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Cas:38642-74-9
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inquiryHot sale & hot cake top quality Estradiol Valerate 979-32-8 Appearance White crystalline powder Identification IR
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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/1035.html Product Name 2-Cyano-phenothiazine CAS No. 38642-74-9
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inquiry2-Cyano-phenothiazine CAS:38642-74-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic in
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inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
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inquiry2-Cyano-phenothiazine CAS: 38642-74-9 Specification product name 2-cyano-phenothiazine cas no. 38642-74-9 appearance yellowish powder assay ≥99% capacity 100mt/year min.packing
Cas:38642-74-9
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Min.Order:1 Gram
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Cas:38642-74-9
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:38642-74-9
Min.Order:10 Gram
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inquiryProduct name: 2-Cyano Phenothiazine CAS No.: 38642-74-9 Molecule Formula:C13H8N2S Molecule Weight:224.28 Purity: 99.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard TESTING ITE
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
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inquiryProduct name: 2-Cyano-phenothiazine Molecular formula : C12H9NS Molecular weight: 166.22 Appearance:gray green powder Storage:Store in cool and dry place, away from sun light. Package:25kg/drum Application:
Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service an
Wuhu Nuovo Chemical Technology Co., Ltd. was established in August 2014, mainly engaged in the development, production and sales of ionic liquids, ribose, nucleosides, nucleotides and related chemicals; Products are mainly used in new energy, new ma
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inquiryR & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
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inquiryhigh purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
Conditions | Yield |
---|---|
With nickel(II) acetylacetonate; potassium fluoride; phenylsilane; ammonia; zinc; bis(2-diphenylphosphinoethyl)phenylphosphine In 1-methyl-pyrrolidin-2-one at 90 - 140℃; under 760.051 Torr; for 20h; Sealed tube; | 94% |
2-chlorophenothiazine
copper(I) cyanide
10H-phenothiazine-2-carbonitrile
Conditions | Yield |
---|---|
With p-toluenesulfonyl chloride; sodium iodide; lithium iodide In quinoline at 120 - 230℃; for 16h; Reagent/catalyst; Temperature; | 92.6% |
Conditions | Yield |
---|---|
With potassium iodide; lithium iodide In cyclohexane at 85 - 218℃; for 10h; Solvent; Inert atmosphere; | 90.2% |
4-cyanobenzoic acid methyl ester
2-(methylthio)-10H-phenothiazine
10H-phenothiazine-2-carbonitrile
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel (0); 1,2-bis-(dicyclohexylphosphino)ethane In o-xylene at 140℃; for 24h; Glovebox; Inert atmosphere; | 54% |
4-((2-aminophenyl)thio)-3-fluorobenzonitrile
A
10H-phenothiazine-2-carbonitrile
B
10H-phenothiazine-3-carbonitrile
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 100℃; for 3h; | A 24% B 52% |
4-((2-aminophenyl)thio)-3-fluorobenzonitrile
10H-phenothiazine-2-carbonitrile
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 140℃; for 48h; | 30% |
phenothiazine-2-carboxamide
10H-phenothiazine-2-carbonitrile
Conditions | Yield |
---|---|
With trichlorophosphate Heating; | |
With trichlorophosphate In N,N-dimethyl-formamide at 0 - 20℃; for 1h; |
2-(3'-cyanophenylaminophenyl)disulfide
A
10H-phenothiazine-2-carbonitrile
B
2-mercapto 3'-cyanodiphenylamine
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 110℃; for 0.666667h; Yield given. Yields of byproduct given; |
Conditions | Yield |
---|---|
With quinoline |
3,4-Difluorobenzonitrile
10H-phenothiazine-2-carbonitrile
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) NaH / 1.) DMF, 0 deg C, 0.5 h, 2.) DMF, 0 deg C, 12 h 2: 30 percent / dimethylformamide / 48 h / 140 °C View Scheme | |
Multi-step reaction with 2 steps 1: 1.) NaH / 1.) DMF, 0 deg C, 0.5 h, 2.) DMF, 0 deg C, 12 h 2: 24 percent / NaH / dimethylformamide / 3 h / 100 °C View Scheme |
2-amino-benzenethiol
10H-phenothiazine-2-carbonitrile
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) NaH / 1.) DMF, 0 deg C, 0.5 h, 2.) DMF, 0 deg C, 12 h 2: 30 percent / dimethylformamide / 48 h / 140 °C View Scheme | |
Multi-step reaction with 2 steps 1: 1.) NaH / 1.) DMF, 0 deg C, 0.5 h, 2.) DMF, 0 deg C, 12 h 2: 24 percent / NaH / dimethylformamide / 3 h / 100 °C View Scheme |
10H-phenothiazine-2-carboxylic acid
10H-phenothiazine-2-carbonitrile
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: (i) PCl5, benzene, (ii) NH3 2: POCl3 / Heating View Scheme |
2-chlorophenothiazine
10H-phenothiazine-2-carbonitrile
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium iodide / 1-methyl-pyrrolidin-2-one / Reflux 2: trichlorophosphate / N,N-dimethyl-formamide / 1 h / 0 - 20 °C View Scheme |
