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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

Phthalonitrile Manufacturer/High quality/Best price/In stock

Cas:91-15-6

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Hebei yanxi chemical co.,LTD.

Hebei yanxi chemical co., LTD is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low carb

Phthalonitrile

Cas:91-15-6

Min.Order:1 Kilogram

FOB Price: $1.0 / 3.0

Type:Manufacturers

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Hefei TNJ chemical industry co.,ltd

1,ISO Certificate 2,Factory price 3,Free sample and Fast delivery Appearance:white crystals Storage:Storage: All products should be stored at a dry and ventilated location away from fire and other dangerous goods, and should avoid direct sunlight.

Phthalonitrile,CAS 91-15-6

Cas:91-15-6

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Trading Company

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Phthalonitrile

Cas:91-15-6

Min.Order:1

Negotiable

Type:Other

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COLORCOM LTD.

Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on

O-Phthalodinitrile

Cas:91-15-6

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Phthalodinitrile

Cas:91-15-6

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 2) All Purity≥99% 3) We are manufacturer and can provide high quality products with factory price. 2, Fast and safe delivery 1) Parcel can be sent out in 24 hours after payment.Tracking number available 2) Secure and disc

Phthalonitrile CAS:91-15-6

Cas:91-15-6

Min.Order:1 Kilogram

FOB Price: $150.0 / 200.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 91-15-6 with best quality

Cas:91-15-6

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Phthalonitrile CAS NO.91-15-6

Cas:91-15-6

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Synonyms: 1,2-Benzenedicarbonitrile 1,2-Dicyanobenzene o-Phthalodinitrile Molecular Formula: C8H4N2 Molecular Weight: 128.13 CAS Registry Number: 91-15-6 EINECS: 202-044-8 Density: 1.24

Phthalonitrile

Cas:91-15-6

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

1,2-Benzenedicarbonitrile 91-15-6

Cas:91-15-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Shanghai Minstar Chemical Co., Ltd

Product Name: Phthalonitrile MF: C8H4N2 MW: 128.13 EINECS: 202-044-8 Mol File: 91-15-6.mol Phthalonitrile Structure Phthalonitrile Chemical Properties Melting point 137-139 °C (lit.) Boiling point 227.54°C (rough est

Phthalonitrile

Cas:91-15-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present

High quality intermediates Phthalonitrile CAS 91-15-6

Cas:91-15-6

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Qingdao Beluga Import and Export Co., LTD

Phthalonitrile CAS:91-15-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediate

Phthalonitrile CAS:91-15-6

Cas:91-15-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

1,2-Benzenedicarbonitrile

Cas:91-15-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:91-15-6

Cas:91-15-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

O-Phthalonitrile

Cas:91-15-6

Min.Order:0

Negotiable

Type:Manufacturers

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Triumph International Development Limilted

Triumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Service 1.Own made fine chemical products 2.Out sourcing and quality c

1,2-Dicyanobenzene

Cas:91-15-6

Min.Order:100 Metric Ton

Negotiable

Type:Lab/Research institutions

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Hubei Jiutian Bio-medical Technology Co., Ltd

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie

CAS91-15-6 Phthalonitrile

Cas:91-15-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Phthalonitrile

Cas:91-15-6

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Afine Chemicals Limited

Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

PHTHALONITRILE

Cas:91-15-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Phthalonitrile

Cas:91-15-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High purity Phthalonitrile

Cas:91-15-6

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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Henan Tianfu Chemical Co., Ltd.

Phthalonitrile Chemical Properties Melting point 137-139 °C(lit.) density 1.24 Fp 162°C storage temp. Store below +30°C. solubility benzene: 50 mg/

91-15-6 Phthalonitrile

Cas:91-15-6

Min.Order:1 Metric Ton

FOB Price: $20.0

Type:Lab/Research institutions

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EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

Phthalonitrile

Cas:91-15-6

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

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TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

Phthalonitrile

Cas:91-15-6

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

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Hangzhou Fandachem Co.,Ltd

Hangzhou Fandachem Co.,Ltd, a China-based chemical company, specialize in exporting Phthalonitrile, cas no: 91-15-6 Please contact us by email freely. We are leading exporter in China. If you really need this cargo, please do not

Phthalonitrile, cas no: 91-15-6 from Fandachem

Cas:91-15-6

Min.Order:1 Kilogram

Negotiable

Type:Other

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Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Phthalonitrile CAS NO.91-15-6

