As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryProduct description: Product name 4-Methoxybenzylamine CAS number 2393-23-9 Assay ≥99% Appearance Colorless transparent liquid Capacity 200mt/year Application Pharmaceutical
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
As a leading and professional manufacturer of APIs and API intermediates in China,Anhui Dexinjia Biopharm Co., Ltd founded in 2006, Except for the R&D center, our company has built a close cooperation relation with Chinese Academy of Sciences, T
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developmen
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by email in time prod
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiryProduct Name 4-Methoxybenzylamine CAS NO. 2393-23-9 Formula C8H11NO Molecular Weight 137.18 Appearance Clear color
1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
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inquiry4-Methoxybenzylamine CAS:2393-23-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inter
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Hebei Mojin Biotechnology Co., Ltd, Our company is a professional chemical raw materials and chemical reagents research and development production enterprises. We have several production line,So we can control the lowest price. We also have sever
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inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Appearance:white powder/crystal Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:Common products:Sea/Ai
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Packing: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Transportation:Express/Sea/Air Port:Ningbo/Shanghai/Qingd
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung, LG, Merck, Thermo Fisher Scientific and so o
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inquiryProduct name: 4-Methoxybenzylamine CAS No.:2393-23-9 Molecule Formula:C8H12NO Molecule Weight:138.19 Purity: 98.0% Package: 200kg/drum Description:Colorless liquid Manufacture Standards:Enterprise Standard TESTING
Cas:2393-23-9
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:2393-23-9
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inquiry4-Methoxybenzylamine Basic information Product Name: 4-Methoxybenzylamine Synonyms: LABOTEST-BB LTBB000703;AKOS BBS-00003589;4-AMINOMETHYL-ANISOLE;4-METHOXYBENZYLAMINE;P-MethoxybenzylamineHydrochloride173.64;4-Methoxybenzylamine, 98+%;forSparf
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryConditions | Yield |
---|---|
With hydrogen; aluminum oxide; silica gel; nickel In methanol; ammonia at 120℃; under 7600 Torr; for 6h; | 100% |
With palladium 10% on activated carbon; hydrogen In methanol at 20℃; for 24h; | 100% |
With [bis(2-methylallyl)cycloocta-1,5-diene]ruthenium(II); potassium tert-butylate; hydrogen bromide; hydrogen; 2-((di-iso-propylphosphino)methyl)-1-methyl-1H-imidazole In tetrahydrofuran; water; acetone; toluene at 20℃; under 37503.8 Torr; for 5.5h; Inert atmosphere; Schlenk technique; Autoclave; | 98% |
2-[(4-methoxyphenyl)methyl]-1H-isoindole-1,3(2H)-dione
4-methoxy-benzylamine
Conditions | Yield |
---|---|
With hydrazine hydrate In tetrahydrofuran for 16h; Reflux; | 99% |
With hydrazine hydrate In 1,4-dioxane at 110℃; Gabriel Amine Synthesis; Inert atmosphere; | 90% |
With sodium hydroxide und anschliessend mit verd.Salzsaeure; |
p-methoxyl benzaldoxime
4-methoxy-benzylamine
Conditions | Yield |
---|---|
With sodium tetrahydroborate at 20℃; for 0.0333333h; neat (no solvent, solid phase); | 98% |
With sodium hydrogensulfate monohydrate; molybdenum(V) chloride; sodium cyanoborohydride In ethanol for 1.1h; Reflux; | 95% |
