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inquiryName: Ethyl glyoxalate Synonmys: Ethyl glyoxylate; Glyoxylic acid ethyl ester; Ethyl oxoacetate; Glyoxylic acid ethyl ester; Oxoacetic acid ethyl ester; ethyl oxoacetate; ethyl 2-oxoacetate CAS: 924-44-7 MF: C4H6O3 Appearance:Colorless Clear Liqui
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inquiryProduct Name: Ethyl glyoxalate CAS: 924-44-7 MF: C4H6O3 MW: 102.09 EINECS: 213-105-3 Mol File: 924-44-7.mol Ethyl glyoxalate Structure Ethyl glyoxalate Chemical Properties Boiling point 110°C density 1.03 g/mL at 20 &d
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inquiryProduct name: Ethyl Glyoxalate CAS No.:924-44-7 Molecule Formula: C4H6O3 Molecule Weight:102.08 Purity: 99.0% Package: 25kg/drum Description:Colorless transparent liquid Manufacture Standards:Enterprise Standard TESTING ITEMS
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inquiryDiethylamino-selenoxo-acetic acid ethyl ester
glyoxylic acid ethyl ester
Conditions | Yield |
---|---|
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 0℃; for 3h; | 100% |
Conditions | Yield |
---|---|
With sodium periodate In dichloromethane; water Heating; | 94% |
With sodium periodate In water at 0℃; for 0.25h; | 66% |
With periodic acid In diethyl ether at 20℃; for 1h; |
Ethyl diethoxyacetate
2,2-dihydroxyacetic acid
glyoxylic acid ethyl ester
Conditions | Yield |
---|---|
Stage #1: Ethyl diethoxyacetate; 2,2-dihydroxyacetic acid With toluene-4-sulfonic acid at 90℃; for 27h; Stage #2: With phosphorus pentoxide at 90 - 100℃; for 2h; | 90% |
diethyl (2S,3S)-tartrate
glyoxylic acid ethyl ester
Conditions | Yield |
---|---|
With periodic acid In diethyl ether; water for 1h; Inert atmosphere; | 82% |
With periodic acid In diethyl ether at 0 - 20℃; for 3h; Inert atmosphere; Cooling with ice; | 80% |
Conditions | Yield |
---|---|
With aluminum oxide; tetrabutylammomium bromide; oxygen; cyclohexene In acetonitrile Hg cathode, Pt anode, -1.0 V vs SCE; | 72% |
N-(ethoxy carbonyl methoxy)-phthalimide
A
phthalimide
B
glyoxylic acid ethyl ester
Conditions | Yield |
---|---|
at 400℃; under 0.01 Torr; for 2.77778E-06h; Kinetics; Temperature; | A 57% B 22% |
Conditions | Yield |
---|---|
With ozone at 20.84℃; under 760 Torr; Kinetics; Darkness; | A 45% B 53% |
Diethyl tartrate
glyoxylic acid ethyl ester
Conditions | Yield |
---|---|
In water periodate oxidation; | 50% |
With lead(IV) acetate; acetic acid at 40 - 50℃; | |
With periodic acid |
ethyl 3-ethoxypropionate
A
glyoxylic acid ethyl ester
B
3-oxo-propionic acid ethyl ester
C
acetaldehyde
E
formic acid ethyl ester
Conditions | Yield |
---|---|
With dodecane; methyl nitrite; nitrogen(II) oxide at 23.9℃; under 760 Torr; Rate constant; Product distribution; Mechanism; Irradiation; | A 25% B 4.8% C 4.9% D 30% E 37% |
(+/-)-diethyl tartrate
glyoxylic acid ethyl ester
Conditions | Yield |
---|---|
With sodium bismuthate; phosphoric acid; water at 40℃; | |
With lead dioxide; acetic acid |
Conditions | Yield |
---|---|
bei laengerem Durchleiten von Luft in der Waerme und am Licht; |
Conditions | Yield |
---|---|
zerfaellt in der Waerme; |
Conditions | Yield |
---|---|
bei der Ozonspaltung; |
Conditions | Yield |
---|---|
bei der Ozonspaltung; |
tetrachloromethane
1,3-dioxo-indan-2-carboxylic acid ethyl ester
A
glyoxylic acid ethyl ester
B
methylammonium carbonate
C
benzene-1,2-dicarboxylic acid
Conditions | Yield |
---|---|
at -20℃; bei der Ozonspaltung; |
diethyl (2R,3R)-tartrate
lead(IV) tetraacetate
acetic acid
glyoxylic acid ethyl ester
Conditions | Yield |