Cas:91-15-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

Phthalonitrile

Cas:91-15-6

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

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Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

1,2-Dicyanobenzene

Cas:91-15-6

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Synthetic route

N,N'-o-phthaloylbis(P,P,P-triphenylphospha-λ5-azene)
112069-03-1

N,N'-o-phthaloylbis(P,P,P-triphenylphospha-λ5-azene)

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
In dimethyl sulfoxide at 140℃; intramolecular aza-Wittig reaction;100%
nitroacetic acid ethyl ester
626-35-7

nitroacetic acid ethyl ester

2-iodobenzonitrile
4387-36-4

2-iodobenzonitrile

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With potassium phenolate; palladium diacetate; potassium carbonate; dimethyl cis-but-2-ene-1,4-dioate; triphenylphosphine In N,N-dimethyl-formamide at 120℃; for 24h; Schlenk technique; Inert atmosphere;95%
2-iodobenzonitrile
4387-36-4

2-iodobenzonitrile

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With sodium carbonate; potassium ferrocyanide In N,N-dimethyl-formamide at 120℃; for 5h;93%
1,2-benzenedimethanamine
17300-02-6

1,2-benzenedimethanamine

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With aluminum oxide In N,N-dimethyl-formamide at 120℃; for 6h; Inert atmosphere;92%
With [Ru(p-cymene)(pzH-NP)(Cl)]Cl; potassium tert-butylate In toluene at 70℃; for 24h; Schlenk technique; Inert atmosphere;68%
2-iodobenzonitrile
4387-36-4

2-iodobenzonitrile

potassium ferrocyanide

potassium ferrocyanide

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 120℃; for 12h;91%
With potassium carbonate In N,N-dimethyl-formamide at 120℃; for 15h; Schlenk technique; Green chemistry;90%
With 3% Pd/CeO2; sodium acetate In N,N-dimethyl-formamide; isopropyl alcohol at 65℃; for 10h; Irradiation;42%
With tri-tert-butyl phosphine; potassium carbonate In N,N-dimethyl-formamide at 120℃; for 24h; Reagent/catalyst; Inert atmosphere;75 %Chromat.
potassium hexacyanoferrate(II) trihydrate

potassium hexacyanoferrate(II) trihydrate

o-cyanobromobenzene
2042-37-7

o-cyanobromobenzene

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With dichloro(2,2-bis(diphenylphosphino)diphenyl ether)palladium(II); potassium acetate In 1,4-dioxane; water at 90℃; for 1.33333h; Sealed tube;91%
potassiumhexacyanoferrate(II) trihydrate

potassiumhexacyanoferrate(II) trihydrate

2-iodobenzonitrile
4387-36-4

2-iodobenzonitrile

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With sodium carbonate In N,N-dimethyl-formamide at 120℃; for 12h; Inert atmosphere;91%
With sodium acetate In N,N-dimethyl-formamide; isopropyl alcohol at 55℃; Irradiation; Sealed tube;
2-(hydroxymethyl)benzenecorbonitrile
89942-45-0

2-(hydroxymethyl)benzenecorbonitrile

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With ammonium hydroxide; copper(l) iodide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical In water for 24h; Reflux; Green chemistry;90%
[2-(dihydroxyboranyl)phenyl]boronic acid
13506-83-7

[2-(dihydroxyboranyl)phenyl]boronic acid

4-bromo-N-(4-chlorophenyl)-N-cyanobenzenesulfonamide

4-bromo-N-(4-chlorophenyl)-N-cyanobenzenesulfonamide

A

4-bromo-benzenesulfonic acid-(4-chloro-anilide)
6295-97-2

4-bromo-benzenesulfonic acid-(4-chloro-anilide)

B

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With Fe3O4/SiO2/(3-chloropropyl)trimethoxysilane/2,2′-(4,4′-(propane-1,3-diyl)bis(piperazine-4,1-diyl))- diethanamine/Pd In acetonitrile for 15h; Catalytic behavior; Reflux;A n/a
B 90%
[2-(dihydroxyboranyl)phenyl]boronic acid
13506-83-7

