3-METHOXYPHENYLMAGNESIUM BROMIDE Basic information Product Name: 3-METHOXYPHENYLMAGNESIUM BROMIDE CAS: 36282-40-3 MF: C7H7BrMgO MW: 211.34 EINECS: Product Categories: Aryl;Grignard Reagents;Organometallic Reagents;Chemical Synthesis;Grignard Reage
Cas:36282-40-3
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inquiryDayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:36282-40-3
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Cas:36282-40-3
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inquiry1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
Cas:36282-40-3
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:36282-40-3
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inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:36282-40-3
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
Cas:36282-40-3
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inquiryAcmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
Cas:36282-40-3
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inquiryTAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Cas:36282-40-3
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inquiryMagnesium,bromo(3-methoxyphenyl)- cas 36282-40-3Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiryBest quality with low priceAppearance:Clear colorless to brown solution Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Cas:36282-40-3
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inquiryGood Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
Cas:36282-40-3
Min.Order:10 Milligram
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inquiryPrice, service, company and transport advantage: 1. Best service, place of origin China, high quality, and reasonable price. 2. It's customers' right to choose the package (EMS, DHL, FEDEX, UPS). 3. It's customers' right
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inquiryAt Share Chemical Company, we scrupulously abide by our policy of “Excellent Quality at a Reasonable Price”. We strive to satisfy all of our customers by providing the finest quality products supported by the finest in customer servi
Cas:36282-40-3
Min.Order:1 Gram
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inquiryYUYONGMEI was established in Aug,1999, located in the industrial park of Nanjing University of Technology, It is a private enterprises in Jiangsu Province with 1200 square meters’ R&D center. Our R&D center has a well-equipped synthetic laboratory a
Cas:36282-40-3
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inquiry3-Methoxy Phenyl Magnesium Bromide (1.0 M In THF)
Cas:36282-40-3
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inquiryPackage:100, 800 mL in Sure/Seal(TM)
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inquirymore information,pls contact with us!
Cas:36282-40-3
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Type:Trading Company
inquiryCas:36282-40-3
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inquirymore information,please contact us
Cas:36282-40-3
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inquiry2,3-dihydro-4H-1-benzopyran-4-one
3-methoxyphenyl bromide
(3-methoxyphenyl)magnesium bromide
Conditions | Yield |
---|---|
With hydrogenchloride In tetrahydrofuran |
Conditions | Yield |
---|---|
In tetrahydrofuran |
3-methoxyphenyl bromide
(3-methoxyphenyl)magnesium bromide
Conditions | Yield |
---|---|
With magnesium; iodine In tetrahydrofuran at 20℃; Heating / reflux; | |
With magnesium In tetrahydrofuran Inert atmosphere; | |
With iodine; magnesium In tetrahydrofuran for 2h; Inert atmosphere; Reflux; |
(3-methoxyphenyl)magnesium bromide
cyclohexanone
1-(m-Methoxyphenyl)cyclohexanol
Conditions | Yield |
---|---|
Stage #1: (3-methoxyphenyl)magnesium bromide; cyclohexanone In diethyl ether at 0 - 20℃; for 4h; Stage #2: With water at 0℃; | 100% |
In tetrahydrofuran for 0.333333h; | |
In tetrahydrofuran; toluene at 0℃; for 5.5h; Inert atmosphere; |
m-bromobenzoic aldehyde
(3-methoxyphenyl)magnesium bromide
3-bromo-α-(3-methoxyphenyl)benzenemethanol
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 0.25h; | 100% |
