Product Description Product website: http://www.finerchem.com/pro01en/id/1653.html Product Name (R)-(+)-1-Phenylethylamine CAS No. 3886-69-9
Cas:3886-69-9
Min.Order:1 Gram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryStock products, own laboratory Product number PC00860 English Name (1R)-1-phenylethanamine CAS Number 3886-69-9 Purity 98% M
Cas:3886-69-9
Min.Order:1 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:3886-69-9
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryItems Standard Result Assay (Ursolic acid) 98%min 98.22% ----------------------------------------------------------------
Cas:3886-69-9
Min.Order:1 Gram
FOB Price: $100.0 / 500.0
Type:Trading Company
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:3886-69-9
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
inquiryFormula: C8H11N MolecularWeight: 121.18 Synonyms: D-(+)-1-Phenylethylamine;D-1-Phenylethylamine;D-a-Phenethylamine;… Founded in 2014, as a professional international pharmaceutical corporation, headquartered in Xi'an (China), KonoChemC
Cas:3886-69-9
Min.Order:1 Kilogram
FOB Price: $400000.0
Type:Other
inquiry(R)-(+)-1-Phenylethylamine, CAS No.:3886-69-9 Name (R)-(+)-1-Phenylethylamine Synonyms D-alpha-Phenylethylamine; R-(+)-alpha-Methylbenzylamine; D(+)-alpha-Methylbenzylamine; (+)-PEA; (R)-(+)-1-Phenylethylamine Molecular Structure
Cas:3886-69-9
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Other
inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:3886-69-9
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryColorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
Cas:3886-69-9
Min.Order:1 Metric Ton
Negotiable
Type:Manufacturers
inquiry
Cas:3886-69-9
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Manufacturers
inquiryOur company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:3886-69-9
Min.Order:1 Kilogram
FOB Price: $1000.0
Type:Lab/Research institutions
inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:3886-69-9
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:3886-69-9
Min.Order:1 Gram
FOB Price: $1000.0 / 1300.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:3886-69-9
Min.Order:10 Gram
FOB Price: $146.0 / 176.0
Type:Trading Company
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:3886-69-9
Min.Order:10 Kilogram
Negotiable
Type:Trading Company
inquiryProduct Name: (R)-(+)-1-Phenylethylamine CAS: 3886-69-9 MW:121.18 MF: C8H11N Appearance: Colorless liquid Purity: 98% Appearance:Colorless transparent liquid Storage:Preserve in well-closed, light-resistant and airtight containers. Package:25kg/
1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:white or off-white powder Storage:Store in sealed containers
Cas:3886-69-9
Min.Order:100 Gram
Negotiable
Type:Other
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:3886-69-9
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:3886-69-9
Min.Order:1 Kilogram
FOB Price: $85.0 / 96.0
Type:Trading Company
inquiry(R)-(+)-1-Phenylethylamine CAS:3886-69-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic
Cas:3886-69-9
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:3886-69-9
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Appearance:Light yellow liquid Storage:kept in a cool, dry and ventilated place Package:as your requirement Application:Only used for research and development. Not as a drug, household or other USES. Transportation:By Sea,by Ai