[2-(dihydroxyboranyl)phenyl]boronic acid

N-(4-chlorophenyl)-N-cyano-4-nitrobenzenesulfonamide

N-(4-chlorophenyl)-N-cyano-4-nitrobenzenesulfonamide

A

4-nitro-N-(4-chlorophenyl)benzenesulfonamide
16937-03-4

4-nitro-N-(4-chlorophenyl)benzenesulfonamide

B

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With Fe3O4/SiO2/(3-chloropropyl)trimethoxysilane/2,2′-(4,4′-(propane-1,3-diyl)bis(piperazine-4,1-diyl))- diethanamine/Pd In acetonitrile for 14h; Catalytic behavior; Reflux;A n/a
B 90%
o-phthalic dicarboxaldehyde
643-79-8

o-phthalic dicarboxaldehyde

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With ammonium hydroxide; sodium persulfate; sodium iodide; iron(II) chloride In 1,2-dichloro-ethane at 20 - 50℃; for 16h;89%
With O-(diphenylphosphinyl)hydroxylamine In toluene at 20 - 85℃; chemoselective reaction;78%
With formic acid; hydroxylamine hydrochloride; silica gel for 0.0333333h; Irradiation;72 % Chromat.
With K2Co4[WZn3(H2O)2][ZnW9O34]2*53H2O; ammonia; dihydrogen peroxide In water at 20℃; for 6h;100 %Spectr.
potassiumhexacyanoferrate(II) trihydrate

potassiumhexacyanoferrate(II) trihydrate

1-Bromo-2-iodobenzene
583-55-1

1-Bromo-2-iodobenzene

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With palladium diacetate; sodium carbonate; 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride In N,N-dimethyl acetamide at 120℃; for 3h;89%
benzoimidazole
51-17-2

benzoimidazole

chloroform
67-66-3

chloroform

A

2-chloroquinoxaline
1448-87-9

2-chloroquinoxaline

B

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
at 390 - 400℃;A 12%
B 88%
[2-(dihydroxyboranyl)phenyl]boronic acid
13506-83-7

[2-(dihydroxyboranyl)phenyl]boronic acid

N-(4-chlorophenyl)-N-cyano-4-methylbenzenesulfonamide
119986-58-2

N-(4-chlorophenyl)-N-cyano-4-methylbenzenesulfonamide

A

4-methyl-N-(4-chlorophenyl)benzenesulfonamide
2903-34-6

4-methyl-N-(4-chlorophenyl)benzenesulfonamide

B

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With Fe3O4/SiO2/(3-chloropropyl)trimethoxysilane/2,2′-(4,4′-(propane-1,3-diyl)bis(piperazine-4,1-diyl))- diethanamine/Pd In acetonitrile for 16h; Catalytic behavior; Reflux;A n/a
B 88%
1-hydrazinophthalazine
1044569-46-1

1-hydrazinophthalazine

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With ammonium cerium (IV) nitrate In methanol at 20℃;87%
potassiumhexacyanoferrate(II) trihydrate

potassiumhexacyanoferrate(II) trihydrate

1,2-dibromobenzene
583-53-9

1,2-dibromobenzene

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With palladium diacetate; sodium carbonate; 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride In N,N-dimethyl acetamide at 120℃; for 10h;86%
nitroacetic acid ethyl ester
626-35-7

nitroacetic acid ethyl ester

o-cyanobromobenzene
2042-37-7

o-cyanobromobenzene

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With potassium phenolate; palladium diacetate; potassium carbonate; dimethyl cis-but-2-ene-1,4-dioate; triphenylphosphine In N,N-dimethyl-formamide at 120℃; for 24h; Schlenk technique; Inert atmosphere;86%
2,3-dicyano-1,4-hydroquinone
4733-50-0

2,3-dicyano-1,4-hydroquinone

Chloromethyltrimethylsilane
2344-80-1

Chloromethyltrimethylsilane

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With hydrogenchloride; potassium carbonate In N,N-dimethyl-formamide84.8%
1,2-Bis(nonaflyl)benzene
41694-39-7