---|---|
at 18℃; Geschwindigkeit; |
diethyl (2E)-3-methyl-2-pentenedioate
ethyl acetate
A
glyoxylic acid ethyl ester
B
ethyl acetoacetate
Conditions | Yield |
---|---|
Liefert bei der Ozonisierung ein oeliges Ozonid,das bei mehrstuendiger Einw. von Wasser; |
4-methyl-3-phenyl-pentenedioic acid diethyl ester
ethyl acetate
A
glyoxylic acid ethyl ester
B
oxalic acid
C
propionic acid
D
ethyl 2-benzoylpropionate
Conditions | Yield |
---|---|
at 0℃; beim Ozonisieren und Zersetzen des Ozonids mit Wasser; substance of bp 5-6: 165-166 degree; |
Conditions | Yield |
---|---|
With dimethyl sulfoxide at 70℃; | |
With trimethylamine-N-oxide In chloroform |
Conditions | Yield |
---|---|
With sodium amalgam; ethanol | |
durch elektrolytische Reduktion; |
Conditions | Yield |
---|---|
With potassium fluoride |
Conditions | Yield |
---|---|
bei der Ozonspaltung; |
methyl iodide
A
2-acetylpropanoic acid ethyl ester
B
glyoxylic acid ethyl ester
C
ethyl acetoacetate
Conditions | Yield |
---|---|
Das Kaliumverbindung reagiert,bei der Ozonspaltung des erhaltenen Produkts; |
ethyl 2-ethoxyglycolate
glyoxylic acid ethyl ester
Conditions | Yield |
---|---|
Heating; | |
acid; |
3-tert-Butyl-4,4-dimethyl-penten-(2)-saeure-ethylester
glyoxylic acid ethyl ester
Conditions | Yield |
---|---|
With ozone In ethyl acetate |
glyoxylic acid ethyl ester
Conditions | Yield |
---|---|
With sodium bismuthate; phosphoric acid |
Conditions | Yield |
---|---|
With dimethylsulfide; ozone 1.) CH2Cl2, -78 deg C, 2.25 h, 2.) 25 deg C, overnight; Yield given. Multistep reaction; | |
With potassium permanganate at 40℃; | 47.9 % Chromat. |
With ozone In dichloromethane at -78℃; |
ethyl (dimethylsulfuranylidene)acetate
A
glyoxylic acid ethyl ester
B
dimethylsulfone
C
ethyl 2-(dimethyl(oxo)-λ6-sulfaneylidene)acetate
D
dimethyl sulfoxide
Conditions | Yield |
---|---|
With triphenyl phosphite ozonide In dichloromethane 1.) -78 deg C to -60 deg C, 3 h, 2.) -60 deg C to 20 deg C; |
acetaldehyde
3-Methyl-5-(toluene-4-sulfonyl)-4-p-tolyl-1,5-dihydro-pyrrol-2-one
A
glyoxylic acid ethyl ester
Conditions | Yield |
---|---|
With tributylphosphine; 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran Ambient temperature; Yield given. Yields of byproduct given; |
glyoxylic acid ethyl ester
ethyl 2-(hydroxyimino)acetate
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; triethylamine In water; toluene; acetonitrile at 20℃; for 1h; | 100% |
Stage #1: glyoxylic acid ethyl ester With hydroxylamine hydrochloride In water; toluene; acetonitrile at 20℃; for 0.0833333h; Stage #2: With triethylamine In water; toluene; acetonitrile at 20℃; | 97% |
With hydroxylamine hydrochloride; triethylamine In water; toluene; acetonitrile at 20℃; for 1.5h; Inert atmosphere; | 95% |
glyoxylic acid ethyl ester
(S)-1-phenyl-ethylamine
ethyl <(S)-1-phenylethyl>iminoethanoate
Conditions | Yield |
---|---|
In toluene for 0.333333h; Heating; | 100% |
In toluene at 110℃; under 760.051 Torr; | 100% |
glyoxylic acid ethyl ester
(R)-1-phenyl-ethyl-amine
((R)-1-phenyl-ethylimino)-acetic acid ethyl ester
Conditions | Yield |
---|---|
In toluene for 0.333333h; Heating; | 100% |
In toluene Heating; | 100% |
In toluene at 15 - 25℃; | 95% |
glyoxylic acid ethyl ester
trimethylsilyl cyanide
(+/-)-ethyl 2-cyano-2-hydroxyacetate
Conditions | Yield |
---|---|
With sodium acetate buffer In ethanol; water for 0.166667h; Ambient temperature; | 100% |
With sodium acetate; acetic acid In ethanol for 0.166667h; Ambient temperature; | 1.29 g |
