CAS No.103-71-9,Phenyl isocyanate Suppliers,MSDS download

: 582-61-6
benzoyl azide

: 103-71-9
phenyl isocyanate

Conditions

Conditions	Yield
In dichloromethane Irradiation;	100%
In acetonitrile for 16h; Inert atmosphere; Reflux;	100%
With water for 5h; Inert atmosphere; UV-irradiation; Sealed tube; chemoselective reaction;	95%

: 32315-10-9
bis(trichloromethyl) carbonate

: 62-53-3
aniline

: 103-71-9
phenyl isocyanate

Conditions

Conditions	Yield
With triethylamine In dichloromethane	100%
In ethyl acetate at 0 - 5℃; for 3h; Solvent; Cooling with ice; Reflux;	89%
In chloroform at 20℃; for 1h; Cooling with ice;	85%

: 101-99-5
N-carboethoxyaniline

: 103-71-9
phenyl isocyanate

Conditions

Conditions	Yield
With Phenyltrichlorosilane at 100 - 180℃; for 1h;	99%
With phosphorus pentoxide
With phosphorus pentoxide at 170℃; under 100 Torr; man fraktioniert das ueberdestillierte Phenylisocyanat;

: 18100-80-6
2,3,5-triphenyl-4-thiazolone

: 762-42-5
dimethyl acetylenedicarboxylate

A: 20851-13-2
dimethyl 2,5-diphenylthiophene-3,4-dicarboxylate

B: 103-71-9
phenyl isocyanate

Conditions

Conditions	Yield
In xylene Heating;	A 99% B n/a

...Expand

: 75-44-5
phosgene

: 62-53-3
aniline

: 103-71-9
phenyl isocyanate

Conditions

Conditions	Yield
In toluene at -5 - 75℃; Solvent;	98%
Stage #1: phosgene; n-butyl isocyanide In chlorobenzene at 81℃; for 2.33333h; Stage #2: aniline In chlorobenzene at 81 - 88℃; for 1h;	76%
With 1-Chloronaphthalene at 230 - 240℃; unter Durchleiten durch ein Porzellanrohr;

: 66702-57-6
2-dimethylamino-5-(4-nitro-phenyl)-4-oxo-3-phenyl-4,5-dihydro-thiazolium betaine

: 762-42-5
dimethyl acetylenedicarboxylate

A: 103-71-9
phenyl isocyanate

B: 85013-66-7
2-Dimethylamino-5-(4-nitro-phenyl)-thiophene-3,4-dicarboxylic acid dimethyl ester

Conditions

Conditions	Yield
In xylene Heating;	A n/a B 98%

...Expand

: 66702-60-1
2-cyano-5-(4-nitro-phenyl)-4-oxo-3-phenyl-4,5-dihydro-thiazolium betaine

: 762-42-5
dimethyl acetylenedicarboxylate

A: 103-71-9
phenyl isocyanate

B: 85013-63-4
2-Cyano-5-(4-nitro-phenyl)-thiophene-3,4-dicarboxylic acid dimethyl ester

Conditions

Conditions	Yield
In xylene Heating;	A n/a B 98%

...Expand

: 59208-07-0
5-(4-nitro-phenyl)-4-oxo-2,3-diphenyl-4,5-dihydro-thiazolium betaine

: 762-42-5
dimethyl acetylenedicarboxylate

A: 103-71-9
phenyl isocyanate

B: 59086-14-5
2-(4-Nitro-phenyl)-5-phenyl-thiophene-3,4-dicarboxylic acid dimethyl ester

Conditions

Conditions	Yield
In xylene Heating;	A n/a B 97%

...Expand

: 103-72-0
phenyl isothiocyanate

: 103-71-9
phenyl isocyanate

Conditions

Conditions	Yield
With air; palladium dichloride In 1,4-dioxane Heating;	96%
With mercury(II) oxide at 170℃;
Multi-step reaction with 3 steps 1: sodium hydride / 5,5-dimethyl-1,3-cyclohexadiene; mineral oil / 2 h / 20 °C / Inert atmosphere 2: chloroform / 1 h / 20 °C 3: acetonitrile / 25 °C View Scheme

: 622-46-8
carbamic acid phenyl ester

: 103-71-9
phenyl isocyanate

Conditions

Conditions	Yield
In chlorobenzene at 160 - 240℃; under 11251.1 Torr; for 1h; Pressure; Solvent; Temperature; Inert atmosphere; Green chemistry;	94.9%

