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Hebei Nengqian Chemical Import and Export Co., LTD

Our Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con

3-azidopropanoic acid CAS 18523-47-2

Cas:18523-47-2

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

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Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

Propanoic acid, 3-azido-

Cas:18523-47-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

Propanoic acid, 3-azido-

Cas:18523-47-2

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

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TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

3-azidopropanoic acid

Cas:18523-47-2

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

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Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

3-azidopropanoic acid

Cas:18523-47-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

3-Azidopropionic acid

Cas:18523-47-2

Min.Order:0

Negotiable

Type:Manufacturers

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Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

3-azidopropanoicacid

Cas:18523-47-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

Propanoic acid, 3-azido-

Cas:18523-47-2

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

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Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

3-azidopropanoic acid

Cas:18523-47-2

Min.Order:0

Negotiable

Type:Other

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Xi`an Eastling Biotech Co., Ltd.

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou

3-azidopropanoic acid

Cas:18523-47-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Antimex Chemical Limied

Our own factory produces direct sales with absolute price advantage Application:Pharmaceutical industry Transportation:By sea Port:Shanghai/tianjin

Propanoic acid, 3-azido-

Cas:18523-47-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hunan Russell Chemicals Technology Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

3-Azidopropionic acid 18523-47-2

Cas:18523-47-2

Min.Order:0

Negotiable

Type:Trading Company

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Shenzhen Foris Technology Co. LTD

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

3-Azidopropionic acid 18523-47-2

Cas:18523-47-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

3-azidopropanoic acid

Cas:18523-47-2

Min.Order:0

Negotiable

Type:Trading Company

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NUTROCHEM- MANUFACTURE PLACE

best seller Application:API

3-azidopropanoic acid

Cas:18523-47-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Finetech Industry Limited

FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the 3-Azidopropionic acid, CAS:18523-47-2 with the most competitive price and the best qu

3-Azidopropionic acid

Cas:18523-47-2

Min.Order:0

Negotiable

Type:Trading Company

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Pure Chemistry Scientific Inc.

3-Azidopropionic acid Application:80083725

3-Azidopropionic acid

Cas:18523-47-2

Min.Order:1 Gram

FOB Price: $500.0

Type:Trading Company

inquiry

Xi'an Confluore Biological Technology Co., Ltd.

1.Company Profile Established in 2018, Xi'an Confluore Biological Technology Co., Ltd. is a high-tech enterprise that develops and sells cutting-edge chemical reagents and biological reagents for scientific research. The company provides high-qu

3-Azidopropionic Acid

Cas:18523-47-2

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Jiangxi shengwei chemical technology co. LTD

Jiangxi Shengwei Chemical Technology Co., Ltd.supplies scientific research products as below:1.High-purity organic chemical reagents;2.Analytical reagents; 3.Biochemical reagents;4.Chemical raw materials;5.Experimental instruments;6.Experimental cons

3-Azidopropanoic acid

Cas:18523-47-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

3-Bromopropionic acid
590-92-1

3-Bromopropionic acid

3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

Conditions
ConditionsYield
With sodium azide In water100%
With sodium azide In acetonitrile at 85℃; for 5h;90%
With sodium azide In N,N-dimethyl-formamide for 4h; Reflux;89%
acrylic acid
79-10-7

acrylic acid

3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

Conditions
ConditionsYield
With trimethylsilylazide In neat (no solvent) at 60℃; for 0.5h;99%
With trimethylsilylazide In water at 60℃; for 0.5h; Reagent/catalyst; Flow reactor; Green chemistry;99%
With trimethylsilylazide; Amberlite IRA900F at 30℃; for 2h; Michael addition; neat (no solvent);73%
chloropropionic acid
107-94-8

chloropropionic acid

3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

Conditions
ConditionsYield
With sodium azide In water for 15h;85%
With sodium azide In water at 100℃; for 22h;81%
With sodium azide In water at 85℃; for 12h;73%
With sodium azide In water at 20℃; for 168h;
β-Propiolactone
57-57-8

β-Propiolactone

3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

Conditions
ConditionsYield
With sodium azide In water at 20℃; for 6h; Inert atmosphere;15%
With sodium azide In water at 20℃; for 6h;15%
With sodium azide
aceton-<β-azido-propionyl-hydrazone>

aceton-<β-azido-propionyl-hydrazone>

3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

Conditions
ConditionsYield
With sulfuric acid
azido-b-alanine methyl ester
23605-39-2

azido-b-alanine methyl ester

3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

Conditions
ConditionsYield
With methanol; lithium hydroxide at 20℃;
With sodium hydroxide In methanol at 20℃; for 48h;
3-amino propanoic acid
107-95-9