Stage #1: glyoxylic acid ethyl ester With copper(II) bis(trifluoromethanesulfonate) In dichloromethane at 20℃; for 0.25h; Stage #2: trimethylsilyl cyanide In dichloromethane at 20℃; for 18h; |
glyoxylic acid ethyl ester
5-methylhex-4-en-1-amine
Ethyl (5-methyl-4-hexenylimino)acetate
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane at 0℃; | 100% |
glyoxylic acid ethyl ester
p-toluidine
ethyl 2-(4-methylphenylimino)acetate
Conditions | Yield |
---|---|
With sodium sulfate In dichloromethane for 0.5h; | 100% |
With magnesium sulfate In toluene at 25℃; for 0.5h; | 100% |
for 1h; Green chemistry; | 75% |
glyoxylic acid ethyl ester
4-chloro-aniline
(4-chloro-phenylimino)-acetic acid ethyl ester
Conditions | Yield |
---|---|
With magnesium sulfate In toluene at 25℃; for 0.5h; | 100% |
With sodium sulfate In toluene at 110℃; for 0.5h; | |
With sodium sulfate In toluene |
glyoxylic acid ethyl ester
4-methoxy-aniline
ethyl (4-methoxyphenylimino)acetate
Conditions | Yield |
---|---|
With sodium sulfate In dichloromethane for 0.5h; | 100% |
With magnesium sulfate In toluene at 25℃; for 0.5h; | 100% |
With magnesium sulfate In dichloromethane; toluene for 3h; Inert atmosphere; Reflux; | 100% |
glyoxylic acid ethyl ester
4-methoxy-aniline
ethyl (E)-2-(p-methoxyphenylimino)acetate
Conditions | Yield |
---|---|
With silica gel In dichloromethane; toluene for 20h; sonication; | 100% |
Stage #1: glyoxylic acid ethyl ester; 4-methoxy-aniline In dichloromethane; toluene at 20℃; for 2h; Schlenk technique; Inert atmosphere; Stage #2: In toluene for 3h; Schlenk technique; Inert atmosphere; Molecular sieve; | 100% |
In toluene for 22h; Inert atmosphere; Molecular sieve; | 100% |
glyoxylic acid ethyl ester
aniline
ethyl 2-(phenylimino)acetate
Conditions | Yield |
---|---|
With magnesium sulfate In toluene at 25℃; for 0.5h; | 100% |
With magnesium sulfate In toluene at 20℃; for 1.5h; Inert atmosphere; | 99% |
With sodium sulfate In toluene for 0.5h; Ambient temperature; |
glyoxylic acid ethyl ester
(R)-1-phenyl-ethyl-amine
<(R)-(1-phenylethyl)imino>acetic acid ethyl ester
Conditions | Yield |
---|---|
In toluene for 1.5h; Heating; | 100% |
With molecular sieve In dichloromethane at 0℃; |
Conditions | Yield |
---|---|
With magnesium sulfate In toluene at 120℃; for 2h; Condensation; | 100% |
In toluene Heating; |
glyoxylic acid ethyl ester
(+/-)-2-(2-aminopropyl)-2-methyl-1,3-dioxane
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane Condensation; Heating; | 100% |
glyoxylic acid ethyl ester
rac-methylbenzylamine
N-[(1-methyl)phenylmethyl]imino-acetic acid ethyl ester
Conditions | Yield |
---|---|
In toluene Heating; | 100% |
With magnesium sulfate In dichloromethane |
glyoxylic acid ethyl ester
4-fluoroaniline
(4-fluoro-phenylimino)-acetic acid ethyl ester
Conditions | Yield |
---|---|
With magnesium sulfate In toluene at 25℃; for 0.5h; | 100% |
In toluene at 3 - 18℃; | 40% |
In dichloromethane; toluene for 2h; Heating; |
glyoxylic acid ethyl ester
isopropenylbenzene
(R)-(-)-2-hydroxy-4-phenyl-pent-4-enoic acid ethyl ester
Conditions | Yield |
---|---|
With 4 A molecular sieve; immobilized chiral bis(binaphthoxide)-based Ti In diethyl ether; toluene at 20℃; for 72h; | 100% |
Stage #1: With titanium(IV) isopropylate; (R)-1,1'-Bi-2-naphthol In toluene at 20℃; for 0.5h; Inert atmosphere; Stage #2: With 3,3',5,5'-tetramethyl-2,2',6,6'-tetrahydroxy biphenyl In diethyl ether; toluene at 60℃; for 0.5h; Inert atmosphere; Stage #3: glyoxylic acid ethyl ester; isopropenylbenzene In diethyl ether; toluene at 0℃; for 30h; Inert atmosphere; | 99% |
With titanium(IV) isopropylate; (R)-6,6'-diiodo-2,2'-dihydroxy-1,1'-binaphthalene In dichloromethane; toluene at 0℃; for 48h; | 98% |
