As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:51-36-5
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryProduct description: Product name 3,5-Dichlorobenzoic acid CAS number 51-36-5 Assay ≥99% Appearance Off-white powder Capacity 200mt/year Application Pesticide/pharmaceutical
Cas:51-36-5
Min.Order:10 Gram
FOB Price: $12.0
Type:Lab/Research institutions
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:51-36-5
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, intermedi
Cas:51-36-5
Min.Order:1 Kilogram
FOB Price: $5.0
Type:Manufacturers
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:51-36-5
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:51-36-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
Cas:51-36-5
Min.Order:1 Kilogram
FOB Price: $15.0 / 50.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:51-36-5
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryName: 3,5-Dichlorobenzoic acid Synonyms: 3,5-Dichlorobenzoic; 3,5-dichlorobenzoate CAS: 51-36-5 MF: C7H4Cl2O2 Appearance:White powder Storage:Store in cool and dry place, away from sun light. Package:25kg/drum Application:Pharmaceutical Interme
1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:51-36-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:51-36-5
Min.Order:5 Gram
FOB Price: $10.0 / 25.0
Type:Trading Company
inquiry3,5-Dichlorobenzoic acid CAS:51-36-50 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic in
Cas:51-36-5
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:51-36-5
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff
Cas:51-36-5
Min.Order:100 Gram
Negotiable
Type:Other
inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:51-36-5
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
advantage: 1. The best price, satisfactory quality; 2. customers have the right to choose the delivery of parcels (EMS, DHL, FedEx, UPS); 3. customers have the right to choose from the recent effective packaging methods of their products packaging
superior quality Appearance:White to beige powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used as Pharmaceutical Intermediates Transportat
Product name: 3,5-Dichlorobenzoic Acid CAS No.:51-36-5 Molecule Formula:C7H4Cl2O2 Molecule Weight:190.00 Purity: 98.0% Package: 25kg/drum Description:White or off-white powder Manufacture Standards:Enterprise Standard
Cas:51-36-5
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiry3,5-Dichlorobenzoic acid Basic information Product Name: 3,5-Dichlorobenzoic acid Synonyms: BENZOIC ACID, 3,5-DICHLORO-;BUTTPARK 45\07-34;RARECHEM AL BO 0040;3.5-Dichlorobe;3, 5-Dichlorobenzoic acid, MTBE;3,5-Dichlorobenzoic Acid Standard;3,5-D
Cas:51-36-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed produc
Cas:51-36-5
Min.Order:1 Kilogram
FOB Price: $32.0 / 52.0
Type:Lab/Research institutions
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:51-36-5
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryLocated in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service an
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
1.High quality : the purity is 99% min . through multiple producing procedures. 2.Competitive price : low price because of our skilled production technolpgy ,save the production cost at most , and give big profit room to our customers 3.Safe a
High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
Conditions | Yield |
---|---|
Stage #1: 1,3,5-trichlorobenzene With magnesium; ethylene dibromide; lithium chloride In tetrahydrofuran at 25℃; for 0.5h; Stage #2: carbon dioxide In tetrahydrofuran at 25℃; for 1h; Further stages; | 99% |
Conditions | Yield |
---|---|