: 66702-58-7
5-(4-nitro-phenyl)-4-oxo-3-phenyl-2-phenylsulfanyl-4,5-dihydro-thiazolium betaine

: 762-42-5
dimethyl acetylenedicarboxylate

A: 103-71-9
phenyl isocyanate

B: 85013-62-3
2-(4-Nitro-phenyl)-5-phenylsulfanyl-thiophene-3,4-dicarboxylic acid dimethyl ester

Conditions

Conditions	Yield
In xylene Heating;	A n/a B 94%

...Expand

: 56409-80-4
5-benzyl-3,4-dihydro-4-oxo-1,2,3-triphenylpyrimidin-1-ium-6-olate

: 2983-74-6
4-methoxyphenyl cyanate

A: 103-71-9
phenyl isocyanate

B: 85037-41-8
5-Benzyl-6-(4-methoxy-phenoxy)-2,3-diphenyl-3H-pyrimidin-4-one

C: 25940-64-1
2,4,6-tris(4-methoxyphenoxy)-1,3,5-triazine

Conditions

Conditions	Yield
In chlorobenzene for 29h; Heating;	A n/a B 93% C n/a

...Expand

: 27983-93-3
3,3-Dimethyl-1-phenyl-2-azetidinone

A: 103-71-9
phenyl isocyanate

B: 115-11-7
isobutene

Conditions

Conditions	Yield
at 750℃; under 0.002 Torr;	A 93% B n/a

: 100-52-7
benzaldehyde

: 103-71-9
phenyl isocyanate

Conditions

Conditions	Yield
In chloroform at 60℃; for 18h;	92%

: 56409-80-4
5-benzyl-3,4-dihydro-4-oxo-1,2,3-triphenylpyrimidin-1-ium-6-olate

: 1122-85-6
phenyl cyanate

A: 1919-48-8
2,4,6-triphenoxy-1,3,5-triazine

B: 103-71-9
phenyl isocyanate

C: 85037-39-4
5-Benzyl-6-phenoxy-2,3-diphenyl-3H-pyrimidin-4-one

Conditions

Conditions	Yield
In chlorobenzene for 18h; Heating;	A n/a B n/a C 92%

...Expand

: 61522-23-4
2-cyano-4-oxo-3,5-diphenyl-4,5-dihydro-thiazolium betaine

: 762-42-5
dimethyl acetylenedicarboxylate

A: 103-71-9
phenyl isocyanate

B: 85013-64-5
2-Cyano-5-phenyl-thiophene-3,4-dicarboxylic acid dimethyl ester

Conditions

Conditions	Yield
In xylene Heating;	A n/a B 92%

...Expand

: 4-Methyl-3,5-dioxo-2,6-diphenyl-2,6-diazabicyclo<2.2.2>oct-7-en-7-carbonsaeure-methylester

A: 103-71-9
phenyl isocyanate

B: 1,2-Dihydro-3-methyl-2-oxo-1-phenyl-5-pyridincarbonsaeure-methylester

Conditions

Conditions	Yield
at 220℃; for 0.166667h;	A n/a B 92%

: 4-Benzyl-7,8-bis(diethylamino)-2,6-diphenyl-2,6-diazabicyclo<2.2.2>oct-7-en-3,5-dion

A: 103-71-9
phenyl isocyanate

B: 3-Benzyl-4,5-bis(diethylamino)-1-phenyl-2(1H)-pyridinon

Conditions

Conditions	Yield
at 150℃; for 0.166667h;	A n/a B 92%

: 2603-10-3
N-phenyl methyl carbamate

: 103-71-9
phenyl isocyanate

Conditions

Conditions	Yield
With Phenyltrichlorosilane at 85 - 184℃; for 1h;	90.8%
With phosphorus pentachloride at 120 - 140℃; for 3h;	68%
With boron trichloride; triethylamine In benzene for 0.5h; Heating;	93 % Chromat.