Cas:3886-69-9
Min.Order:1 Gram
FOB Price: $1.0 / 10.0
Type:Lab/Research institutions
inquiryOur Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
Cas:3886-69-9
Min.Order:1 Kilogram
FOB Price: $1.0 / 100000.0
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:3886-69-9
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:3886-69-9
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:3886-69-9
Min.Order:4 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryTop quality 3886-69-9 (R)-(+)-1-Phenylethylamine factory in China Hot saler Molecular Formula C8H11N Molar Mass 121.187 Density 0.952 g/mL at 20 °C(lit.) Melting Point -10℃ Boling Point
Cas:3886-69-9
Min.Order:1 Gram
Negotiable
Type:Other
inquirymethanol
A
(S)-methyl 2-(2-oxopyrrolidin-1-yl)-2-butanoate
B
(R)-1-phenyl-ethyl-amine
Conditions | Yield |
---|---|
Stage #1: (-)-(S)-alpha-ethyl-2-oxo-1-pyrrolidineacet-N-(+)-(R)-(1-phenylethyl)-amide With sulfonic acid type-ion exchange resin; water In toluene for 6h; not specified; Heating / reflux; Stage #2: methanol With sulfonic acid type-ion exchange resin In water; toluene at 60℃; for 3h; | A 100% B n/a |
Conditions | Yield |
---|---|
With ammonia at 25℃; optical yield given as %ee; | 100% |
A
(R)-1-phenyl-ethyl-amine
B
(S)‐1,4‐benzodioxane‐2‐carboxylic acid
Conditions | Yield |
---|---|
With hydrogenchloride In 1,4-dioxane at 90℃; | A 100% B 100% |
A
(R)-1-phenyl-ethyl-amine
B
(+)-(2R)-2,3-dihydro-1,4-benzodioxine-2-carboxylic acid
Conditions | Yield |
---|---|
With hydrogenchloride In 1,4-dioxane at 90℃; | A 100% B 100% |
C12H17NOS
(R)-1-phenyl-ethyl-amine
Conditions | Yield |
---|---|
Stage #1: C12H17NOS With [RhCl2(p-cymene)]2; potassium tert-butylate; (1S,2R)-1-amino-2-indanol In isopropyl alcohol at 40℃; for 2h; Molecular sieve; Stage #2: With hydrogenchloride In methanol optical yield given as %ee; stereoselective reaction; | 99% |
(R)-1-phenyl-ethyl-amine
Conditions | Yield |
---|---|
With aluminum (III) chloride; methoxybenzene In dichloromethane at 30℃; for 2h; | 98.4% |
With aluminum (III) chloride; methoxybenzene In dichloromethane at 20℃; for 2h; Inert atmosphere; enantioselective reaction; | 95% |
N-[(R)-(+)-1-phenylethyl]decanamide
(R)-1-phenyl-ethyl-amine
Conditions | Yield |
---|---|
With Candida antarctica lipase B In phosphate buffer at 70℃; for 48h; pH=7; | 98% |
N-acetyl-1-phenylethylamine
(R)-1-phenyl-ethyl-amine
Conditions | Yield |
---|---|
Stage #1: N-acetyl-1-phenylethylamine With hydrogenchloride; methanol; water at 80℃; for 15h; Stage #2: With water; sodium hydroxide | 98% |
(R)-1-phenyl-ethyl-amine
Conditions | Yield |
---|---|
With hydrogenchloride; D-sorbitol; choline chloride In water at 25℃; for 3h; | 98% |
Conditions | Yield |
---|---|
With Candida boidinii formate dehydrogenase; Geobacillus stearothermophilus ε‐deaminating L‐lysine dehydrogenase variant 22; nicotinamide adenine dinucleotide In aq. buffer at 50℃; for 48h; pH=8.5; Reagent/catalyst; Enzymatic reaction; | 97% |
With glucose dehydrogenase; sodium hydroxide; D-Alanine; ATA-117 transaminase; NADH; 2,3,4,5,6-pentahydroxy-hexanal; pyridoxal 5'-phosphate; lactate dehydrogenase at 30℃; for 10h; pH=7.5; aq. phosphate buffer; Enzymatic reaction; optical yield given as %ee; | 96% |
