benzene at 30℃; for 2h; | 92% |
Conditions | Yield |
---|---|
With copper(l) iodide; trans-1,2-Diaminocyclohexane; potassium carbonate In dimethyl sulfoxide at 140℃; Inert atmosphere; | 99% |
With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; caesium carbonate In toluene at 100℃; for 12h; | 97% |
With 1,1'-bis-(diphenylphosphino)ferrocene; tetrakis(triphenylphosphine) palladium(0); caesium carbonate In toluene at 100℃; for 24h; Glovebox; Inert atmosphere; | 92% |
9H-carbazole
4-benzyloxybenzyl chloride
9-(4-Benzyloxy-benzyl)-9H-carbazole
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide Ambient temperature; | 99% |
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; potassium carbonate; tris-(dibenzylideneacetone)dipalladium(0); 18-crown-6 ether In o-xylene at 20 - 120℃; for 2h; Product distribution / selectivity; | 99% |
Stage #1: 9H-carbazole With methylmagnesium chloride In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene at 5 - 20℃; for 0.166667h; Inert atmosphere; Stage #2: bromobenzene With PdCl(π-allyl)(cyclohexyl-(1-methyl-2,2-diphenylcyclopropylphophine)) In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene at 108 - 112℃; for 0.5h; Inert atmosphere; | 99% |
With di-tert-butyl(2,2-diphenyl-1-methyl-1-cyclopropyl)phosphine; bis(η3-allyl-μ-chloropalladium(II)); sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene at 120℃; for 3h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; (S,S)-1,2-diaminocyclohexane In 1,4-dioxane; dodecane at 110℃; for 24h; | 99% |
With copper(I) oxide; potassium phosphate; N1,N2-bis(furan-2-ylmethyl)oxalamide In acetonitrile at 80℃; | 94% |
With copper(l) iodide; 1,10-Phenanthroline; potassium hydroxide In 1,2-dimethoxyethane; water at 95℃; for 20h; Catalytic behavior; Solvent; Schlenk technique; Inert atmosphere; Sealed tube; | 91% |
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene at 90℃; for 7h; Product distribution; Further Variations:; Temperatures; Solvents; Pressures; Reagents; reaction times; microwave irradiation; | 99% |
With 1,4-diaza-bicyclo[2.2.2]octane In N,N-dimethyl-formamide at 94 - 95℃; for 24h; | 97% |
With 1,4-diaza-bicyclo[2.2.2]octane at 90 - 95℃; for 24h; | 97% |
Conditions | Yield |
---|---|
With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide In water; toluene at 80℃; for 14h; | 99% |
With potassium hydroxide In acetone Reflux; | 99% |
Stage #1: 9H-carbazole With potassium hydroxide In N,N-dimethyl-formamide at 20℃; for 0.666667h; Stage #2: 1-bromo-hexane In N,N-dimethyl-formamide at 20℃; for 9h; | 98% |
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