NITROCEFIN, 3-(2,4-DINITROSTYRYL)-(6R, 7R)-7-(2-THIENYLACETAMIDO)-CEPH-3-EM-4 CARBOXYLIC ACID, E-ISOMER;(6R)-3-[(E)-2-(2,4-Dinitrophenyl)ethenyl]-8-oxo-7α-[(2-thienylacetyl)amino]-5-thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylic acid CAS No.:4
Cas:41906-86-9
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factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryAppearance: Off-White crystalline powder Water: ≤1.0% Melting point :129.0 ~ 134.0℃ Specific rotation (C=0.5,Acetone) -6.5…Appearance:Off-White crystalline powder Storage:cool and dry Package:25kg/drum Application:Preservative
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inquiry41906-86-9 Nitrocefin / high quality /Best price/In stock Application:41906-86-9 Nitrocefin / high quality /Best price/In stock
Cas:41906-86-9
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Nitrocefin
Conditions | Yield |
---|---|
With methoxybenzene; trifluoroacetic acid In dichloromethane at 0℃; for 0.5h; | 87% |
Conditions | Yield |
---|---|
With N,N'-bis(trimethylsilyl)urea; ammonium bromide 1.) CH2Cl2, reflux, 1.5 h, 2.) CH2Cl2, -10 deg C, 1.5 h; Yield given. Multistep reaction; |
Nitrocefin
Conditions | Yield |
---|---|
In chloroform; dimethyl sulfoxide at 20℃; for 24h; | 120 mg |
A
Nitrocefin
Conditions | Yield |
---|---|
With methoxybenzene; trifluoroacetic acid In dichloromethane for 0.25h; cooling; Title compound not separated from byproducts; |
2-thienylacetic acid chloride
Nitrocefin
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: 78 percent / potassium trimethylsilanolate / CH2Cl2; acetonitrile / 1 h / 20 °C 2.1: sodium iodide / butan-2-one / 20 °C 3.1: potassium trimethylsilanolate / CH2Cl2; acetonitrile / 1 h / -10 °C 3.2: 0.90 g / CH2Cl2; acetonitrile / 5 h / -10 - 20 °C 4.1: trifluoroacetic acid; anisole / CH2Cl2 / 0.25 h / cooling View Scheme | |
Multi-step reaction with 5 steps 1.1: 78 percent / potassium trimethylsilanolate / CH2Cl2; acetonitrile / 1 h / 20 °C 2.1: sodium iodide / butan-2-one / 20 °C 3.1: potassium trimethylsilanolate / CH2Cl2; acetonitrile / 1 h / -10 °C 3.2: 0.90 g / CH2Cl2; acetonitrile / 5 h / -10 - 20 °C 4.1: trifluoroacetic acid; anisole / CH2Cl2 / 0.25 h / cooling 5.1: 120 mg / CHCl3; dimethylsulfoxide / 24 h / 20 °C View Scheme |
(6R,7R)-4-methoxybenzyl-3-(chloromethyl)-8-oxo-7-(2-(thiophen-2-yl)acetamido)-5-thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylate
Nitrocefin
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: sodium iodide / butan-2-one / 20 °C 2.1: potassium trimethylsilanolate / CH2Cl2; acetonitrile / 1 h / -10 °C 2.2: 0.90 g / CH2Cl2; acetonitrile / 5 h / -10 - 20 °C 3.1: trifluoroacetic acid; anisole / CH2Cl2 / 0.25 h / cooling View Scheme | |
Multi-step reaction with 4 steps 1.1: sodium iodide / butan-2-one / 20 °C 2.1: potassium trimethylsilanolate / CH2Cl2; acetonitrile / 1 h / -10 °C 2.2: 0.90 g / CH2Cl2; acetonitrile / 5 h / -10 - 20 °C 3.1: trifluoroacetic acid; anisole / CH2Cl2 / 0.25 h / cooling 4.1: 120 mg / CHCl3; dimethylsulfoxide / 24 h / 20 °C View Scheme |
Nitrocefin
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: 78 percent / potassium trimethylsilanolate / CH2Cl2; acetonitrile / 1 h / 20 °C 2.1: sodium iodide / butan-2-one / 20 °C 3.1: potassium trimethylsilanolate / CH2Cl2; acetonitrile / 1 h / -10 °C 3.2: 0.90 g / CH2Cl2; acetonitrile / 5 h / -10 - 20 °C 4.1: trifluoroacetic acid; anisole / CH2Cl2 / 0.25 h / cooling View Scheme | |