With Ru(2+)*2C2H3O2(1-)*C77H108O6P2; hydrogen; sodium acetate In 2,2,2-trifluoroethanol at 100℃; under 42754.3 Torr; for 24h; Autoclave; enantioselective reaction; | 96% |
(R(S))-N-(1-phenylethylidene)-tert-butanesulfinamide
(R)-1-phenyl-ethyl-amine
Conditions | Yield |
---|---|
Stage #1: (R(S))-N-(1-phenylethylidene)-tert-butanesulfinamide With [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; potassium tert-butylate; 2-Amino-2-methyl-1-propanol In isopropyl alcohol at 50℃; for 2h; Molecular sieve; Stage #2: With hydrogenchloride In methanol optical yield given as %ee; diastereoselective reaction; | 97% |
Stage #1: (R(S))-N-(1-phenylethylidene)-tert-butanesulfinamide With [RhCl2(p-cymene)]2; potassium tert-butylate; 2-Amino-2-methyl-1-propanol; isopropyl alcohol at 50℃; for 0.5h; Inert atmosphere; Microwave irradiation; Molecular sieve; Stage #2: With hydrogenchloride In methanol at 20℃; Catalytic behavior; Temperature; Inert atmosphere; enantioselective reaction; | 95% |
Multi-step reaction with 2 steps 1: [RhCl2(p-cymene)]2; potassium tert-butylate; 2-Amino-2-methyl-1-propanol; isopropyl alcohol / 2 h / 50 °C / Inert atmosphere; Molecular sieve 2: hydrogenchloride / methanol / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: 2-Amino-2-methyl-1-propanol; [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 / isopropyl alcohol / 0.25 h / 50 °C / Inert atmosphere; Molecular sieve 1.2: 2 h / 50 °C / Inert atmosphere; Molecular sieve 2.1: hydrogenchloride / methanol; diethyl ether / 3 h / 0 - 20 °C / Inert atmosphere View Scheme |
A
(S)-1-phenyl-ethylamine
B
(R)-1-phenyl-ethyl-amine
C
(R)-(-)-o-(1-pivaloylaminoethyl)benzene sulfinic acid
Conditions | Yield |
---|---|
With trifluoroacetic acid In methanol Yields of byproduct given; | A n/a B n/a C 96% |
Conditions | Yield |
---|---|
With nickel at 110℃; for 1h; Reagent/catalyst; Inert atmosphere; | 94% |
With ωTA ATA-117 102907WW; Vibrio fluvialis Vf-ωTA 2100208MW; pyridoxal 5'-phosphate; pentan-3-one at 30℃; for 24h; pH=7; aq. phosphate buffer; Enzymatic reaction; | |
With hydrogen In toluene at 70℃; for 35h; chemoselective reaction; |
(R)-1-phenyl-ethyl-amine
Conditions | Yield |
---|---|
With sodium hydroxide In water pH=11; | 94% |
(R)-1-phenyl-ethyl-amine
Conditions | Yield |
---|---|
With sodium hydroxide In water pH=11; | 93.3% |
(R)-2-methoxy-N-(1-phenylethyl)acetamide
(R)-1-phenyl-ethyl-amine
Conditions | Yield |
---|---|
With sodium hydroxide; triethanolamine In water at 120℃; for 6h; optical yield given as %ee; | 93% |
(RS)-2-methyl-N-((R)-1-phenylethyl)propane-2-sulfinamide
(R)-1-phenyl-ethyl-amine
Conditions | Yield |
---|---|
With hydrogenchloride In 1,4-dioxane; methanol at 25℃; for 0.5h; Inert atmosphere; | 92% |
With hydrogenchloride In methanol; diethyl ether at 0 - 20℃; for 3h; Inert atmosphere; | 88% |
Stage #1: (RS)-2-methyl-N-((R)-1-phenylethyl)propane-2-sulfinamide With thionyl chloride In methanol at 20℃; Inert atmosphere; Stage #2: With hydrogenchloride In water Inert atmosphere; Stage #3: With ammonia; ammonium chloride In water Inert atmosphere; optical yield given as %ee; enantioselective reaction; | |
Stage #1: (RS)-2-methyl-N-((R)-1-phenylethyl)propane-2-sulfinamide With hydrogenchloride In methanol at 20℃; Stage #2: With ammonia; ammonium chloride In water |