3-amino propanoic acid

3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

Conditions
ConditionsYield
With imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; potassium carbonate In methanol at 20℃; for 16h;
3-azidopropionic acid ethyl ester
40139-55-7

3-azidopropionic acid ethyl ester

3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

Conditions
ConditionsYield
With sodium hydroxide In methanol Inert atmosphere;
3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

3-azidopropionyl chloride
14468-87-2

3-azidopropionyl chloride

Conditions
ConditionsYield
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 0 - 20℃;100%
With oxalyl dichloride In dichloromethane at 20℃; for 6h;
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane for 3h;
With oxalyl dichloride In dichloromethane for 6h;
With thionyl chloride In dichloromethane at 20℃; for 12h;
3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

phenylacetylene
536-74-3

phenylacetylene

3-(4-phenyl-1H-[1,2,3]triazol-1-yl)-propionic acid
40139-46-6

3-(4-phenyl-1H-[1,2,3]triazol-1-yl)-propionic acid

Conditions
ConditionsYield
With copper(II) acetate monohydrate; triethylamine In water; acetonitrile at 20℃; for 8h;100%
With copper(ll) sulfate pentahydrate; sodium L-ascorbate In water; tert-butyl alcohol at 20℃; for 12h;46%
N,N-Dimethylpropargylamin
7223-38-3

N,N-Dimethylpropargylamin

3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

C8H14N4O2
1331989-96-8

C8H14N4O2

Conditions
ConditionsYield
With copper(II) acetate monohydrate; triethylamine In methanol; water at 20℃; for 8h;98%
3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

2,3,4,5,6-pentafluorophenol
771-61-9

2,3,4,5,6-pentafluorophenol

3-azidopropanoic acid pentafluorophenol ester
1240801-10-8

3-azidopropanoic acid pentafluorophenol ester

Conditions
ConditionsYield
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In ethyl acetate Cooling with ice;97%
(4aR,6S,7S,8R,8aS)-8-benzyloxy-6-methoxy-2-phenylhexahydropyrano[3,2-d]-[1,3]-dioxin-7-ylamine

(4aR,6S,7S,8R,8aS)-8-benzyloxy-6-methoxy-2-phenylhexahydropyrano[3,2-d]-[1,3]-dioxin-7-ylamine

3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

(4aR,6S,7S,8R,8aS)-N-(8-benzyloxy-6-methoxy-2-phenylhexahydropyrano[3,2-d]-[1,3]-dioxin-7-yl)-3-azidopropionamide

(4aR,6S,7S,8R,8aS)-N-(8-benzyloxy-6-methoxy-2-phenylhexahydropyrano[3,2-d]-[1,3]-dioxin-7-yl)-3-azidopropionamide

Conditions
ConditionsYield
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 0.5h;92%
3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

phenylhydrazine hydrochloride
59-88-1

phenylhydrazine hydrochloride

2-phenyl-pyrazolidin-3-one
16860-34-7

2-phenyl-pyrazolidin-3-one

Conditions
ConditionsYield
Stage #1: 3-azidopropanoic acid With triethylamine; diisopropyl-carbodiimide In N,N-dimethyl-formamide at 25℃; for 0.0833333h;
Stage #2: phenylhydrazine hydrochloride In N,N-dimethyl-formamide at 25℃; for 5h; Inert atmosphere; Darkness;
92%
2,2-dimethyl-3-butyne
917-92-0

2,2-dimethyl-3-butyne

3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

C9H15N3O2
1331989-98-0

C9H15N3O2

Conditions
ConditionsYield
With copper(II) acetate monohydrate; triethylamine In water; acetonitrile at 20℃; for 8h;90%
3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

2-(4-chloro-7H-pyrrolo[2,3-d]pyrimidin-7-yl)propyl propiolate

2-(4-chloro-7H-pyrrolo[2,3-d]pyrimidin-7-yl)propyl propiolate

3-(4-((2-(4-chloro-7H-pyrrolo[2,3-d]pyrimidin-7-yl)propoxy)carbonyl)-1H-1,2,3-triazol-1-yl)propanoic acid

3-(4-((2-(4-chloro-7H-pyrrolo[2,3-d]pyrimidin-7-yl)propoxy)carbonyl)-1H-1,2,3-triazol-1-yl)propanoic acid