Multi-step reaction with 5 steps 1.1: 78 percent / potassium trimethylsilanolate / CH2Cl2; acetonitrile / 1 h / 20 °C 2.1: sodium iodide / butan-2-one / 20 °C 3.1: potassium trimethylsilanolate / CH2Cl2; acetonitrile / 1 h / -10 °C 3.2: 0.90 g / CH2Cl2; acetonitrile / 5 h / -10 - 20 °C 4.1: trifluoroacetic acid; anisole / CH2Cl2 / 0.25 h / cooling 5.1: 120 mg / CHCl3; dimethylsulfoxide / 24 h / 20 °C View Scheme |
Nitrocefin
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: trifluoroacetic acid; anisole / CH2Cl2 / 0.25 h / cooling 2: 120 mg / CHCl3; dimethylsulfoxide / 24 h / 20 °C View Scheme |
Nitrocefin
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: potassium trimethylsilanolate / CH2Cl2; acetonitrile / 1 h / -10 °C 1.2: 0.90 g / CH2Cl2; acetonitrile / 5 h / -10 - 20 °C 2.1: trifluoroacetic acid; anisole / CH2Cl2 / 0.25 h / cooling View Scheme | |
Multi-step reaction with 3 steps 1.1: potassium trimethylsilanolate / CH2Cl2; acetonitrile / 1 h / -10 °C 1.2: 0.90 g / CH2Cl2; acetonitrile / 5 h / -10 - 20 °C 2.1: trifluoroacetic acid; anisole / CH2Cl2 / 0.25 h / cooling 3.1: 120 mg / CHCl3; dimethylsulfoxide / 24 h / 20 °C View Scheme |
7-Aminocephalosporanic acid
Nitrocefin
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: water; sodium hydroxide / methanol / -20 - -10 °C 2.1: sodium hydroxide / acetone; water / 0 °C / pH 8 2.2: 0.5 h 3.1: phosphorus tribromide / tetrahydrofuran / -5 °C / Inert atmosphere 4.1: ethyl acetate / 15 h / 20 °C 5.1: sodium carbonate / dichloromethane / 2.5 h / 0 - 20 °C 6.1: methoxybenzene; trifluoroacetic acid / dichloromethane / 0.5 h / 0 °C View Scheme |
(6R,7R)-7-amino-3-hydroxymethyl-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid
Nitrocefin
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: sodium hydroxide / acetone; water / 0 °C / pH 8 1.2: 0.5 h 2.1: phosphorus tribromide / tetrahydrofuran / -5 °C / Inert atmosphere 3.1: ethyl acetate / 15 h / 20 °C 4.1: sodium carbonate / dichloromethane / 2.5 h / 0 - 20 °C 5.1: methoxybenzene; trifluoroacetic acid / dichloromethane / 0.5 h / 0 °C View Scheme |
3-hydroxymethyl-8-oxo-7-[(2-thienylacetyl)amino]-5-thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylic acid diphenylmethyl ester
Nitrocefin
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: phosphorus tribromide / tetrahydrofuran / -5 °C / Inert atmosphere 2: ethyl acetate / 15 h / 20 °C 3: sodium carbonate / dichloromethane / 2.5 h / 0 - 20 °C 4: methoxybenzene; trifluoroacetic acid / dichloromethane / 0.5 h / 0 °C View Scheme |
(6R)-3-bromomethyl-8-oxo-7t-(2-thiophen-2-yl-acetylamino)-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzhydryl ester
Nitrocefin
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: ethyl acetate / 15 h / 20 °C 2: sodium carbonate / dichloromethane / 2.5 h / 0 - 20 °C 3: methoxybenzene; trifluoroacetic acid / dichloromethane / 0.5 h / 0 °C View Scheme |
Nitrocefin
nitrocefin complexed with oxacillin bound N146K/E150K double mutant variant of penicillin binding protein 2a (residues 23-668) from staphylococcus aureus ATCC 700699
Conditions | Yield |
---|---|
In aq. buffer at 20℃; for 0.166667h; pH=7; Kinetics; |
Nitrocefin
nitrocefin complexed with oxacillin bound N146K/E150K/H351N triple mutant variant of penicillin binding protein 2a (residues 23-668) from staphylococcus aureus ATCC 700699
Conditions | Yield |
---|---|
In aq. buffer at 20℃; for 0.166667h; pH=7; Kinetics; |
Nitrocefin
Conditions | Yield |
---|---|
With β-lactamase Enzymatic reaction; |
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