Stage #1: m-bromobenzoic aldehyde; (3-methoxyphenyl)magnesium bromide In tetrahydrofuran at 80℃; for 3h; Grignard reaction; Inert atmosphere; Stage #2: With water; sodium chloride In tetrahydrofuran at 20℃; |
(3-methoxyphenyl)magnesium bromide
Conditions | Yield |
---|---|
Stage #1: 3-(4-methoxy-benzyl)-3-aza-bicyclo[3.2.1]octan-8-one; (3-methoxyphenyl)magnesium bromide In tetrahydrofuran at -78 - 20℃; Stage #2: With hydrogenchloride In water pH=1; | 100% |
ethyl 3-(3,4-methylenedioxyphenyl)-1-oxoindene-2-carboxylate
(3-methoxyphenyl)magnesium bromide
Ethyl (1RS)-1-Hydroxy-1-(3-methoxyphenyl)-3-(3,4-methylenedioxyphenyl)indene-2-carboxylate
Conditions | Yield |
---|---|
In tetrahydrofuran | 100% |
(3-methoxyphenyl)magnesium bromide
tert-butyl 2-oxopyrrolidine-1-carboxylate
tert-butyl (4-(3-methoxyphenyl)-4-oxobutyl)carbamate
Conditions | Yield |
---|---|
In tetrahydrofuran at -40 - 0℃; for 3h; | 100% |
In tetrahydrofuran at -78 - 20℃; for 14h; Inert atmosphere; Schlenk technique; | 45% |
diethyl 2-(4-bromobenzylidene)malonate
(3-methoxyphenyl)magnesium bromide
Conditions | Yield |
---|---|
Stage #1: diethyl 2-(4-bromobenzylidene)malonate; (3-methoxyphenyl)magnesium bromide In tetrahydrofuran; diethyl ether at 0℃; for 3.3h; Stage #2: With water; ammonium chloride | 100% |
(3-methoxyphenyl)magnesium bromide
4-bromo-benzaldehyde
(4-bromo-phenyl)-(3-methoxy-phenyl)-methanol
Conditions | Yield |
---|---|
Stage #1: (3-methoxyphenyl)magnesium bromide; 4-bromo-benzaldehyde In tetrahydrofuran at 80℃; for 3h; Grignard reaction; Inert atmosphere; Stage #2: With water; sodium chloride In tetrahydrofuran at 20℃; | 100% |
Conditions | Yield |
---|---|
With 1-methyl-pyrrolidin-2-one; palladium diacetate; tricyclohexylphosphine In tetrahydrofuran at 20℃; for 20h; Kumada coupling; | 99% |
With 1,3-bis(mesityl)imidazolium chloride; palladium diacetate In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 20℃; for 1h; Kumada reaction; | 99% |
Conditions | Yield |
---|---|
Stage #1: C17H16O3; (3-methoxyphenyl)magnesium bromide In tetrahydrofuran at 0 - 20℃; for 0.5h; Inert atmosphere; Stage #2: With water In tetrahydrofuran at 0℃; diastereoselective reaction; | 99% |
3-iodo-1,2-dicarba-closo-dodecaborane
(3-methoxyphenyl)magnesium bromide
B
3-meta-methoxyphenyl-o-carborane
Conditions | Yield |
---|---|
With copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride In tetrahydrofuran Ar, a soln. of Mg compd. (8.5 equiv.) added dropwise to a soln. of B compd., CuI and catalyst, refluxed for 34 h; quenched (dilute HCl), extd. (ethyl acetate), washed (water), dried (MgSO4), concd., chromy. (silica gel); | A 0% B 99% |
(3-methoxyphenyl)magnesium bromide
Conditions | Yield |
---|---|
at 20℃; for 13h; Inert atmosphere; | 99% |
8-methoxy-3,4-dihydroisocoumarin
(3-methoxyphenyl)magnesium bromide
[2-(2-hydroxy-ethyl)-6-methoxy-phenyl]-(3-methoxy-phenyl)-methanone
Conditions | Yield |
---|---|
In tetrahydrofuran; dichloromethane at -78 - 20℃; | 98% |
3-bromobenzoyl chloride
(3-methoxyphenyl)magnesium bromide
(3-bromophenyl)-(3-methoxyphenyl)-methanone
Conditions | Yield |
---|---|
Stage #1: 3-bromobenzoyl chloride With tributylphosphine In tetrahydrofuran at 20℃; for 0.333333h; Stage #2: (3-methoxyphenyl)magnesium bromide In tetrahydrofuran at 20℃; for 0.166667h; | 98% |
(3-methoxyphenyl)magnesium bromide
(2-isocyanophenyl)(phenyl)methanone
2-(3-methoxyphenyl)-3-phenyl-3H-indol-3-ol
Conditions | Yield |
---|---|
Stage #1: (3-methoxyphenyl)magnesium bromide; (2-isocyanophenyl)(phenyl)methanone In tetrahydrofuran; diethyl ether at 0℃; Stage #2: With water; ammonium chloride In tetrahydrofuran; diethyl ether at 0℃; | 98% |
quinolin-6-yl 4-methylbenzene-1-sulfonate
(3-methoxyphenyl)magnesium bromide
6-(3'-methoxyphenyl)quinoline
Conditions | Yield |
---|---|
Stage #1: (3-methoxyphenyl)magnesium bromide With C24H52Cl2O12P4Pd2 In tetrahydrofuran; 1,4-dioxane at 20℃; for 0.0833333h; Kumada-Corriu cross-coupling reaction; Inert atmosphere; Stage #2: quinolin-6-yl 4-methylbenzene-1-sulfonate In tetrahydrofuran; 1,4-dioxane at 80℃; for 24h; Kumada-Corriu cross-coupling reaction; Inert atmosphere; regioselective reaction; | 98% |
(3-methoxyphenyl)magnesium bromide
