CAS No.40682-54-0,([1-PHENYL-METH-(E)-YLIDENE]-AMINO)-ACETIC ACID ETHYL ESTER Suppliers

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([1-Phenyl-Meth-(E)-Ylidene]-Amino)-Aceticacidethylester china manufacture

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Chemsigma International Co.,Ltd.

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Antimex Chemical Limied

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Glycine,N-(phenylmethylene)-, ethyl ester

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Henan Kanbei Chemical Co.,LTD

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ZHEJIANG JIUZHOU CHEM CO.,LTD

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Amadis Chemical Co., Ltd.

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2-[(phenylmethylene)amino]acetic acid ethyl ester

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Debye Scientific

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ethyl 2-(benzylideneamino)acetate

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NovaChemistry

high purity Application:Drug intermediates Materials intermediates and active molecules

N-Benzylideneglycine Ethyl Ester

Cas:40682-54-0

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Synthetic route

: 100-52-7
benzaldehyde

: 459-73-4
GlyOEt*HCl

: 40682-54-0
ethyl N-benzylideneglycinate

Conditions

Conditions	Yield
With magnesium sulfate In dichloromethane at 20℃;	100%
With diethyl ether
In ethanol Heating;

: 623-33-6
glycine ethyl ester hydrochloride

: 100-52-7
benzaldehyde

: 40682-54-0
ethyl N-benzylideneglycinate

Conditions

Conditions	Yield
Stage #1: glycine ethyl ester hydrochloride With ammonia In dichloromethane; water Stage #2: benzaldehyde With magnesium sulfate In dichloromethane at 20℃; Inert atmosphere;	100%
With magnesium sulfate; triethylamine In dichloromethane at 20℃; for 10h;	98%
With magnesium sulfate; triethylamine In dichloromethane at 20℃; for 8h; Time;	94%

: N-Benzyl-N-(ethoxycarbonylmethyl)nitroamine

: 40682-54-0
ethyl N-benzylideneglycinate

Conditions

Conditions	Yield
With sodium hydride In tetrahydrofuran Ambient temperature;

: 100-39-0
benzyl bromide

aq.-ethanolic KOH: aq.-ethanolic KOH

: 40682-54-0
ethyl N-benzylideneglycinate

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 82 percent / dimethylsulfoxide / 2 h 2: NaH / tetrahydrofuran / Ambient temperature View Scheme

: ethyl 2-aminoacetate hydrochloride

: 100-52-7
benzaldehyde

: 40682-54-0
ethyl N-benzylideneglycinate

Conditions

Conditions	Yield
Stage #1: ethyl 2-aminoacetate hydrochloride With magnesium sulfate; triethylamine In dichloromethane at 20℃; for 1h; Stage #2: benzaldehyde In dichloromethane at 20℃;

: 40682-54-0
ethyl N-benzylideneglycinate

: 70591-46-7
(S)-5-methoxycarbonylmethyl-6,6-dimethyl-2-cyclohexen-1-one

: ((S)-3-Methoxycarbonylmethyl-4,4-dimethyl-5-oxo-cyclohexyl)-{[1-phenyl-meth-(E)-ylidene]-amino}-acetic acid ethyl ester

Conditions

Conditions	Yield
With n-butyllithium; diisopropylamine In tetrahydrofuran; hexane at -78℃; for 3h;	100%

: 40682-54-0
ethyl N-benzylideneglycinate

: (E)-6-chloro-9-(2-tosylvinyl)-9H-purine

: (2R,3R,4R,5R)-ethyl 3-(6-chloro-9H-purin-9-yl)-5-phenyl-4-tosylpyrrolidine-2-carboxylate

Conditions

Conditions	Yield
With tetrakis(acetonitrile)copper(I) perchlorate; (R,R,R)-[2-(4,5-diphenyl-4,5-dihydro-1,3-oxazol-2-yl)ferrocenyl]diphenylphosphine; potassium carbonate In dichloromethane at 20℃; for 10h; Inert atmosphere; stereoselective reaction;	98%

: 40682-54-0
ethyl N-benzylideneglycinate

: 107-13-1
acrylonitrile

: (2S,4S,5R)-ethyl 4-cyano-5-phenylpyrrolidine-2-carboxylate

Conditions

Conditions	Yield
With copper(I) tetrafluoroborate; C42H32F6N3O2P; triethylamine In dichloromethane Molecular sieve; Inert atmosphere;	98%
With tetrakis(acetonitrile)copper(I)tetrafluoroborate; C42H32F6N3O2P; triethylamine In dichloromethane at 0℃; Molecular sieve; Inert atmosphere; stereoselective reaction;	98%

: 40682-54-0
ethyl N-benzylideneglycinate

: 100-39-0
benzyl bromide

: 78843-66-0
3-Phenyl-2-{[1-phenyl-meth-(E)-ylidene]-amino}-propionic acid ethyl ester

Conditions

Conditions	Yield
With sodium carbonate; potassium carbonate; N-benzyl-N,N,N-triethylammonium chloride In acetonitrile for 10h; Ambient temperature;	97%

