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bis(trichloromethyl) carbonate
4-methoxy-benzylamine
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane | 100% |
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran at -80℃; | |
With sodium hydrogencarbonate In dichloromethane; water at 0℃; for 2.5h; |
2-(4-methoxy-benzyloxy)-tetrahydro-pyran
tetrabutylammonium isocyanate
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
With triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone In acetonitrile for 5h; Reflux; | 98% |
tetrabutylammonium isocyanate
4-Methoxybenzyl alcohol
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
With triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone In acetonitrile at 20℃; | 97% |
Conditions | Yield |
---|---|
In diethyl ether for 18h; Heating; | 74% |
phosgene
N-(4-methoxybenzyl)-1,1,1-trimethylsilanamine
B
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
In toluene at 0℃; Title compound not separated from byproducts.; | A 7% B 58.4% |
Conditions | Yield |
---|---|
With toluene at 120℃; | |
With sodium hydrogencarbonate In dichloromethane; toluene at 0℃; for 3h; |
phosgene
4-methoxybenzylamine hydrochloride
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
In chlorobenzene at 115℃; |
(4-Methoxy-phenyl)-acetyl azide
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
In chloroform for 0.5h; Heating; | |
Heating; Neat (no solvent); |
sodium isocyanate
(4-methoxybenzyl)dimethylsulfonium
A
4-Methoxybenzyl alcohol
C
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
With sodium chloride In water-d2 at 80℃; Rate constant; Mechanism; Product distribution; other reagents; |
4-Methoxyphenylacetic acid
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
With diphenyl phosphoryl azide; triethylamine | |
Multi-step reaction with 2 steps 1: thionyl chloride 2: sodium azide / toluene / 1 h / Heating View Scheme | |
Multi-step reaction with 3 steps 1: oxalyl chloride, dimethylformamide / CH2Cl2 / 0.42 h 2: NaN3 / acetone; H2O / 0.5 h / 0 - 5 °C 3: CHCl3 / 0.5 h / Heating View Scheme |
4-methoxyphenyl-acetic chloride
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
With sodium azide In toluene for 1h; Heating; | |
Multi-step reaction with 2 steps 1: NaN3 / acetone; H2O / 0.5 h / 0 - 5 °C 2: CHCl3 / 0.5 h / Heating View Scheme |
4-methoxy-benzylamine
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 96.5 percent / H2SO4 / 2 h / Heating 2: 58.4 percent / toluene / 0 °C View Scheme |
p-Methoxybenzyl bromide
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: AcOH; aq. NaOH 2: thionyl chloride 3: sodium azide / toluene / 1 h / Heating View Scheme |
p-methoxybenzylnitrile
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: AcOH; aq. NaOH 2: thionyl chloride 3: sodium azide / toluene / 1 h / Heating View Scheme |
4-Methoxybenzyl alcohol
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: PBr3 / CH2Cl2 2: AcOH; aq. NaOH 3: thionyl chloride 4: sodium azide / toluene / 1 h / Heating View Scheme |
2-(4-methoxyphenyl)acetamide
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
With [N-(p-tolylsulfonyl)imino]phenyliodinane In dichloromethane at 20℃; for 1.5h; Hofmann rearrangement; Inert atmosphere; |
4-methoxy-benzylamine
trichloromethyl chloroformate
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
With dmap In dichloromethane at 0 - 20℃; for 0.75h; |
ethyl 3-amino-1-cyclopentyl-1H-pyrazole-4-carboxylate
4-methoxybenzyl isocyanate
ethyl 1-cylcopentyl-3-(3-(4-methoxybenzyl)ureido)-1H-pyrazole-4-carboxylate
Conditions | Yield |
---|---|
With triethylamine In toluene Heating / reflux; | 100% |
1-(4-methoxy-benzyl)-4-nitro-1H-pyrazole-3-carboxylic acid hydrazide
4-methoxybenzyl isocyanate
C21H22N6O6
Conditions | Yield |
---|---|
In tetrahydrofuran at 0℃; for 0.166667h; | 100% |
(R)-2-(4-Methoxy-phenyl)-thiazolidine-4-carboxylic acid
4-methoxybenzyl isocyanate
C20H20N2O4S
Conditions | Yield |
---|---|
In tetrahydrofuran | 100% |
(+/-)-2-phenylpropionic acid vinyl ester
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
With lipase from Candida cylindracea In aq. phosphate buffer at 20℃; for 48h; pH=7.4; Enzymatic reaction; chemoselective reaction; | 99% |
1,2-benzisothiazolin-3-one
4-methoxybenzyl isocyanate
N-(4-methoxybenzyl)benzisothiazol-3-one-2-amide
Conditions | Yield |
---|---|
In tetrahydrofuran; dichloromethane for 0.5h; Reflux; | 98% |
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
In dichloromethane for 20h; | 96.1% |
1-amino-3-methylbutane
