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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

2,3-Dimethyl-1H-benzo[e]indole Manufacturer/High quality/Best price/In stock

Cas:55970-05-3

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Large Stock 99.0% 2,3-Dimethyl-1H-benzo[e]indole 55970-05-3 Producer

Cas:55970-05-3

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

2,3-Dimethyl-1H-benzo[e]indole

Cas:55970-05-3

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Top Purity CAS 55970-05-3 with fast shipping

Cas:55970-05-3

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

3H-Benz[e]indole,1,2-dimethyl-

Cas:55970-05-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Siwei Development Group Ltd.

Product name: 2,3-Dimethyl-Benz[e]indole CAS No.: 55970-05-3 Molecule Formula:C14H15N Molecule Weight:197.28 Purity: 99.0% Package: 25kg/drum Description:Off-white crystalline powder Manufacture Standards:Enterprise Standard

Lower Price 2,3-Dimethyl-Benz[e]indole

Cas:55970-05-3

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

3H-Benz[e]indole,1,2-dimethyl-

Cas:55970-05-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

2,3-Dimethyl-1H-benzo[e]indole

Cas:55970-05-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Greenutra Resource Inc

2,3-Dimethyl-1H-benzo[e]indoleAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air

2,3-Dimethyl-1H-benzo[e]indole

Cas:55970-05-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

2,3-Dimethyl-1H-benzo[e]indole

Cas:55970-05-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

2,3-Dimethyl-1H-benzo[e]indole

Cas:55970-05-3

Min.Order:0

Negotiable

Type:Other

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

2,3-Dimethyl-1H-benzo[e]indole

Cas:55970-05-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hunan Russell Chemicals Technology Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

2,3-Dimethyl-1H-benzo[e]indole 55970-05-3

Cas:55970-05-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Antimex Chemical Limied

hight degree of purity Application:Fine chemical intermediates, used as the main raw material for he synthesis of various pesticides, medicines, surfactants, polymer monomers, Ond Ontifungal agents

3H-Benz[e]indole,1,2-dimethyl-

Cas:55970-05-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Circle Star Chem-medical Technology co.,Ltd.

good quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:25kg,50kg,180kg,200kg,250kg,1000kg,customization Application:Pharma;Industry;Agricultural;chemical reaserch Tran

2,3-Dimethyl-1H-benzo[e]indole

Cas:55970-05-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

BOC Sciences

We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as primary a

2.3-Dimethyl-benz[e]indole

Cas:55970-05-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Fandachem Co.,Ltd

2,3-Dimethyl-1H-benzo[e]indole cas 55970-05-3Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

2,3-Dimethyl-1H-benzo[e]indole cas 55970-05-3

Cas:55970-05-3

Min.Order:0

Negotiable

Type:Other

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

2,3-Dimethyl-1H-benzo[e]indole

Cas:55970-05-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

AOPHARM

Aopharm is specialized in APIs, pharmaceutical intermediates & fine chemicals.1. The best quality, competitive price.2. The best service before or after shipment.3. Rich experience in export operation.4. Rich experience in modes of transportation614.

2,3-Dimethyl-1H-benzo[e]indole ,99.0% min (HPLC)

Cas:55970-05-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Capot Chemical Co., Ltd.

At Capot,We can synthesize and purify your complex molecules from 100 gram to 10 tons.Appearance:Clear colorless to light yellow liquid Storage:Dry,Seal and Cool place Package:1G,5G,10G,25G,100G,250G,500G,1KG,5KG,10KG,25KG,50KG,100KG,150KG,200KG. App

2-Methyl benz[e]indole

Cas:55970-05-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shaanxi Mingqi Chemical Co., Ltd

Known for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers. Our advantages:1, High quality with competitive price:1) Standard:BP/USP/EP/Enterprise standard2) All Purity≥99%3) We are manufacturer

2,3-Dimethyl-1H-benzo[e]indole

Cas:55970-05-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Finetech Industry Limited

FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the 2,3-Dimethyl-1H-benzo[e]indole, CAS:55970-05-3 with the most competitive price and th

2,3-Dimethyl-1H-benzo[e]indole

Cas:55970-05-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Pure Chemistry Scientific Inc.