Conditions
ConditionsYield
With copper(ll) sulfate pentahydrate; sodium L-ascorbate In water; tert-butyl alcohol at 20℃; for 16h;90%
formaldehyd
50-00-0

formaldehyd

Cyclohexyl isocyanide
931-53-3

Cyclohexyl isocyanide

3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

Propargylamine
2450-71-7

Propargylamine

3-azido-N-(2-(cyclohexylamino)-2-oxoethyl)-N-(prop-2-yn-1-yl)propanamide

3-azido-N-(2-(cyclohexylamino)-2-oxoethyl)-N-(prop-2-yn-1-yl)propanamide

Conditions
ConditionsYield
In methanol; acetonitrile at 80℃; for 0.0666667h; Ugi Condensation; Microwave irradiation;88%
3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

(2S,4S)-2-(4-((4-((E)-(4-(2-aminoacetamido)phenyl)diazenyl)phenyl)amino)-4-oxobutyl)-4-((tertbutoxycarbonyl)amino)pentanedioic acid

(2S,4S)-2-(4-((4-((E)-(4-(2-aminoacetamido)phenyl)diazenyl)phenyl)amino)-4-oxobutyl)-4-((tertbutoxycarbonyl)amino)pentanedioic acid

(2S,4S)-2-(4-((4-((E)-(4-(2-(3-azidopropanamido)acetamido)phenyl)diazenyl)phenyl)amino)-4-oxobutyl)-4-((tertbutoxycarbonyl)amino)pentanedioic acid

(2S,4S)-2-(4-((4-((E)-(4-(2-(3-azidopropanamido)acetamido)phenyl)diazenyl)phenyl)amino)-4-oxobutyl)-4-((tertbutoxycarbonyl)amino)pentanedioic acid

Conditions
ConditionsYield
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 0 - 20℃; Schlenk technique; Inert atmosphere;88%
3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

o-phenylenediamine hydrochloride
39145-59-0

o-phenylenediamine hydrochloride

2,3,4,5-tetrahydro-1H-1,5-benzodiazepin-2-one
5755-07-7

2,3,4,5-tetrahydro-1H-1,5-benzodiazepin-2-one

Conditions
ConditionsYield
Stage #1: 3-azidopropanoic acid With triethylamine; diisopropyl-carbodiimide In N,N-dimethyl-formamide at 25℃; for 0.0833333h;
Stage #2: o-phenylenediamine hydrochloride In N,N-dimethyl-formamide at 25℃; for 5h; Inert atmosphere; Darkness;
87%
3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

152-N-(12-aminododecyl)-3-ethoxycarbonyl-2,12-diethyl-5-methoxy-8,8,18,18-tetramethylbacteriochlorin-13,15-dicarboximide

152-N-(12-aminododecyl)-3-ethoxycarbonyl-2,12-diethyl-5-methoxy-8,8,18,18-tetramethylbacteriochlorin-13,15-dicarboximide

152-[12-(3-azidopropionamido)dodecyl]-3-ethoxycarbonyl-2,12-diethyl-5-methoxy-8,8,18,18-tetramethylbacteriochlorin-13,15-dicarboximide

152-[12-(3-azidopropionamido)dodecyl]-3-ethoxycarbonyl-2,12-diethyl-5-methoxy-8,8,18,18-tetramethylbacteriochlorin-13,15-dicarboximide

Conditions
ConditionsYield
With dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 16h;87%
3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

C22H44N2OS2

C22H44N2OS2

C25H47N5O2S2

C25H47N5O2S2

Conditions
ConditionsYield
Stage #1: 3-azidopropanoic acid With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine In N,N-dimethyl-formamide at 20℃; for 0.166667h;
Stage #2: C22H44N2OS2 With triethylamine In N,N-dimethyl-formamide at 20℃; for 3h;
87%
formaldehyd
50-00-0

formaldehyd

3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

1-(isocyanomethyl)-4-(prop-2-yn-1-yloxy)benzene

1-(isocyanomethyl)-4-(prop-2-yn-1-yloxy)benzene

tert-butylamine
75-64-9

tert-butylamine

3-azido-N-(tert-butyl)-N-(2-oxo-2-((4-(prop-2-yn-1-yloxy)-benzyl)amino)ethyl)propanamide

3-azido-N-(tert-butyl)-N-(2-oxo-2-((4-(prop-2-yn-1-yloxy)-benzyl)amino)ethyl)propanamide

Conditions
ConditionsYield
In methanol; acetonitrile at 80℃; for 0.0666667h; Ugi Condensation; Microwave irradiation;86%
2-propyl[1,3]thiazolo[4,5-c]quinolin-4-amine
256922-53-9