1,2-Bis(nonaflyl)benzene

dicyanozinc
557-21-1

dicyanozinc

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
tetrakis(triphenylphosphine) palladium(0) In N,N-dimethyl-formamide Substitution;83%
zinc(II) cyanide
557-21-1

zinc(II) cyanide

2-Chlorobenzonitrile
873-32-5

2-Chlorobenzonitrile

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With dmap; 1,1'-bis-(diphenylphosphino)ferrocene; nickel(II) chloride hexahydrate; zinc In acetonitrile at 80℃; for 6h; Schlenk technique; Inert atmosphere; Sealed tube;83%
With dmap; 1,1'-bis-(diphenylphosphino)ferrocene; nickel(II) chloride hexahydrate; zinc In acetonitrile at 80℃; for 6h; Inert atmosphere; Sealed tube;83%
o-formylbenzonitrile
7468-67-9

o-formylbenzonitrile

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With hydroxylamine hydrochloride In glycerol at 90℃; for 9.5h; Green chemistry;83%
Multi-step reaction with 2 steps
1: hydroxylamine hydrochloride; sodium carbonate / methanol; water / Reflux
2: fluorosulfonyl fluoride; triethylamine / acetonitrile / 0.25 h / 20 °C / Schlenk technique
View Scheme
potassium ferrocyanide

potassium ferrocyanide

1,2-dibromobenzene
583-53-9

1,2-dibromobenzene

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With copper(l) iodide; potassium iodide at 80℃; for 1h; Inert atmosphere; Sonication;80%
With sodium carbonate In N,N-dimethyl-formamide at 120℃; for 12h;65%
With 1-Butylimidazole; copper(l) iodide In toluene at 160℃; for 16h; Inert atmosphere;78 %Chromat.
potassium hexacyanoferrate(II)

potassium hexacyanoferrate(II)

1,2-dibromobenzene
583-53-9

1,2-dibromobenzene

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With 1-Butylimidazole; copper(l) iodide In toluene at 160℃; for 16h;78%
(1-chloroethyl)trimethylsilane
7787-87-3

(1-chloroethyl)trimethylsilane

4-hydroxy-1,2-benzenedicarbonitrile
30757-50-7

4-hydroxy-1,2-benzenedicarbonitrile

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With hydrogenchloride; potassium carbonate In N,N-dimethyl-formamide77%
3-nitrobenzene-1,2-dicarbonitrile
51762-67-5

3-nitrobenzene-1,2-dicarbonitrile

Chloromethyltrimethylsilane
2344-80-1

Chloromethyltrimethylsilane

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With hydrogenchloride; potassium carbonate; sodium nitrite In 1-methyl-pyrrolidin-2-one; N,N-dimethyl acetamide74.7%
3-hydroxylphthalonitrile
116039-49-7

3-hydroxylphthalonitrile

Chloromethyltrimethylsilane
2344-80-1

Chloromethyltrimethylsilane

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With hydrogenchloride; potassium carbonate In N,N-dimethyl-formamide73%
(3-chloropropyl)trimethylsilane
2344-83-4

(3-chloropropyl)trimethylsilane

3-hydroxylphthalonitrile
116039-49-7

3-hydroxylphthalonitrile

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With hydrogenchloride; potassium carbonate In N,N-dimethyl acetamide; dimethyl sulfoxide71.2%
tetra-n-butylammonium cyanide
10442-39-4

tetra-n-butylammonium cyanide

C13H9N3S
114650-54-3

C13H9N3S

A

2-(phenylthio)benzonitrile
91804-55-6

2-(phenylthio)benzonitrile

B

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
In dimethyl sulfoxide at 25℃; for 0.75h; Irradiation;A 13%
B 63%
C13H9N3S
114650-54-3

C13H9N3S

A

2-(phenylthio)benzonitrile
91804-55-6

2-(phenylthio)benzonitrile

B

phthalonitrile
91-15-6

phthalonitrile

Conditions
ConditionsYield
With tetra-n-butylammonium cyanide In dimethyl sulfoxide at 25℃; for 1h; Irradiation;A 13%
B 63%
Conditions
ConditionsYield
With ammonia; sulfur at 100℃; for 6h; titanium autoclave; var. cat.: sodium hydrosulfide, benzenethiol; add of MeOH;100%
With ammonia; sodium methylate In methanol 1 h then reflux, 3 h;90%
With ammonia for 5h; Heating;52%
phthalonitrile
91-15-6

phthalonitrile

29H,31H-Phthalocyanine
574-93-6

29H,31H-Phthalocyanine

Conditions
ConditionsYield
With 1,8-diazabicyclo[5.4.0]-undecen-7-ene In ethylene glycol at 35 - 40℃; for 3h; Product distribution; Further Variations:; Temperatures; Solvents; Reagents; UV-irradiation;100%
With sodium methylate; blue zeolite In methanol at 40℃; for 72h;76%
With ammonium sulfate; 1,1,1,3,3,3-hexamethyl-disilazane In N,N-dimethyl-formamide at 150℃; for 24h;72%
(S)-valinol
2026-48-4

