As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap
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inquiryColorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/1112.html Product Name 5-(2R)-2-Oxiranyl-8-benzyloxy-2(1H)-quinolinone CAS No.
Cas:173140-90-4
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inquiryOur company was built in 2009 with an ISO certificate. In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so o
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by email in time prod
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryAdvantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best s
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiry5-(2R)-2-Oxiranyl-8-benzyloxy-2(1H)-quinolinone CAS:173140-90-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
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inquiryProduct name: sodium metabisulfite / sodium metabisulphite Molecular weight: 190.10 Specification: 25Kg woven bag Quality guarantee period: 6 months Appearance:white crystalline powder Storage:Room temperature, tight from air Packa
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryWhy Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiry(R)-8-(benzyloxy)-5-(oxiran-2-yl)quinolin-2(1H)-one CAS: 173140-90-4Appearance:Powder Storage:preserve in well sealed container, store in cool and dry place, away from strong light and heat, when store under above condition, the retest date is 2 yea
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:173140-90-4
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inquiryProduct name: 2(1H)-Quinlinone,5-(2R)-Oxiranyl-8-(Phenylmethoxy)- CAS No.:173140-90-4 Molecule Formula:C18H15NO3 Molecule Weight:293.31 Purity: 98% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standa
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiry5-(2R)-2-Oxiranyl-8-benzyloxy-2(1H)-quinolinone Basic information Product Name: 5-(2R)-2-Oxiranyl-8-benzyloxy-2(1H)-quinolinone Synonyms: (R)-8-(Benzyloxy)-5-(oxiran-2-yl)quinolin-2(1H)-one;2(1H)-Quinolinone, 5-(2R)-oxiranyl-8-(phenylmethoxy)-
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inquiryHANGZHOU THINK CHEMICAL CO., LTD. (THINKCHEM) is an integrative corporation of trade, research and contract manufacture. With about ten years of business experiences on the marketing & distribution, thinkchem specializes in exp
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inquiry(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
Conditions | Yield |
---|---|
With potassium carbonate In water; acetone for 5 - 10h; Heating / reflux; | |
With potassium carbonate In water; acetone for 5 - 10h; Heating / reflux; | |
With potassium carbonate In water; butanone Product distribution / selectivity; Heating / reflux; | |
With potassium carbonate In water; acetone Product distribution / selectivity; Heating / reflux; |
8-(benzyloxy)-5-[(1R)-2-bromo-1-hydroxyethyl]quinolin-2(1H)-one
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
Conditions | Yield |
---|---|
With potassium carbonate In water; acetone for 2.5h; Product distribution / selectivity; Heating / reflux; |
8-benzyloxy-5-(2-bromoacetyl)-1H-quinolin-2-one
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
Conditions | Yield |
---|---|
Stage #1: 8-benzyloxy-5-(2-bromoacetyl)-1H-quinolin-2-one With dimethylsulfide borane complex; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole In tetrahydrofuran; toluene at 0 - 2℃; for 1.75h; Stage #2: With piperidine; water In tetrahydrofuran; toluene at 0 - 2℃; for 1h; Product distribution / selectivity; | |
Multi-step reaction with 2 steps 1.1: dimethylsulfide borane complex / (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran; toluene / 3.25 - 3.33 h / 0 - 2 °C 1.2: 0.25 - 0.33 h 2.1: potassium carbonate / water; acetone / 2.5 h / Heating / reflux View Scheme |
8-quinolinol
