Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:354-38-1
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryItems Standard Result Assay (Ursolic acid) 98%min 98.22% ----------------------------------------------------------------
Cas:354-38-1
Min.Order:1 Gram
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inquiryManufacturer supply Trifluoroacetamide CAS 354-38-1 with attractive price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/
Cas:354-38-1
Min.Order:10 Kilogram
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:354-38-1
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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/1155.html Product Name Trifluoroacetamide CAS No. 354-38-1
Cas:354-38-1
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:354-38-1
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:354-38-1
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:354-38-1
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inquiryProduct Name Trifluoroacetamide Synonyms Trifluoroacetamide;CF3CONH2 CAS: 354-38-1 MF: - MW: - EINECS: -
Cas:354-38-1
Min.Order:5 Metric Ton
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inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:White Crystalline Powder Storage:Store in sealed conta
Cas:354-38-1
Min.Order:10 Gram
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:354-38-1
Min.Order:1 Kilogram
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inquiryTrifluoroacetamide CAS:354-38-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermed
Cas:354-38-1
Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:354-38-1
Min.Order:1 Kilogram
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
ISO9001 We have been specializing in organic fluoro chemicals since 1984. We have been supplying it to Europe, USA, Japan, Korea etc. regularly for several years Appearance:Yellowish crystal Package:25kg/fibre drum Application:Used as reagent
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
1. Well-equipped, stable and high-quality raw material supply chain, to provide customers with the best quality products. 2.Strict quality inspection process and professional certificate testing to ensure the quality level of the final product. 3.E
Cas:354-38-1
Min.Order:1 Kilogram
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inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures
Cas:354-38-1
Min.Order:1 Kilogram
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inquirySuperiority We can customize and synthesize products that other suppliers may not be able to provide. best service, company and transport advantage: 1. best service, high quality and reasonable way for his produccts from many rec
Cas:354-38-1
Min.Order:100 Kilogram
Negotiable
Type:Trading Company
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:354-38-1
Min.Order:0 Metric Ton
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Type:Lab/Research institutions
inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
Cas:354-38-1
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:354-38-1
Min.Order:4 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryPacking: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Transportation:Express/Sea/Air Port:Ningbo/Shanghai/Qingd
Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff
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Cas:354-38-1
Min.Order:1 Gram
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Type:Other
inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:354-38-1