(S)-valinol

phthalonitrile
91-15-6

phthalonitrile

1,2-bis[(4S)-(4-isopropyl-Δ2-1,3-oxazolin-2-yl)]benzene
131380-80-8

1,2-bis[(4S)-(4-isopropyl-Δ2-1,3-oxazolin-2-yl)]benzene

Conditions
ConditionsYield
In neat (no solvent) at 150℃; for 1h; Microwave irradiation;100%
With zinc(II) chloride In toluene for 96h; Heating;92%
With zinc(II) chloride In chlorobenzene for 24h; Heating;89%
With polyvinylpyrrolidone capped poly [Zn(2,6-bis(2H-1,2,3,4-tetrazol-2-id-5-yl)pyridine)H2O] nanocrystal In chlorobenzene for 15h; Reflux;84%
phthalonitrile
91-15-6

phthalonitrile

/PBGZJ115-1120/

/PBGZJ115-1120/

2-(4-Methoxy-phenyl)-3-[(Z)-4-methoxy-phenylimino]-2,3-dihydro-isoindol-1-one

2-(4-Methoxy-phenyl)-3-[(Z)-4-methoxy-phenylimino]-2,3-dihydro-isoindol-1-one

Conditions
ConditionsYield
In tetrahydrofuran at 55℃; for 1h;100%
phthalonitrile
91-15-6

phthalonitrile

phthalimide
136918-14-4

phthalimide

Conditions
ConditionsYield
With manganese(IV) oxide; silica gel In chlorobenzene for 5h; Heating;100%
With 1,3-dimethyl-1H-imidazol-3-ium hydrogen carbonate; water In ethanol at 80℃; for 4h; Catalytic behavior; Green chemistry; chemoselective reaction;90%
With copper(II) acetate monohydrate In water; acetic acid Reflux;71%
With sodium tetrahydroborate In ethanol; water at 80℃; for 4h; regioselective reaction;94 %Chromat.
nickel
7440-02-0

nickel

phthalonitrile
91-15-6

phthalonitrile

nickel(II) phthalocyanine
14055-02-8

nickel(II) phthalocyanine

Conditions
ConditionsYield
With sodium methylate In methanol pyrophoric Ni under water layer added to a methanol soln. containing an equivalent quantity of phthalonitrile and 5 drops of 30% soln of CH3ONa in methanol; flask maintained at 25°C for 24-72 h; blue product separated from unreacted metal by shaking and decanting with the solvent, washed with ethanol in Soxhlet equipment and dried in air; purity of 95-97%; elem. anal.;100%
With sodium methylate In methanol; water pyrophoric metal:phthalonitrile=1:4 and few drops of CH3ONa under water layer treated for 24 h at 25°C; septd., washed (ethanol), dried in air, elem. anal.;100%
With sodium methylate In ethanol pyrophoric Ni under water layer added to an ethanol soln. containing an equivalent quantity of phthalonitrile and 5 drops of 30% soln of CH3ONa in methanol; flask maintained at 25°C for 24-72 h; blue product separated from unreacted metal by shaking and decanting with the solvent, washed with ethanol in Soxhlet equipment and dried in air; purity of 95-97%; elem. anal.;100%
phthalonitrile
91-15-6

phthalonitrile

zinc(II) phthalocyanine
14320-04-8

zinc(II) phthalocyanine

Conditions
ConditionsYield
With sodium methylate In methanol Sonication; Zn added to a methanol soln. containing an equivalent quantity of phthalonitrile and 5 drops of 30% soln of CH3ONa in methanol; flask put into an ultrasonic cleaner and maintained at 50°C for 24-72 h; blue product separated from unreacted metal by shaking and decanting with the solvent, washed with ethanol in Soxhlet equipment and dried in air; purity of 95-97%; elem. anal.;100%
With sodium methylate In further solvent(s) Sonication; Zn added to an 1-octanol soln. containing an equivalent quantity of phthalonitrile and 5 drops of 30% soln of CH3ONa in methanol; flask put intoan ultrasonic cleaner and maintained at 50°C for 24-72 h; blue product separated from unreacted metal by shaking and decanting with the solvent, washed with ethanol in Soxhlet equipment and dried in air; purity of 95-97%; elem. anal.;100%
With sodium methylate In methanol Sonication; Zn added to a methanol soln. containing an equivalent quantity of phthalonitrile and 5 drops of 30% soln of CH3ONa in methanol; flask put into an ultrasonic cleaner and maintained at 40°C for 24-72 h; blue product separated from unreacted metal by shaking and decanting with the solvent, washed with ethanol in Soxhlet equipment and dried in air; purity of 95-97%; elem. anal.;85%
sodium hexachloroiridate