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1.1: 1,2-dichloro-ethane / 2.25 - 2.33 h / 30 °C 1.2: 15.25 - 16.33 h / 25 - 70 °C 1.3: 0.25 - 0.33 h / 0 - 30 °C 2.1: hydrogenchloride; water / 0.25 - 0.33 h 3.1: potassium carbonate / acetone / 14 h / Heating / reflux 4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3.5 h / 20 - 30 °C 5.1: acetic anhydride / 2 h / 25 - 40 °C 6.1: boron trifluoride diethyl etherate / dichloromethane / Heating / reflux 6.2: 4.5 h / Heating / reflux 6.3: 30 °C / pH 8 - 9 7.1: dimethylsulfide borane complex / (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran; toluene / 1.75 h / 0 - 2 °C 7.2: 1 h / 0 - 2 °C View Scheme | |
Multi-step reaction with 8 steps 1.1: 1,2-dichloro-ethane / 2.25 - 2.33 h / 30 °C 1.2: 15.25 - 16.33 h / 25 - 70 °C 1.3: 0.25 - 0.33 h / 0 - 30 °C 2.1: hydrogenchloride; water / 0.25 - 0.33 h 3.1: potassium carbonate / acetone / 14 h / Heating / reflux 4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3.5 h / 20 - 30 °C 5.1: acetic anhydride / 2 h / 25 - 40 °C 6.1: boron trifluoride diethyl etherate / dichloromethane / Heating / reflux 6.2: 4.5 h / Heating / reflux 6.3: 30 °C / pH 8 - 9 7.1: dimethylsulfide borane complex / (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran; toluene / 3.25 - 3.33 h / 0 - 2 °C 7.2: 0.25 - 0.33 h 8.1: potassium carbonate / water; acetone / 2.5 h / Heating / reflux View Scheme |
5-acetyl-8-hydroxyquinoline
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: potassium carbonate / acetone / 14 h / Heating / reflux 2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3.5 h / 20 - 30 °C 3.1: acetic anhydride / 2 h / 25 - 40 °C 4.1: boron trifluoride diethyl etherate / dichloromethane / Heating / reflux 4.2: 4.5 h / Heating / reflux 4.3: 30 °C / pH 8 - 9 5.1: dimethylsulfide borane complex / (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran; toluene / 1.75 h / 0 - 2 °C 5.2: 1 h / 0 - 2 °C View Scheme | |
Multi-step reaction with 6 steps 1.1: potassium carbonate / acetone / 14 h / Heating / reflux 2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3.5 h / 20 - 30 °C 3.1: acetic anhydride / 2 h / 25 - 40 °C 4.1: boron trifluoride diethyl etherate / dichloromethane / Heating / reflux 4.2: 4.5 h / Heating / reflux 4.3: 30 °C / pH 8 - 9 5.1: dimethylsulfide borane complex / (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran; toluene / 3.25 - 3.33 h / 0 - 2 °C 5.2: 0.25 - 0.33 h 6.1: potassium carbonate / water; acetone / 2.5 h / Heating / reflux View Scheme |
1-(8-benzyloxyquinolin-5-yl)ethanone
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3.5 h / 20 - 30 °C 2.1: acetic anhydride / 2 h / 25 - 40 °C 3.1: boron trifluoride diethyl etherate / dichloromethane / Heating / reflux 3.2: 4.5 h / Heating / reflux 3.3: 30 °C / pH 8 - 9 4.1: dimethylsulfide borane complex / (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran; toluene / 1.75 h / 0 - 2 °C 4.2: 1 h / 0 - 2 °C View Scheme | |
Multi-step reaction with 5 steps 1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3.5 h / 20 - 30 °C 2.1: acetic anhydride / 2 h / 25 - 40 °C 3.1: boron trifluoride diethyl etherate / dichloromethane / Heating / reflux 3.2: 4.5 h / Heating / reflux 3.3: 30 °C / pH 8 - 9 4.1: dimethylsulfide borane complex / (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran; toluene / 3.25 - 3.33 h / 0 - 2 °C 4.2: 0.25 - 0.33 h 5.1: potassium carbonate / water; acetone / 2.5 h / Heating / reflux View Scheme |
5-Acetyl-8-benzyloxyquinoline-N-oxide
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: acetic anhydride / 2 h / 25 - 40 °C 2.1: boron trifluoride diethyl etherate / dichloromethane / Heating / reflux 2.2: 4.5 h / Heating / reflux 2.3: 30 °C / pH 8 - 9 3.1: dimethylsulfide borane complex / (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran; toluene / 1.75 h / 0 - 2 °C 3.2: 1 h / 0 - 2 °C View Scheme | |