2-propyl[1,3]thiazolo[4,5-c]quinolin-4-amine

3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

C16H16N6OS
1421771-51-8

C16H16N6OS

Conditions
ConditionsYield
Stage #1: 3-azidopropanoic acid With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine In N,N-dimethyl-formamide at 20℃; for 0.25h;
Stage #2: 2-propyl[1,3]thiazolo[4,5-c]quinolin-4-amine In N,N-dimethyl-formamide for 4h;
85%
3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

1H-benzoimidazol-2-ylamine hydrochloride
26893-41-4, 70665-64-4

1H-benzoimidazol-2-ylamine hydrochloride

2,10-dihydropyrimido[1,2-a]benzimidazol-4(3H)-one
24811-77-6

2,10-dihydropyrimido[1,2-a]benzimidazol-4(3H)-one

Conditions
ConditionsYield
Stage #1: 3-azidopropanoic acid With triethylamine; diisopropyl-carbodiimide In N,N-dimethyl-formamide at 25℃; for 0.0833333h;
Stage #2: 1H-benzoimidazol-2-ylamine hydrochloride In N,N-dimethyl-formamide at 25℃; for 5h; Inert atmosphere; Darkness;
85%
3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

prop-2-yn-1-yl 2-(1,3-dimethyl-2,6-dioxo-2,3-dihydro-1H-purin-7(6H)-yl)acetate

prop-2-yn-1-yl 2-(1,3-dimethyl-2,6-dioxo-2,3-dihydro-1H-purin-7(6H)-yl)acetate

3-(4-((2-(1,3-dimethyl-2,6-dioxo-2,3-dihydro-1H-purin-7 (6H)-yl)acetoxy)methyl)-1H-1,2,3-triazol-1-yl)propanoic acid

3-(4-((2-(1,3-dimethyl-2,6-dioxo-2,3-dihydro-1H-purin-7 (6H)-yl)acetoxy)methyl)-1H-1,2,3-triazol-1-yl)propanoic acid

Conditions
ConditionsYield
With copper(ll) sulfate pentahydrate; sodium L-ascorbate In water; tert-butyl alcohol at 20℃; for 16h;85%
3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

6-bromo-4-cyclopropyl-1-(prop-2-ynyl)pyrazino[2,3-b]pyrazine-2,3(1H,4H)-dione

6-bromo-4-cyclopropyl-1-(prop-2-ynyl)pyrazino[2,3-b]pyrazine-2,3(1H,4H)-dione

3-(4-((7-bromo-1-cyclopropyl-2,3-dihydro-2,3-dioxopyrazino[2,3-b]pyrazin-4(1H)-yl)methyl)-1H-1,2,3-triazol-1-yl)propanoic acid

3-(4-((7-bromo-1-cyclopropyl-2,3-dihydro-2,3-dioxopyrazino[2,3-b]pyrazin-4(1H)-yl)methyl)-1H-1,2,3-triazol-1-yl)propanoic acid

Conditions
ConditionsYield
With copper(ll) sulfate pentahydrate; sodium L-ascorbate In water; tert-butyl alcohol at 20℃; for 16h;84%
3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

4-methoxyphenylacetylen
768-60-5

4-methoxyphenylacetylen

C12H13N3O3
500024-35-1

C12H13N3O3

Conditions
ConditionsYield
With copper diacetate; N-ethyl-N,N-diisopropylamine In water; tert-butyl alcohol at 20℃; for 2.5h;83%
3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

m-chlorophenylhydrazine hydrochloride
2312-23-4

m-chlorophenylhydrazine hydrochloride

2-(3-chlorophenyl)pyrazolidin-3-one
1056615-31-6

2-(3-chlorophenyl)pyrazolidin-3-one

Conditions
ConditionsYield
Stage #1: 3-azidopropanoic acid With triethylamine; diisopropyl-carbodiimide In N,N-dimethyl-formamide at 25℃; for 0.0833333h;
Stage #2: m-chlorophenylhydrazine hydrochloride In N,N-dimethyl-formamide at 25℃; for 5h; Reagent/catalyst; Solvent; Inert atmosphere; Darkness;
82%
3-(3,5,7,9,11,13,15-heptaisobutylpentacyclo[9,5,1,1(3,9),1(7,13),1(5,15)]octasiloxane-1-yl)propylamine
444315-15-5

3-(3,5,7,9,11,13,15-heptaisobutylpentacyclo[9,5,1,1(3,9),1(7,13),1(5,15)]octasiloxane-1-yl)propylamine