: 201230-82-2
carbon monoxide

: 98-95-3
nitrobenzene

: 103-71-9
phenyl isocyanate

Conditions

Conditions	Yield
With pyridine; di(rhodium)tetracarbonyl dichloride; pyridine hydrochloride In chlorobenzene at 205℃; under 50 Torr; for 1h;	90%
With di(rhodium)tetracarbonyl dichloride; pyridine hydrochloride In chlorobenzene at 190℃; under 38000 Torr; for 1h;	80%
Stage #1: nitrobenzene at 120℃; under 75007.5 Torr; for 4h; Inert atmosphere; Autoclave; Stage #2: carbon monoxide Catalytic behavior; Temperature; Reagent/catalyst; Inert atmosphere; Autoclave;	72.2%

: 109853-15-8
C16H16N4OS2

A: 103-71-9
phenyl isocyanate

B: 13281-49-7
3-Mercapto-1-methyl-5-phenyl-1,2,4-triazol

Conditions

Conditions	Yield
N-benzyl-N,N,N-triethylammonium chloride In sodium hydroxide; dichloromethane for 12h; Ambient temperature;	A n/a B 89%

: 77219-88-6
bis(trimethylsilyl)benzohydroxamic acid

A: 107-46-0
Hexamethyldisiloxane

B: 103-71-9
phenyl isocyanate

Conditions

Conditions	Yield
at 120℃;	A n/a B 88%

: N-(2,2-dimethyl-3-butynoyl)-N,N'-diphenylurea

A: 103-71-9
phenyl isocyanate

B: 2,2-dimethyl-N-phenyl-3-butynamide

Conditions

Conditions	Yield
In benzene for 2h; Heating;	A n/a B 88%

: 5099-95-6
1-phenylazetidin-2-one

A: 74-85-1
ethene

B: 103-71-9
phenyl isocyanate

Conditions

Conditions	Yield
at 750℃; under 0.002 Torr; Mechanism; regioselectivity, other substituted 1-phenylazetidin-2-ones, var. temp.;	A n/a B 88%
at 750℃; under 0.002 Torr;	A n/a B 88%

: 24424-95-1
di-tert-butyl tricarbonate

: 62-53-3
aniline

: 103-71-9
phenyl isocyanate

Conditions

Conditions	Yield
In dichloromethane for 0.0833333h; Ambient temperature;	87%

: 495-18-1
Benzohydroxamic acid

: 103-71-9
phenyl isocyanate

Conditions

Conditions	Yield
With Phenyltrichlorosilane at 55 - 197℃; for 2h;	86%
With Phenyltrichlorosilane at 55 - 197℃; for 2h; Product distribution; var. silanes, var. time, var. temp.;	86%
With Phenyltrichlorosilane at 100 - 130℃; for 2h;	81.9%

: 67723-48-2
N-Benzoyl-N,O-bis(trimethylsilyl)hydroxylamine

A: 1821-33-6
N-phenyl-N'-benzoylurea

B: 103-71-9
phenyl isocyanate

Conditions

Conditions	Yield
In decalin at 160℃; for 0.0833333h;	A 5.7% B 86%

: 22513-32-2
acid sodium salt of benzohydroxamic acid

: 103-71-9
phenyl isocyanate

Conditions

Conditions	Yield
With Phenyltrichlorosilane at 130 - 140℃; for 2h;	86%
With Phenyltrichlorosilane at 130 - 140℃; for 2h;	85.8%

: 4-Methyl-3,5-dioxo-2,6-diphenyl-2,6-diazabicyclo<2.2.2>oct-7-en-7,8-dicarbonsaeure-dimethylester

A: 103-71-9
phenyl isocyanate

B: 1,2-Dihydro-3-methyl-2-oxo-1-phenyl-4,5-pyridindicarbonsaeure-dimethylester

Conditions

Conditions	Yield
at 220℃; for 0.166667h;	A n/a B 85%

: 110-91-8
morpholine

: 103-71-9
phenyl isocyanate

: 4559-92-6
N-phenylmorpholine-4-carboxamide

Conditions

Conditions	Yield
at 0 - 20℃; for 48.3333h;	100%
In diethyl ether at 20℃; for 18h;	99.2%
In diethyl ether at 20℃; for 0.75h; Addition;	97%

: 288-32-4
1H-imidazole

: 103-71-9
phenyl isocyanate

: 33876-94-7
N-phenyl-1H-imidazole-1-carboxamide

Conditions

Conditions	Yield
In dichloromethane at 20℃; for 1h;	100%
In 1,4-dioxane at 0 - 20℃;	87%
In diethyl ether for 3h; Heating;	84%

