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Cas:2345-34-8
Min.Order:1 Kilogram
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Cas:2345-34-8
Min.Order:1 Gram
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Type:Manufacturers
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Cas:2345-34-8
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Type:Trading Company
inquiry4-Acetoxybenzoic acid Basic information Product Name: 4-Acetoxybenzoic acid Synonyms: RARECHEM AL BE 0082;P-ACETOXYBENZOIC ACID;4-(Acetyloxy)benzoic acid;4-(acetylo
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Min.Order:1 Kilogram
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Type:Trading Company
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Type:Lab/Research institutions
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inquiry4-Acetoxybenzoic acid CAS:2345-34-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inte
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Min.Order:1 Gram
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Min.Order:1 Kilogram
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Min.Order:10 Gram
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Type:Lab/Research institutions
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Type:Lab/Research institutions
inquiry4-Acetoxybenzoic AcidAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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Min.Order:1 bottle
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Type:Lab/Research institutions
inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
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Min.Order:0
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Type:Lab/Research institutions
inquiryAppearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China
Cas:2345-34-8
Min.Order:0
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Type:Trading Company
inquiryWe are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white to light yellow crystal powder Storage:Room temperature with sealed well Package:according to the clients requirement Appl
4-Acetoxybenzoic acid cas 2345-34-8Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
Best quality with low priceAppearance:white crystalline powder Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai
Conditions | Yield |
---|---|
With pyridine In tetrahydrofuran; toluene at 0 - 20℃; for 16h; | 100% |
With Sulfate; titanium(IV) oxide In cyclohexane at 81℃; for 0.166667h; | 98% |
With lanthanum(III) nitrate at 20℃; for 0.333333h; | 97% |
methyl 4-acetoxybenzoate
4-acetyloxy-benzoic acid
Conditions | Yield |
---|---|
With iodine; aluminium In acetonitrile at 80℃; for 18h; | 99% |
Conditions | Yield |
---|---|
With pyridine In tetrahydrofuran for 1h; Cooling with ice; | 98.6% |
In cyclohexane at 30 - 40℃; for 2h; Concentration; | 97% |
In pyridine at 0 - 20℃; for 1.58333h; | 82.3% |
Conditions | Yield |
---|---|
With dihydrogen peroxide at 20℃; for 0.5h; | 94% |
With oxygen; C34H4F60NiO4 In toluene at 64℃; under 760 Torr; for 12h; | 74% |
With oxygen; acetic anhydride; butyraldehyde; cobalt(II) chloride In acetonitrile Ambient temperature; | 62% |
In water at 25℃; Rate constant; xanthine oxidase; also in aerosol OT/isooctane system; |
Conditions | Yield |
---|---|
With oxygen; CoCl2 In 1,2-dichloro-ethane at 25℃; | 93% |
With oxygen; cobalt(II) chloride In 1,2-dichloro-ethane at 25℃; for 20h; | 93% |
methyl 4-acetoxybenzoate
A
4-acetyloxy-benzoic acid
B
methyl 4-hydroxylbenzoate
Conditions | Yield |
---|---|
With 1-methyl-pyrrolidin-2-one; potassium carbonate; 2-amino-benzenethiol at 100℃; for 0.75h; Hydrolysis; | A 7% B 93% |
Conditions | Yield |