3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

C33H72N4O13Si8

C33H72N4O13Si8

Conditions
ConditionsYield
Stage #1: 3-(3,5,7,9,11,13,15-heptaisobutylpentacyclo[9,5,1,1(3,9),1(7,13),1(5,15)]octasiloxane-1-yl)propylamine; 3-azidopropanoic acid With dmap In dichloromethane at 0℃; for 0.0833333h;
Stage #2: With diisopropyl-carbodiimide In dichloromethane at 0 - 20℃; for 24.5h;
81%
3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

C54H39N5O3S2

C54H39N5O3S2

C57H44N8O5S2

C57H44N8O5S2

Conditions
ConditionsYield
With copper(II) sulfate; sodium L-ascorbate In water; dimethyl sulfoxide at 20℃;81%
Cyclohexyl isocyanide
931-53-3

Cyclohexyl isocyanide

3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

4-chlorobenzylamine
104-86-9

4-chlorobenzylamine

p-methoxyphenylglyoxal
1076-95-5

p-methoxyphenylglyoxal

C26H30ClN5O4
1245707-61-2

C26H30ClN5O4

Conditions
ConditionsYield
Stage #1: 4-chlorobenzylamine; p-methoxyphenylglyoxal In methanol at 20℃; for 0.5h; Ugi reaction;
Stage #2: Cyclohexyl isocyanide; 3-azidopropanoic acid In methanol at 20℃; for 48h; Ugi reaction;
80%
3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

o-tolylhydrazine hydrochloride
635-26-7

o-tolylhydrazine hydrochloride

2-(2-methylphenyl)pyrazolidin-3-one
1471999-73-1

2-(2-methylphenyl)pyrazolidin-3-one

Conditions
ConditionsYield
Stage #1: 3-azidopropanoic acid With triethylamine; diisopropyl-carbodiimide In N,N-dimethyl-formamide at 25℃; for 0.0833333h;
Stage #2: o-tolylhydrazine hydrochloride In N,N-dimethyl-formamide at 25℃; for 5h; Inert atmosphere; Darkness;
80%
3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

(6R,7R)-3-methyl-8-oxo-7-(propiolamido)-5-thia-1-azaicyclo[4.2.0]oct-2-ene-2-carboxylic acid

(6R,7R)-3-methyl-8-oxo-7-(propiolamido)-5-thia-1-azaicyclo[4.2.0]oct-2-ene-2-carboxylic acid

(6R,7R)-7-(1-(propionic acid)-1H-1,2,3-triazole-4-carboxamido)-3-methyl-8-oxo-5-thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylic acid

(6R,7R)-7-(1-(propionic acid)-1H-1,2,3-triazole-4-carboxamido)-3-methyl-8-oxo-5-thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylic acid

Conditions
ConditionsYield
With formic acid; copper(II) sulfate; sodium L-ascorbate In water; tert-butyl alcohol at 30℃;80%
3-amino-7-((3aR,4R,7R,7aR)-7-methoxy-6,6-dimethyl-2-oxooxotetrahydro-3aH-[1,3]dioxolo[4,5-c]pyran-4-yloxy)-8-methyl-2H-chromen-2-one
915118-12-6

3-amino-7-((3aR,4R,7R,7aR)-7-methoxy-6,6-dimethyl-2-oxooxotetrahydro-3aH-[1,3]dioxolo[4,5-c]pyran-4-yloxy)-8-methyl-2H-chromen-2-one

3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

3-azido-N-(7-((3aR,4R,7R,7aR)-7-methoxy-6,6-dimethyl-2-oxotetrahydro-3aH-[1,3]dioxolo[4,5-c]pyran-4-yloxy)-8-methyl-2-oxo-2H-chromen-3-yl)propanamide
915118-36-4

3-azido-N-(7-((3aR,4R,7R,7aR)-7-methoxy-6,6-dimethyl-2-oxotetrahydro-3aH-[1,3]dioxolo[4,5-c]pyran-4-yloxy)-8-methyl-2-oxo-2H-chromen-3-yl)propanamide

Conditions
ConditionsYield
With pyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane for 14h;79%
3-azidopropanoic acid
18523-47-2

3-azidopropanoic acid

aniline
62-53-3

aniline

1-phenylimidazolidin-2-one
1848-69-7

1-phenylimidazolidin-2-one

Conditions
ConditionsYield
Stage #1: 3-azidopropanoic acid With triethylamine; diisopropyl-carbodiimide In N,N-dimethyl-formamide at 25℃; for 0.0833333h;
Stage #2: aniline In N,N-dimethyl-formamide at 50℃; for 5h; Temperature; Time; Inert atmosphere; Darkness;
79%

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