2,3-Dimethyl-1H-benzo[e]indole Application:825564

2,3-Dimethyl-1H-benzo[e]indole

Cas:55970-05-3

Min.Order:1 Gram

FOB Price: $500.0

Type:Trading Company

inquiry

GZ HONESTCHEM CO., LTD

2,3-Dimethyl-1H-benzo[e]indoleAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air

2,3-Dimethyl-1H-benzo[e]indole

Cas:55970-05-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Jiaxing Isen Chemical Co.,Ltd

1, We supply best price with high quality 2,We could suppli different kinds of package as customer's request 3,Products could be sent by courier/air/sea 883,We could do customized service Package:As requested Application:Phar

2,3-Dimethyl-1H-benzo[e]indole

Cas:55970-05-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

NovaChemistry

high purity Application:Drug intermediates Materials intermediates and active molecules

2,3-dimethyl-1,2-dihydrobenzo[e]indole

Cas:55970-05-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

2-naphthylhydrazine hydrochloride
2243-58-5

2-naphthylhydrazine hydrochloride

butanone
78-93-3

butanone

2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

Conditions
ConditionsYield
With 4-methylbenzenesulfonic acid-based ionic liquid supported on silica gel In ethanol at 20℃; for 5h; Fischer Indole Synthesis;86%
With acetic acid at 100℃; for 3h; Fischer Indole Synthesis; Inert atmosphere;
naphthalen-2-ylamine
91-59-8

naphthalen-2-ylamine

2.3-butanediol
513-85-9

2.3-butanediol

2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

Conditions
ConditionsYield
With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; methanesulfonic acid at 170℃; for 48h; Inert atmosphere;76%
2-naphthylhydrazine hydrochloride
2243-58-5

2-naphthylhydrazine hydrochloride

2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

Conditions
ConditionsYield
With ethanol; sodium acetate; butan-1-ol und Erwaermen der Reaktionsloesung mit konz.Schwefelsaeure;
naphthalen-2-ylamine
91-59-8

naphthalen-2-ylamine

β-bromo-levulinic acid

β-bromo-levulinic acid

2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

Conditions
ConditionsYield
Man kocht das Reaktionsprodukt mit sehr verduennter Salzsaeure aus und destilliert den Rueckstand unter vermindertem Druck;
<2-methyl-4.5-benzo-indolyl-(3)>-acetic acid

<2-methyl-4.5-benzo-indolyl-(3)>-acetic acid

2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

Conditions
ConditionsYield
at 210℃;
methylethyl ketone-β-naphthylhydrazone

methylethyl ketone-β-naphthylhydrazone

2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

Conditions
ConditionsYield
With zinc(II) chloride at 180℃;
2-naphthylhydrazine hydrochloride
2243-58-5

2-naphthylhydrazine hydrochloride

2-Pentanone
107-87-9

2-Pentanone

2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

Conditions
ConditionsYield
Stage #1: 2-naphthylhydrazine hydrochloride With acetic acid for 0.5h;
Stage #2: 2-Pentanone Reflux;
2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

Allyl acetate
591-87-7

Allyl acetate

3-allyl-1,2-dimethyl-3H-benzo[e]indole

3-allyl-1,2-dimethyl-3H-benzo[e]indole

Conditions
ConditionsYield
With palladium(II) trifluoroacetate; trifuran-2-yl-phosphane In water for 2h; Reflux; Inert atmosphere; Green chemistry;98%
2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

Allyl acetate
591-87-7

Allyl acetate

A

3-allyl-1,2-dimethyl-3H-benzo[e]indole

3-allyl-1,2-dimethyl-3H-benzo[e]indole

B

1-allyl-1,2-dimethyl-1H-benzo[e]indole

1-allyl-1,2-dimethyl-1H-benzo[e]indole

Conditions
ConditionsYield
With platinum(II) 2,4-pentanedionate; tri(4-chlorophenyl)phosphine In water for 2h; Inert atmosphere; Reflux; regioselective reaction;A 96%
B 3%
styrene
100-42-5

styrene

2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

5-(cyano)dibenzothiophenium triflate

5-(cyano)dibenzothiophenium triflate

C23H20N2

C23H20N2

Conditions
ConditionsYield
Stage #1: 2,3-dimethylbenz<4,5>indole; 5-(cyano)dibenzothiophenium triflate In dichloromethane at 20℃; for 0.166667h; Inert atmosphere;
Stage #2: styrene In dichloromethane at 20℃; for 11h; Inert atmosphere;
89%
2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

5-(cyano)dibenzothiophenium triflate

5-(cyano)dibenzothiophenium triflate

C15H12N2

C15H12N2

Conditions
ConditionsYield
In acetonitrile at 20℃; Inert atmosphere;86%
2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