sodium hexachloroiridate

phthalonitrile
91-15-6

phthalonitrile

chloro(phthalodinitile)phthalocyaninato(2-)iridate(III)
14096-14-1, 187386-26-1

chloro(phthalodinitile)phthalocyaninato(2-)iridate(III)

Conditions
ConditionsYield
With NH4I In neat (no solvent) byproducts: [IrI(PDN)Pc(2-)]; boiling (10 min); extraction (acetone), pptn. (HCl, boiling), centrifugation, washing (H2O), drying (vac.);100%
aluminum (III) chloride
7446-70-0, 7784-13-6

aluminum (III) chloride

urea
57-13-6

urea

phthalonitrile
91-15-6

phthalonitrile

chloroaluminum phthalocyanine
14154-42-8, 62905-77-5

chloroaluminum phthalocyanine

Conditions
ConditionsYield
With ammonium molybdate at 200℃; for 12h;99.26%
methylamine
74-89-5

methylamine

phthalonitrile
91-15-6

phthalonitrile

1,3-bis(methylimino)-isoindoline
88988-76-5, 89130-82-5, 93698-08-9, 93698-09-0

1,3-bis(methylimino)-isoindoline

Conditions
ConditionsYield
sulfur at 40℃; for 3h; titanium autoclave;99%
sulfur at 40℃; for 3h; titanium autoclave; var. primary amines;99%
phthalonitrile
91-15-6

phthalonitrile

5-(2-cyanophenyl)tetrazole
71515-74-7

5-(2-cyanophenyl)tetrazole

Conditions
ConditionsYield
With sodium azide In water at 100℃; for 0.666667h; Reagent/catalyst;99%
With sodium azide at 120℃; for 0.583333h; Reagent/catalyst;99%
With sodium azide at 120℃; for 0.0833333h;97%
Conditions
ConditionsYield
With sodium methylate In methanol Sonication; Cu added to a methanol soln. containing an equivalent quantity of phthalonitrile and 5 drops of 30% soln of CH3ONa in methanol; flask put into an ultrasonic cleaner and maintained at 50°C for 24-72 h; blue product separated from unreacted metal by shaking and decanting with the solvent, washed with ethanol in Soxhlet equipment and dried in air; purity of 95-97%; elem. anal.;99%
With sodium methylate In ethanol Sonication; Cu added to an ethanol soln. containing an equivalent quantity of phthalonitrile and 5 drops of 30% soln of CH3ONa in methanol; flask put into an ultrasonic cleaner and maintained at 50°C for 24-72 h; blue product separated from unreacted metal by shaking and decanting with the solvent, washed with ethanol in Soxhlet equipment and dried in air; purity of 95-97%; elem. anal.;99%
With sodium methylate In methanol Sonication; Cu added to a methanol soln. containing an equivalent quantity of phthalonitrile and 5 drops of 30% soln of CH3ONa in methanol; flask put into an ultrasonic cleaner and maintained at 25°C for 24-72 h; blue product separated from unreacted metal by shaking and decanting with the solvent, washed with ethanol in Soxhlet equipment and dried in air; purity of 95-97%; elem. anal.;60%
4-(2-cyanoacetyl)benzoic acid
122545-30-6

4-(2-cyanoacetyl)benzoic acid

phthalonitrile
91-15-6

phthalonitrile

C28H15N3O6

C28H15N3O6

Conditions
ConditionsYield
Stage #1: phthalonitrile With sodium methylate In 5,5-dimethyl-1,3-cyclohexadiene at 5℃; for 6.5h;
Stage #2: 4-(2-cyanoacetyl)benzoic acid With acetic acid In 5,5-dimethyl-1,3-cyclohexadiene at 5 - 45℃; for 26h; Solvent;
99%
Stage #1: phthalonitrile With sodium methylate In methanol at 5℃; for 13.5h;
Stage #2: 4-(2-cyanoacetyl)benzoic acid With acetic acid In methanol at 20 - 40℃; for 100h;
silver hexafluoroantimonate

silver hexafluoroantimonate

C104H108Au2Cl2N2O12P2

C104H108Au2Cl2N2O12P2

phthalonitrile
91-15-6

phthalonitrile

C112H112Au2N4O12P2(2+)*2F6Sb(1-)

