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inquiryName:3-Trifluoromethylbenzylcyanide Other name: 3-(Trifluoromethyl)phenylacetonitrile Synonyms:2-[3-(Trifluoromethyl)phenyl]acetonitrile Cas: 2338-76-3 EINECS: 219-053-8 Keywords:3-trifluoromethylbenzylcyanide;3-(Trifluoromethyl)phenylace
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Min.Order:5 Metric Ton
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inquiryProduct name: 3-(Trifluoromethyl)Phenylacetonitrile CAS No.:2338-76-3 Molecule Formula:C9H6F3N Molecule Weight:185.14 Purity: 99% Package: 25kg/drum Description:Yellow liquid Manufacture Standards:Enterprise Standard TESTING ITEM
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Min.Order:1 Kilogram
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Min.Order:0
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Min.Order:1 Kilogram
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inquirypotassium cyanide
1-bromomethyl-3-trifluoromethylbenzene
3-trifluoromethylphenylacetonitrile
Conditions | Yield |
---|---|
In ethanol; water for 1.5h; Heating / reflux; | 100% |
In dimethyl sulfoxide |
sodium cyanide
3-Trifluoromethylbenzyl chloride
3-trifluoromethylphenylacetonitrile
Conditions | Yield |
---|---|
With N-benzyl-N,N,N-triethylammonium chloride In water at 55 - 65℃; for 10h; Temperature; | 91% |
3-chlorotrifluoromethylbenzene
ethyl 2-cyanoacetate
3-trifluoromethylphenylacetonitrile
Conditions | Yield |
---|---|
Stage #1: 3-chlorotrifluoromethylbenzene; ethyl 2-cyanoacetate With N-(2-methylnaphthalen-1-yl)-N’-(pyridin-2-ylmethyl)oxalamide; copper(I) bromide; sodium t-butanolate In isopropyl alcohol at 105℃; for 24h; Schlenk technique; Inert atmosphere; Stage #2: With water In isopropyl alcohol at 105℃; for 12h; Schlenk technique; Inert atmosphere; Cooling; | 71% |
potassium cyanide
3-Trifluoromethylbenzyl chloride
3-trifluoromethylphenylacetonitrile
Conditions | Yield |
---|---|
With potassium iodide In methanol |
(+/-)-ethyl cyano[3-(trifluoromethyl)phenyl]acetate
3-trifluoromethylphenylacetonitrile
Conditions | Yield |
---|---|
With sulfuric acid In water; acetic acid at 80 - 90℃; for 3h; Yield given; |
3-trifluoromethylphenylacetonitrile
Conditions | Yield |
---|---|
With methanol In dimethyl sulfoxide at 25℃; Equilibrium constant; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NBS View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NaH, CuI / hexamethylphosphoric acid triamide / 5 h / 150 - 160 °C 2: H2SO4 / H2O; acetic acid / 3 h / 80 - 90 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: (bromination) 2: dimethylsulfoxide View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 2: (bromination) 3: dimethylsulfoxide View Scheme |
Conditions | Yield |
---|---|
In dimethyl sulfoxide | |
In dimethyl sulfoxide | |
In dimethyl sulfoxide |
(α,α,α-trifluoro-m-tolyl)acetamide
3-trifluoromethylphenylacetonitrile
Conditions | Yield |
---|---|
In acetonitrile | |
In acetonitrile |
Conditions | Yield |
---|---|
With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide In water at 50℃; | 100% |
With benzyltriethylammonium bromide; sodium hydroxide In water; toluene at 0 - 20℃; for 96h; Inert atmosphere; | 72% |
With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide In water at 50℃; |
Conditions | Yield |
---|---|
Stage #1: 3-trifluoromethylphenylacetonitrile With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.166667h; Stage #2: ethylene dibromide In N,N-dimethyl-formamide at 20℃; for 3h; | 100% |
2-Aminonicotinaldehyde
3-trifluoromethylphenylacetonitrile
3-[3-(trifluoromethyl)phenyl][1,8]naphthyridin-2-amine
Conditions | Yield |
---|---|
With potassium hydroxide for 0.0416667h; Microwave irradiation; | 98% |
phenylacetyl chloride