ethanone-1-phenyl-O-(phenylmethyl)oxime
A
(S)-1-phenyl-ethylamine
B
(R)-1-phenyl-ethyl-amine
Conditions | Yield |
---|---|
With sodium tetrahydroborate; (S)-valinol; zirconium(IV) chloride In tetrahydrofuran Ambient temperature; Title compound not separated from byproducts; | A 91% B n/a |
(2S)-2-phenyl-2-({[(1R)-1-phenylethyl]amino}oxy)ethanol
A
(R)-1-phenyl-ethyl-amine
B
(S)-1-phenyl-1,2-ethanediol
Conditions | Yield |
---|---|
With hexacarbonyl molybdenum In water; acetonitrile at 85℃; for 1h; | A 90% B n/a |
A
(R)-1-phenyl-ethyl-amine
B
(R)-(+)-2-methyl-2-(3-oxobutyl)cyclohexanone
Conditions | Yield |
---|---|
With acetic acid at 20℃; for 1h; Yields of byproduct given; | A n/a B 88% |
(R)-1-phenylethylamine hydrochloride
(R)-1-phenyl-ethyl-amine
Conditions | Yield |
---|---|
With potassium carbonate In water at 70℃; for 1h; pH=9; | 88% |
With sodium hydroxide In dichloromethane; water pH=10 - 11; |
(R)-1-phenyl-ethyl-amine
Conditions | Yield |
---|---|
With diethylamine; palladium diacetate; trisodium tris(3-sulfophenyl)phosphine In water; acetonitrile at 20℃; for 0.0833333h; | 85% |
(R)-1-phenyl-ethyl-amine
Conditions | Yield |
---|---|
With samarium diiodide In tetrahydrofuran for 4h; Ambient temperature; | 83% |
(E)-ethanone-1-phenyl-O-(phenylmethyl)oxime
(R)-1-phenyl-ethyl-amine
Conditions | Yield |
---|---|
Stage #1: (E)-ethanone-1-phenyl-O-(phenylmethyl)oxime With C10H18BNO In tetrahydrofuran at 20℃; for 24h; Stage #2: With borane-THF In tetrahydrofuran for 24h; Reflux; optical yield given as %ee; enantioselective reaction; Further stages; | 82% |
With dimethylsulfide borane complex; (R)-(+)-2-(1,3,2-dioxaborolan-2-yloxy)-1,2,2-triphenylethanamine In toluene at 50 - 110℃; for 15h; Product distribution / selectivity; | n/a |
With dimethylsulfide borane complex; C11H14BNO3 In toluene at 50 - 110℃; for 15h; Product distribution / selectivity; | n/a |
With borane-THF; N-isopropyl-N,2-dimethylpropan-2-amine; C22H22BNO3 In 1,4-dioxane at 20℃; for 48h; Product distribution / selectivity; | 100 %Chromat. |
(R)-N-(4-methoxyphenyl)-(1-phenylethyl)amine
(R)-1-phenyl-ethyl-amine
Conditions | Yield |
---|---|
Stage #1: (R)-N-(4-methoxyphenyl)-(1-phenylethyl)amine With ammonium cerium (IV) nitrate In methanol; water at 0℃; for 6h; Stage #2: With sodium hydroxide In water | 81.3% |
(R)-1-phenyl-ethyl-amine
Conditions | Yield |
---|---|
With thiophenol; zinc(II) chloride In dichloromethane at 20℃; for 6h; | 81% |
(Z)-acetophenone O-benzyloxime
(R)-1-phenyl-ethyl-amine
Conditions | Yield |
---|---|
With borane-THF; C19H23BNO3(1-)*H(1+) In tetrahydrofuran; 1,4-dioxane at 0℃; Temperature; Solvent; Reagent/catalyst; Time; Inert atmosphere; enantioselective reaction; | 76% |
(R)-1-phenyl-ethyl-amine
chloroformic acid ethyl ester
(R)-(1-phenylethyl)-carbamic acid ethyl ester
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at -30 - 20℃; | 100% |
With triethylamine In diethyl ether at 0 - 20℃; for 2.5h; | 95% |
Stage #1: (R)-1-phenyl-ethyl-amine With triethylamine In dichloromethane at 20℃; Inert atmosphere; Stage #2: chloroformic acid ethyl ester at -30 - 20℃; for 8h; Inert atmosphere; | 90.5% |
With sodium carbonate | |
With sodium hydroxide |
Conditions | Yield |