10H-phenothiazine-2-carbonitrile
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 110℃; Green chemistry; regioselective reaction; |
di-tert-butyl dicarbonate
10H-phenothiazine-2-carbonitrile
Conditions | Yield |
---|---|
Stage #1: 10H-phenothiazine-2-carbonitrile With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.25h; Stage #2: di-tert-butyl dicarbonate In N,N-dimethyl-formamide at 20℃; for 3h; | 100% |
Stage #1: 10H-phenothiazine-2-carbonitrile With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃; for 0.5h; Inert atmosphere; Stage #2: di-tert-butyl dicarbonate In N,N-dimethyl-formamide; mineral oil at 20℃; Inert atmosphere; | 75% |
With sodium hydride In N,N-dimethyl-formamide at 20℃; for 18h; | 72% |
Conditions | Yield |
---|---|
With oxygen In acetic acid at 150℃; for 24h; Sealed tube; | 98% |
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate In acetonitrile at 20℃; for 72h; Irradiation; | 94% |
10H-phenothiazine-2-carbonitrile
N,N-diethylaniline
Conditions | Yield |
---|---|
With tert-butylammonium hexafluorophosphate(V) In acetonitrile at 20℃; for 3h; Electrolysis; | 94% |
10H-phenothiazine-2-carbonitrile
10H-phenothiazine-2-carboxylic acid
Conditions | Yield |
---|---|
With hydrogenchloride; acetic acid at 117℃; for 18h; Inert atmosphere; | 92% |
With hydrogenchloride; acetic acid at 120℃; for 18h; | 90% |
With hydrogenchloride; water In methanol at 100℃; |
Conditions | Yield |
---|---|
With copper(I) bromide In N,N-dimethyl-formamide at 60℃; for 24h; Schlenk technique; | 83% |
With copper(I) bromide In N,N-dimethyl-formamide at 60℃; for 24h; | 83% |
Conditions | Yield |
---|---|
With sodium periodate; acetic acid In dichloromethane at 40℃; for 24h; Inert atmosphere; | 80% |
Methyl 4-(bromomethyl)benzoate
10H-phenothiazine-2-carbonitrile
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; Inert atmosphere; | 79% |
10H-phenothiazine-2-carbonitrile
4-methoxy-phenol
Conditions | Yield |
---|---|
With tetrabutylammonium tetrafluoroborate In methanol; acetonitrile at 20℃; for 1.66667h; Electrochemical reaction; Inert atmosphere; | 67% |
Conditions | Yield |
---|---|
With copper(I) bromide In N,N-dimethyl-formamide at 60℃; for 24h; | 66% |
10H-phenothiazine-2-carbonitrile
10H-phenothiazine-2-carbaldehyde
Conditions | Yield |
---|---|
With diisobutylaluminium hydride In dichloromethane at -78 - 20℃; for 16h; | 63% |
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate In acetonitrile at 20℃; for 1h; Schlenk technique; | 54% |
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate In acetonitrile at 20℃; for 24h; Schlenk technique; | 51% |
Conditions | Yield |
---|---|
With sodium sulfate In water; acetonitrile at 20℃; for 1.25h; Inert atmosphere; Electrolysis; Electrochemical reaction; | 46% |
10H-phenothiazine-2-carbonitrile
methyl (2E)-3-[4-(bromomethyl)phenyl]methacrylate
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 7h; Inert atmosphere; | 42% |
4-HYDROXYPIPERIDINE
10H-phenothiazine-2-carbonitrile
1,3-chlorobromopropane
periciazine
Conditions | Yield |
---|---|
Stage #1: 10H-phenothiazine-2-carbonitrile; 1.3-chlorobromopropane With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 7h; Stage #2: 4-HYDROXYPIPERIDINE With triethylamine In N,N-dimethyl-formamide at 0 - 60℃; for 42h; | 40% |
10H-phenothiazine-2-carbonitrile
2-(3-iodo-2-methylpropyl)isoindoline-1,3-dione
10-(3-(1,3-dioxoisoindolin-2-yl)-2-methylpropyl)-10H-phenothiazine-2-carbonitrile
Conditions | Yield |
---|---|
Stage #1: 10H-phenothiazine-2-carbonitrile With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.5h; Inert atmosphere; Stage #2: 2-(3-iodo-2-methylpropyl)isoindoline-1,3-dione In N,N-dimethyl-formamide at 0 - 20℃; for 16.5h; | 15% |
3-(N-methylpiperazinyl)propyl chloride
10H-phenothiazine-2-carbonitrile
Propericiazin
Conditions | Yield |
---|---|
With sodium amide; xylene |
phosgene
10H-phenothiazine-2-carbonitrile
2-cyano-phenothiazine-10-carbonyl chloride
Conditions | Yield |
---|---|
With toluene at 110℃; |
N-(γ-chloro-isobutyl)-N-methyl-formamide
10H-phenothiazine-2-carbonitrile
N-Demethylcyamemazine
Conditions | Yield |
---|---|
With sodium amide; xylene anschliessendes Erwaermen mit wss.-methanol. HCl und Behandeln mit Maleinsaeure; dextrorotatory maleate; |
1,3-bis(dimethylamino)-2-chloropropane
10H-phenothiazine-2-carbonitrile
A
10-(β,β'-bis-dimethylamino-isopropyl)-phenothiazine-2-carbonitrile
B
10-(2,3-bis-dimethylamino-propyl)-phenothiazine-2-carbonitrile
Conditions | Yield |
---|---|
With sodium amide; xylene |
10H-phenothiazine-2-carbonitrile
2-chloro-1-dimethylaminopropane
10-(2-dimethylamino-propyl)-10H-phenothiazine-2-carbonitrile
Conditions | Yield |
---|---|
With sodium amide; xylene |
10H-phenothiazine-2-carbonitrile
3-(Dimethylamino)propyl chloride
10-(3-(dimethylamino)propyl)-10H-phenothiazine-2-carbonitrile
Conditions | Yield |
---|---|
Reaktion ueber mehrere Stufen; |
10H-phenothiazine-2-carbonitrile
3-(dimethylamino)-2-methylpropylchloride
cyamemazine
Conditions | Yield |
---|---|
(i) NaNH2, toluene, (ii) /BRN= 506000/; Multistep reaction; |
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