3-trifluoromethylphenylacetonitrile
(3-trifluoromethylphenyl)benzylcarbonylacetonitrile
Conditions | Yield |
---|---|
With sodium t-butanolate In tetrahydrofuran at 10℃; for 24h; Reagent/catalyst; Solvent; Temperature; Autoclave; | 94.1% |
methyl 2-bromo-3-methylbutanoic ester
3-trifluoromethylphenylacetonitrile
methyl 2-isopropyl-3-oxo-4-(3-trifluoromethylphenyl)butyrate
Conditions | Yield |
---|---|
With zinc In tetrahydrofuran for 0.5h; Heating; | 94% |
Conditions | Yield |
---|---|
With ammonium hydroxide; ruthenium-carbon composite In tetrahydrofuran at 30℃; for 25h; Time; | 94% |
With ammonium hydroxide; 5 wt% ruthenium/carbon; oxygen In tetrahydrofuran at 30℃; for 25h; | 94% |
Conditions | Yield |
---|---|
With potassium phosphate; palladium diacetate; XPhos In dichloromethane; tert-butyl alcohol at 110℃; for 4h; Inert atmosphere; Schlenk technique; Sealed tube; | 93% |
3-trifluoromethylphenylacetonitrile
2-(3-(trifluoromethyl)phenyl)ethanethioamide
Conditions | Yield |
---|---|
With hydrogenchloride; O,O-Diethyl hydrogen phosphorodithioate In ethyl acetate at 20℃; Product distribution / selectivity; | 92% |
With hydrogenchloride; O,O-Diethyl hydrogen phosphorodithioate In ethyl acetate at 0 - 20℃; | 65% |
cyclohexylamine
3-trifluoromethylphenylacetonitrile
N-cyclohexyl-3-(trifluoromethyl)benzamide
Conditions | Yield |
---|---|
With 5 wt% ruthenium/carbon; oxygen In tetrahydrofuran at 30℃; for 23h; | 92% |
3-trifluoromethylphenylacetonitrile
2-bromobutyric acid ethyl ester
ethyl 2-ethyl-3-oxo-4-(3-trifluoromethylphenyl)butyrate
Conditions | Yield |
---|---|
With zinc In tetrahydrofuran for 0.5h; Heating; | 91% |
methyllithium
1,2-Epoxy-3-bromopropane
3-trifluoromethylphenylacetonitrile
3-hydroxy-1-[3-(trifluoromethyl)phenyl]cyclobutanecarbonitrile
Conditions | Yield |
---|---|
Stage #1: methyllithium; 3-trifluoromethylphenylacetonitrile In tetrahydrofuran; diethyl ether at -75℃; for 1h; Stage #2: 1,2-Epoxy-3-bromopropane In tetrahydrofuran; diethyl ether at -75℃; for 1h; Stage #3: With hydrogenchloride; methylmagnesium bromide In tetrahydrofuran; diethyl ether; water at -75 - 20℃; | 91% |
1,2-Epoxy-3-bromopropane
3-trifluoromethylphenylacetonitrile
3-hydroxy-1-[3-(trifluoromethoxy)phenyl]cyclobutanecarbonitrile
Conditions | Yield |
---|---|
Stage #1: 3-trifluoromethylphenylacetonitrile In tetrahydrofuran; diethyl ether at -75℃; for 1h; Stage #2: 1,2-Epoxy-3-bromopropane In tetrahydrofuran; diethyl ether at -75℃; for 1h; Stage #3: With hydrogenchloride; methylmagnesium bromide In tetrahydrofuran; diethyl ether; water at -75 - 20℃; | 91% |
1,2-Epoxy-3-bromopropane
3-trifluoromethylphenylacetonitrile
3-hydroxy-1-[3-(trifluoromethyl)phenyl]cyclobutanecarbonitrile
Conditions | Yield |
---|---|
Stage #1: 3-trifluoromethylphenylacetonitrile With methyllithium In tetrahydrofuran; diethyl ether at -75℃; for 1h; Stage #2: 1,2-Epoxy-3-bromopropane In tetrahydrofuran; diethyl ether at -75℃; for 1h; Stage #3: With methylmagnesium bromide In tetrahydrofuran; diethyl ether at 20℃; | 91% |
Stage #1: 3-trifluoromethylphenylacetonitrile With methyllithium In tetrahydrofuran; diethyl ether at -75℃; for 1h; Stage #2: 1,2-Epoxy-3-bromopropane With methylmagnesium bromide In tetrahydrofuran; diethyl ether at -75℃; for 1h; Stage #3: With methylmagnesium bromide In tetrahydrofuran; diethyl ether at -75 - 20℃; for 16h; | 91% |
3-trifluoromethylphenylacetonitrile
Conditions | Yield |
---|---|
With pyridine; sodium t-butanolate for 6h; Reflux; | 90% |
piperidine
3-trifluoromethylphenylacetonitrile
(piperidin-1-yl)(3-(trifluoromethyl)phenyl)methanone
Conditions | Yield |
---|---|
With 5 wt% ruthenium/carbon; oxygen In tetrahydrofuran at 30℃; for 21h; | 88% |
ethyl 2-amino-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate
3-trifluoromethylphenylacetonitrile
Conditions | Yield |
---|---|
With hydrogenchloride In 1,4-dioxane at 20℃; for 18h; | 88% |
Conditions | Yield |
---|---|
Stage #1: 3-trifluoromethylphenylacetonitrile With sodium hydroxide; water Heating / reflux; Stage #2: With hydrogenchloride In water pH=2; | 87% |
With sodium hydroxide In ethanol | |
With sulfuric acid; acetic acid |
salicylaldehyde
p-toluenesulfonyl chloride
3-trifluoromethylphenylacetonitrile
Conditions | Yield |
---|---|
Stage #1: salicylaldehyde; 3-trifluoromethylphenylacetonitrile With 1,4-diaza-bicyclo[2.2.2]octane In 2-methyltetrahydrofuran at 80℃; for 8h; Reflux; Stage #2: p-toluenesulfonyl chloride With 1,4-diaza-bicyclo[2.2.2]octane In 2-methyltetrahydrofuran at 0℃; | 87% |
3-trifluoromethylphenylacetonitrile
Conditions | Yield |
---|---|
With 5% active carbon-supported ruthenium; potassium carbonate In 1,2-dichloro-benzene at 160℃; for 35h; | 87% |
With methanol; iodine; sodium In diethyl ether at -78 - 0℃; for 2.25h; Inert atmosphere; | 65% |
Conditions | Yield |
---|---|
With Amberlite IRA 900 (OH-) In cyclohexane for 15h; Condensation; Heating; | 85% |
3-oxa-1,5-dichloropentane
3-trifluoromethylphenylacetonitrile
4-(3-(trifluoromethyl)phenyl)-tetrahydro-2H-pyran-4-carbonitrile
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide; mineral oil at 20 - 55℃; for 21.5h; Inert atmosphere; | 85% |
With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20 - 55℃; for 21.5h; | 85% |
Stage #1: 3-trifluoromethylphenylacetonitrile With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.5h; Cooling with ice; Stage #2: 3-oxa-1,5-dichloropentane In N,N-dimethyl-formamide at 0℃; for 0.5h; | 84% |
Stage #1: 3-trifluoromethylphenylacetonitrile With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 0.5h; Cooling with ice; Stage #2: 3-oxa-1,5-dichloropentane In N,N-dimethyl-formamide at 20℃; for 2h; Stage #3: With lithium chloride In N,N-dimethyl-formamide | 84% |
Stage #1: 3-trifluoromethylphenylacetonitrile With potassium tert-butylate In N,N-dimethyl-formamide at 0℃; for 0.166667h; Stage #2: 3-oxa-1,5-dichloropentane In N,N-dimethyl-formamide at 0 - 20℃; for 6h; |
N,N-dimethyl-formamide
3-trifluoromethylphenylacetonitrile
N,N-dimethyl 3-(trifluoromethyl)benzamide
Conditions | Yield |
---|---|
With copper(I) oxide; 1,10-Phenanthroline; oxygen; toluene-4-sulfonic acid at 140℃; under 760.051 Torr; for 24h; Sealed tube; | 84% |
Conditions | Yield |
---|---|
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; triphenylphosphine; potassium hydroxide In tert-Amyl alcohol at 130℃; for 2h; Microwave irradiation; | 84% |
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; triphenylphosphine; potassium hydroxide at 130℃; for 2h; Microwave irradiation; Green chemistry; | 84% |
Conditions | Yield |
---|---|
With sodium methylate In methanol; toluene at 75 - 80℃; for 12h; | 83% |
Conditions | Yield |
---|---|
Stage #1: salicylaldehyde With amberlite IRA-900 form OH In toluene at 85℃; for 3h; Inert atmosphere; Stage #2: 3-trifluoromethylphenylacetonitrile In toluene for 12h; Reflux; Inert atmosphere; | 83% |
4-[(E)-2-{4-[(E)-2-(4-formylphenyl)ethenyl]-2,5-bis(octyloxy)phenyl}ethenyl]benzaldehyde
3-trifluoromethylphenylacetonitrile
Conditions | Yield |
---|---|
With potassium tert-butylate In tetrahydrofuran; tert-butyl alcohol | 79% |
Knoevenagel condensation; |
Conditions | Yield |
---|---|
With sodium hydroxide | 79% |
naphthalen-2-yl methanesulfonate
3-trifluoromethylphenylacetonitrile
Conditions | Yield |
---|---|
With potassium phosphate; palladium diacetate; XPhos In dichloromethane; tert-butyl alcohol at 110℃; for 4h; Inert atmosphere; Schlenk technique; Sealed tube; | 79% |
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