With water; sodium hydroxide for 6h; Reflux; | 93% |
With sulfuric acid |
3,5-dichloro-4-(triethylsilyl)benzoic acid
3,5-dichlorobenzoic acid
Conditions | Yield |
---|---|
With potassium hydroxide In methanol; water for 2h; Heating; | 91% |
Conditions | Yield |
---|---|
Stage #1: 1-bromo-3,5-dichlorobenzene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Inert atmosphere; Stage #2: carbon dioxide In tetrahydrofuran; hexane at -78 - 20℃; | 80.1% |
Conditions | Yield |
---|---|
With chlorine In hydrogenchloride; ethanol; water | 75% |
Conditions | Yield |
---|---|
With tetrahydrofuran; tert.-butylnitrite; dimethyl sulfoxide at 30℃; for 1h; Green chemistry; | 64% |
In ethanol | |
With sodium nitrite In water; isopropyl alcohol | |
With hydrogenchloride; sodium nitrite In ethanol; water | |
With sodium nitrite In water; isopropyl alcohol |
Conditions | Yield |
---|---|
With copper(II) tetrafluroborate hexahydrate; sodium chloride In water; acetone at -25 - 10℃; for 1h; Sandmeyer Reaction; chemoselective reaction; | A 21% B 40% |
3,5-dichlorobenzaldehyde
A
3,5-dichlorobenzyl alcohol
B
3,5-dichlorobenzoic acid
Conditions | Yield |
---|---|
With potassium hydroxide | |
With potassium hydroxide |
Conditions | Yield |
---|---|
With copper chloride Diazotization; |
3,5-dichlorotoluene
3,5-dichlorobenzoic acid
Conditions | Yield |
---|---|
With nitric acid at 170℃; | |
With chlorine at 185 - 190℃; Irradiation.anschliessendes Behandeln mit H2SO4 <8prozent SO3 enthaltend>; |
3-nitro-5-sulfo-benzoic acid
3,5-dichlorobenzoic acid
Conditions | Yield |
---|---|
With phosphorus pentachloride at 180 - 200℃; |
4-amino-3,5-dichlorobenzoic acid
3,5-dichlorobenzoic acid
Conditions | Yield |
---|---|
With potassium disulphite; nitric acid Diazotization.Erwaermen der Diazoloesung mit Alkohol und Kupfersulfat; | |
With hydrogenchloride; copper(l) chloride; sodium nitrite 1) DMF 2) a) 30 min, 0-5 deg C b) 1h, r.t. c) 70 deg C; Yield given. Multistep reaction; |
4-amino-3,5-dichlorobenzoic acid
A
3,5-dichlorobenzoic acid
B
3,5-dichloro-1-nitrobenzene
Conditions | Yield |
---|---|
With potassium disulphite; nitric acid Diazotization.Erwaermen der mit Eiswasser verduennten Diazoniumsalz-Loesung mit Alkohol in Gegenwart von Kupfersulfat; |
Thiosalicylic acid
A
3,5-dichlorobenzoic acid
B
2,2'-dithiobis<5-chlorobenzoic acid>
Conditions | Yield |
---|---|
With tetrachloromethane; chlorine; iron(III) chloride Erhitzen der in Wasser loeslichen Anteile des Reaktionsprodukts mit wss. Ammoniak; |
1,3,5-trichlorobenzene
carbon dioxide
A
3,5-dichlorobenzoic acid
B
chlorobenzene
C
3-chlorobenzoate
D
1,3-Dichlorobenzene
Conditions | Yield |
---|---|
With tetrabutylammomium bromide In N,N-dimethyl-formamide at 5℃; electrolysis (I=0.4 A); Yield given. Yields of byproduct given; |
3,5-dichlorobenzaldehyde
3,5-dichlorobenzoic acid
Conditions | Yield |
---|---|
With rat hepatic microsomal aldehyde dehydrogenase; NAD In phosphate buffer; N,N-dimethyl-formamide at 37℃; pH=7.4; Enzyme kinetics; Dehydrogenation; |
tetrachloromethane
chlorine
iron(III) chloride
Thiosalicylic acid
A
3,5-dichlorobenzoic acid
B
2,2'-dithiobis<5-chlorobenzoic acid>
C
3-chlorobenzoate
Conditions | Yield |
---|---|
at 20℃; Erhitzen der in Wasser loeslichen Anteile des Reaktionsprodukts mit wss. Ammoniak; |
3',5'-dichloroacetophenone
3,5-dichlorobenzoic acid
Conditions | Yield |
---|---|
at 145℃; |
1,3-dichloro-5-dichloromethyl-benzene
water
A
3,5-dichlorobenzyl alcohol
B
3,5-dichlorobenzoic acid
Conditions | Yield |
---|---|
at 200℃; |
phosphorus pentachloride
3-nitro-5-sulfo-benzoic acid
3,5-dichlorobenzoic acid
Conditions | Yield |
---|---|