---|---|
at 55℃; for 2h; | 100% |
In chloroform at 0℃; | 95% |
In benzene 1.) 90 deg C, 1 h, 2.) r.t., 12 h; | 86% |
glyoxylic acid ethyl ester
(R)-1-phenyl-ethyl-amine
((R)-1-phenyl-ethylimino)-acetic acid ethyl ester
Conditions | Yield |
---|---|
In toluene for 0.333333h; Heating; | 100% |
In toluene Heating; | 100% |
In toluene at 15 - 25℃; | 95% |
(R)-1-phenyl-ethyl-amine
formic acid ethyl ester
(R)-(+)-α-methylbenzyl formamide
Conditions | Yield |
---|---|
for 8h; Reflux; | 100% |
With amberlyst 15 In tetrahydrofuran for 21h; Reflux; Inert atmosphere; | 99% |
With Novozyme 435 CALB In tetrahydrofuran at 20℃; Green chemistry; Enzymatic reaction; | 92% |
8-oxo-(E)-non-2-enoic acid methyl ester
(R)-1-phenyl-ethyl-amine
(E)-8-[(E)-(R)-1-Phenyl-ethylimino]-non-2-enoic acid methyl ester
Conditions | Yield |
---|---|
With molecular sieve In cyclohexane at 40℃; for 1h; | 100% |
(E)-9-Oxo-2-decanoic acid methyl ester
(R)-1-phenyl-ethyl-amine
(E)-9-[(E)-(R)-1-Phenyl-ethylimino]-dec-2-enoic acid methyl ester
Conditions | Yield |
---|---|
With molecular sieve In cyclohexane at 40℃; for 1h; | 100% |
(R)-1-phenyl-ethyl-amine
7-oxo-2(E)-octenoic acid methyl ester
(E)-7-[(E)-(R)-1-Phenyl-ethylimino]-oct-2-enoic acid methyl ester
Conditions | Yield |
---|---|
With molecular sieve In cyclohexane at 40℃; for 1h; | 100% |
(R)-1-phenyl-ethyl-amine
(E)-7-(2-Oxo-cyclohexyl)-hept-2-enoic acid methyl ester
(E)-7-{2-[(E)-(R)-1-Phenyl-ethylimino]-cyclohexyl}-hept-2-enoic acid methyl ester
Conditions | Yield |
---|---|
In cyclohexane for 3h; Heating; | 100% |
(R)-1-phenyl-ethyl-amine
Conditions | Yield |
---|---|
100% |
(R)-1-phenyl-ethyl-amine
Conditions | Yield |
---|---|
100% |
(R)-1-phenyl-ethyl-amine
benzaldehyde
(R)-1-phenylethyl(benzylidene)amine
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane at 20℃; for 12h; | 100% |
In benzene for 2h; Condensation; Heating; | 96% |
With magnesium sulfate In tetrahydrofuran for 3.5h; | 83% |
succinic acid anhydride
(R)-1-phenyl-ethyl-amine
1-[(1R)-1-phenylethyl]pyrrolidine-2,5-dione
Conditions | Yield |
---|---|
Stage #1: succinic acid anhydride; (R)-1-phenyl-ethyl-amine In toluene for 18h; Reflux; Stage #2: In acetic anhydride for 2h; Reflux; | 100% |
Stage #1: succinic acid anhydride; (R)-1-phenyl-ethyl-amine In tetrahydrofuran Heating; Stage #2: With acetic anhydride In tetrahydrofuran for 2h; Heating; | 60% |
With acetic anhydride 1.) THF, reflux, 2 h, 2.) reflux, 2 h; Yield given. Multistep reaction; |
glyoxylic acid ethyl ester
(R)-1-phenyl-ethyl-amine
<(R)-(1-phenylethyl)imino>acetic acid ethyl ester
Conditions | Yield |
---|---|
In toluene for 1.5h; Heating; | 100% |
With molecular sieve In dichloromethane at 0℃; |
di-tert-butyl dicarbonate
(R)-1-phenyl-ethyl-amine
(R)-(1-phenylethyl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With indium(III) bromide at 30 - 35℃; for 0.0333333h; | 100% |
With perchloric acid at 30 - 35℃; for 0.0166667h; | 100% |
With sulfonic-acid-functionalized silica In dichloromethane at 20℃; for 0.0833333h; | 99% |
ethyl trifluoroacetate,
(R)-1-phenyl-ethyl-amine
N-<(R)-(+)-α-phenylethyl>-2,2,2-trifluoroacetamide
Conditions | Yield |
---|---|
With sodium hydride In diethyl ether at 0 - 20℃; Condensation; | 100% |
at 25℃; for 20h; Sealed tube; | 100% |
at 20℃; for 0.05h; Acylation; | 89% |
