DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:5018-38-2
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inquiryAbout Product Details 4,6-Dichloro-5-methoxypyrimidine Basic information
Cas:5018-38-2
Min.Order:1 Kilogram
FOB Price: $1.0 / 5.0
Type:Lab/Research institutions
inquiry4,6-Dichloro-5-methoxypyrimidine Basic information Product Name: 4,6-Dichloro-5-methoxypyrimidine Synonyms: 4,6-DICHLORO-5-METHOXYPYRIMIDINE;2,4-dimethoxy-2-methylmercapyrimidine;4,6-Dic
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Min.Order:1 Metric Ton
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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Min.Order:1 Kilogram
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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Min.Order:100 Gram
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Min.Order:10 Kilogram
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inquiry4,6-Dichloro-5-methoxypyrimidine CAS:5018-38-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality o
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Min.Order:1 Gram
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Type:Lab/Research institutions
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Min.Order:1 Kilogram
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Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryProduct name: 4,6-Dichloro-5-Methoxypyrimidine CAS No.:5018-38-2 Molecule Formula:C5H4Cl2N2O Molecule Weight:179.00 Purity: 99% Package:25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS
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Min.Order:1 Kilogram
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Min.Order:1 Milligram
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Min.Order:100 Gram
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Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With triethylamine; trichlorophosphate In toluene at 100 - 105℃; for 1.5h; Reflux; | 86% |
With N,N-diethylaniline; trichlorophosphate In heptane-ethyl acetate | 75.6% |
Stage #1: 4,6-Dihydroxy-5-methoxypyrimidine With trichlorophosphate for 1h; Heating / reflux; Stage #2: With N,N-diethylaniline at 20℃; Heating / reflux; | 40% |
ethanolamine
4,6-dichloro-5-methoxypyrimidine
2-((6-chloro-5-methoxypyrimidin-4-yl)amino)ethanol
Conditions | Yield |
---|---|
With potassium carbonate In 1,4-dioxane at 125℃; Inert atmosphere; | 100% |
With potassium carbonate In 1,4-dioxane at 140℃; for 1h; Microwave irradiation; | |
With potassium carbonate In 1,4-dioxane at 125℃; for 8h; | 10.5 g |
4-amino-3-nitrophenylboronic acid pinacol ester
4,6-dichloro-5-methoxypyrimidine
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In 1,4-dioxane; water at 80℃; for 3h; Suzuki Coupling; | 100% |
isopropyl 4-hydroxypiperidine-1-carboxylate
4,6-dichloro-5-methoxypyrimidine
4-(6-chloro-5-methoxy-pyrimidin-4-yloxy)-piperidine-1-carboxylic acid isopropyl ester
Conditions | Yield |
---|---|
With potassium tert-butylate In tetrahydrofuran at 5 - 10℃; for 2h; Inert atmosphere; | 98.6% |
With potassium tert-butylate In tetrahydrofuran at 0℃; for 0.75h; | 85% |
Stage #1: isopropyl 4-hydroxypiperidine-1-carboxylate With potassium tert-butylate In tetrahydrofuran at 20℃; for 0.5h; Stage #2: 4,6-dichloro-5-methoxypyrimidine In tetrahydrofuran at 20℃; for 8h; | 65% |
