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Cas:18523-47-2
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FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the 3-Azidopropionic acid, CAS:18523-47-2 with the most competitive price and the best qu
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Cas:18523-47-2
Min.Order:1 Gram
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inquiryJiangxi Shengwei Chemical Technology Co., Ltd.supplies scientific research products as below:1.High-purity organic chemical reagents;2.Analytical reagents; 3.Biochemical reagents;4.Chemical raw materials;5.Experimental instruments;6.Experimental cons
3-Bromopropionic acid
3-azidopropanoic acid
Conditions | Yield |
---|---|
With sodium azide In water | 100% |
With sodium azide In acetonitrile at 85℃; for 5h; | 90% |
With sodium azide In N,N-dimethyl-formamide for 4h; Reflux; | 89% |
acrylic acid
3-azidopropanoic acid
Conditions | Yield |
---|---|
With trimethylsilylazide In neat (no solvent) at 60℃; for 0.5h; | 99% |
With trimethylsilylazide In water at 60℃; for 0.5h; Reagent/catalyst; Flow reactor; Green chemistry; | 99% |
With trimethylsilylazide; Amberlite IRA900F at 30℃; for 2h; Michael addition; neat (no solvent); | 73% |
chloropropionic acid
3-azidopropanoic acid
Conditions | Yield |
---|---|
With sodium azide In water for 15h; | 85% |
With sodium azide In water at 100℃; for 22h; | 81% |
With sodium azide In water at 85℃; for 12h; | 73% |
With sodium azide In water at 20℃; for 168h; |
β-Propiolactone
3-azidopropanoic acid
Conditions | Yield |
---|---|
With sodium azide In water at 20℃; for 6h; Inert atmosphere; | 15% |
With sodium azide In water at 20℃; for 6h; | 15% |
With sodium azide |
3-azidopropanoic acid
Conditions | Yield |
---|---|
With sulfuric acid |
azido-b-alanine methyl ester
3-azidopropanoic acid
Conditions | Yield |
---|---|
With methanol; lithium hydroxide at 20℃; | |
With sodium hydroxide In methanol at 20℃; for 48h; |
3-amino propanoic acid
3-azidopropanoic acid
Conditions | Yield |
---|---|
With imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; potassium carbonate In methanol at 20℃; for 16h; |
3-azidopropionic acid ethyl ester
3-azidopropanoic acid
Conditions | Yield |
---|---|
With sodium hydroxide In methanol Inert atmosphere; |
3-azidopropanoic acid
3-azidopropionyl chloride
Conditions | Yield |
---|---|
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 0 - 20℃; | 100% |
With oxalyl dichloride In dichloromethane at 20℃; for 6h; | |
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane for 3h; | |
With oxalyl dichloride In dichloromethane for 6h; | |
With thionyl chloride In dichloromethane at 20℃; for 12h; |
3-azidopropanoic acid
phenylacetylene
3-(4-phenyl-1H-[1,2,3]triazol-1-yl)-propionic acid
Conditions | Yield |
---|---|
With copper(II) acetate monohydrate; triethylamine In water; acetonitrile at 20℃; for 8h; | 100% |
With copper(ll) sulfate pentahydrate; sodium L-ascorbate In water; tert-butyl alcohol at 20℃; for 12h; | 46% |
Conditions | Yield |
---|---|
With copper(II) acetate monohydrate; triethylamine In methanol; water at 20℃; for 8h; | 98% |
3-azidopropanoic acid
2,3,4,5,6-pentafluorophenol
3-azidopropanoic acid pentafluorophenol ester
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In ethyl acetate Cooling with ice; | 97% |
3-azidopropanoic acid
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 0.5h; | 92% |
3-azidopropanoic acid
phenylhydrazine hydrochloride
2-phenyl-pyrazolidin-3-one
Conditions | Yield |
---|---|
Stage #1: 3-azidopropanoic acid With triethylamine; diisopropyl-carbodiimide In N,N-dimethyl-formamide at 25℃; for 0.0833333h; Stage #2: phenylhydrazine hydrochloride In N,N-dimethyl-formamide at 25℃; for 5h; Inert atmosphere; Darkness; | 92% |
Conditions | Yield |
---|---|
With copper(II) acetate monohydrate; triethylamine In water; acetonitrile at 20℃; for 8h; | 90% |
3-azidopropanoic acid
Conditions | Yield |
---|---|
With copper(ll) sulfate pentahydrate; sodium L-ascorbate In water; tert-butyl alcohol at 20℃; for 16h; | 90% |
formaldehyd
Cyclohexyl isocyanide
3-azidopropanoic acid
Propargylamine
Conditions | Yield |
---|---|
In methanol; acetonitrile at 80℃; for 0.0666667h; Ugi Condensation; Microwave irradiation; | 88% |
3-azidopropanoic acid
Conditions | Yield |
---|---|
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 0 - 20℃; Schlenk technique; Inert atmosphere; | 88% |
3-azidopropanoic acid
o-phenylenediamine hydrochloride
2,3,4,5-tetrahydro-1H-1,5-benzodiazepin-2-one