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:354-38-1
Min.Order:10 Gram
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Type:Lab/Research institutions
inquirySuperior quality Appearance:white to pale yellow or beige crystalline powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:pharmaceutical interm
Conditions | Yield |
---|---|
With hydrogenchloride; triethylamine In ethanol; ethyl acetate | 100% |
With diethyl ether; ammonia | |
With methanol; ammonia |
Conditions | Yield |
---|---|
With methylamine at 150℃; under 750.075 Torr; for 10h; Gas phase; | 99.1% |
nitropentafluoroacetone
A
difluoro-nitro-methane
B
2,2,2-trifluoroacetamide
Conditions | Yield |
---|---|
With ammonia in bomb tube; | A 14% B 99% |
With NH3 in bomb tube; | A 14% B 99% |
2,2,2-trifluoro-N-{2,2,2-trifluoro-1-(trifluoromethyl) ethylidene}acetamide
N-ethyl-N-phenylamine
A
2-(4-(ethylamino)phenyl)-1,1,1,3,3,3-hexafluoropropan-2-ol
B
hexafluoroacetone hydrate
C
2,2,2-trifluoroacetamide
D
2,4,4-tris(trifluoromethyl)-1-ethyl-1,4-dihydroquinazoline
Conditions | Yield |
---|---|
In chloroform at 20℃; for 1440h; Mechanism; | A n/a B n/a C n/a D 87% E n/a |
N-trifluoroacetyl-Se-(p-bromophenyl)-Se-methylselenimide
A
2,2,2-trifluoroacetamide
B
methyl (p-bromophenyl)selenium dichloride
Conditions | Yield |
---|---|
With acetyl chloride In chloroform at 20℃; for 3h; | A 55% B 85% |
1-(2,2,2-trifluoroacetyl)-3-(E)-styrylurea
A
2,2,2-trifluoroacetamide
B
(E)-N-(2-phenylethenyl)-2,2,2-trifluoroacetamide
Conditions | Yield |
---|---|
In trifluoroacetic acid at 230℃; for 0.333333h; | A 69% B 22% |
1-(2,2,2-trifluoroacetyl)-3-<2-(2,2,2-trifluoroacetyloxy)-2-phenylethyl>urea
A
2,2,2-trifluoroacetamide
B
(E)-N-(2-phenylethenyl)-2,2,2-trifluoroacetamide
Conditions | Yield |
---|---|
In neat (no solvent) at 230℃; for 0.5h; | A 69% B 19% |
1-(2,2,2-trifluoroacetyl)-3-(E)-styrylurea
2,2,2-trifluoroacetamide
Conditions | Yield |
---|---|
In neat (no solvent) at 230℃; for 0.333333h; | 68% |
dimedone
N-(trifluoroacetyl)-di(p-methoxyphenyl)tellurimide
A
2,2,2-trifluoroacetamide
B
di(p-metoxyphenyl)telluroniodimedonide
Conditions | Yield |
---|---|
In chloroform Ambient temperature; overnight; | A 58% B 67% |
Conditions | Yield |
---|---|
With zirconium(IV) chloride; ammonium carbamate In toluene at 120℃; for 24h; Inert atmosphere; Molecular sieve; | 67% |
[(trifluoroacetyl)imino]tris-(2-methylphenyl)-λ(5)-bismuthane
A
2,2,2-trifluoroacetamide
B
tri-o-tolylbismuth
Conditions | Yield |
---|---|
In benzene 60°C, 48 h; | A n/a B 61% |
2,5-bis(trifluoromethyl)-1,3,4-oxadiazole
2,3-dimethyl-buta-1,3-diene
B
2,2,2-trifluoroacetamide
C
2-(trifluoromethyl)-4,5-dimethylpyridine
Conditions | Yield |
---|---|
at 150℃; for 18h; | A 32% B 15% C 30% |
2-trifluoromethyl-5-ethoxycarbonyl-1,3,4-oxadiazole
2,3-dimethyl-buta-1,3-diene
B
2,2,2-trifluoroacetamide
C
2-(trifluoromethyl)-4,5-dimethylpyridine
Conditions | Yield |
---|---|
at 150℃; for 14h; | A 27% B n/a C n/a |
N-bromo-trifluoroacetamide
A
2,2,2-trifluoroacetamide
(+/-)-trifluoroacetic acid-(trans-2-bromo-cyclohexylamide)
N-((1R,2S)-2-Bromo-cyclohexyl)-2,2,2-trifluoro-acetamide
Conditions | Yield |
---|---|
With cyclohexene In dichloromethane at 15 - 20℃; for 0.2h; Irradiation; Yields of byproduct given; | A 7% B n/a C n/a |
N-bromo-trifluoroacetamide
cyclohexene
A
2,2,2-trifluoroacetamide
(+/-)-trifluoroacetic acid-(trans-2-bromo-cyclohexylamide)
N-((1R,2S)-2-Bromo-cyclohexyl)-2,2,2-trifluoro-acetamide
Conditions | Yield |
---|---|
In dichloromethane at 15 - 20℃; for 0.2h; Irradiation; Yield given. Yields of byproduct given; | A 7% B n/a C n/a |