(S)-1-(4-Fluoro-phenyl)-ethylamine
4,6-dichloro-5-methoxypyrimidine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 50℃; for 24h; | 98% |
1-(tert-butoxycarbonyl)-4-aminopiperidine
4,6-dichloro-5-methoxypyrimidine
tert-butyl 4-(6-chloro-5-methoxypyrimidin-4-ylamino)piperidine-1-carboxylate
Conditions | Yield |
---|---|
With potassium carbonate In tetrahydrofuran at 20℃; for 16h; | 96% |
t-butyl 4-hydroxy piperidine-1-carboxylate
4,6-dichloro-5-methoxypyrimidine
4-(6-Chloro-5-methoxy-pyrimidin-4-yloxy)-piperidine-1-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
With potassium tert-butylate In tetrahydrofuran at 0℃; for 1h; | 94.8% |
Conditions | Yield |
---|---|
With ammonium hydroxide In water; isopropyl alcohol at 70℃; for 48h; Autoclave; | 94% |
With ammonia In water; butan-1-ol at 85℃; for 8h; Sealed tube; | 90% |
With ammonium hydroxide In butan-1-ol at 85℃; for 8h; Sealed tube; | 90% |
Conditions | Yield |
---|---|
With sodium methylate In methanol at 0 - 5℃; for 1h; | 93% |
With sodium methylate In methanol |
4,6-dichloro-5-methoxypyrimidine
4,6-dichloropyrimidin-5-ol
Conditions | Yield |
---|---|
With aluminum (III) chloride In dichloromethane at 0 - 50℃; for 6h; | 91.11% |
Stage #1: 4,6-dichloro-5-methoxypyrimidine With aluminum (III) chloride In 1,2-dichloro-ethane at 0 - 50℃; for 6h; Stage #2: With hydrogenchloride; water In methanol; 1,2-dichloro-ethane at 0 - 20℃; for 0.166667h; | 91.11% |
With aluminum (III) chloride In 1,2-dichloro-ethane at 0 - 50℃; for 6h; |
2-methyl-3-pyridinol
4,6-dichloro-5-methoxypyrimidine
4-chloro-5-methoxy-6-[(2-methylpyridin-3-yl)oxy]pyrimidine
Conditions | Yield |
---|---|
With potassium tert-butylate In tetrahydrofuran; N,N-dimethyl-formamide at 70℃; for 1.5h; Inert atmosphere; | 87% |
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 20℃; | 86% |
sodium 4-aminobenzenesulfonylacetamide
4,6-dichloro-5-methoxypyrimidine
4-(p-aminobenzenesulfonamido)-5-methoxy-6-chloropyrimidine
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 88 - 90℃; for 3h; | 85.3% |
N-(3R,4R)-(1-benzyl-4-methylpiperidin-3-yl)-methylamine
4,6-dichloro-5-methoxypyrimidine
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 70℃; Inert atmosphere; | 85% |
4,6-dichloro-5-methoxypyrimidine
4-(p-aminobenzenesulfonamido)-5-methoxy-6-chloropyrimidine
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide | 85% |
2-[2-fluoro-4-[[2-(trifluoromethyl)-4-pyridyl]oxy]phenyl]ethanamine hydrochloride
4,6-dichloro-5-methoxypyrimidine
6-chloro-N-[2-[2-fluoro-4-[[4-(trifluoromethyl)-2-pyridyl]oxy]phenyl]ethyl]-5-methoxy-pyrimidin-4-amine
Conditions | Yield |
---|---|
Stage #1: 2-[2-fluoro-4-[[2-(trifluoromethyl)-4-pyridyl]oxy]phenyl]ethanamine hydrochloride With N-ethyl-N,N-diisopropylamine In 1-methyl-pyrrolidin-2-one at 20℃; for 0.0833333h; Stage #2: 4,6-dichloro-5-methoxypyrimidine In 1-methyl-pyrrolidin-2-one at 80℃; | 78% |
4,6-dichloro-5-methoxypyrimidine
6-chloro-N-[2-[2-fluoro-4-[[4-(trifluoromethyl)-2-pyridyl]oxy]phenyl]ethyl]-5-methoxy-pyrimidin-4-amine
Conditions | Yield |
---|---|
Stage #1: 2-[2-fluoro-4-[[4-(trifluoromethyl)-2-pyridyl]oxy]phenyl]ethanamine hydrochloride With N-ethyl-N,N-diisopropylamine In 1-methyl-pyrrolidin-2-one at 20℃; for 0.0833333h; Stage #2: 4,6-dichloro-5-methoxypyrimidine In 1-methyl-pyrrolidin-2-one at 80℃; | 78% |