Conditions | Yield |
---|---|
Stage #1: 3-azidopropanoic acid With triethylamine; diisopropyl-carbodiimide In N,N-dimethyl-formamide at 25℃; for 0.0833333h; Stage #2: o-phenylenediamine hydrochloride In N,N-dimethyl-formamide at 25℃; for 5h; Inert atmosphere; Darkness; | 87% |
3-azidopropanoic acid
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 16h; | 87% |
Conditions | Yield |
---|---|
Stage #1: 3-azidopropanoic acid With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine In N,N-dimethyl-formamide at 20℃; for 0.166667h; Stage #2: C22H44N2OS2 With triethylamine In N,N-dimethyl-formamide at 20℃; for 3h; | 87% |
Conditions | Yield |
---|---|
In methanol; acetonitrile at 80℃; for 0.0666667h; Ugi Condensation; Microwave irradiation; | 86% |
2-propyl[1,3]thiazolo[4,5-c]quinolin-4-amine
3-azidopropanoic acid
C16H16N6OS
Conditions | Yield |
---|---|
Stage #1: 3-azidopropanoic acid With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine In N,N-dimethyl-formamide at 20℃; for 0.25h; Stage #2: 2-propyl[1,3]thiazolo[4,5-c]quinolin-4-amine In N,N-dimethyl-formamide for 4h; | 85% |
3-azidopropanoic acid
1H-benzoimidazol-2-ylamine hydrochloride
2,10-dihydropyrimido[1,2-a]benzimidazol-4(3H)-one
Conditions | Yield |
---|---|
Stage #1: 3-azidopropanoic acid With triethylamine; diisopropyl-carbodiimide In N,N-dimethyl-formamide at 25℃; for 0.0833333h; Stage #2: 1H-benzoimidazol-2-ylamine hydrochloride In N,N-dimethyl-formamide at 25℃; for 5h; Inert atmosphere; Darkness; | 85% |
3-azidopropanoic acid
Conditions | Yield |
---|---|
With copper(ll) sulfate pentahydrate; sodium L-ascorbate In water; tert-butyl alcohol at 20℃; for 16h; | 85% |
3-azidopropanoic acid
Conditions | Yield |
---|---|
With copper(ll) sulfate pentahydrate; sodium L-ascorbate In water; tert-butyl alcohol at 20℃; for 16h; | 84% |
Conditions | Yield |
---|---|
With copper diacetate; N-ethyl-N,N-diisopropylamine In water; tert-butyl alcohol at 20℃; for 2.5h; | 83% |
3-azidopropanoic acid
m-chlorophenylhydrazine hydrochloride
2-(3-chlorophenyl)pyrazolidin-3-one
Conditions | Yield |
---|---|
Stage #1: 3-azidopropanoic acid With triethylamine; diisopropyl-carbodiimide In N,N-dimethyl-formamide at 25℃; for 0.0833333h; Stage #2: m-chlorophenylhydrazine hydrochloride In N,N-dimethyl-formamide at 25℃; for 5h; Reagent/catalyst; Solvent; Inert atmosphere; Darkness; | 82% |
3-(3,5,7,9,11,13,15-heptaisobutylpentacyclo[9,5,1,1(3,9),1(7,13),1(5,15)]octasiloxane-1-yl)propylamine
3-azidopropanoic acid
Conditions | Yield |
---|---|
Stage #1: 3-(3,5,7,9,11,13,15-heptaisobutylpentacyclo[9,5,1,1(3,9),1(7,13),1(5,15)]octasiloxane-1-yl)propylamine; 3-azidopropanoic acid With dmap In dichloromethane at 0℃; for 0.0833333h; Stage #2: With diisopropyl-carbodiimide In dichloromethane at 0 - 20℃; for 24.5h; | 81% |
Conditions | Yield |
---|---|
With copper(II) sulfate; sodium L-ascorbate In water; dimethyl sulfoxide at 20℃; | 81% |
Cyclohexyl isocyanide
3-azidopropanoic acid
4-chlorobenzylamine
p-methoxyphenylglyoxal
C26H30ClN5O4
Conditions | Yield |
---|---|
Stage #1: 4-chlorobenzylamine; p-methoxyphenylglyoxal In methanol at 20℃; for 0.5h; Ugi reaction; Stage #2: Cyclohexyl isocyanide; 3-azidopropanoic acid In methanol at 20℃; for 48h; Ugi reaction; | 80% |
3-azidopropanoic acid
o-tolylhydrazine hydrochloride
2-(2-methylphenyl)pyrazolidin-3-one
Conditions | Yield |
---|---|
Stage #1: 3-azidopropanoic acid With triethylamine; diisopropyl-carbodiimide In N,N-dimethyl-formamide at 25℃; for 0.0833333h; Stage #2: o-tolylhydrazine hydrochloride In N,N-dimethyl-formamide at 25℃; for 5h; Inert atmosphere; Darkness; | 80% |
3-azidopropanoic acid
Conditions | Yield |
---|---|
With formic acid; copper(II) sulfate; sodium L-ascorbate In water; tert-butyl alcohol at 30℃; | 80% |
3-amino-7-((3aR,4R,7R,7aR)-7-methoxy-6,6-dimethyl-2-oxooxotetrahydro-3aH-[1,3]dioxolo[4,5-c]pyran-4-yloxy)-8-methyl-2H-chromen-2-one
3-azidopropanoic acid
3-azido-N-(7-((3aR,4R,7R,7aR)-7-methoxy-6,6-dimethyl-2-oxotetrahydro-3aH-[1,3]dioxolo[4,5-c]pyran-4-yloxy)-8-methyl-2-oxo-2H-chromen-3-yl)propanamide
Conditions | Yield |
---|---|
With pyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane for 14h; | 79% |
Conditions | Yield |
---|---|
Stage #1: 3-azidopropanoic acid With triethylamine; diisopropyl-carbodiimide In N,N-dimethyl-formamide at 25℃; for 0.0833333h; Stage #2: aniline In N,N-dimethyl-formamide at 50℃; for 5h; Temperature; Time; Inert atmosphere; Darkness; | 79% |
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