With ammonium formate; zinc In methanol for 0.05h; Heating; | 92% |
4-methoxy-benzylamine
Conditions | Yield |
---|---|
With 2-hydroxyethanethiol In N,N-dimethyl-formamide at 20℃; for 1h; | 98% |
Conditions | Yield |
---|---|
With nickel(II) tetrafluoroborate hexahydrate; ammonia; hydrogen; bis(2-diphenylphosphinoethyl)phenylphosphine In 2,2,2-trifluoroethanol at 100℃; for 24h; chemoselective reaction; | 97% |
With ammonium hydroxide; hydrogen In ethanol at 130℃; under 7500.75 Torr; for 12h; Autoclave; | 93.4% |
With ammonia; hydrogen In methanol at 30℃; for 15h; Autoclave; | 92% |
N-(4-methoxybenzyl)-2-nitro-N-(prop-2-yn-1-yl)benzenesulfonamide
4-methoxy-benzylamine
Conditions | Yield |
---|---|
With polystyrene-thiophenol; caesium carbonate; triphenylphosphine In tetrahydrofuran at 20℃; for 24h; | 96% |
With potassium carbonate; thiophenol In acetonitrile at 50℃; | 93% |
With caesium carbonate; thiophenol In N,N-dimethyl-formamide at 20℃; for 0.5h; | 88% |
Conditions | Yield |
---|---|
With copper(ll) sulfate pentahydrate; ammonium hydroxide In PEG1000-DIL; methyl cyclohexane at 60℃; for 3h; | 96% |
With ammonia at 25℃; Kinetics; Activation energy; Temperature; Reagent/catalyst; | |
Multi-step reaction with 2 steps 1: N,N-dimethyl-formamide / 18 h / Reflux 2: hydrazine hydrate / tetrahydrofuran / 16 h / Reflux View Scheme |
1-(azidomethyl)-4-methoxybenzene
4-methoxy-benzylamine
Conditions | Yield |
---|---|
With hydrogenchloride; indium In tetrahydrofuran at 20℃; for 3h; | 95% |
With 1,3-diphenyl-disiloxane; triphenylphosphine In toluene at 23℃; for 24h; Reagent/catalyst; Solvent; Staudinger Azide Reduction; | 93% |
With cerium(III) chloride; sodium iodide In acetonitrile for 24h; Heating; | 80% |
4-methoxy-selenobenzamide
4-methoxy-benzylamine
Conditions | Yield |
---|---|
With samarium diiodide; water In tetrahydrofuran at 20℃; for 1h; Inert atmosphere; | 94% |
4-methoxy-benzylamine
Conditions | Yield |
---|---|
Stage #1: N-(2-(4-methoxyphenyl)-2-oxoethyl)picolinamide With hydrogenchloride In water at 20℃; for 0.0833333h; Inert atmosphere; Stage #2: With zinc In water at 20℃; for 16h; Inert atmosphere; | 91% |
methyl N-(4'-methoxybenzyl)carbamate
A
methanol
B
4-methoxy-benzylamine
Conditions | Yield |
---|---|
With C25H19BrMnN2O2P; potassium tert-butylate; hydrogen In toluene at 130℃; under 15001.5 Torr; for 48h; | A 87 %Spectr. B 91% |
Conditions | Yield |
---|---|
With ammonia In toluene at 110℃; under 5250.53 Torr; for 30h; | 89% |
With ammonium hydroxide; C19H37IrN4(2+)*2I(1-) at 170℃; for 100h; Sealed tube; | 45% |
Stage #1: 4-Methoxybenzyl alcohol With N-Boc-o-nitrobenzenesulfonamide-aminomethyl polystyrene res; triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 20℃; Mitsunobu reaction; Stage #2: With trifluoroacetic acid In dichloromethane at 20℃; Stage #3: With mercaptoethyl alcohol; 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 20℃; |
N-(4-methoxybenzyl)-2-methylpropane-2-sulfinamide
4-methoxy-benzylamine
Conditions | Yield |
---|---|
With hydrogenchloride In 1,4-dioxane; methanol at 25℃; for 0.5h; Inert atmosphere; | 89% |
A
S-(2,4-Dinitrophenyl)-cystein
B
sulfur dioxide
C
4-methoxy-benzylamine
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B 84% C n/a |
Conditions | Yield |
---|---|
With titanium tetrachloride; magnesium In tetrahydrofuran at 0 - 20℃; Inert atmosphere; | 80% |
With 1,10-Phenanthroline; diethoxymethylane; iron(II) acetate In toluene at 100℃; for 28h; Inert atmosphere; chemoselective reaction; | 60% |
With benzo[b]thiophene-2-boronic acid; phenylsilane In toluene at 130℃; for 24h; Inert atmosphere; Schlenk technique; chemoselective reaction; | 42% |