---|---|
With acetic acid | A 92% B n/a |
4-acetyloxy-benzoic acid
Conditions | Yield |
---|---|
With sodium hydrogen sulfate; silica gel In dichloromethane at 20℃; for 5.5h; | 89% |
4-O-acetylbenzaldehyde oxime
4-acetyloxy-benzoic acid
Conditions | Yield |
---|---|
With [hydroxy(tosyloxy)iodo]benzene; water In dimethyl sulfoxide at 20℃; for 24h; | 89% |
Conditions | Yield |
---|---|
With Oxone; 2-iodo-3,4,5,6-tetramethylbenzoic acid In water; acetonitrile for 19h; | 88% |
With tert.-butylhydroperoxide In water at 50℃; for 12h; Sealed tube; Green chemistry; | 80% |
With Oxone; mesoporous silicate MCM-48 - osmium In N,N-dimethyl-formamide at 25℃; for 3h; | 75% |
With ammonium thiocyanate; oxygen In acetic acid at 25℃; for 8h; | 30% |
Conditions | Yield |
---|---|
With oxygen In water; tert-butyl alcohol at 120℃; under 52505.3 Torr; for 0.533333h; Flow reactor; Green chemistry; | 84% |
4-acetyloxy-benzoic acid
Conditions | Yield |
---|---|
With water; N,N-dimethyl-formamide at 45℃; for 12h; Green chemistry; chemoselective reaction; | 84% |
Conditions | Yield |
---|---|
With zinc(II) oxide In N,N-dimethyl-formamide for 0.133333h; microwave irradiation; | 83% |
With oxygen; manganese (II) acetate tetrahydrate; cobalt(II) diacetate tetrahydrate; acetic acid at 100℃; for 15h; | 83% |
With cerium(III) chloride; 1,1,1-trichloroethanol; oxygen In acetonitrile at 60℃; Irradiation; | 80% |
1-acetoxy-4-methylbenzene
azobisisobutyronitrile
1N,3N,5N-trihydroxy-1,3,5-triazin-2,4,6[1H,3H,5H]-trione
4-acetyloxy-benzoic acid
Conditions | Yield |
---|---|
With acetic acid | 82% |
4-acetyloxyacetophenone
4-acetyloxy-benzoic acid
Conditions | Yield |
---|---|
With oxygen; manganese (II) acetate tetrahydrate; cobalt(II) diacetate tetrahydrate In acetic acid at 100℃; under 760.051 Torr; for 15h; | 74% |
With hydrogen bromide; acetic anhydride; acetic acid In titanium-clad | |
With hydrogen bromide; acetic anhydride; acetic acid In titanium-clad | |
With cobalt(II) nitrate hexahydrate; manganese (II) nitrate tetrahydrate; oxygen at 100℃; for 8h; |
1-acetoxy-4-methylbenzene
manganese(II) acetate
A
4-acetyloxy-benzoic acid
B
acetyloxy(4-acetyloxyphenyl)methyl acetate
C
4-(acetyloxy)benzyl acetate
Conditions | Yield |
---|---|
With sulfuric acid; ozone; potassium bromide at 5℃; under 760.051 Torr; | A n/a B 70% C 18% |
Conditions | Yield |
---|---|
With sodium hydroxide for 1h; cooling; | 63% |
4-(oxiran-2-yl)phenyl acetate
A
4-acetyloxy-benzoic acid
B
4-(1,2-dihydroxyethyl)phenyl acetate
C
4-hydroxy-benzoic acid
Conditions | Yield |
---|---|
With oxygen; bismuth mandelate In dimethyl sulfoxide at 80℃; under 760 Torr; for 4.3h; | A 4% B 17% C 61% |
Conditions | Yield |
---|---|
Stage #1: 4-acetoxycinnamic acid amide With oxygen; ozone; acetic acid In water at 0 - 10℃; for 2h; Stage #2: With dihydrogen peroxide In water at 15 - 90℃; for 2h; | A 59% B 36% |
3-(4-acetoxyphenyl)acrylic acid
A
4-acetyloxy-benzoic acid
B
4-hydroxy-benzoic acid
Conditions | Yield |
---|---|
Stage #1: 3-(4-acetoxyphenyl)acrylic acid With oxygen; ozone; acetic acid In water at 0 - 10℃; for 1.16667h; Stage #2: With dihydrogen peroxide In water at 15 - 95℃; for 3h; | A 51% B 30% |
1-acetoxy-4-methylbenzene
acetic anhydride
A
4-acetyloxy-benzoic acid
B
4-(acetyloxy)benzyl acetate
Conditions | Yield |
---|---|
With ozone at 5℃; Kinetics; | A 9.2% B 7.8% |
Conditions | Yield |
---|---|
With tetrachloromethane |
acetic anhydride
benzene
4-hydroxy-benzoic acid
4-acetyloxy-benzoic acid
Conditions | Yield |
---|---|
With dihydrogen peroxide; trifluoroacetic anhydride In chloroform |
4-nitrophenol acetate
4-hydroxy-benzoic acid
A
4-acetyloxy-benzoic acid
B
p-nitrophenolate
Conditions | Yield |