C112H112Au2N4O12P2(2+)*2F6Sb(1-)

Conditions
ConditionsYield
In dichloromethane at 23℃; for 1h; Inert atmosphere;99%
aluminum (III) chloride
7446-70-0, 7784-13-6

aluminum (III) chloride

phthalonitrile
91-15-6

phthalonitrile

chloroaluminum phthalocyanine
14154-42-8

chloroaluminum phthalocyanine

Conditions
ConditionsYield
With ammonium chloride at 200℃; for 10.5h; Reagent/catalyst; Concentration;98.4%
With 1,8-diazabicyclo[5.4.0]undec-7-ene In pentan-1-ol at 136℃; for 5h; Inert atmosphere;
With 1,8-diazabicyclo[5.4.0]undec-7-ene In pentan-1-ol at 136℃; for 5h;
1-(pyridine-4-oxy) 3,4-dicyanobenzene
380896-89-9

1-(pyridine-4-oxy) 3,4-dicyanobenzene

indium(III) chloride

indium(III) chloride

phthalonitrile
91-15-6

phthalonitrile

2-[4-(pyridyloxy)phthalocyaninato]chloroindium(III)

2-[4-(pyridyloxy)phthalocyaninato]chloroindium(III)

Conditions
ConditionsYield
With 1,8-diazabicyclo[5.4.0]undec-7-ene In pentan-1-ol for 18h; Inert atmosphere; Reflux;98.2%
benzylamine
100-46-9

benzylamine

phthalonitrile
91-15-6

phthalonitrile

1,3-Bis-[(Z)-benzylimino]-2,3-dihydro-1H-isoindole
32313-76-1

1,3-Bis-[(Z)-benzylimino]-2,3-dihydro-1H-isoindole

Conditions
ConditionsYield
sulfur at 40℃; for 1h;98%
(2S)-2-phenylglycinol
20989-17-7

(2S)-2-phenylglycinol

phthalonitrile
91-15-6

phthalonitrile

1,2-bis<(4S)-4-phenyl-2-oxazolin-2-yl>benzene
131380-82-0

1,2-bis<(4S)-4-phenyl-2-oxazolin-2-yl>benzene

Conditions
ConditionsYield
at 150℃; for 1h; Microwave irradiation;98%
With zinc(II) chloride In chlorobenzene for 24h; Heating;66%
phthalonitrile
91-15-6

phthalonitrile

copper phthalocyanine
147-14-8

copper phthalocyanine

Conditions
ConditionsYield
With CuCl2*2H2O for 0.166667h; microwave irradiation;98%
With CuCl2*2H2O at 190 - 210℃; for 0.25h; microwave irradiation;88%
With copper diacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene at 140℃; for 0.0833333h;76%
With 1,1,1,3,3,3-hexamethyl-disilazane; copper(ll) bromide In N,N-dimethyl-formamide at 100℃; for 10h;74%
4-Butyl-cyclohexanecarboxylic acid hydrazide

4-Butyl-cyclohexanecarboxylic acid hydrazide

phthalonitrile
91-15-6

phthalonitrile

N'-(3-amino-1H-isoindol-1-ylidene)-4-butylcyclohexanecarbohydrazide

N'-(3-amino-1H-isoindol-1-ylidene)-4-butylcyclohexanecarbohydrazide

Conditions
ConditionsYield
With sodium hydroxide In methanol for 5h; Heating;98%
Trimethylenediamine
109-76-2

Trimethylenediamine

phthalonitrile
91-15-6

phthalonitrile

2-(1,4,5,6-tetrahydropyrimidin-2-yl)benzonitrile
1476807-78-9

2-(1,4,5,6-tetrahydropyrimidin-2-yl)benzonitrile

Conditions
ConditionsYield
With bis(2-hydroxy-κO-2-phenylacetato)copper(II); iodine; sodium acetate In toluene at 90℃; for 0.333333h; Time; Microwave irradiation; chemoselective reaction;97%
(3-(trifluoromethyl)benzyl)zinc chloride * lithium chloride