4-methoxy-benzylamine
Conditions | Yield |
---|---|
With triethylamine; 1-butyl-3-methylimidazolium Tetrafluoroborate In neat (no solvent) at 25℃; for 0.133333h; Green chemistry; | 80% |
With piperidine In N,N-dimethyl-formamide at 25℃; for 0.166667h; | |
With piperidine In N,N-dimethyl-formamide at 20℃; for 2h; |
4-methoxy-benzylamine
Conditions | Yield |
---|---|
With methanol; sodium hydroxide at 80℃; for 0.166667h; Microwave irradiation; | 80% |
N,N-bis(p-methoxybenzyl)amine
A
4-methoxy-benzaldehyde
B
4-methoxy-benzylamine
Conditions | Yield |
---|---|
With sodium periodate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; acetic acid In water; acetonitrile for 20h; | A 80% B 8% |
ammonium formate
4-methoxy-benzaldehyde
A
N-(4-methoxybenzyl)formamide
B
4-methoxy-benzylamine
Conditions | Yield |
---|---|
With [pentamethylcyclopentadienyl*Ir(N-phenyl-2-pyridinecarboxamidate)Cl] In methanol at 37℃; for 15h; chemoselective reaction; | A 21 %Spectr. B 79% |
1-hexene
4-Methoxybenzyl alcohol
A
1-(4-methoxyphenyl)-1-heptanone
B
4-methoxy-benzylamine
Conditions | Yield |
---|---|
With 2-Amino-4-methylpyridine; Wilkinson's catalyst; polystyrene-based diphenylphosphine In toluene at 130℃; for 72h; Addition; dehydrogenation; | A 68% B 2% |
4-methoxybenzonitrile
A
N,N-bis(p-methoxybenzyl)amine
B
4-methoxy-benzylamine
Conditions | Yield |
---|---|
With sodium tetrahydroborate; nickel dichloride In ethanol at 20℃; for 0.0833333h; | A 6% B 64% |
With hydrogen In carbon dioxide at 50℃; under 90009 Torr; for 4h; chemoselective reaction; |
methanol
1-(azidomethyl)-4-methoxybenzene
A
N,N-dimethyl-4-methoxylbenzylamine
B
4-methoxy-N-methylbenzylamine
C
4-methoxy-benzylamine
Conditions | Yield |
---|---|
With trans-RuCl(phenpyra-Me)(PPh3)2PF6; sodium hydroxide at 125℃; for 2.5h; Sealed tube; Inert atmosphere; Glovebox; | A 17 %Chromat. B 62% C 6 %Chromat. |
4-methoxybenzylidenediphenylmethylamine
A
Diphenylmethane
B
(diphenylmethyl)[(4-methoxyphenyl)methyl]amine
C
4-methoxy-benzylamine
Conditions | Yield |
---|---|
With sodium In 1,4-dioxane a. 10h, reflux, b. 6h, RT; | A 26% B 39% C 27% |
With sodium In 1,4-dioxane a. 10h, reflux, b. 6h, RT; other educts; | A 26% B 39% C 27% |
1-(azidomethyl)-4-methoxybenzene
A
4-methoxy-benzylamine
B
N-methyl-N-(4-methoxyphenyl)amine
Conditions | Yield |
---|---|
With triethylsilane; tin(IV) chloride In dichloromethane at 0 - 5℃; Rearrangement; Reduction; Addition; | A 13% B 8% C 34% |
N,N'-Bis-[1-(4-methoxy-phenyl)-meth-(E)-ylidene]-hydrazine
A
(1R,2S)/(1S,2R)-1,2-diamino-1,2-bis(4-methoxyphenyl)ethane
B
4-methoxy-benzylamine
Conditions | Yield |
---|---|
With titanium tetrachloride; zinc In tetrahydrofuran at 25℃; for 8h; reduction; | A 13% B 26% C n/a |
With methanesulfonic acid; zinc In tetrahydrofuran at 25℃; for 8h; reduction; | A n/a B 13% C n/a |
p-methoxyl benzaldoxime
A
(1R,2S)/(1S,2R)-1,2-diamino-1,2-bis(4-methoxyphenyl)ethane
B
4-methoxy-benzylamine
Conditions | Yield |
---|---|
With methanesulfonic acid; zinc In acetonitrile at 25℃; reduction; | A n/a B 17% C n/a |
Conditions | Yield |
---|---|
With C5H11NO*CHF3O3S In ethanol; water at 10℃; for 12h; pH=7.4; Inert atmosphere; Sealed tube; Enzymatic reaction; | 17% |
4-methoxyphenylacetamide
A
4-methoxy-benzylamine
B
4-Methoxybenzyl alcohol
Conditions | Yield |
---|---|
With sulfuric acid at 35 - 40℃; bei der elektrolytischen Reduktion; |
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane at 20℃; for 12h; | 100% |
With magnesium sulfate In dichloromethane for 3h; Reflux; | 100% |
In dichloromethane for 18h; Molecular sieve; | 92% |
4-methoxy-benzaldehyde
4-methoxy-benzylamine