: 40682-54-0
ethyl N-benzylideneglycinate

: 343830-62-6
1-benzyl-(Z)-3-(benzylidene)indolin-2-one

: ethyl (2'S,3R,4'S,5'S)-1-benzyl-2-oxo-2',4'-diphenylspiro[indoline-3,3'-pyrrolidine]-5'-carboxylate

Conditions

Conditions	Yield
With C24H29F6N4O2S(1+)*Br(1-); potassium carbonate In diethyl ether at 20℃; for 4h; stereoselective reaction;	97%

: 40682-54-0
ethyl N-benzylideneglycinate

: 37465-31-9
1,1-bis(diethylphosphono)ethylene

: 120355-29-5
ethyl N-benzylidene-2-amino-4,4-bis(diethoxyphosphoryl)butyrate

Conditions

Conditions	Yield
With sodium ethanolate In ethanol at 25℃; for 0.5h;	96%
With sodium ethanolate 1.) EtOH 2.) 15 min; Yield given. Multistep reaction;

: 40682-54-0
ethyl N-benzylideneglycinate

: 292638-85-8
acrylic acid methyl ester

: 109918-38-9
2-{[1-Phenyl-meth-(Z)-ylidene]-amino}-pentanedioic acid 1-ethyl ester 5-methyl ester

Conditions

Conditions	Yield
With potassium carbonate; N-benzyl-N,N,N-triethylammonium chloride In acetonitrile Ambient temperature;	93%
With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate In acetonitrile for 2h; Ambient temperature;	93%

: 40682-54-0
ethyl N-benzylideneglycinate

: 102-96-5
(2-nitroethenyl)benzene

: (2R,3R,4S,5R)-ethyl 4-nitro-3,5-diphenylpyrrolidine-2-carboxylate

Conditions

Conditions	Yield
With 2-((1R)-((tert-butylsulfinyl)amino)(phenyl)methyl)-6-(diphenylphosphanyl)-N,N-diisopropylbenzamide; silver fluoride In tetrahydrofuran at -20℃; for 10h; stereoselective reaction;	93%

: 40682-54-0
ethyl N-benzylideneglycinate

: 107-13-1
acrylonitrile

: 82672-93-3
4-Cyano-2-{[1-phenyl-meth-(Z)-ylidene]-amino}-butyric acid ethyl ester

Conditions

Conditions	Yield
With potassium carbonate; N-benzyl-N,N,N-triethylammonium chloride In acetonitrile Ambient temperature;	92%
With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate In acetonitrile for 2h; Ambient temperature;	92%

: 40682-54-0
ethyl N-benzylideneglycinate

: 102-96-5
(2-nitroethenyl)benzene

: (2c,3t,4r,5c)-3,5-diphenyl-2-ethoxycarbonyl-4-nitro-pyrrolidine

Conditions

Conditions	Yield
With cellulose sulfuric acid In ethanol at 20℃; for 34h; diastereoselective reaction;	92%
With silver(I) acetate; triethylamine In toluene at 20℃;

: 222159-48-0
C26H17Cl3O2

: 40682-54-0
ethyl N-benzylideneglycinate

: ethyl 3-(2-chlorophenyl)-4-((E)-3-(2-chlorophenyl)acryloyl)-5-phenylpyrrolidine-2-carboxylate

Conditions

Conditions	Yield
With bis(cyclopentadienyl)titanium dichloride; triethylamine In acetonitrile at 20℃; for 3h; Huisgen cycloaddition; stereospecific reaction;	90%

: 1165938-89-5
C26H17F3O2

: 40682-54-0
ethyl N-benzylideneglycinate

: ethyl 3-(4-fluorophenyl)-4-((E)-3-(4-fluorophenyl)acryloyl)-5-phenylpyrrolidine-2-carboxylate

Conditions

Conditions	Yield
With bis(cyclopentadienyl)titanium dichloride; triethylamine In acetonitrile at 20℃; for 3h; Huisgen cycloaddition; stereospecific reaction;	90%

: 941-69-5
N-phenyl-maleimide

: 40682-54-0
ethyl N-benzylideneglycinate

: 1443277-94-8
ethyl (1S,3R,3aS,6aR)-4,6-dioxo-3,5-diphenyloctahydropyrrole[3,4-c]pyrrole-1-carboxylate

Conditions

Conditions	Yield
With C32H29FeN2OP; silver(I) acetate; triethylamine In toluene at -20℃; for 12h; Inert atmosphere; stereoselective reaction;	90%

: 40682-54-0
ethyl N-benzylideneglycinate

: icyano(6,7-dimethylphthalazin-2-ium-2-yl)methanide

: (1S,3S,11bR)-ethyl 4,4-dicyano-9,10-dimethyl-3-phenyl-2,3,4,11b-tetrahydro-1H-pyrazino[2,1-a]phthalazine-1-carboxylate

Conditions

Conditions	Yield
With C28H28FeNOP; tetrakis(acetonitrile)copper(I) tetrafluoroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene In 1,2-dichloro-ethane at -20℃; Inert atmosphere; stereoselective reaction;	90%