With N-ethyl-N,N-diisopropylamine In 1-methyl-pyrrolidin-2-one at 80℃; | 78% |
sodium salt of sulfanilamide
4,6-dichloro-5-methoxypyrimidine
4-(p-aminobenzenesulfonamido)-5-methoxy-6-chloropyrimidine
Conditions | Yield |
---|---|
Stage #1: sodium salt of sulfanilamide; 4,6-dichloro-5-methoxypyrimidine With 1-butyl-3-methylimidazolium chloride at 60 - 92℃; for 1.5h; pH=8 - 9; Stage #2: With hydrogenchloride In water; N,N-dimethyl-formamide pH=7 - 7.2; | 77.5% |
tert-butyl (3S)-3-aminopiperidine-1-carboxylate
4,6-dichloro-5-methoxypyrimidine
3-(S)-(6-chloro-5-methoxypyrimidin-4-ylamino)piperidine-1-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In isopropyl alcohol at 80℃; for 15h; | 74% |
7-(piperidin-4-yl)-1,2,3,4-tetrahydro-1,8-naphthyridine
4,6-dichloro-5-methoxypyrimidine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In ISOPROPYLAMIDE at 130℃; for 2h; | 68% |
sulfanilamide
4,6-dichloro-5-methoxypyrimidine
4-(p-aminobenzenesulfonamido)-5-methoxy-6-chloropyrimidine
Conditions | Yield |
---|---|
Stage #1: sulfanilamide With sodium hydroxide at 70℃; for 1h; Stage #2: 4,6-dichloro-5-methoxypyrimidine With N,N-dimethyl-formamide at 95℃; for 3h; | 64% |
sodium methylate
4,6-dichloro-5-methoxypyrimidine
4-chloro-5,6-dimethoxypyrimidine
Conditions | Yield |
---|---|
In methanol at 0 - 20℃; for 19h; | 57% |
methanol
sodium methylate
4,6-dichloro-5-methoxypyrimidine
4-chloro-5,6-dimethoxypyrimidine
Conditions | Yield |
---|---|
at 0 - 20℃; for 19h; Inert atmosphere; | 57% |
4-cyano-2-fluoroaniline
4,6-dichloro-5-methoxypyrimidine
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 65℃; | 55% |
With potassium carbonate In N,N-dimethyl-formamide at 65℃; | 55% |
4,6-dichloro-5-methoxypyrimidine
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 120℃; for 21h; Sealed tube; | 51% |
1-(2-fluorophenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazole
4,6-dichloro-5-methoxypyrimidine
Conditions | Yield |
---|---|
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sodium carbonate In 1,4-dioxane; water at 90℃; for 16h; | 40% |
4,6-dichloro-5-methoxypyrimidine
Conditions | Yield |
---|---|
Stage #1: 1-[4-[[4-(trifluoromethyl)-2-pyridyl]oxy]phenoxy]propan-2-amine hydrochloride With N-ethyl-N,N-diisopropylamine In 1-methyl-pyrrolidin-2-one at 20℃; for 0.0833333h; Stage #2: 4,6-dichloro-5-methoxypyrimidine In 1-methyl-pyrrolidin-2-one at 80℃; | 37% |
2-tri-n-butylstannylpyridine
4,6-dichloro-5-methoxypyrimidine
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0) In toluene for 5h; Inert atmosphere; Reflux; | 34% |
tyramine hydrochloride
4,6-dichloro-5-methoxypyrimidine
6-chloro-N-[2-[4-(6-chloro-5-methoxypyrimidin-4-yl)oxyphenyl]ethyl]-5-methoxypyrimidin-4-amine
Conditions | Yield |
---|---|
Stage #1: tyramine hydrochloride; 4,6-dichloro-5-methoxypyrimidine With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 16h; Stage #2: With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.333333h; Stage #3: 4,6-dichloro-5-methoxypyrimidine In N,N-dimethyl-formamide at 20℃; for 48h; | 31% |
With sodium hydride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 64h; | 31% |
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