N-(4-methoxybenzylidene)-4-methoxybenzylamine
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane for 3h; Reflux; | 100% |
In toluene for 24h; Condensation; Heating; | 95% |
(2S)-3-(benzyloxy)-2-methylpropanal
sodium cyanide
4-methoxy-benzylamine
(3R)-2-(4-methoxybenzylamino)-3-benzyloxymethylbutyronitrile
Conditions | Yield |
---|---|
With hydrogenchloride In methanol; water for 2h; Ambient temperature; | 100% |
Conditions | Yield |
---|---|
With oxygen; methylene blue; potassium carbonate In acetonitrile at 20℃; for 10h; Irradiation; Green chemistry; | 100% |
With cobalt nanoparticles encapsulated within nitrogen doped graphitic shells prepared via pyrolysis of poly([1,3-bis(4-vinylbenzyl)imidazolium]CoCl4) at 800 oC In toluene at 120℃; for 12h; Catalytic behavior; Reagent/catalyst; Solvent; Inert atmosphere; Schlenk technique; Sealed tube; | 99% |
With 2',3',4'-trihydroxyacetophenone In water at 20℃; for 24h; | 98% |
Conditions | Yield |
---|---|
Stage #1: 4-methoxy-benzylamine With hydrogenchloride In 1,4-dioxane; dichloromethane at 20℃; for 0.166667h; Stage #2: 1,1'-carbonyldiimidazole In N,N-dimethyl-formamide at 0℃; for 0.116667h; | 100% |
Stage #1: 4-methoxy-benzylamine With hydrogenchloride In 1,4-dioxane; dichloromethane at 20℃; for 0.0833333h; Inert atmosphere; Stage #2: 1,1'-carbonyldiimidazole In N,N-dimethyl-formamide for 2h; Inert atmosphere; | 98% |
Stage #1: 4-methoxy-benzylamine With hydrogenchloride In dichloromethane; isopropyl alcohol Stage #2: 1,1'-carbonyldiimidazole In dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol at 20℃; for 1.5h; | 87% |
2,3,5-tri-O-benzyl-β-D-arabinofuranoside
4-methoxy-benzylamine
Conditions | Yield |
---|---|
With 4 A molecular sieve In benzene Heating; | 100% |
citraconic acid anhydride
4-methoxy-benzylamine
1-(4-Methoxy-benzyl)-3-methyl-pyrrole-2,5-dione
Conditions | Yield |
---|---|
With acetic acid at 100℃; for 5h; | 100% |
In toluene for 13h; Heating; | 80% |
4-methoxy-benzylamine
Conditions | Yield |
---|---|
In methanol for 5h; Ambient temperature; | 100% |
4-methoxy-benzylamine
2,3-isopropylidene-glyceraldehyde
[1-((S)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-meth-(E)-ylidene]-(4-methoxy-benzyl)-amine
Conditions | Yield |
---|---|
With magnesium sulfate In diethyl ether at 0℃; for 3h; | 100% |
With magnesium sulfate In diethyl ether at 0℃; Condensation; | |
With magnesium sulfate In dichloromethane for 0.5h; |
2,3,5-tri-O-benzyl-D-arabinofuranose
4-methoxy-benzylamine
((3S,4R,5R)-3,4-Bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-yl)-(4-methoxy-benzyl)-amine
Conditions | Yield |
---|---|
With 4 A molecular sieve In chloroform; benzene Substitution; Heating; | 100% |
With MS 4 Angstroem In chloroform; benzene Condensation; reflux; | 100% |
4-methoxy-benzylamine
N-[(tert-butoxy)carbonyl]-N-(2-oxo-4-phenylbutyl)glycine
4-[(tert-butoxy)carbonyl]-1-[(4-methoxyphenyl)methyl]-6-(2-phenylethyl)piperazin-2-one
Conditions | Yield |
---|---|
Stage #1: 4-methoxy-benzylamine; N-[(tert-butoxy)carbonyl]-N-(2-oxo-4-phenylbutyl)glycine With sodium tris(acetoxy)borohydride; acetic acid at 25℃; Condensation; Stage #2: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 25℃; Cyclization; | 100% |
4-methoxy-benzylamine
acrylonitrile
3-(4-methoxybenzylamino)propanenitrile
Conditions | Yield |
---|---|
With aluminum oxide In neat (no solvent) at 90℃; for 4h; Michael Addition; Green chemistry; | 100% |
aza-Michael reaction; | 84% |
at 20℃; for 45h; | 81% |
4-methoxy-benzylamine
4-Oxo-1-(3-pyridyl)-1-butanone
Conditions | Yield |
---|---|
In methanol; dichloromethane at 20℃; for 1h; | 100% |
4-methoxy-benzylamine