: 40682-54-0
ethyl N-benzylideneglycinate

: 1169882-37-4
6-methoxybenzo[e][1,2,3]oxathiazine 2,2-dioxide

: C19H19NO4

Conditions

Conditions	Yield
With triethylamine; quinidine In dichloromethane at 20℃; for 36h;	90%

: 40682-54-0
ethyl N-benzylideneglycinate

: 106-95-6
allyl bromide

: 119933-90-3
2-{[1-Phenyl-meth-(E)-ylidene]-amino}-pent-4-enoic acid ethyl ester

Conditions

Conditions	Yield
With potassium hydroxide; potassium carbonate; N-benzyl-N,N,N-triethylammonium chloride In acetonitrile for 14h; Ambient temperature;	89%

: 40682-54-0
ethyl N-benzylideneglycinate

: 52509-29-2
3-(Chloromethyl)-2-phenylmethoxyanisole

: C26H27NO4

Conditions

Conditions	Yield
With sodium ethanolate In tetrahydrofuran at 0 - 50℃;	88.3%

: 1165938-88-4
C20H14O2S3

: 40682-54-0
ethyl N-benzylideneglycinate

: ethyl 5-phenyl-3-(thiophen-2-yl)-4-((E)-3-(thiophen-2-yl)acryloyl)-pyrrolidine-2-carboxylate

Conditions

Conditions	Yield
With bis(cyclopentadienyl)titanium dichloride; triethylamine In acetonitrile at 20℃; for 2h; Huisgen cycloaddition; stereospecific reaction;	88%

: 124081-76-1
C29H26O2

: 40682-54-0
ethyl N-benzylideneglycinate

: ethyl 5-phenyl-3-(p-tolyl)-4-((E)-3-p-tolylacryloyl)pyrrolidine-2-carboxylate

Conditions

Conditions	Yield
With bis(cyclopentadienyl)titanium dichloride; triethylamine In acetonitrile at 20℃; for 2.5h; Huisgen cycloaddition; stereospecific reaction;	88%

: 40682-54-0
ethyl N-benzylideneglycinate

: 103-26-4
methyl cinnamate

: 113845-89-9
3-Phenyl-2-{[1-phenyl-meth-(Z)-ylidene]-amino}-pentanedioic acid dimethyl ester

Conditions

Conditions	Yield
With potassium carbonate In methanol	87%

: 1046149-74-9, 1166996-02-6
C20H17N3O2S3

: 40682-54-0
ethyl N-benzylideneglycinate

: ethyl 3-(4-methylthiazol-5-yl)-4-((E)-3-(4-methylthiazol-5-yl)acryloyl)-5-phenylpyrrolidine-2-carboxylate

Conditions

Conditions	Yield
With bis(cyclopentadienyl)titanium dichloride; triethylamine In acetonitrile at 20℃; for 2.5h; Huisgen cycloaddition; stereospecific reaction;	87%

: 40682-54-0
ethyl N-benzylideneglycinate

: 78032-08-3
5-chloro phthalazine

: (1S,3S,11bR)-ethyl 4,4-dicyano-9,10-dimethyl-3-phenyl-2,3,4,11b-tetrahydro-1H-pyrazino[2,1-a]phthalazine-1-carboxylate

Conditions

Conditions	Yield
With C28H28FeNOP; tetrakis(acetonitrile)copper(I) tetrafluoroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene In 1,2-dichloro-ethane at -20℃; Inert atmosphere; stereoselective reaction;	87%

: 40682-54-0
ethyl N-benzylideneglycinate

: 147720-85-2
<<3-(bromomethyl)-2-quinoxalinyl>methyl>phosphonic acid dimethyl ester

: 147720-93-2
α-amino-3-<(dimethoxyphosphinyl)methyl>-2-quinoxalinepropanoic acid ethyl ester

Conditions

Conditions	Yield
With potassium tert-butylate In tetrahydrofuran at -78℃; for 2h;	85%

: 40682-54-0
ethyl N-benzylideneglycinate

: 147720-88-5
<<3-(bromomethyl)-6,7-dimethoxy-2-quinoxalinyl>methyl>phosphonic acid dimethyl ester

: 143154-20-5
α-amino-6,7-dimethyl-3-<(dimethoxyphosphinyl)methyl>-2-quinoxalinepropanoic acid ethyl ester

Conditions

Conditions	Yield
With potassium tert-butylate In tetrahydrofuran at -78℃; for 2h;	85%

: 40682-54-0
ethyl N-benzylideneglycinate

: 959-33-1
3-(4-methoxyphenyl)-1-phenylprop-2-en-1-one

: 111396-04-4
4-Benzoyl-3-(4-methoxy-phenyl)-5-phenyl-pyrrolidine-2-carboxylic acid ethyl ester

Conditions

Conditions	Yield
With potassium carbonate In ethanol	85%

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Hangzhou ZeErRui Chemical Co., Ltd.

Chemsigma International Co.,Ltd.

Antimex Chemical Limied

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