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FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the 2-Chloro-3-methoxybenzoic acid, CAS:33234-36-5 with the most competitive price and th
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carbon dioxide
2,3-dichloroanisole
A
1-chloro-3-methoxy-benzene
B
2-Chloroanisole
C
2-chloro-6-methoxybenzoic acid
D
2-chloro-3-methoxybenzoic acid
Conditions | Yield |
---|---|
With tetrabutylammomium bromide In N,N-dimethyl-formamide at 5℃; electrolysis (I=0.4 A); Yields of byproduct given; | A n/a B n/a C n/a D 78% |
With tetrabutylammomium bromide In N,N-dimethyl-formamide at 5℃; electrolysis (I=0.4 A); Yields of byproduct given; | A n/a B n/a C 78% D n/a |
3-Methoxybenzoic acid
2-chloro-3-methoxybenzoic acid
Conditions | Yield |
---|---|
Stage #1: 3-Methoxybenzoic acid With 2,2,6,6-tetramethylpiperidinyl-lithium In tetrahydrofuran at 0℃; for 2h; Stage #2: With hexachloroethane In tetrahydrofuran at 0 - 65℃; for 2.5h; Stage #3: With hydrogenchloride at 20℃; | 47% |
With hexachloroethane; 2,2,6,6-tetramethylpiperidinyl-lithium In tetrahydrofuran at 0 - 65℃; for 2.5h; | 47% |
2-chloro-1-methoxy-3-methylbenzene
2-chloro-3-methoxybenzoic acid
Conditions | Yield |
---|---|
With permanganate(VII) ion |
2-chloro-3-methoxy benzaldehyde
2-chloro-3-methoxybenzoic acid
Conditions | Yield |
---|---|
With potassium permanganate; water | |
With permanganate(VII) ion |
2-chloro-3-methoxy benzaldehyde
A
2-chloro-3-methoxybenzyl alcohol
B
2-chloro-3-methoxybenzoic acid
Conditions | Yield |
---|---|
With potassium hydroxide at 60 - 70℃; |
2-amino-3-methoxybenzoic acid
A
6,6'-dimethoxy-1,1'-biphenyl-2,2'-dicarboxylic acid
B
2-chloro-3-methoxybenzoic acid
Conditions | Yield |
---|---|
With hydrogenchloride; ammonium hydroxide; sodium hydroxide; hydroxylamine hydrochloride; copper(II) sulfate; sodium nitrite Yield given. Multistep reaction. Yields of byproduct given; |
2-amino-3-methoxybenzoic acid
A
6,6'-dimethoxy-1,1'-biphenyl-2,2'-dicarboxylic acid
B
3-methoxydithiosalicylic acid
C
2-chloro-3-methoxybenzoic acid
Conditions | Yield |
---|---|
With hydrogenchloride; ammonium hydroxide; sodium disulfite; iron(III) chloride; copper(II) sulfate; sodium nitrite Multistep reaction. Title compound not separated from byproducts; |
2-Chloro-3-methoxybenzoic acid methyl ester
2-chloro-3-methoxybenzoic acid
Conditions | Yield |
---|---|
With sodium hydroxide |
2-chloro-3-methoxy benzaldehyde
2-chloro-3-methoxybenzoic acid
1-methoxy-3-methyl-2-nitro-benzene
2-chloro-3-methoxybenzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: tin (II)-chloride; hydrochloric acid 3: permanganate; alkali View Scheme | |
Multi-step reaction with 3 steps 1: tin (II)-chloride; hydrochloric acid 3: permanganate; alkali View Scheme |
2-methoxy-6-methylbenzeneamine
2-chloro-3-methoxybenzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 2: permanganate; alkali View Scheme |
methyl 2-amino-3-methoxybenzoate
2-chloro-3-methoxybenzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: (i) aq. HCl, NaNO2, (ii) CuCl, aq. HCl 2: aq. NaOH View Scheme |
methyl 3-methoxybenzoate
2-chloro-3-methoxybenzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: (nitration) 2: H2 / Pd-C 3: (i) aq. HCl, NaNO2, (ii) CuCl, aq. HCl 4: aq. NaOH View Scheme |
methyl 3-methoxy-2-nitrobenzoate
2-chloro-3-methoxybenzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: H2 / Pd-C 2: (i) aq. HCl, NaNO2, (ii) CuCl, aq. HCl 3: aq. NaOH View Scheme |
2-thiazolylamine
2-chloro-3-methoxybenzoic acid
Conditions | Yield |
---|---|
With copper; potassium carbonate In N,N-dimethyl-formamide at 25℃; for 0.25h; sonication; | 94% |
With copper Ullmann condensation; Sonication; |
