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inquiryProtoporphyrin IX CAS:553-12-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedi
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Min.Order:1 Gram
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Min.Order:1 Kilogram
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A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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Conditions | Yield |
---|---|
With potassium hydroxide In methanol Reflux; Inert atmosphere; Darkness; | 76.6% |
With hydrogenchloride In water | |
With zinc diacetate In methanol; dichloromethane; chloroform; water |
Conditions | Yield |
---|---|
With 1H-imidazole; Bacillus subtilis protoporphyrinogen oxidase; flavin adenine dinucleotide In phosphate buffer; dimethyl sulfoxide at 25℃; pH=7.4; Enzyme kinetics; Further Variations:; Reagents; |
protoporphyrin IX
Conditions | Yield |
---|---|
With ammonium hydroxide; phosphoric acid tributyl ester; sulfuric acid In benzene at 40℃; for 1.5h; |
Conditions | Yield |
---|---|
With sulfuric acid at -10℃; for 18h; | 95% |
Conditions | Yield |
---|---|
Stage #1: protoporphyrin IX With 1-hydroxy-pyrrolidine-2,5-dione; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 0 - 20℃; for 4h; Stage #2: N-(2-aminoethyl)maleimide trifluoroacetate In N,N-dimethyl-formamide at 20℃; for 5h; | 73% |
methanol
protoporphyrin IX
20-amino-3,6,9,12,15,18-hexaoxaeicosanoic acid tert-butyl ester
Conditions | Yield |
---|---|
Stage #1: protoporphyrin IX With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide Inert atmosphere; Stage #2: methanol With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride Stage #3: 20-amino-3,6,9,12,15,18-hexaoxaeicosanoic acid tert-butyl ester Further stages; | 72% |
rac-5-(2-hydroxyl(cyclohexylethyl))-5H-imidazo[5,1-a]isoindole
protoporphyrin IX
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 60℃; for 5h; | 65.8% |
Conditions | Yield |
---|---|
Stage #1: protoporphyrin IX With dmap; di-tert-butyl dicarbonate In pyridine at 20℃; for 6h; Stage #2: tert-butyl alcohol In pyridine at 20℃; for 1h; Further stages.; | 64% |
With pyridine; dmap at 20℃; | 64% |
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 0 - 20℃; | 58% |
Conditions | Yield |
---|---|
Stage #1: protoporphyrin IX With pyridine; pivaloyl chloride; triethylamine In dichloromethane at -5℃; Stage #2: benzyl alcohol In dichloromethane at 5 - 8℃; for 12h; | A 47% B 18% |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 48h; | 29% |
Conditions | Yield |
---|---|
Stage #1: protoporphyrin IX With pyridine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate at 20℃; for 0.333333h; Stage #2: Glycyl-L-(1-methyl)histidinemethyl ester In N,N-dimethyl-formamide at 20℃; for 2.5h; Stage #3: methanol In N,N-dimethyl-formamide for 18h; | 25% |
Conditions | Yield |
---|---|
Stage #1: protoporphyrin IX With triethylamine In pyridine for 0.166667h; Stage #2: Stage #3: 3-(1H-imidazol-1-yl)propan-1-amine; methylamine With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate more than 3 stages; | 19% |
protoporphyrin IX
3-[(5Z,10Z,14Z,19Z)-18-(2-Carboxy-ethyl)-7,12-diformyl-3,8,13,17-tetramethyl-porphyrin-2-yl]-propionic acid
Conditions | Yield |
---|---|
With oxygen; 2,4-dichlorophenoxyacetic acid dimethylamine Mechanism; Irradiation; other porphyrine derivatives, influence of solvents; | |
With oxygen; 2,4-dichlorophenoxyacetic acid dimethylamine Irradiation; |
protoporphyrin IX
A
3-[(5Z,10Z,14Z,19Z)-18-(2-Carboxy-ethyl)-7,12-diformyl-3,8,13,17-tetramethyl-porphyrin-2-yl]-propionic acid
B
3-[(5Z,10Z,14Z,19Z)-18-(2-Carboxy-ethyl)-7-formyl-3,8,13,17-tetramethyl-12-vinyl-porphyrin-2-yl]-propionic acid
C
3-[(5Z,10Z,14Z,19Z)-18-(2-Carboxy-ethyl)-12-formyl-3,8,13,17-tetramethyl-7-vinyl-porphyrin-2-yl]-propionic acid
D
3-{(1Z,5Z,9Z,14Z)-18-(2-Carboxy-ethyl)-7-hydroxy-3,7,12,17-tetramethyl-8-[2-oxo-eth-(Z)-ylidene]-13-vinyl-7,8,22,24-tetrahydro-porphin-2-yl}-propionic acid
E
3-{(5Z,10Z,14Z,19Z)-18-(2-Carboxy-ethyl)-8-hydroxy-3,8,13,17-tetramethyl-7-[2-oxo-eth-(Z)-ylidene]-12-vinyl-7,8,21,23-tetrahydro-porphin-2-yl}-propionic acid
Conditions | Yield |
---|---|
With oxygen In benzene for 2.5h; Product distribution; Mechanism; Irradiation; var. environment, time; |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide for 0.333333h; |
Conditions | Yield |
---|---|
With sodium hydroxide at 20℃; complex formation; |
Conditions | Yield |
---|---|
With sodium hydroxide at 20℃; complex formation; |
protoporphyrin IX
Conditions | Yield |
---|---|
With oxalyl dichloride In dichloromethane for 1h; Heating; | |
With oxalyl dichloride for 0.5h; Reflux; Inert atmosphere; |
Conditions | Yield |
---|---|
With sodium amalgam | |
With sodium amalgam |
Conditions | Yield |
---|---|
With pyridine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate at 20 - 40℃; for 4.5h; |
4-(N-(2-methylimidazolyl))butylamine
protoporphyrin IX
Conditions | Yield |
---|---|
With pyridine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate at 20 - 40℃; for 0.075h; |
protoporphyrin IX
O-methyl-L-histydyl-glycine
Conditions | Yield |
---|---|
With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate In N,N-dimethyl-formamide at 20 - 40℃; for 4.5h; |
protoporphyrin IX
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: pyridine; BOP / 4.5 h / 20 - 40 °C 2: 75 mg / 12 h / 40 °C View Scheme |
protoporphyrin IX
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: pyridine; BOP / 4.5 h / 20 - 40 °C 2: 12 h / 40 °C View Scheme |
protoporphyrin IX
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: BOP; pyridine / 0.07 h / 20 - 40 °C 2: 12 h / 40 °C View Scheme |
protoporphyrin IX
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: BOP / dimethylformamide / 4.5 h / 20 - 40 °C 2: 12 h / 40 °C View Scheme |
protoporphyrin IX
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: DMAP; (Boc)2O / pyridine / 6 h / 20 °C 1.2: 64 percent / pyridine / 1 h / 20 °C 2.1: 72 percent / DPPA; Et3N / dimethylformamide / 11 h / 20 °C View Scheme |
protoporphyrin IX
4-bis(2-hydroxyethyl)-6,7-bis[2-(methoxycarbonyl)ethyl]-1,3,5,8-tetramethylporphyrin
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: 95 percent / 5 percent H2SO4 / 18 h / -10 °C 2.1: Tl(NO3)3*3H2O; MeOH 2.2: HCOOH 2.3: NaBH4 View Scheme |
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