glyoxylic acid ethyl ester
(1-p-tolylvinyl)carbamic acid benzyl ester
Conditions | Yield |
---|---|
With (1R,2R)-N,N'-di(4'-bromobenzylidene)-1,2-diaminocyclohexane In dichloromethane at 0℃; for 1h; | 100% |
tetrakis(acetonitrile)copper(I) perchlorate; (1R,2R)-N,N'-bis(5-bromobenzylidene)diiminocyclohexane In dichloromethane at 0℃; for 1h; Product distribution / selectivity; | 100% |
2-azetidinone
glyoxylic acid ethyl ester
ethyl 2-hydroxy-2-(2-oxo-azetidin-1-yl)acetate
Conditions | Yield |
---|---|
In toluene for 3h; Heating; | 100% |
glyoxylic acid ethyl ester
cinnamamide
ethyl 2-cinnamamido-2-hydroxyacetate
Conditions | Yield |
---|---|
In tetrahydrofuran; toluene at 80℃; Inert atmosphere; | 100% |
In tetrahydrofuran at 20℃; | 65% |
In toluene Inert atmosphere; Reflux; |
glyoxylic acid ethyl ester
2,4-Xylidine
ethyl 2-(2,4-dimethylphenylimino)acetate
Conditions | Yield |
---|---|
With sodium sulfate In dichloromethane for 0.5h; | 100% |
In methanol; toluene at 70℃; for 7h; | 47% |
With magnesium sulfate In toluene; acetonitrile for 1h; Inert atmosphere; |
6-methylnicotinic acid
glyoxylic acid ethyl ester
6-[(1E)-3-ethoxy-3-oxoprop-1-en-1-yl]nicotinic acid
Conditions | Yield |
---|---|
With acetic anhydride In toluene at 20 - 130℃; for 20h; | 100% |
glyoxylic acid ethyl ester
1-methoxy-3-<(trimethylsilyl)oxy>01,3-butadiene
4-oxo-3,4-dihydro-2H-pyran-2-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
With zinc(II) chloride In tetrahydrofuran; toluene at 20℃; for 0.5h; | 100% |
With zinc(II) chloride In tetrahydrofuran; benzene at 20℃; for 72h; | 75% |
zinc(II) chloride In tetrahydrofuran; benzene at 20℃; for 72h; | 75% |
glyoxylic acid ethyl ester
(1-phenylvinyl)carbamic acid benzyl ester
Conditions | Yield |
---|---|
C22H26N2; tetrakis(acetonitrile)copper(I) perchlorate In dichloromethane at 0℃; for 1h; Product distribution / selectivity; | 100% |
tetrakis(acetonitrile)copper(I) perchlorate; N,N'-bis-(4-methyl-benzylidene)-cyclohexane-1,2-diamine In dichloromethane at 0℃; for 1h; Product distribution / selectivity; | 98% |
C22H26N2; tetrakis(acetonitrile)copper(I) perchlorate In dichloromethane at 0℃; for 1h; Product distribution / selectivity; | 97% |
glyoxylic acid ethyl ester
N-amino-(4-nitrophenyl)carboxamide
ethyl (2E)-[(4-nitrobenzoyl)hydrazono]ethanoate
Conditions | Yield |
---|---|
In ethanol; toluene at 80℃; Inert atmosphere; | 100% |
glyoxylic acid ethyl ester
benzo[1,3]dioxolo-5-ylamine
Conditions | Yield |
---|---|
With magnesium sulfate In toluene at 25℃; for 0.5h; | 100% |
In toluene at 23℃; for 1h; Molecular sieve; Inert atmosphere; | |
In dichloromethane for 0.333333h; Inert atmosphere; |
glyoxylic acid ethyl ester
(E)-3-(3-(benzyloxy)-4-methoxyphenyl)acrylamide
(E)-ethyl 2-(3-(3-(benzyloxy)-4-methoxyphenyl)acrylamido)-2-hydroxyacetate
Conditions | Yield |
---|---|
In tetrahydrofuran; toluene at 80℃; Inert atmosphere; | 100% |
glyoxylic acid ethyl ester
diethyl carbamoylmethylphosphonate
ethyl 2-(2-(diethoxyphosphoryl)acetamido)-2-hydroxyacetate
Conditions | Yield |
---|---|
In tetrahydrofuran; toluene at 80℃; Inert atmosphere; | 100% |
glyoxylic acid ethyl ester
Chloroacetamide
ethyl 2-(2-chloroacetamido)-2-hydroxyacetate
Conditions | Yield |
---|---|
In tetrahydrofuran; toluene at 80℃; Inert atmosphere; | 100% |
glyoxylic acid ethyl ester
2,2-dimethylpropionamide
methyl 2-hydroxy-2-pivalamidoacetate
Conditions | Yield |
---|---|
In toluene Inert atmosphere; Radiolysis; | 100% |
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