(3-(trifluoromethyl)benzyl)zinc chloride * lithium chloride

phthalonitrile
91-15-6

phthalonitrile

2-(3-(trifluoromethyl)benzyl)benzonitrile
670-74-6

2-(3-(trifluoromethyl)benzyl)benzonitrile

Conditions
ConditionsYield
In tetrahydrofuran at 40℃; for 0.5h; Reagent/catalyst; Inert atmosphere; Microwave irradiation;97%
propylamine
107-10-8

propylamine

phthalonitrile
91-15-6

phthalonitrile

1,3-Bis-[(Z)-propylimino]-2,3-dihydro-1H-isoindole
93423-55-3

1,3-Bis-[(Z)-propylimino]-2,3-dihydro-1H-isoindole

Conditions
ConditionsYield
sulfur for 2h; Heating;96%
isobutyric acid hydrazide
3619-17-8

isobutyric acid hydrazide

phthalonitrile
91-15-6

phthalonitrile

N'-(3-amino-1H-isoindol-1-ylidene)-2-methytlpropanohydrazide

N'-(3-amino-1H-isoindol-1-ylidene)-2-methytlpropanohydrazide

Conditions
ConditionsYield
In methanol for 5h; Heating;96%
phthalonitrile
91-15-6

phthalonitrile

tin(ll) chloride

tin(ll) chloride

phthalocyanine tin(IV) dichloride
18253-54-8

phthalocyanine tin(IV) dichloride

Conditions
ConditionsYield
In further solvent(s) SnCl2 and phthalonitrile were added to 1-chloronaphthalene (solvent); brought to reflux over a period of 1 h; was allowed to reflux for 3 h; cooled slowly to room temperature; filtered; washed in benzene in a Soxhlet extractor for 24 h; elem. anal.;96%
3-methylpyridin-2-ylamine
1603-40-3

3-methylpyridin-2-ylamine

phthalonitrile
91-15-6

phthalonitrile

Co(3-MeBPI)2
79062-08-1

Co(3-MeBPI)2

Conditions
ConditionsYield
With sodium hydroxide In methanol; toluene 1,2-dicyanobenzene and 2-amino-3-methylpyridine heated in oil bath to 210°C for 3 h, mixt. cooled to ambient temp., toluene added, temp.increased to 90°C, NaOH in methanol added, Co(OAc)2 in methanol added and mixt. heated for 1 h; mixt. cooled to 40°C, product filtered, washed with methanol, diethyl ether and dried;96%
With sodium hydroxide In methanol; toluene 1,2-dicyanobenzene and 2-amino-3-methylpyridine heated in oil bath to 210°C for 4 h, mixt. cooled to 210°C., toluene added, NaOH in methanol added and stirred for 5 min, Co(OAc)2 in methanol added and mixt. stirredd for 45 min; mixt. cooled to 40°C, product filtered, washed with methanol, diethyl ether and dried in vacuo at 80°C;
(2-picolyl)diethylborane dimer
1393596-93-4

(2-picolyl)diethylborane dimer

phthalonitrile
91-15-6

phthalonitrile

(Et2B)2(1,2-(NHC(CHC5H4N))2C6H4)
1393596-99-0

(Et2B)2(1,2-(NHC(CHC5H4N))2C6H4)

Conditions
ConditionsYield
In toluene (inert atm.); reaction of boron compd. and 1 equiv. of dicyanobenzene intoluene at 70°C for 4 h;96%
In toluene at 70℃; for 4h; Inert atmosphere;96%
thiosemicarbazide
79-19-6

thiosemicarbazide

phthalonitrile
91-15-6

phthalonitrile

3-amino-1H-isoindol-1-one thiosemicarbazone

3-amino-1H-isoindol-1-one thiosemicarbazone

Conditions
ConditionsYield
With sodium hydroxide for 2h; Reflux;96%
phthalonitrile
91-15-6

phthalonitrile

zinc phthalocyanine
14320-04-8

zinc phthalocyanine

Conditions
ConditionsYield
With zinc acetate dihydrate; N,N-dimethyl-formamide at 200℃; for 0.166667h; Microwave irradiation; Sealed tube;95%
With N-ethyl-N-hydroxy-ethanamine; zinc(II) chloride at 80℃; for 0.25h;45%

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