6-(5-benzyloxycarbonylamino-5-methoxycarbonyl-pentylcarbamoyl)-1,3-dihydro-isoindole-2,5-dicarboxylic acid 2-tert-butyl ester
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 25℃; for 16h; | 100% |
4-methoxy-benzylamine
polymer; monomer(s): 2-methyl-3a,4,7,7a-tetrahydro-4,7-methano-1H-isoindole-1,3(2H)-dione; 2-{4-[(4,6-dichloro-1,3,5-triazin-2-yl)amino]benzyl}-3a,4,7,7a-tetrahydro-4,7-methano-1H-isoindole-1,3(2H)-dione
polymer; monomer(s): 2-methyl-3a,4,7,7a-tetrahydro-4,7-methano-1H-isoindole-1,3(2H)-dione; 2-{4-[(4,6-dichloro-1,3,5-triazin-2-yl)amino]benzyl}-3a,4,7,7a-tetrahydro-4,7-methano-1H-isoindole-1,3(2H)-dione; 4-methoxybenzylamine
Conditions | Yield |
---|---|
With poly(vinylpyridine) In 1,2-dichloro-ethane at 90℃; for 42h; | 100% |
Conditions | Yield |
---|---|
Stage #1: 4-methoxy-benzylamine; 1,1'-Thiocarbonyldiimidazole In acetonitrile at 20℃; for 1h; Stage #2: methyl iodide In acetonitrile at 20℃; | 100% |
4-methoxy-benzylamine
[6-benzylsulfonyl-9-(tetrahydropyran-2-yl)-9H-purin-2-yl]-3-methyl-pent-1-yn-3-ol
Conditions | Yield |
---|---|
In tert-butyl alcohol at 20℃; for 0.416667h; | 100% |
bis(trichloromethyl) carbonate
4-methoxy-benzylamine
4-methoxybenzyl isocyanate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane | 100% |
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran at -80℃; | |
With sodium hydrogencarbonate In dichloromethane; water at 0℃; for 2.5h; |
4-methoxy-benzylamine
methyl 3-(R)-methyl-5-hydroxypentanoate
(3R)-5-hydroxy-N-(4-methoxybenzyl)-3-methylpentanamide
Conditions | Yield |
---|---|
In toluene at 105 - 110℃; for 4h; | 100% |
In toluene for 3h; Heating; | 97% |
Conditions | Yield |
---|---|
In methanol at 20℃; | 100% |
4-methoxy-benzylamine
benzotriazole-1-carbothioic acid (1,5-dimethylhexyl)amide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 24h; | 100% |
4-methoxy-benzylamine
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; | 100% |
benzaldehyde
4-methoxy-benzylamine
(E)-N-benzylidene-1-(4-methoxyphenyl)methanamine
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane at 20℃; for 12h; | 100% |
With sodium sulfate In dichloromethane at 20℃; for 24h; | 95% |
Stage #1: 4-methoxy-benzylamine In dichloromethane for 0.0833333h; Molecular sieve; Stage #2: benzaldehyde In dichloromethane at 20℃; | 95% |
perfluorobenzaldehyde
4-methoxy-benzylamine
(E)-4-methoxy-N-(pentafluorobenzylidene)benzylamine
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 3h; | 100% |
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane at 20℃; Inert atmosphere; Darkness; | 100% |
In methanol at 20℃; | 88% |
In benzene Heating; |
2,3,5-tri-O-benzyl-L-xylofuranose
4-methoxy-benzylamine
Conditions | Yield |
---|---|
With 4 A molecular sieve In dichloromethane at 50℃; for 15h; | 100% |
4-methoxy-benzylamine
acrylic acid methyl ester
methyl 3-((4-methoxybenzyl)amino)propanoate
Conditions | Yield |
---|---|
In methanol at 0℃; for 15.5h; | 100% |
With aluminum oxide In neat (no solvent) at 75℃; for 3.5h; Michael Addition; Green chemistry; | 91% |
aza-Michael reaction; | 89% |
With CLEA Pseudomonas stutzeri lipase (PSL) In hexane at 60℃; for 96h; Michael Addition; Sealed tube; Enzymatic reaction; | 74% |
With Pseudomonas fluorescence lipase immobilized on hyroxypropyl methyl cellulose support In toluene at 50℃; for 3h; Reagent/catalyst; Michael Addition; Enzymatic reaction; chemoselective reaction; |
2,2-dimethylsuccinic anhydride
4-methoxy-benzylamine
1-(4-methoxybenzyl)-3,3-dimethylpyrrolidine-2,5-dione
Conditions | Yield |
---|---|
In toluene for 11h; Heating; | 100% |
With dmap; acetic acid Autoclave; Inert atmosphere; | 99% |
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