Multi-step reaction with 4 steps 1.1: acetic anhydride / 2 h / 25 - 40 °C 2.1: boron trifluoride diethyl etherate / dichloromethane / Heating / reflux 2.2: 4.5 h / Heating / reflux 2.3: 30 °C / pH 8 - 9 3.1: dimethylsulfide borane complex / (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran; toluene / 3.25 - 3.33 h / 0 - 2 °C 3.2: 0.25 - 0.33 h 4.1: potassium carbonate / water; acetone / 2.5 h / Heating / reflux View Scheme |
5-acetyl-8-hydroxyquinoline hydrochloride
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: hydrogenchloride; water / 0.25 - 0.33 h 2.1: potassium carbonate / acetone / 14 h / Heating / reflux 3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3.5 h / 20 - 30 °C 4.1: acetic anhydride / 2 h / 25 - 40 °C 5.1: boron trifluoride diethyl etherate / dichloromethane / Heating / reflux 5.2: 4.5 h / Heating / reflux 5.3: 30 °C / pH 8 - 9 6.1: dimethylsulfide borane complex / (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran; toluene / 1.75 h / 0 - 2 °C 6.2: 1 h / 0 - 2 °C View Scheme | |
Multi-step reaction with 7 steps 1.1: hydrogenchloride; water / 0.25 - 0.33 h 2.1: potassium carbonate / acetone / 14 h / Heating / reflux 3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3.5 h / 20 - 30 °C 4.1: acetic anhydride / 2 h / 25 - 40 °C 5.1: boron trifluoride diethyl etherate / dichloromethane / Heating / reflux 5.2: 4.5 h / Heating / reflux 5.3: 30 °C / pH 8 - 9 6.1: dimethylsulfide borane complex / (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran; toluene / 3.25 - 3.33 h / 0 - 2 °C 6.2: 0.25 - 0.33 h 7.1: potassium carbonate / water; acetone / 2.5 h / Heating / reflux View Scheme |
benzyl bromide
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: potassium carbonate / acetone / 14 h / Heating / reflux 2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3.5 h / 20 - 30 °C 3.1: acetic anhydride / 2 h / 25 - 40 °C 4.1: boron trifluoride diethyl etherate / dichloromethane / Heating / reflux 4.2: 4.5 h / Heating / reflux 4.3: 30 °C / pH 8 - 9 5.1: dimethylsulfide borane complex / (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran; toluene / 1.75 h / 0 - 2 °C 5.2: 1 h / 0 - 2 °C View Scheme | |
Multi-step reaction with 6 steps 1.1: potassium carbonate / acetone / 14 h / Heating / reflux 2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3.5 h / 20 - 30 °C 3.1: acetic anhydride / 2 h / 25 - 40 °C 4.1: boron trifluoride diethyl etherate / dichloromethane / Heating / reflux 4.2: 4.5 h / Heating / reflux 4.3: 30 °C / pH 8 - 9 5.1: dimethylsulfide borane complex / (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran; toluene / 3.25 - 3.33 h / 0 - 2 °C 5.2: 0.25 - 0.33 h 6.1: potassium carbonate / water; acetone / 2.5 h / Heating / reflux View Scheme |
5-acetyl-8-benzyloxy-1H-quinolin-2-one
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: boron trifluoride diethyl etherate / dichloromethane / Heating / reflux 1.2: 4.5 h / Heating / reflux 1.3: 30 °C / pH 8 - 9 2.1: dimethylsulfide borane complex / (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran; toluene / 1.75 h / 0 - 2 °C 2.2: 1 h / 0 - 2 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: boron trifluoride diethyl etherate / dichloromethane / Heating / reflux 1.2: 4.5 h / Heating / reflux 1.3: 30 °C / pH 8 - 9 2.1: dimethylsulfide borane complex / (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran; toluene / 3.25 - 3.33 h / 0 - 2 °C 2.2: 0.25 - 0.33 h 3.1: potassium carbonate / water; acetone / 2.5 h / Heating / reflux View Scheme |
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
N-benzyltyramine
C33H32N2O4
Conditions | Yield |
---|---|
In toluene at 100℃; for 12h; | 88% |
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
D-glucoheptonic acid
5,6-diethyl-2,3-dihydro-1H-inden-2-amine
Conditions | Yield |
---|---|
Stage #1: (R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone; 5,6-diethyl-2,3-dihydro-1H-inden-2-amine at 90℃; for 5h; Stage #2: D-glucoheptonic acid In ethanol at 60℃; for 0.0833333h; | 81.2% |