(R)-1-phenyl-ethyl-amine
1-(trifluoroacetyl)benzotriazole
A
1,2,3-Benzotriazole
B
N-<(R)-(+)-α-phenylethyl>-2,2,2-trifluoroacetamide
Conditions | Yield |
---|---|
In tetrahydrofuran for 4h; Ambient temperature; | A n/a B 100% |
pyridine-2-carbaldehyde
(R)-1-phenyl-ethyl-amine
(R,E)-N-(1-phenylethyl)-1-(pyridin-2-yl)methanimine
Conditions | Yield |
---|---|
In toluene Reflux; Inert atmosphere; Dean-Stark; | 100% |
With magnesium sulfate In diethyl ether for 4h; Ambient temperature; | 90% |
With aluminum oxide | |
In diethyl ether for 1h; Molecular sieve; Inert atmosphere; |
(R)-1-phenyl-ethyl-amine
chloroacetyl chloride
(R)-N-(α-methylbenzyl)chloroacetamide
Conditions | Yield |
---|---|
In dichloromethane | 100% |
With potassium carbonate In acetonitrile | 98% |
With triethylamine In dichloromethane at 0 - 20℃; for 6h; | 86.07% |
carbon disulfide
(R)-1-phenyl-ethyl-amine
(R,R)-N,N'-bis[α-methylbenzyl]thiourea
Conditions | Yield |
---|---|
aluminum oxide; zinc(II) oxide at 100℃; for 2h; Condensation; | 100% |
at 47℃; | 97% |
In ethanol Inert atmosphere; Reflux; | 95% |
MCM-41-TBD; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine at 90℃; for 15h; | 91% |
In ethanol at 88℃; for 24h; | 74% |
(R)-1-phenyl-ethyl-amine
5,5'-(2,2'-bipyridine)diacid chloride
Conditions | Yield |
---|---|
Condensation; | 100% |
(R)-1-phenyl-ethyl-amine
(SS)-(+)-2-(p-Tolylsulfinyl)prop-2-en-1-ol
Conditions | Yield |
---|---|
In dichloromethane at 0 - 20℃; | 100% |
Conditions | Yield |
---|---|
at 20℃; for 6h; | 100% |
(R)-1-phenyl-ethyl-amine
ethyl 4-allyloxy-3-oxobutanoate
(Z)-4-Allyloxy-3-((R)-1-phenyl-ethylamino)-but-2-enoic acid ethyl ester
Conditions | Yield |
---|---|
With acetic acid In tetrahydrofuran at 60℃; | 100% |
4,5-Dihydro-2-methylthiophen-3-(2H)-on
(R)-1-phenyl-ethyl-amine
(R)-(2-methyl-dihydrothiophen-3-ylidene)(1-phenylethyl)amine
Conditions | Yield |
---|---|
With aluminum oxide; 5A molecular sieve; silica gel In cyclohexane at 20℃; for 144h; | 100% |
With aluminum oxide; silica gel In cyclohexane at 20℃; for 100h; |
(R)-1-phenyl-ethyl-amine
4-(((tert-butyldimethylsilyl)oxy)methyl)cyclohexane carbaldehyde
(R)-N-[(4'-tert-butyldimethylsilyloxymethyl-cyclohexyl)methylidene]-1-phenylethanamine
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane at 20℃; | 100% |
With magnesium sulfate In dichloromethane |
Conditions | Yield |
---|---|
In butan-1-ol for 0.166667h; Zincke's reaction; microwave irradiation; | 100% |
pyridine-4-carbaldehyde
(R)-1-phenyl-ethyl-amine
((R)-1-Phenyl-ethyl)-[1-pyridin-4-yl-meth-(E)-ylidene]-amine
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane at 20℃; for 12h; | 100% |
With boron trifluoride diethyl etherate at 20℃; for 0.0166667h; |
(R)-1-phenyl-ethyl-amine
Conditions | Yield |
---|---|
In chloroform-d1 at 24℃; | 100% |
(R)-1-phenyl-ethyl-amine
Conditions | Yield |
---|---|
In chloroform-d1 at 24℃; | 100% |
(R)-1-phenyl-ethyl-amine
ethyl (E,E)-4-oxo-2-styrylbut-2-enoate
Conditions | Yield |
---|---|
In chloroform-d1 at 24℃; | 100% |
About|Contact|Cas|Product Name|Molecular|Country|Encyclopedia
Message|New Cas|MSDS|Service|Advertisement|CAS DataBase|Article Data|Manufacturers | Chemical Catalog
©2008 LookChem.com,License: ICP
NO.:Zhejiang16009103
complaints:service@lookchem.com Desktop View