N-(1-formylnaphthalen-2-yl)acetamide
42900-57-2

N-(1-formylnaphthalen-2-yl)acetamide

Conditions
ConditionsYield
With potassium phosphate; oxygen; Rose Bengal lactone In water; N,N-dimethyl-formamide for 46h; Inert atmosphere; Irradiation;73%
2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

oxalic acid diethyl ester
95-92-1

oxalic acid diethyl ester

(1,2-Dimethyl-benzo[e]indol-3-yl)-oxo-acetic acid ethyl ester
114570-15-9

(1,2-Dimethyl-benzo[e]indol-3-yl)-oxo-acetic acid ethyl ester

Conditions
ConditionsYield
With ethylmagnesium bromide In ethanol for 2h;72%
1-Phenylprop-1-yne
673-32-5

1-Phenylprop-1-yne

2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

1-cinnamyl-1,2-dimethyl-1H-benzo[e]indole

1-cinnamyl-1,2-dimethyl-1H-benzo[e]indole

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); 4-Fluorobenzoic acid; tricyclohexylphosphine In toluene at 100℃; for 24h; Sealed tube; Inert atmosphere;56%
2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

bis(4-tert-butylphenyl)iodonium hexafluorophosphate
61358-25-6

bis(4-tert-butylphenyl)iodonium hexafluorophosphate

1,2-dimethyl-1-(4-tert-butylphenyl)-1H-benzo[e]indole

1,2-dimethyl-1-(4-tert-butylphenyl)-1H-benzo[e]indole

Conditions
ConditionsYield
Stage #1: 2,3-dimethylbenz<4,5>indole With potassium tert-butylate In toluene at 50℃; for 0.166667h; Inert atmosphere;
Stage #2: bis(4-tert-butylphenyl)iodonium hexafluorophosphate In toluene at 50℃; for 18h; Inert atmosphere;
45%
2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

methyl 3-[[(methoxycarbonyl)imino]amino]but-2-enoate
63160-33-8

methyl 3-[[(methoxycarbonyl)imino]amino]but-2-enoate

(7aS*,10aR*)-methyl 8-((methoxycarbonyl)amino)-7a,9,10a-trimethyl-7,7a,8,10a-tetrahydrobenzo[e]pyrrolo[2,3-b]indole-10-carboxylate

(7aS*,10aR*)-methyl 8-((methoxycarbonyl)amino)-7a,9,10a-trimethyl-7,7a,8,10a-tetrahydrobenzo[e]pyrrolo[2,3-b]indole-10-carboxylate

Conditions
ConditionsYield
With zinc(II) chloride In dichloromethane at 25℃; diastereoselective reaction;38%
2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

acetic anhydride
108-24-7

acetic anhydride

3,5-diacetyl-1,2-dimethyl-3H-benzo[e]indole
55993-18-5

3,5-diacetyl-1,2-dimethyl-3H-benzo[e]indole

Conditions
ConditionsYield
unter Zusatz von wenig Phosphorsaeure oder Sulfanilsaeure;
2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

3-acetyl-1,2-dimethyl-3H-benzo[e]indole
55970-09-7

3-acetyl-1,2-dimethyl-3H-benzo[e]indole

Conditions
ConditionsYield
With ethyl bromide; diethyl ether; magnesium und Erwaermen der Reaktionsloesung mit Acetylchlorid;
hydrogenchloride
7647-01-0

hydrogenchloride

2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

ethanol
64-17-5

ethanol

zinc dust

zinc dust

2.3-dimethyl-2.3-dihydro-4.5-benzo-indole

2.3-dimethyl-2.3-dihydro-4.5-benzo-indole

2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

methyl iodide
74-88-4

methyl iodide

hydriodide of 2.3.3-trimethyl-4.5-benzo-indolenine

hydriodide of 2.3.3-trimethyl-4.5-benzo-indolenine

Conditions
ConditionsYield
at 100℃;
2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

1,2-Dimethyl-5,5-diphenyl-5H-benzo[e]pyrrolo[3,2,1-hi]indol-4-one
114570-23-9

1,2-Dimethyl-5,5-diphenyl-5H-benzo[e]pyrrolo[3,2,1-hi]indol-4-one

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 72 percent / ethylmagnesium bromide / ethanol / 2 h
2: 68 percent / diethyl ether
3: 92 percent / H2SO4 / acetic acid / Heating
View Scheme
2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