: 61-54-1
tryptamine

: 103-71-9
phenyl isocyanate

: 32585-51-6
N-[2-(1H-indol-3-yl)ethyl]-N'-phenylurea

Conditions

Conditions	Yield
Stage #1: tryptamine; phenyl isocyanate In dichloromethane at 60℃; Stage #2: With isatoic anhydride-N-(CH2)3-C8F17 In dichloromethane at 60℃; for 2.5h;	100%
In dichloromethane at 60℃; for 5h; Inert atmosphere; Sealed reaction vessel;	98%

: 34803-66-2
1-(2-pyridyl)piperazine

: 103-71-9
phenyl isocyanate

: 4-[2]pyridyl-piperazine-1-carboxylic acid anilide

Conditions

Conditions	Yield
Stage #1: 1-(2-pyridyl)piperazine; phenyl isocyanate In dichloromethane at 60℃; Stage #2: With isatoic anhydride-N-(CH2)3-C8F17 In dichloromethane at 60℃; for 2.5h;	100%

: 67-56-1
methanol

: 103-71-9
phenyl isocyanate

: 2603-10-3
N-phenyl methyl carbamate

Conditions

Conditions	Yield
With cerium(IV) oxide; carbon dioxide at 170℃; under 30003 Torr; for 12h; Inert atmosphere; Autoclave;	100%
With dibutyltin dilaurate at 50℃; for 3h;	100%
at 80℃; for 0.5h; Inert atmosphere;	98%

: 103-71-9
phenyl isocyanate

: 556-82-1
3-methyl-2-buten-1-ol

: 105902-61-2
3-methylbut-2-en-1-yl phenylcarbamate

Conditions

Conditions	Yield
In acetonitrile at 70℃; for 23h; Inert atmosphere;	100%
With triethylamine In dichloromethane at 20℃; Inert atmosphere;	88%
With triethylamine In dichloromethane at 20℃;	88%

: 2216-51-5
(-)-menthol

: 103-71-9
phenyl isocyanate

: 637336-84-6
phenylcarbamic acid (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl ester

Conditions

Conditions	Yield
With MoCl2O2(dmf)2 In dichloromethane at 20℃; for 0.333333h;	100%
With MoCl2O2(dmf)2 In dichloromethane at 20℃; for 0.333333h; Reagent/catalyst; Inert atmosphere; Sealed tube;	100%

: 103-71-9
phenyl isocyanate

: 107-19-7
propargyl alcohol

: 5416-67-1
2-propynyl phenylcarbamate

Conditions

Conditions	Yield
With dmap; triethylamine In tetrahydrofuran at 20℃; for 90h;	100%
With MoCl2O2(dmf)2 In dichloromethane at 20℃; for 0.333333h;	100%
With MoCl2O2(dmf)2 In dichloromethane at 20℃; for 0.333333h; Inert atmosphere; Sealed tube;	100%

: 103-71-9
phenyl isocyanate

: 109-73-9
N-butylamine

: 3083-88-3
N-butyl-N'-phenylurea

Conditions

Conditions	Yield
Stage #1: phenyl isocyanate; N-butylamine In dichloromethane at 60℃; Stage #2: With isatoic anhydride-N-(CH2)3-C8F17 In dichloromethane at 60℃; for 2.5h;	100%
at 20℃;	98%
In hexane at 25℃; Cooling with ice;	98%

: 103-71-9
phenyl isocyanate

: 62-53-3
aniline

: 102-07-8
bis(diphenyl)urea

Conditions

Conditions	Yield
With triethylamine In dichloromethane	100%
In acetic acid for 0.0833333h;	98%
In hexane	95%

: 103-71-9
phenyl isocyanate

: 156-43-4
4-Ethoxyaniline

: 4345-85-1
1-(4-ethoxy-phenyl)-3-phenyl urea

Conditions

Conditions	Yield
In tetrahydrofuran for 0.166667h;	100%
With diethyl ether

: 103-71-9
phenyl isocyanate

: 115-19-5
2-methyl-but-3-yn-2-ol

: 6289-19-6
O-α,α-dimethylpropargyl N-phenylcarbamate

Conditions

Conditions	Yield
With MoCl2O2(dmf)2 In dichloromethane at 20℃; for 0.333333h;	100%
With triethylamine In tetrahydrofuran at 70℃; for 12h; Inert atmosphere;	94%
With dmap; triethylamine In tetrahydrofuran at 20℃; for 90h;	88%