methyl 4,4,4-trifluoroacetoacetate
A
acetamide
B
2,2,2-trifluoroacetamide
C
3-amino-4,4,4-trifluorobut-2-enoic acid
Conditions | Yield |
---|---|
With ammonia In diethyl ether at 100℃; for 10h; Product distribution; NH3 amount dependence; | A n/a B n/a C 5% |
Conditions | Yield |
---|---|
With ammonia In diethyl ether |
Conditions | Yield |
---|---|
With hydrogenchloride In diethyl ether |
N-(trimethylsilyl)trifluoroacetamide
2,2,2-trifluoroacetamide
Conditions | Yield |
---|---|
With boron trifluoride |
Conditions | Yield |
---|---|
With ammonia In benzene |
2,2-Dibromo-4,4,4-trifluoro-3-oxo-butyric acid methyl ester
A
dibromoacetamide
B
2,2,2-trifluoroacetamide
Conditions | Yield |
---|---|
With ammonia In diethyl ether at -40 - -10℃; Yield given. Yields of byproduct given; |
Conditions | Yield |
---|---|
With ammonia In diethyl ether at -40 - -10℃; Yield given. Yields of byproduct given; |
2,2,2-trifluoroacetyl isocyanate
trifluorothioacetic acid
A
2,2,2-trifluoroacetamide
B
bistrifluoroacetamide
Conditions | Yield |
---|---|
Yield given; |
glycolic Acid
N,O-bis(trimethylsilyl)trifluoroacetamide
A
2,2,2-trifluoroacetamide
B
trimethylsilyl [(trimethylsilyl)oxy]acetate
C
N-(trimethylsilyl)trifluoroacetamide
Conditions | Yield |
---|---|
In hexane; dichloromethane at 60℃; for 0.666667h; Substitution; |
LACTIC ACID
N,O-bis(trimethylsilyl)trifluoroacetamide
A
2,2,2-trifluoroacetamide
B
propanoic acid,2-[(trimethylsilyl)oxy] trimethylsilyl ester
C
N-(trimethylsilyl)trifluoroacetamide
Conditions | Yield |
---|---|
In hexane; dichloromethane at 60℃; for 0.666667h; Substitution; |
1,5-pentanedioic acid
N,O-bis(trimethylsilyl)trifluoroacetamide
A
2,2,2-trifluoroacetamide
B
bis-trimethylsilyl glutarate
C
N-(trimethylsilyl)trifluoroacetamide
Conditions | Yield |
---|---|
In hexane; dichloromethane at 60℃; for 0.666667h; Substitution; |
Adipic acid
N,O-bis(trimethylsilyl)trifluoroacetamide
A
2,2,2-trifluoroacetamide
B
Bis(trimethylsilyl) adipate
C
N-(trimethylsilyl)trifluoroacetamide
Conditions | Yield |
---|---|
In hexane; dichloromethane at 60℃; for 0.666667h; Substitution; |
oenanthic acid
N,O-bis(trimethylsilyl)trifluoroacetamide
A
2,2,2-trifluoroacetamide
B
l'heptanoate de trimethylsilyle
C
N-(trimethylsilyl)trifluoroacetamide
Conditions | Yield |
---|---|
In hexane; dichloromethane at 60℃; for 0.666667h; Substitution; |
Octanoic acid
N,O-bis(trimethylsilyl)trifluoroacetamide
A
2,2,2-trifluoroacetamide
B
N-(trimethylsilyl)trifluoroacetamide
Conditions | Yield |
---|---|
In hexane; dichloromethane at 60℃; for 0.666667h; Substitution; |
malonic acid
N,O-bis(trimethylsilyl)trifluoroacetamide
A
2,2,2-trifluoroacetamide
B
bis(trimethylsilyl) malonate
C
N-(trimethylsilyl)trifluoroacetamide
Conditions | Yield |
---|---|
In hexane; dichloromethane at 60℃; for 0.666667h; Substitution; |
2,2,2-trifluoroacetamide
N-(trimethylstannyl)-2,2,2-trifluoroacetamide
Conditions | Yield |
---|---|
In benzene byproducts: water; absence of moisture; equimolar amts., refluxing for 3 h (distn. off of water); solvent removal (vac.); | 100% |
2,2,2-trifluoroacetamide
2-(4-(trifluoromethyl)phenyl)-4,5-dihydrooxazole
Conditions | Yield |
---|---|
With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; [bis(acetoxy)iodo]benzene In dichloromethane at 40℃; for 16h; Inert atmosphere; regioselective reaction; | 100% |
Conditions | Yield |
---|---|
With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; [bis(acetoxy)iodo]benzene In dichloromethane at 40℃; for 16h; Inert atmosphere; regioselective reaction; | 100% |