at 180 - 200℃; Kochen das Reaktionsprodukt mit Kalilauge; |
4-amino-3,5-dichlorobenzoic acid
nitric acid
A
3,5-dichlorobenzoic acid
B
3,5-dichloro-1-nitrobenzene
Conditions | Yield |
---|---|
Erwaermen der erhaltenen Diazoniumsalz-Loesung mit waessrig-alkoholischer Kupfersulfatloesung.Diazotization; |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 89 percent / sec-butyllithium / cyclohexane; tetrahydrofuran / -75 °C 2: 71 percent / sec-butyllithium / cyclohexane; tetrahydrofuran / 0.75 h / -75 °C 3: 91 percent / potassium hydroxide / methanol; H2O / 2 h / Heating View Scheme |
(2,6-dichlorophenyl)triethylsilane
3,5-dichlorobenzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 71 percent / sec-butyllithium / cyclohexane; tetrahydrofuran / 0.75 h / -75 °C 2: 91 percent / potassium hydroxide / methanol; H2O / 2 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 45 percent / SO2Cl2 / acetic acid / 1.42 h / 60 °C 2: 1) NaNO2, conc. HCl 2) CuCl, dil. HCl / 1) DMF 2) a) 30 min, 0-5 deg C b) 1h, r.t. c) 70 deg C View Scheme |
N-(2-chloro-4-methylphenyl)acetamide
3,5-dichlorobenzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: glacial acetic acid; chlorine 2: concentrated hydrochloric acid / 100 - 120 °C 3: concentrated sulfuric acid; ethyl nitrite; alcohol 4: diluted nitric acid / 170 °C View Scheme |
2,6-dichloro-4-methylaniline
3,5-dichlorobenzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: concentrated sulfuric acid; ethyl nitrite; alcohol 2: diluted nitric acid / 170 °C View Scheme |
acetic acid-(2,6-dichloro-4-methyl-anilide)
3,5-dichlorobenzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: concentrated hydrochloric acid / 100 - 120 °C 2: concentrated sulfuric acid; ethyl nitrite; alcohol 3: diluted nitric acid / 170 °C View Scheme |
Conditions | Yield |
---|---|
With thionyl chloride for 5h; Reflux; | 100% |
With thionyl chloride; N,N-dimethyl-formamide In toluene for 3h; Reflux; | 100% |
With thionyl chloride |
3,5-dichlorobenzoic acid
tert-butyl 4-(aminomethyl)piperidine-1-carboxylate
tert-butyl 4-{[(3,5-dichlorobenzoyl)amino]methyl}piperidine-1-carboxylate
Conditions | Yield |
---|---|
With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane; N,N-dimethyl-formamide at 20℃; | 100% |
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 16h; |
3,5-dichlorobenzoic acid
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 24h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 16h; | 99% |
Conditions | Yield |
---|---|
Stage #1: 3,5-dichlorobenzoic acid With sodium tetrahydroborate In tetrahydrofuran at 60℃; for 0.2h; Inert atmosphere; Stage #2: With potassium chloride In tetrahydrofuran at 110℃; under 1520.1 Torr; for 4h; Temperature; Reagent/catalyst; Solvent; Pressure; Sonication; Inert atmosphere; | 98.8% |
Multi-step reaction with 2 steps 1: LiAlH4 / tetrahydrofuran / 0 °C / r.t., overnight 2: SOCl2 / 2 h / reflux View Scheme | |
Multi-step reaction with 2 steps 1: borane-THF / tetrahydrofuran / 2 h / 0 - 20 °C 2: thionyl chloride / 2 h / 60 °C View Scheme |
Conditions | Yield |
---|---|
With 4-methyl-morpholine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate In dichloromethane for 2h; | 98% |
Conditions | Yield |
---|---|
With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane for 2h; | 97% |
(2R,4S)-2-benzyl-4-piperidine azide
3,5-dichlorobenzoic acid
(2R,4S)-2-benzyl-1-(3,5-dichlorobenzoyl)-4-piperidine azide
Conditions | Yield |
---|---|
With thionyl chloride | 96% |
3,5-dichlorobenzoic acid
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 0 - 20℃; | 96% |
3,5-dichlorobenzoic acid
(1S)-1-<(2R)-2-(2,4-difluorophenyl)-2-oxiranyl>ethanol