: 103-71-9
phenyl isocyanate

: 104-84-7
para-methylbenzylamine

: 35305-46-5
N-(4-methylbenzyl)-N’-phenylurea

Conditions

Conditions	Yield
Stage #1: phenyl isocyanate; para-methylbenzylamine In dichloromethane at 60℃; Stage #2: With isatoic anhydride-N-(CH2)3-C8F17 In dichloromethane at 60℃; for 2.5h;	100%

: 103-71-9
phenyl isocyanate

: 71-36-3
butan-1-ol

: 1538-74-5
N-phenyl-carbamic acid butyl ester

Conditions

Conditions	Yield
chlorodi-(n-butyl)tin acetate In chloroform for 0.833333h; Product distribution; Mechanism; Ambient temperature; catalytic activity, various tin(IV) catalysts;	100%
chlorodi-(n-butyl)tin acetate In chloroform for 0.833333h; Ambient temperature;	100%
With diallyltin(IV)di(2-ethyl hexanoate) In dichloromethane for 0.0833333h; Product distribution; Heating; other alcohols and isocyanates; var. temp. and time;	93%

: 103-71-9
phenyl isocyanate

: 108-95-2
phenol

: 4930-03-4
phenyl N-phenylcarbamate

Conditions

Conditions	Yield
at 20℃; for 2h;	100%
With cesium fluoride	93.1%
With triethylamine In acetonitrile for 24.5h; Esterification;	89%

: 103-71-9
phenyl isocyanate

: 1785-02-0
triphenyl isocyanurate

Conditions

Conditions	Yield
With triethylamine In dichloromethane at 70℃; under 6000480 Torr; for 20h;	100%
With sodium nitrite for 0.166667h; Cyclization; microwave irradiation;	99%
With 1,3-bis(2,6-diisopropylphenyl)dihydroimidazol-2-ylidene In tetrahydrofuran at 20℃; for 1h;	99%

: 1483-24-5
1-methyl-1-benzoylhydrazine

: 103-71-9
phenyl isocyanate

: 13136-26-0
1-Benzoyl-1-methyl-4-phenylsemicarbazid

Conditions

Conditions	Yield
In tetrahydrofuran Heating;	100%
In diethyl ether
In ethanol

: 103-71-9
phenyl isocyanate

: 78-27-3
1-Ethynyl-1-cyclohexanol

: 73623-16-2
1-ethynylcyclohexyl phenylcarbamate

Conditions

Conditions	Yield
With dmap; triethylamine In tetrahydrofuran at 20℃; for 90h;	100%
In 1,2-dichloro-ethane at 20℃; for 16h;	82%
With 1-methyl-pyrrolidin-2-one

: 103-71-9
phenyl isocyanate

: 30389-18-5
1-Ethynylcyclohexylamine

: 42785-83-1
1-(1-ethynylcyclohexyl)-3-phenylurea

Conditions

Conditions	Yield
In tetrahydrofuran at 20℃;	100%
In diethyl ether

: 103-71-9
phenyl isocyanate

: 111-42-2
2,2'-iminobis[ethanol]

: 20074-78-6
1,1-[Di-(2-hydroxyethyl)]-3-phenylurea

Conditions

Conditions	Yield
In dichloromethane	100%
In benzene
In dichloromethane; toluene at 20℃;
In dichloromethane at 20℃; for 0.0166667h; Inert atmosphere;	1.14 g

: 2167-39-7
(+/-)-2-methyloxetane

: 103-71-9
phenyl isocyanate

: 99855-05-7
6-methyl-3-phenyl-1,3-oxazinan-2-one

Conditions

Conditions	Yield
With N,N,N,N,N,N-hexamethylphosphoric triamide; diphenyltin diiodide at 80℃; for 3h; sealed tube;	100%
With tetraphenyl stibonium iodide In tetrahydrofuran at 60℃; for 23h;	27%

: 106-88-7
ethyloxirane

: 103-71-9
phenyl isocyanate

: 105873-71-0
4-ethyl-3-phenyl-1,3-oxazolidine-2-one

Conditions

Conditions	Yield
With tetraphenyl stibonium iodide In dichloromethane at 40℃;	100%
tetraphenyl stibonium iodide In dichloromethane at 45℃; for 1h;	100%
tetraphenyl stibonium iodide In dichloromethane at 45℃; for 1h; Heating;	84%