(E)-1-(3-methoxyphenyl)cyclohept-1-en
Conditions | Yield |
---|---|
With N,N'-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene hydrochloride; palladium diacetate In tetrahydrofuran at 50℃; for 3h; Schlenk technique; Inert atmosphere; Sealed tube; | 98% |
(3-methoxyphenyl)magnesium bromide
Conditions | Yield |
---|---|
With copper acetylacetonate In tetrahydrofuran at -18 - 0℃; for 2h; enantiospecific reaction; | 98% |
(3-methoxyphenyl)magnesium bromide
allyl bromide
1-allyl-3-methoxybenzene
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 24h; | 97% |
In tetrahydrofuran; toluene at 0 - 20℃; for 18h; | 81% |
(3-methoxyphenyl)magnesium bromide
3-methoxy-benzaldehyde
bis(3-methoxyphenyl)methanol
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 3h; Grignard Reaction; | 97% |
(3-methoxyphenyl)magnesium bromide
propionic acid anhydride
1-(3-methoxyphenyl)propan-1-one
Conditions | Yield |
---|---|
In tetrahydrofuran; diethyl ether at -70℃; | 97% |
(3-methoxyphenyl)magnesium bromide
(1E)-4,4-bis(methylthio)-2-nitro-1-pyrrolidino-1,3-butadiene
(E)-4-(3-methoxyphenyl)-1,1-bis(methylthio)-3-nitro-1,3-butadiene
Conditions | Yield |
---|---|
In tetrahydrofuran at -78℃; | 97% |
4-benzyloxy-6-bromo-3-methoxybenzaldehyde
(3-methoxyphenyl)magnesium bromide
[4-(benzyloxy)-2-bromo-5-methoxyphenyl](3-methoxyphenyl)methanol
Conditions | Yield |
---|---|
In diethyl ether at 0 - 20℃; for 3h; Inert atmosphere; | 97% |
1-bromo-3,5-dimethoxybenzene
(3-methoxyphenyl)magnesium bromide
3,3',5-trimethoxy-1,1'-biphenyl
Conditions | Yield |
---|---|
With nickel(II) fluoride; 1,3-bis(3,6-diisopropylphenyl)imidazolium hydrochloride In tetrahydrofuran at 0 - 80℃; for 12.5h; Inert atmosphere; | 97% |
(3-methoxyphenyl)magnesium bromide
3,3'-dimethoxybiphenyl
Conditions | Yield |
---|---|
With iron(III) chloride; 1,2-dichloro-ethane In tetrahydrofuran at 20℃; for 0.166667h; | 96% |
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical In tetrahydrofuran at 66℃; for 0.166667h; Inert atmosphere; | 87% |
With 4-oxo-2,2,6,6-tetramethylpiperidin-oxyl In tetrahydrofuran at 66℃; for 0.166667h; Inert atmosphere; | 87% |
(3-methoxyphenyl)magnesium bromide
Conditions | Yield |
---|---|
In tetrahydrofuran for 0.5h; Grignard reaction; | 96% |
(triphenylphosphine)gold(I) chloride
(3-methoxyphenyl)magnesium bromide
(3-methoxyphenyl)(triphenyl-λ5-phosphanyl)gold
Conditions | Yield |
---|---|
In tetrahydrofuran 3-methoxyphenylmagnesium bromide added dropwise at -78°C to soln.ClAuPPh3 in THF in Schlenk techniques under Ar; mixt. warmed to room te mp., mixed for 16 h; treated with satd. soln. of NH4Cl, extd. with Et2O; org. layers washed with satd. soln. of NaCl, dried over MgSO4; solvents removed under vac.; crystals obtained via crystn. from CHCl3; | 96% |
(3-methoxyphenyl)magnesium bromide
Conditions | Yield |
---|---|
Stage #1: (1RS,5RS,6RS,7RS)-3-methoxy-6-methyl-7-phenylbicyclo[3.2.1]-oct-3-ene-2,8-dione; (3-methoxyphenyl)magnesium bromide In tetrahydrofuran at 0 - 20℃; for 0.5h; Inert atmosphere; Stage #2: With water In tetrahydrofuran at 0℃; diastereoselective reaction; | 96% |
1-bromocyclohexane
(3-methoxyphenyl)magnesium bromide
1-cyclohexyl-3-methoxybenzene
Conditions | Yield |
---|---|
With Iron(III) amine-bis(phenolate) complex In diethyl ether at 20℃; for 0.5h; Inert atmosphere; | 96% |
With C54H80Cl2Fe2N2O4 In diethyl ether at 22℃; for 0.5h; Inert atmosphere; | > 95 %Chromat. |
With [Fe(n-propylamino-N,N-bis(2-methylene-4-tert-butyl-6-methylphenolate))(chloride)]2 In diethyl ether at 22℃; for 0.5h; Catalytic behavior; | > 95 %Chromat. |
Conditions | Yield |
---|---|
Stage #1: 4-vinylbenzyl chloride With cobalt(III) acetylacetonate In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 30℃; for 1h; Stage #2: (3-methoxyphenyl)magnesium bromide In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 30℃; for 0.333333h; | 96% |
5-benzyloxy-2-bromo-4-methoxybenzaldehyde
(3-methoxyphenyl)magnesium bromide
[5-(benzyloxy)-2-bromo-4-methoxyphenyl](3-methoxyphenyl)methanol
Conditions | Yield |
---|---|
In diethyl ether at 0 - 20℃; for 3h; Inert atmosphere; | 96% |
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