1-(1,2-Dimethyl-benzo[e]indol-3-yl)-2-hydroxy-2,2-diphenyl-ethanone
114570-22-8

1-(1,2-Dimethyl-benzo[e]indol-3-yl)-2-hydroxy-2,2-diphenyl-ethanone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 72 percent / ethylmagnesium bromide / ethanol / 2 h
2: 68 percent / diethyl ether
View Scheme
2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

3-acetyl-5-bromo-1,2-dimethyl-3H-benz[e]indole

3-acetyl-5-bromo-1,2-dimethyl-3H-benz[e]indole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: magnesium; ethyl bromide; diethyl ether / und Erwaermen der Reaktionsloesung mit Acetylchlorid
2: acetic acid; bromine
View Scheme
2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

3,5-diacetyl-1,2-dimethyl-3H-benzo[e]indole
55993-18-5

3,5-diacetyl-1,2-dimethyl-3H-benzo[e]indole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: magnesium; ethyl bromide; diethyl ether / und Erwaermen der Reaktionsloesung mit Acetylchlorid
2: aluminium chloride; carbon disulfide
View Scheme
2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

N-(1-acetyl-[2]naphthyl)-diacetamide

N-(1-acetyl-[2]naphthyl)-diacetamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: magnesium; ethyl bromide; diethyl ether / und Erwaermen der Reaktionsloesung mit Acetylchlorid
2: CrO3; acetic acid
View Scheme
2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

1,4-diacetyl-[2]naphthylamine

1,4-diacetyl-[2]naphthylamine

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: unter Zusatz von wenig Phosphorsaeure oder Sulfanilsaeure
2: aqueous acetic acid; CrO3
3: aqueous HCl
4: aqueous HCl
View Scheme
Multi-step reaction with 5 steps
1: magnesium; ethyl bromide; diethyl ether / und Erwaermen der Reaktionsloesung mit Acetylchlorid
2: aluminium chloride; carbon disulfide
3: aqueous acetic acid; CrO3
4: aqueous HCl
5: aqueous HCl
View Scheme
2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

N-(1,4-diacetyl-[2]naphthyl)-acetamide
861055-13-2

N-(1,4-diacetyl-[2]naphthyl)-acetamide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: unter Zusatz von wenig Phosphorsaeure oder Sulfanilsaeure
2: aqueous acetic acid; CrO3
3: aqueous HCl
View Scheme
Multi-step reaction with 4 steps
1: magnesium; ethyl bromide; diethyl ether / und Erwaermen der Reaktionsloesung mit Acetylchlorid
2: aluminium chloride; carbon disulfide
3: aqueous acetic acid; CrO3
4: aqueous HCl
View Scheme
2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

N-(1,4-diacetyl-[2]naphthyl)-diacetamide
666840-45-5

N-(1,4-diacetyl-[2]naphthyl)-diacetamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: unter Zusatz von wenig Phosphorsaeure oder Sulfanilsaeure
2: aqueous acetic acid; CrO3
View Scheme
Multi-step reaction with 3 steps
1: magnesium; ethyl bromide; diethyl ether / und Erwaermen der Reaktionsloesung mit Acetylchlorid
2: aluminium chloride; carbon disulfide
3: aqueous acetic acid; CrO3
View Scheme
2,3-dimethylbenz<4,5>indole
55970-05-3

2,3-dimethylbenz<4,5>indole

1-phenyl-4-penten-1-yne
4289-20-7

1-phenyl-4-penten-1-yne

A

1,2-dimethyl-1-((2E,4E)-5-phenylpenta-2,4-dien-1-yl)-1H-benzo[e]indole

1,2-dimethyl-1-((2E,4E)-5-phenylpenta-2,4-dien-1-yl)-1H-benzo[e]indole

B

1,2-dimethyl-1-(5-phenylpenta-2,4-dien-1-yl)-1H-benzo[e]indole

1,2-dimethyl-1-(5-phenylpenta-2,4-dien-1-yl)-1H-benzo[e]indole

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); mesitylenecarboxylic acid; tricyclohexylphosphine In toluene at 100℃; for 24h; Sealed tube; Inert atmosphere; Overall yield = 55 %; Overall yield = 37.1 mg; chemoselective reaction;A n/a
B n/a
With tetrakis(triphenylphosphine) palladium(0); mesitylenecarboxylic acid; tricyclohexylphosphine In toluene at 100℃; for 24h; Sealed tube; Inert atmosphere; Overall yield = 55 percent; Overall yield = 37.1 mg;A n/a
B n/a

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