2-(4-methoxyphenyl)-4,5-dihydrooxazole
2,2,2-trifluoroacetamide
Conditions | Yield |
---|---|
With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; [bis(acetoxy)iodo]benzene In dichloromethane at 40℃; for 16h; Inert atmosphere; regioselective reaction; | 100% |
With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; [bis(acetoxy)iodo]benzene In dichloromethane at 40℃; for 16h; Schlenk technique; Inert atmosphere; Sealed tube; | 100% |
2,2,2-trifluoroacetamide
Conditions | Yield |
---|---|
With dirhodium tetraacetate; [bis(acetoxy)iodo]benzene; magnesium oxide In dichloromethane for 3h; Reflux; | 100% |
2,2,2-trifluoroacetamide
Conditions | Yield |
---|---|
With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; sodium hydride In tetrahydrofuran at 20℃; for 2h; | 100% |
2,2,2-trifluoroacetamide
Conditions | Yield |
---|---|
Stage #1: 2,2,2-trifluoroacetamide With potassium hexamethylsilazane In tetrahydrofuran at -78℃; for 0.5h; Inert atmosphere; Stage #2: (S)-2-methyl-1-[(2-nitrophenyl)sulfonyl]aziridine In tetrahydrofuran; dichloromethane at 20℃; for 18h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With copper(II) oxide at 400℃; under 750.075 Torr; for 10h; Gas phase; | 99.1% |
With pyridine; pivaloyl chloride; trifluoroacetic acid at 20℃; for 5h; Product distribution / selectivity; | 92% |
With phosphorus pentoxide Heating; | 90% |
2,2,2-trifluoroacetamide
N-Methoxymethylmonoaza-15-crown-5 ether
2,2,2-Trifluoro-N-(1,4,7,10-tetraoxa-13-aza-cyclopentadec-13-ylmethyl)-acetamide
Conditions | Yield |
---|---|
In tetrachloromethane Heating; | 99% |
2,2,2-trifluoroacetamide
4-bromo-N,N-dimethylaniline
2,2,2-trifluoro-(4-N,N-dimethyphenyl)acetamide
Conditions | Yield |
---|---|
With potassium carbonate; N,N`-dimethylethylenediamine; copper(l) iodide In 1,4-dioxane at 75℃; | 99% |
Conditions | Yield |
---|---|
With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 1,1'-bis(diphenylphosphino)ferrocene In toluene at 100℃; for 3h; Inert atmosphere; optical yield given as %de; stereoselective reaction; | 99% |
Conditions | Yield |
---|---|
With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 1,1'-bis(diphenylphosphino)ferrocene In toluene at 100℃; for 3h; Inert atmosphere; optical yield given as %de; stereoselective reaction; | 99% |
2,2,2-trifluoroacetamide
1-isocyanato-2-(2-phenylethynyl)benzene
C17H11F3N2O2
Conditions | Yield |
---|---|
With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 1,1'-bis(diphenylphosphino)ferrocene In toluene at 100℃; for 3h; Inert atmosphere; optical yield given as %de; stereoselective reaction; | 99% |
7-bromo-hept-1-ene
2,2,2-trifluoroacetamide
2,2,2-trifluoro-N-(hept-6-en-1-yl)acetamide
Conditions | Yield |
---|---|
Stage #1: 2,2,2-trifluoroacetamide With sodium hydride In N,N-dimethyl-formamide at 0℃; Inert atmosphere; Stage #2: 7-bromo-hept-1-ene In N,N-dimethyl-formamide at 50℃; for 3h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
Stage #1: 2,2,2-trifluoroacetamide With sodium hydride In N,N-dimethyl-formamide at 0℃; Inert atmosphere; Stage #2: bromopentene In N,N-dimethyl-formamide at 50℃; for 3h; Inert atmosphere; | 99% |
Stage #1: 2,2,2-trifluoroacetamide With sodium hydride In N,N-dimethyl-formamide; paraffin oil at 20℃; for 2h; Stage #2: bromopentene In N,N-dimethyl-formamide; paraffin oil at 50℃; for 21h; | 63% |
2,2,2-trifluoroacetamide
Conditions | Yield |
---|---|