---|---|
With borate buffer; azoniacyclophane CP66 In 1,4-dioxane at 25℃; Rate constant; |
Conditions | Yield |
---|---|
With acetic acid; sodium bromide; cobalt(II) acetate; manganese(II) acetate 1.) 110 deg C, 60 min, 2.) 105 deg C; |
A
4-acetyloxy-benzoic acid
Conditions | Yield |
---|---|
With sodium hydroxide at 18℃; |
Conditions | Yield |
---|---|
With pyridine | |
With sodium hydroxide at 0℃; |
4-acetyloxy-benzoic acid
4-acetoxybenzoyl chloride
Conditions | Yield |
---|---|
With oxalyl dichloride at 20℃; for 4h; | 100% |
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20℃; for 4h; | 100% |
With oxalyl dichloride In dichloromethane at 20℃; for 6h; | 100% |
Conditions | Yield |
---|---|
Stage #1: 4-acetyloxy-benzoic acid With sodium hydroxide; water at 90℃; for 15h; Stage #2: With hydrogenchloride In water | 100% |
With aluminum oxide In neat (no solvent) at 75℃; for 0.05h; microwave irradiation; | 84% |
With bismuth mandelate In dimethyl sulfoxide at 95℃; for 24h; | 73% |
Conditions | Yield |
---|---|
With magnesium chloride at 40℃; for 18h; | 95% |
4-acetyloxy-benzoic acid
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide at 20℃; for 2h; | 94% |
4-acetyloxy-benzoic acid
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 2h; | 94% |
4-acetyloxy-benzoic acid
Conditions | Yield |
---|---|
Stage #1: 4-acetyloxy-benzoic acid With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20 - 25℃; for 1.5h; Stage #2: 6-[4-(4-aminophenyl)piperazin-1-yl]pyridine-3-carbonitrile With N-ethyl-N,N-diisopropylamine In dichloromethane at 20 - 25℃; for 0.5h; | 92% |
Conditions | Yield |
---|---|
Stage #1: 4-acetyloxy-benzoic acid With trichloroisocyanuric acid; triphenylphosphine In toluene at 0℃; for 0.25h; Stage #2: potassium thioacyanate In toluene at 0 - 20℃; for 1.5h; | 90% |
4-acetyloxy-benzoic acid
diisopropylamine
4-hydroxy-N,N-bis(1-methylethyl)benzamide
Conditions | Yield |
---|---|
Stage #1: 4-acetyloxy-benzoic acid With thionyl chloride at 80℃; for 1h; Stage #2: diisopropylamine With triethylamine In dichloromethane at 20℃; for 0.5h; Cooling; | 89% |
Conditions | Yield |
---|---|
With cesium fluoride In acetonitrile for 2h; Heating; | 88% |
piperidine
4-acetyloxy-benzoic acid
Acetic acid 4-(piperidine-1-carbonyl)-phenyl ester
Conditions | Yield |
---|---|
With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide In dichloromethane | 88% |
4-acetyloxy-benzoic acid
1-t-Butoxycarbonylpiperazine
4-(4-acetoxy-benzoyl)-piperazine-1-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide In dichloromethane | 88% |
4-acetyloxy-benzoic acid
Conditions | Yield |
---|---|
With dimethylallyl diphosphate; dicyclohexyl-carbodiimide In tetrahydrofuran at 0 - 20℃; for 5h; | 87% |
4-acetyloxy-benzoic acid
Acetic acid 4-{(S)-2-methyl-1-[(S)-2-(3,3,3-trifluoro-2-hydroxy-1-isopropyl-propylcarbamoyl)-pyrrolidine-1-carbonyl]-propylcarbamoyl}-phenyl ester
Conditions | Yield |
---|---|
With 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In tetrahydrofuran for 18h; Ambient temperature; | 86% |
Conditions | Yield |
---|---|
With pyridine; thionyl chloride In toluene | 86% |
Conditions | Yield |
---|---|
With pyridine; trichlorophosphate at 20℃; for 24h; | 85% |
4-acetyloxy-benzoic acid
Conditions | Yield |
---|---|
Stage #1: 4-acetyloxy-benzoic acid With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; ethyl cyanoglyoxylate-2-oxime In dichloromethane at 20℃; for 0.166667h; Stage #2: 2-(2-pyridinyldisulfanyl)ethanamine hydrochloride With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; | 84% |
4-acetyloxy-benzoic acid
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; | 84% |
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