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
5,6-diethyl-2,3-dihydro-1H-inden-2-amine
p-(acetylamino)benzoic acid
Conditions | Yield |
---|---|
Stage #1: (R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone; 5,6-diethyl-2,3-dihydro-1H-inden-2-amine at 100℃; for 5h; Stage #2: p-(acetylamino)benzoic acid In ethanol at 60℃; for 0.0833333h; | 80.4% |
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
5,6-diethyl-2,3-dihydro-1H-inden-2-amine
D-galacturonic acid
Conditions | Yield |
---|---|
Stage #1: (R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone; 5,6-diethyl-2,3-dihydro-1H-inden-2-amine In butanone at 70℃; for 6h; Stage #2: D-galacturonic acid In ethanol; butanone at 60℃; for 0.0833333h; | 79.8% |
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
5,6-diethyl-2,3-dihydro-1H-inden-2-amine
meso-tartaric acid
Conditions | Yield |
---|---|
Stage #1: (R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone; 5,6-diethyl-2,3-dihydro-1H-inden-2-amine In cyclohexanone at 80℃; for 6h; Stage #2: meso-tartaric acid In ethanol; cyclohexanone at 60℃; for 0.0833333h; | 78.3% |
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
5,6-diethyl-2,3-dihydro-1H-inden-2-amine
4-methoxybenzoic acid
Conditions | Yield |
---|---|
Stage #1: (R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone; 5,6-diethyl-2,3-dihydro-1H-inden-2-amine In dimethyl sulfoxide at 110℃; for 7h; Stage #2: 4-methoxybenzoic acid In ethanol; dimethyl sulfoxide at 60℃; | 70.1% |
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
5,6-diethyl-2,3-dihydro-1H-inden-2-amine
Conditions | Yield |
---|---|
In diethylene glycol dimethyl ether at 110℃; for 15h; Heating / reflux; | A 7.8% B 68.7% C 12.4% |
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
5,6-diethyl-2,3-dihydro-1H-inden-2-amine
Conditions | Yield |
---|---|
Stage #1: (R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone; 5,6-diethyl-2,3-dihydro-1H-inden-2-amine In diethylene glycol dimethyl ether at 110℃; for 15h; Stage #2: With hydrogenchloride Product distribution / selectivity; | A 68.7% B 7.8% C 12.4% |
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
benzyl-(4,5,6,7-tetramethyl-indan-2yl)-1-amine
C38H40N2O3
Conditions | Yield |
---|---|
In butan-1-ol at 110℃; for 22h; | 67% |
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
5,6-diethyl-2,3-dihydro-1H-inden-2-amine
p-Toluic acid
Conditions | Yield |
---|---|
Stage #1: (R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone; 5,6-diethyl-2,3-dihydro-1H-inden-2-amine In dimethyl sulfoxide at 110℃; for 7h; Stage #2: p-Toluic acid In ethanol; dimethyl sulfoxide at 60℃; | 63.5% |
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
5,6-diethyl-2,3-dihydro-1H-inden-2-amine
4-nitro-benzoic acid
Conditions | Yield |
---|---|
Stage #1: (R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone; 5,6-diethyl-2,3-dihydro-1H-inden-2-amine In dimethyl sulfoxide at 110℃; for 7h; Stage #2: 4-nitro-benzoic acid In ethanol; dimethyl sulfoxide at 60℃; | 63% |
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
5,6-Dimethoxy-2-indanylamine
8-benzyloxy-5-[(R)-1-hydroxy-2-(5,6-dimethoxyindan-2-ylamino)-ethyl]-1H-quinolin-2-one
Conditions | Yield |
---|---|
In butan-1-ol at 110℃; under 760.051 Torr; for 1h; Inert atmosphere; Microwave irradiation; regioselective reaction; | 36% |
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
2-amino-5,6-di-n-butylindan
8-benzyloxy-5-[(R)-1-hydroxy-2-(5,6-di-n-butylindan-2-ylamino)-ethyl]-1H-quinolin-2-one
Conditions | Yield |
---|---|
In butan-1-ol at 110℃; under 760.051 Torr; for 1h; Inert atmosphere; Microwave irradiation; regioselective reaction; | 34% |
Conditions | Yield |
---|---|
In N,N-dimethyl acetamide at 180℃; for 0.133333h; Microwave irradiation; | 31% |
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