Stage #1: 2,2,2-trifluoroacetamide With potassium hexamethylsilazane In tetrahydrofuran at -78℃; for 0.5h; Inert atmosphere; Stage #2: (S)-2-benzyl-1-((2-nitrophenyl)sulfonyl)aziridine In tetrahydrofuran; dichloromethane at 20℃; for 18h; Inert atmosphere; | 99% |
2,2,2-trifluoroacetamide
[1-(1-Cyano-3-methyl-butylcarbamoyl)-2-phenyl-ethyl]-carbamic acid methyl ester
{1-[4-Isobutyl-5-(2,2,2-trifluoro-acetylamino)-oxazol-2-yl]-2-phenyl-ethyl}-carbamic acid methyl ester
Conditions | Yield |
---|---|
trifluoroacetic acid | 98% |
2,2,2-trifluoroacetamide
Cbz-l-Leu-dl-Phe-N-benzyl amide
2-<1(S)-(carbobenzyloxyamino)-3-methylbutyl>-4-benzyl-5-(N-benzyltrifluoroacetamido)oxazole
Conditions | Yield |
---|---|
trifluoroacetic acid In dichloromethane | 98% |
2,2,2-trifluoroacetamide
6-Bromo-1-hexene
2,2,2-trifluoro-N-(hex-5-en-1-yl)acetamide
Conditions | Yield |
---|---|
Stage #1: 2,2,2-trifluoroacetamide With sodium hydride In N,N-dimethyl-formamide at 0℃; Inert atmosphere; Stage #2: 6-Bromo-1-hexene In N,N-dimethyl-formamide at 50℃; for 3h; Inert atmosphere; | 98% |
With sodium hydride 1) DMF, 0.5 h; 2) DMF, 80 deg C, 10 h; Yield given. Multistep reaction; |
2,2,2-trifluoroacetamide
diphenyl sulfide
S,S-diphenyl-N-(trifluoroacetyl)sulfilimine
Conditions | Yield |
---|---|
With [bis(acetoxy)iodo]benzene; magnesium oxide; dirhodium tetraacetate In dichloromethane at 20℃; for 6h; | 98% |
With rhodium(II) acetate dimer; [bis(acetoxy)iodo]benzene; magnesium oxide In dichloromethane at 20℃; for 18h; Inert atmosphere; |
2,2,2-trifluoroacetamide
4-bromo-1,1'-biphenyl
2,2,2-trifluoro-4'-phenylacetanilide
Conditions | Yield |
---|---|
With potassium carbonate; N,N`-dimethylethylenediamine; copper(l) iodide In 1,4-dioxane at 75℃; | 98% |
2,2,2-trifluoroacetamide
(3R)-4-(2-chloro-6-[(methylsulfinyl)methyl]-4-pyrimidinyl)-3-methylmorpholine
Conditions | Yield |
---|---|
With rhodium(II) acetate; [bis(acetoxy)iodo]benzene; magnesium oxide In dichloromethane at 20℃; for 16h; Inert atmosphere; | 98% |
With [bis(acetoxy)iodo]benzene; magnesium oxide; dirhodium tetraacetate In dichloromethane at 20℃; for 96h; | 82% |
With dirhodium tetraacetate; [bis(acetoxy)iodo]benzene; magnesium oxide In dichloromethane at 20℃; for 96h; | 82% |
With rhodium(II) acetate dimer; [bis(acetoxy)iodo]benzene In dichloromethane at 20℃; for 36h; Reagent/catalyst; | 64.82% |
Conditions | Yield |
---|---|
With potassium phosphate; [methanesulfonato2-dicyclohexylphosphino-2-(N,N-dimethylamino)biphenyl(2′-amino-1,1′-biphenyl-2-yl)palladium(II)] In toluene at 100℃; for 12h; Inert atmosphere; Sealed tube; Schlenk technique; | 98% |
2,2,2-trifluoroacetamide
Conditions | Yield |
---|---|
Stage #1: 2,2,2-trifluoroacetamide With potassium hexamethylsilazane In tetrahydrofuran at -78℃; for 0.5h; Inert atmosphere; Stage #2: (S)-2-isobutyl-1-[(2-nitrophenyl)sulfonyl]aziridine In tetrahydrofuran; dichloromethane at 20℃; for 18h; Inert atmosphere; | 98% |
2,2,2-trifluoroacetamide
Conditions | Yield |
---|---|
With tris(2,2'-bipyridyl)ruthenium dichloride; sodium carbonate In 1,2-dichloro-ethane at 20℃; for 8h; Irradiation; | 98% |
2,2,2-trifluoroacetamide
3-(3-phenylpropyl-2-yn-1-ylidene)-2,4-pentanedione
Conditions | Yield |
---|---|
With tris(2,2'-bipyridyl)ruthenium dichloride; sodium carbonate In 1,2-dichloro-ethane at 20℃; for 8h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Irradiation; | 98% |
2,2,2-trifluoroacetamide
1-benzyloxy-3-tosyloxypropane
N-(3-Benzyloxypropyl)-2,2,2-trifluoroacetamide
Conditions | Yield |
---|---|
With potassium tert-butylate; sodium iodide In tetrahydrofuran for 4h; | 97% |
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