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inquiryITEM STANDARD Identification Infrared absorption should conform HPLC retention time should conform Sulphated Ash ≤0.1% Organic volatile impurities ≤0.1% Heavy metals ≤10ppm
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inquiryProduct Name: Adenosine 5'-monophosphate disodium salt Synonyms: disodium adenosine 5'-phosphate;5'-ADENYLIC ACID SODIUM SALT;5-ADENYLIC ACID, SODIUM SALT;5'-AMP 2NA;5'-AMP DISODIUM SALT;5'-AMP-NA2;5'-AMP SODIUM SALT;A
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inquiryConditions | Yield |
---|---|
Stage #1: adenosine In various solvent(s) at 20 - 100℃; for 0.333333h; Stage #2: With 2,6-dimethylpyridine; trichlorophosphate In various solvent(s) at 0℃; for 3h; | A 28% B 48% |
A
adenosine-5'-monophosphate disodium salt
Conditions | Yield |
---|---|
With phosphorating extract from S. cerevisiae at 28℃; for 8h; | A 8% B 30.5 mg C 11% |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: various solvent(s) / 0.33 h / 20 - 100 °C 1.2: 48 percent / PSCl3; 2,6-lutidine / various solvent(s) / 3 h / 0 °C 2.1: 8 percent / phosphorating extract from S. cerevisiae / 8 h / 28 °C View Scheme |
Acridin-9-yl-[3-(1,13-dioxa-4,7,10,16,19,22-hexaaza-cyclotetracos-7-yl)-propyl]-amine; hydrochloride
adenosine diphosphate disodium salt
A
adenosine-5'-monophosphate disodium salt
Conditions | Yield |
---|---|
In water; water-d2 at 80℃; Rate constant; |
adenosine-5'-monophosphate disodium salt
Conditions | Yield |
---|---|
With water; zinc(II) cation pH=5.5; |
Conditions | Yield |
---|---|
With diadenosine 5',5'''-P1,P4-tetraphosphate (Ap4A) phosphorylase from Mycobacterium tuberculosis H37Rv at 37℃; for 0.5h; pH=7.6; Kinetics; aq. buffer; Enzymatic reaction; |
CoN(C3H6NH2)3(OH2)2(3+)
adenosine-5'-monophosphate disodium salt
Conditions | Yield |
---|---|
In water Kinetics; react. for about 6 h at 25°C;; elem. anal.; | 100% |
Conditions | Yield |
---|---|
With Dowex 50W×8 resin In water at 20℃; for 0.5h; | 99% |
With Dowex 50WX-8 200 mesh, H+ |
adenosine-5'-monophosphate disodium salt
α,β-D-ribofuranose-5-phophate disodium salt
Conditions | Yield |
---|---|
With Dowex 50 W-X8 (H+ form) In water for 0.141667h; Heating; | 94% |
adenosine-5'-monophosphate disodium salt
A
dirhodium tetracetate dihydrate
Conditions | Yield |
---|---|
In water slight excess of nucleotide, stirring for 5 h (dissoln.); pptn. on acetone addn.; elem. anal.; | A n/a B 80% |
cysteinato-O-methylester-palladium(II)-μ-dichloro-cysteinato-O-methylester-palladium(II)
adenosine-5'-monophosphate disodium salt
Conditions | Yield |
---|---|
In water Pd complex and nucleoside suspended in water, stirred at 55°C until complete dissolution; added ethanol, ppt. filtered, washed with 80% ethanol until free from chloride, then with abs. ethanol and ether, dried at 60°C under vac., elem. anal.; | 50% |
Conditions | Yield |
---|---|
Stage #1: 4,4'-bipyridine; copper(II) nitrate hexahydrate; water In ethanol for 0.25h; Stage #2: adenosine-5'-monophosphate disodium salt In ethanol Stage #3: With nitric acid In ethanol for 1h; pH=3.65; | 49% |
adenosine-5'-monophosphate disodium salt
di-n-butylthioxophosphoranyl bromide
adenosine 5'-phosphoric di-n-butylphosphinothioic anhydride
Conditions | Yield |
---|---|
With pyridine; N,N'-dicyclohexyl-4-morpholine carboxamidine for 3h; Ambient temperature; |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 94 percent / Dowex 50 W-X8 (H+ form) / H2O / 0.14 h / Heating 2: 70 mmol / Na2ATP, MgCl2*6H2O, PEP-K+, K2HPOu, Na2EDTA / 96 h / 30 °C / immobilized PRPP synthetase, pyruvate kinase, adenylate kinase, pH 7.4 3: MgCl2*6H2O, DTT / 192 h / PAN-immobilized O-5-decarboxylase, O-5-P-pyrophosphorylase, PPiase View Scheme |
adenosine-5'-monophosphate disodium salt
5-phospho-D-ribosyl α-1-pyrophosphate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 94 percent / Dowex 50 W-X8 (H+ form) / H2O / 0.14 h / Heating 2: 70 mmol / Na2ATP, MgCl2*6H2O, PEP-K+, K2HPOu, Na2EDTA / 96 h / 30 °C / immobilized PRPP synthetase, pyruvate kinase, adenylate kinase, pH 7.4 View Scheme |
adenosine-5'-monophosphate disodium salt
Conditions | Yield |
---|---|
With potassium nitrate In water (N2); mixing cobalt complex and AMP in 0.2 M aq. KNO3 at pH 7.0; not isolated, detected by UV; |
Conditions | Yield |
---|---|
In water addn. of a soln. of Na2(5'AMP) (pH = 4.2) to a soln. of Cr(L-Cys)Cl2*2H2O, 40°C, 3 h, pptn.; filtration, ppt. washed with EtOH, dried in vac. (P4O10), elem. anal.; |
Conditions | Yield |
---|---|
In water addn. of a soln. of Na2(5'AMP) (pH = 7.0) to a soln. of Cr(L-Cys)2Cl*2H2O, the mixture (pH = 5.9) at 40°C, 6 h (final pH = 5.8); concd. to 5 ml, chromy. (Sephadex G-10), evapn., ppt. washed with EtOH, dried in vac. (P4O10), elem. anal.; |
adenosine-5'-monophosphate disodium salt
Conditions | Yield |
---|---|
In sodium hydroxide react. at 25°C in triethanoleamine*HCl-NaOH buffer (pH 7.5); |
Conditions | Yield |
---|---|
In water soln. of Cr(NO3)3 and nucleotide were mixed and heated at 50°C for 2 h, soln. of ligand in H2O was added (pH=3.5); filtered, washed, dried over P2O5; elem. anal.; |
adenosine-5'-monophosphate disodium salt
Conditions | Yield |
---|---|
In water mixing a soln. of Cr-complex dissolved in water and Na25'AMP in water (starting pH=5.8), placed in a thermostatic bath at 45°C for 21 h, pptn. with small amount, addn. of EtOH, pptn.; filtration, washed with EtOH, vac. dried over P4O10; elem. anal.; |
Conditions | Yield |
---|---|
In water mixing a soln. of Cr-complex dissolved in water and Na25'AMP in water (pH=3.5-3.6), thermostatic bath at 45°C for 11-16 h; soln concd. (rotavapor), ppt. obtained with 5'AMP before elution, dried over P4O10; |
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