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
for 3h; | 95% |
C10H13N3O2
4-methoxybenzyl isocyanate
1-((2R,3S,3aS,9aR)-2-hydroxy-5-oxo-2,3,3a,4,5,9a-hexahydro-1H-cyclopenta[e]pyrrolo[1,2-a]pyrazin-3-yl)-3-(4-methoxybenzyl)urea
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; for 1.33333h; | 94% |
In N,N-dimethyl-formamide at 20℃; for 1.33333h; | 94% |
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
With hydrazine hydrate In dichloromethane at 20℃; for 2h; Cooling with ice; | 93% |
With hydrazine hydrate In dichloromethane at 20℃; for 2h; Cooling with ice; | 93% |
Conditions | Yield |
---|---|
In acetonitrile Ambient temperature; | 92% |
Conditions | Yield |
---|---|
In acetonitrile at 20℃; Addition; | 92% |
2',3',4',9'-tetrahydro-N,N-dimethyl-4-butyl-spiro[cyclohexane-1,1'(1'H)-pyrido[3,4-b]indol]-4-amine
4-methoxybenzyl isocyanate
2',3',4',9'-tetrahydro-N,N-dimethyl-4-butyl-2'-4-methoxybenzylaminocarbonyl-spiro[cyclohexane-1,1'(1'H)-pyrido[3,4-b]indol]-4-amine
Conditions | Yield |
---|---|
With triethylamine In acetonitrile for 13h; Reflux; | 92% |
(S)-2-azido-3-phenylpropionic acid methyl ester
4-methoxybenzyl isocyanate
A
(S)-5-benzyl-N,3-bis(4-methoxybenzyl)-2,4-dioxoimidazolidine-1-carboxamide
Conditions | Yield |
---|---|
With triphenylphosphine In acetonitrile at 20℃; for 3h; | A 92% B n/a |
(2S,4S,5R,6S)-6-isobutyl-2-((2R,3S)-3-isobutylaziridin-2-yl)-3-oxa-1-aza-bicyclo[3.1.0]hexan-4-ol
4-methoxybenzyl isocyanate
(4R,5R,6S)-4-hydroxy-6-isobutyl-3-(4-methoxybenzyl)-1,3-diazabicyclo[3.1.0]hexan-2-one
Conditions | Yield |
---|---|
In 1,1,1,3',3',3'-hexafluoro-propanol; water at 20℃; 8:2 HFIPl :H2O (v/v); diastereoselective reaction; | 90% |
benzyl 2-azidoacetate
4-methoxybenzyl isocyanate
N,3-diethyl-2,4-dioxoimidazolidine-1-carboxamide
Conditions | Yield |
---|---|
With triphenylphosphine In acetonitrile at 20℃; for 3h; | 89% |
N-(2-acetylphenyl)-2-[(triphenylphosphoranylidene)amino]benzamide
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
In toluene aza-Wittig reaction; Heating; | 88% |
In toluene at 20℃; Inert atmosphere; Reflux; | 88% |
2-(4-hydroxyphenyl)-4,5-dihydro-1,3-thiazole
4-methoxybenzyl isocyanate
(4-methoxy)-benzylcarbamic acid 4-(4,5-dihydrothiazol-2-yl)phenyl ester
Conditions | Yield |
---|---|
With triethylamine In toluene for 2.5h; Inert atmosphere; Reflux; | 88% |
piperidine
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
for 3h; | 87% |
5-acetamido-7,8,9-tri-O-acetyl-2,6-anhydro-4-amino-3,4,5-trideoxy-D-glycero-D-galacto-non-2-enonic acid methyl ester
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
With dmap In dichloromethane at 20℃; Inert atmosphere; | 87% |
1-(5-nitrothiazol-2-yl)piperidin-4-amine
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
With triethylamine In N,N-dimethyl-formamide at 0 - 20℃; for 6h; | 85.9% |
ethyl-2-azidoacetate
4-methoxybenzyl isocyanate
N,3-bis(4-methoxybenzyl)-2,4-dioxoimidazolidine-1-carboxamide
Conditions | Yield |
---|---|
With triphenylphosphine In acetonitrile at 20℃; for 3h; | 85% |
4-methoxybenzyl isocyanate
2-[4-(3-hydrazinocarbonylpropyl)phenoxy]-2-methylpropionic acid tert-butyl ester
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 2h; | 85% |
In dichloromethane at 20℃; for 2h; | 6.37 g |
2-carbomethoxyaniline
4-methoxybenzyl isocyanate
3-(4-methoxybenzyl)-2,4-dioxo-1,2,3,4-tetrahydroquinazoline
Conditions | Yield |
---|---|
With triethylamine In 1,4-dioxane at 140℃; for 0.75h; Microwave irradiation; Sealed vial; | 84% |
Stage #1: 2-carbomethoxyaniline; 4-methoxybenzyl isocyanate In toluene at 0 - 20℃; Stage #2: With sodium hydroxide In toluene at 70℃; for 6h; |
1-aminocyclohexanecarboxylic acid benzyl ester
4-methoxybenzyl isocyanate
1-[3-(4-methoxy-benzyl)-ureido]-cyclohexanecarboxylic acid benzyl ester
Conditions | Yield |
---|---|
In chloroform at 20℃; for 3h; | 83% |
6-methyl-N-[3-(4-piperidinyloxy)phenyl]-4'-(trifluoromethoxy)-[1,1'-biphenyl]-2-carboxamide
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
Stage #1: 6-methyl-N-[3-(4-piperidinyloxy)phenyl]-4'-(trifluoromethoxy)-[1,1'-biphenyl]-2-carboxamide; 4-methoxybenzyl isocyanate In dichloromethane for 8h; Stage #2: In dichloromethane at 20℃; | 82% |
4-(4-chlorophenyl)-2-thiazolamine
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
In tetrahydrofuran at 120℃; for 2h; Microwave irradiation; | 82% |
2-hydrazinyl-3-iodo-4-methylpyridine
4-methoxybenzyl isocyanate
C15H17IN4O2
Conditions | Yield |
---|---|
In dichloromethane at 20℃; | 81% |
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