2,3-dihydro-1H-inden-2-amine
8-benzyloxy-5-[(R)-1-hydroxy-2-(indan-2-ylamino)-ethyl]-1H-quinolin-2-one
Conditions | Yield |
---|---|
In butan-1-ol at 110℃; under 760.051 Torr; for 1h; Inert atmosphere; Microwave irradiation; regioselective reaction; | 30% |
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
5,6-diethyl-2-methyl-indan-2-ylamine
C32H36N2O3
Conditions | Yield |
---|---|
In butan-1-ol at 100℃; for 1.25h; Microwave irradiation; | 30% |
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide; potassium hydroxide In toluene at 50℃; for 6h; | 30% |
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
5,6-diethyl-2,3-dihydro-1H-inden-2-amine
(R)-8-(benzyloxy)-5-[2-[(5,6-diethyl-2,3-dihydro-1H-indole-2-yl)amino]-1-hydroxyethyl]quinolin-2(1H)-one
Conditions | Yield |
---|---|
In butan-1-ol at 110℃; under 760.051 Torr; for 1h; Inert atmosphere; Microwave irradiation; regioselective reaction; | 28% |
In diethylene glycol dimethyl ether at 108 - 114℃; Inert atmosphere; | |
In dimethyl sulfoxide for 18h; Reflux; Large scale; | |
In butan-1-ol at 120℃; for 6h; Temperature; |
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
2-amino-5,6-dimethylindan
8-benzyloxy-5-[(R)-1-hydroxy-2-(5,6-dimethylindan-2-ylamino)-ethyl]-1H-quinolin-2-one
Conditions | Yield |
---|---|
In butan-1-ol at 110℃; under 760.051 Torr; for 1h; Inert atmosphere; Microwave irradiation; regioselective reaction; | 27% |
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
2-amino-4,7-diethylindan
8-hydroxy-5-[(R)-1-hydroxy-2-(4,7-diethylindan-2-ylamino)-ethyl]-1H-quinolin-2-one
Conditions | Yield |
---|---|
In butan-1-ol at 110℃; under 760.051 Torr; for 1h; Inert atmosphere; Microwave irradiation; regioselective reaction; | 22% |
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
2-amino-5,6-di-n-propylindan
8-benzyloxy-5-[(R)-1-hydroxy-2-(5,6-di-n-propylindan-2-ylamino)-ethyl]-1H-quinolin-2-one
Conditions | Yield |
---|---|
In butan-1-ol at 110℃; under 760.051 Torr; for 1h; Inert atmosphere; Microwave irradiation; regioselective reaction; | 21% |
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
8-benzyloxy-5-[R-2-(5,6-diethyl-2,3,4,7-tetrahydro-1H-inden-2-ylamino)-1-hydroxy-ethyl]-1H-quinolin-2-one
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 80℃; for 36h; | 21% |
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
benzylamine
8-benzyloxy-5-[(R)-2-benzylamino-1-hydroxyethyl]-(1H)-quinolin-2-one
Conditions | Yield |
---|---|
at 150℃; for 0.25h; Microwave rewactor; | |
at 150℃; for 0.25h; Microwave oven; |
Conditions | Yield |
---|---|
In dichloromethane; isopropyl alcohol at 70℃; for 40h; Heating / reflux; |
Conditions | Yield |
---|---|
In isopropyl alcohol at 70℃; for 24h; Heating / reflux; |
Conditions | Yield |
---|---|
In isopropyl alcohol at 70℃; for 36h; Heating / reflux; | |
In isopropyl alcohol |
Conditions | Yield |
---|---|
In isopropyl alcohol at 70℃; for 34h; Heating / reflux; | |
In isopropyl alcohol at 78℃; for 16h; |
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
8-benzyloxy-5-[R-1-hydroxy-2-(2,3,4,7-tetrahydro-1H-inden-2-ylamino)ethyl]-1H-quinolin-2-one
Conditions | Yield |
---|---|
Stage #1: 2,3,4,7-tetrahydro-1H-inden-2-ylamine With N,O-bis-(trimethylsilyl)-acetamide In DMF (N,N-dimethyl-formamide) at 20℃; for 0.5h; Stage #2: (R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone In DMF (N,N-dimethyl-formamide) at 80℃; for 96h; Heating / reflux; |
(R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone
8-benzyloxy-5-[R-2-(S-5-(furan-2-yl)-indan-2-ylamino)-1-hydroxyethyl]-1H-quinolin-2-one
Conditions | Yield |
---|---|
Stage #1: S-5-(furan-2-yl)indan-2-ylamine With N,O-bis-(trimethylsilyl)-acetamide In DMF (N,N-dimethyl-formamide) for 0.5h; Stage #2: (R)-5-(2-oxiranyl)-8-benzyloxy-2(1H)-quinolinone In DMF (N,N-dimethyl-formamide) at 85℃; for 48h; Heating / reflux; |
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