3,5-dimethylphenyl iodide
2-chloro-3-methoxybenzoic acid
3-chloro-4-methoxy-3',5'-dimethyl-[1,1'-biphenyl]-2-carboxylic acid
Conditions | Yield |
---|---|
With silver (II) carbonate; palladium diacetate; potassium carbonate; acetic acid at 120℃; for 24h; Inert atmosphere; | 87% |
2-chloro-3-methoxybenzoic acid
Conditions | Yield |
---|---|
With bromine In water at 60℃; | 83% |
2-chloro-3-methoxybenzoic acid
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 0.5h; Inert atmosphere; | 78% |
ethanol
2-chloro-3-methoxybenzoic acid
ethyl 2-chloro-3-methoxybenzoate
Conditions | Yield |
---|---|
With sulfuric acid Reflux; | 65% |
3,5-dimethylphenyl iodide
2-chloro-3-methoxybenzoic acid
3-chloro-4-methoxy-3',5'-dimethyl-1,1'-biphenyl
Conditions | Yield |
---|---|
Stage #1: 3,5-dimethylphenyl iodide; 2-chloro-3-methoxybenzoic acid With palladium diacetate; acetic acid; silver carbonate at 150℃; for 16h; Stage #2: With silver carbonate In dimethyl sulfoxide at 170℃; for 4h; regioselective reaction; | 64% |
4-(4-chlorobenzoyl)piperidine
2-chloro-3-methoxybenzoic acid
Conditions | Yield |
---|---|
Stage #1: 2-chloro-3-methoxybenzoic acid With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: 4-(4-chlorobenzoyl)piperidine In N,N-dimethyl-formamide at 20℃; | 59% |
tert-butylisonitrile
((3S,4R)-4-(benzyloxy)-3,4-dihydroisoquinolin-3-yl)methanol
2-chloro-3-methoxybenzoic acid
Conditions | Yield |
---|---|
In methanol at 20℃; for 0.25h; Ugi Condensation; diastereoselective reaction; | A 51% B n/a |
2-chloro-3-methoxybenzoic acid
methyl 1,2,3,4-tetrahydro-5,8-dimethoxy-6-naphthylacetate
methyl 7-(2-chloro-3-methoxybenzoyl)-1,2,3,4-tetrahydro-5,8-dimethoxy-6-naphthylacetate
Conditions | Yield |
---|---|
With trifluoroacetic anhydride at 60℃; for 144h; | 49% |
2-chloro-3-methoxybenzoic acid
(1,4-Dimethoxy-6-methoxymethyl-5,6,7,8-tetrahydro-naphthalen-2-yl)-acetic acid methyl ester
methyl 7-(2-chloro-3-methoxybenzoyl)-1,2,3,4-tetrahydro-5,8-dimethoxy-2-methoxymethyl-6-naphthylacetate
Conditions | Yield |
---|---|
With trifluoroacetic anhydride at 60℃; for 144h; | 47% |
2-methoxy-phenylamine
2-chloro-3-methoxybenzoic acid
N-(2-methoxyphenyl)-3-methoxyanthranilic acid
Conditions | Yield |
---|---|
With i-Amyl alcohol; copper; potassium carbonate |
2-chloro-3-methoxybenzyl alcohol
2-chloro-3-methoxybenzoic acid
2-chloro-3-methoxy benzaldehyde
Conditions | Yield |
---|---|
With potassium hydroxide at 60 - 70℃; |
2-chloro-3-methoxybenzoic acid
aniline
2-anilino-3-methoxy-benzoic acid
Conditions | Yield |
---|---|
With copper; potassium carbonate | |
With copper diacetate In N,N-dimethyl-formamide at 90℃; |
2-chloro-3-methoxybenzoic acid
4-Ethoxyaniline
3-methoxy-2-p-phenetidino-benzoic acid
Conditions | Yield |
---|---|
With pentan-1-ol; copper; potassium carbonate |
2-chloro-3-methoxybenzoic acid
2-Chloro-3-hydroxy benzoic acid
Conditions | Yield |
---|---|
With hydrogen bromide |
2-chloro-3-methoxybenzoic acid
4,5-dimethoxyacridine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: potassium carbonate; copper; isoamyl alcohol 2: phosphoryl chloride / 160 - 165 °C 3: sodium-amalgam; sodium hydrogencarbonate / 80 °C 4: concentrated sulfuric acid; acetic acid; sodium nitrite / Reagens 4:Wasser View Scheme |
2-chloro-3-methoxybenzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: potassium carbonate; copper; isoamyl alcohol 2: phosphoryl chloride / 160 - 165 °C 3: sodium-amalgam; sodium hydrogencarbonate / 80 °C View Scheme |
2-chloro-3-methoxybenzoic acid
4,5-dimethoxyacridine-9(10H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium carbonate; copper; isoamyl alcohol 2: phosphoryl chloride / 160 - 165 °C View Scheme |
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