Conditions | Yield |
---|---|
Stage #1: 3,5-dichlorobenzoic acid With di-isopropyl azodicarboxylate; triphenylphosphine In toluene at 0℃; for 1.5h; Stage #2: (1S)-1-<(2R)-2-(2,4-difluorophenyl)-2-oxiranyl>ethanol In toluene for 2h; | 96% |
3,5-dichlorobenzoic acid
3,5-dichloro-2-nitrobenzoic acid
Conditions | Yield |
---|---|
With sulfuric acid; nitric acid at 20℃; for 2.5h; | 95.3% |
With Concentrated HNO3 In sulfuric acid; water | 94% |
With sulfuric acid; nitric acid at 0℃; | 80% |
3,5-dichlorobenzoic acid
sodium methylate
3-chloro-5-methoxy-benzoic acid
Conditions | Yield |
---|---|
With HMPA at 120℃; for 48h; | 95% |
With N,N,N,N,N,N-hexamethylphosphoric triamide In methanol at 115 - 120℃; for 15h; | 80% |
With N,N,N,N,N,N-hexamethylphosphoric triamide at 115 - 120℃; for 15h; | 54% |
3,5-dichlorobenzoic acid
monomethyl monopotassium malonate
Conditions | Yield |
---|---|
Stage #1: monomethyl monopotassium malonate With magnesium chloride In tetrahydrofuran Reflux; Stage #2: 3,5-dichlorobenzoic acid With 1,1'-carbonyldiimidazole In tetrahydrofuran at 20℃; | 95% |
3,5-dichlorobenzoic acid
[3,5-D2]benzoic acid
Conditions | Yield |
---|---|
With deuterated hypophosphorous acid; palladium 10% on activated carbon; sodium carbonate In water-d2 at 50℃; regioselective reaction; | 94% |
3,5-dichlorobenzoic acid
Conditions | Yield |
---|---|
With trichlorophosphate at 110 - 120℃; Reflux; | 93% |
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 18h; Inert atmosphere; | 93% |
3,5-dichlorobenzoic acid
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 18h; | 92% |
3,5-dichlorobenzoic acid
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 18h; | 92% |
2-amino-8-quinolinol
3,5-dichlorobenzoic acid
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 20℃; for 3h; Reagent/catalyst; Cooling with ice; Inert atmosphere; chemoselective reaction; | 90% |
3,5-dichlorobenzoic acid
triphenylbismuth dibromide
Conditions | Yield |
---|---|
With triethylamine In toluene for 2h; Inert atmosphere; | 90% |
tris(p‐tolyl)bismuth dibromide
3,5-dichlorobenzoic acid
Conditions | Yield |
---|---|
With triethylamine In toluene for 2h; Inert atmosphere; | 90% |
3,5-dichlorobenzoic acid
5,7-dimethoxy-1H-quinolin-4-one
5,7-dimethoxyquinolin-4-yl 3,5-dichlorobenzoate
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; | 88% |
goniothalenol
3,5-dichlorobenzoic acid
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; | 88% |
3,5-dichlorobenzoic acid
3-amino-2-mercapto-5,6,7,8-tetrahydro-3H-benzo[4,5]thieno[2,3-d]pyrimidin-4-one
Conditions | Yield |
---|---|
With trichlorophosphate Heating; | 87% |
3,5-dichlorobenzoic acid
3,5-dichlorobenzyl alcohol
Conditions | Yield |
---|---|
With borane-THF In tetrahydrofuran at 0 - 20℃; for 2h; | 86.9% |
With lithium aluminium tetrahydride; potassium borohydride In tetrahydrofuran at 5 - 20℃; for 3h; | 75% |
With lithium aluminium tetrahydride | |
With sodium hydroxide; polymethylhydrosiloxane; tetrabutyl ammonium fluoride 1.) THF, room t., 2.) THF; Yield given. Multistep reaction; | |
With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; Reduction; r.t., overnight; |
Conditions | Yield |
---|---|
Stage #1: 3,5-dichlorobenzoic acid; 2-[5-amino-2-[(1r,4r)-4-(hydroxymethyl)cyclohexyl]indazol-6-yl]propan-2-ol trifluoroacetate With 2-chloro-1-methyl-pyridinium iodide; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 25℃; for 1h; Inert atmosphere; Stage #2: formic acid Inert atmosphere; | 86% |
3,5-dichlorobenzoic acid
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 16h; Inert atmosphere; | 85% |
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