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styrene oxide
1-pyridin-2-yl-ethanone oxime
4'-phenyl-2,2':6',2-terpyridine
Conditions | Yield |
---|---|
at 200℃; for 3h; Sealed tube; | 93% |
1-pyridin-2-yl-ethanone oxime
benzaldehyde
4'-phenyl-2,2':6',2-terpyridine
Conditions | Yield |
---|---|
In neat (no solvent) at 200℃; for 3h; Sealed tube; Neutral conditions; | 93% |
Conditions | Yield |
---|---|
With ammonium acetate; bis(trifluoromethanesulfonyl)amide In neat (no solvent) at 80℃; for 0.75h; | 90% |
With [((CH3)3C)2Sn(OH)(H2O)]2(2+)*2(OSO2CF3)(1-)=[((CH3)3C)2Sn(OH)(OSO2CF3)(H2O)]2; ammonium acetate In water at 100℃; for 0.75h; Green chemistry; | 90% |
With ammonium acetate In water at 130℃; for 0.4h; Kroehnke reaction; microwave irradiation; | 82% |
Conditions | Yield |
---|---|
With tris(pentafluorophenyl)borate; oxygen at 120℃; under 760.051 Torr; for 12h; | 81% |
With tris(pentafluorophenyl)borate; oxygen In neat (no solvent) at 120℃; under 760.051 Torr; for 12h; | 56% |
1-phenyl-3-(2-pyridyl)propen-1-one
4'-phenyl-2,2':6',2-terpyridine
Conditions | Yield |
---|---|
Stage #1: 1-phenyl-3-(2-pyridyl)propen-1-one; C10H10FNO3 With caesium carbonate In acetonitrile at 40℃; for 1h; Stage #2: With ammonium acetate In acetonitrile at 120℃; for 24h; regioselective reaction; | 68% |
methyl (4-pyridyl) ketone
benzaldehyde
4'-phenyl-2,2':6',2-terpyridine
Conditions | Yield |
---|---|
Stage #1: benzaldehyde With potassium hydroxide In ethanol at 20℃; for 0.166667h; Stage #2: methyl (4-pyridyl) ketone With ammonium hydroxide In water at 20℃; for 4h; | 60% |
With ammonium hydroxide; sodium hydroxide In ethanol at 20℃; for 12h; | 43% |
4'-{[(Trifluoromethyl)sulfonyl]oxy}-2,2':6',2''-terpyridine
phenylboronic acid
4'-phenyl-2,2':6',2-terpyridine
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In tetrahydrofuran Suzuki cross-coupling reaction; Heating; | 10% |
3-phenyl-1,5-bis(pyridine-2-yl)pentane-1,5-dione
4'-phenyl-2,2':6',2-terpyridine
Conditions | Yield |
---|---|
With hydrogenchloride; ethanol; hydroxylamine at 160℃; | |
With ammonium acetate In acetic acid for 2h; Heating; | 4.05 g |
With ammonium hydroxide In various solvent(s) at 100℃; for 2h; |
1-(2-oxo-2-(2-pyridyl)ethyl)pyridinium iodide
(E)-3-phenyl-1-(pyridin-2-yl)-2-propen-1-one
4'-phenyl-2,2':6',2-terpyridine
Conditions | Yield |
---|---|
With ammonium acetate In methanol |
Trimethyl borate
4'-(4-bromo-phenyl)-[2,2';6',2'']terpyridine
B
4'-phenyl-2,2':6',2-terpyridine
Conditions | Yield |
---|---|
Stage #1: 4'-(4-bromo-phenyl)-[2,2';6',2'']terpyridine With n-butyllithium at -78 - 20℃; Stage #2: Trimethyl borate at -78 - 20℃; |
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
4'-(4-bromo-phenyl)-[2,2';6',2'']terpyridine
A
4′-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-2,2′,6′,2″-terpyridine
B
4'-phenyl-2,2':6',2-terpyridine
Conditions | Yield |
---|---|
Stage #1: 4'-(4-bromo-phenyl)-[2,2';6',2'']terpyridine With n-butyllithium at -78 - 20℃; Stage #2: 2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane at -78 - 20℃; |
2-acetylpyridine
4'-phenyl-2,2':6',2-terpyridine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NaOH / various solvent(s) / 2 h / 0 °C 2: aq. NH3 / various solvent(s) / 2 h / 100 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: aq. NH3; KOH / ethanol / Heating 2.1: C4H9Li / -78 - 20 °C 2.2: -78 - 20 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: aq. NH3; KOH / ethanol / Heating 2.1: C4H9Li / -78 - 20 °C 2.2: -78 - 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: NaOH / 0.17 h 2: 4.05 g / NH4OAc / acetic acid / 2 h / Heating View Scheme |
benzaldehyde
4'-phenyl-2,2':6',2-terpyridine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NaOH / various solvent(s) / 2 h / 0 °C 2: aq. NH3 / various solvent(s) / 2 h / 100 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: aq. NH3; KOH / ethanol / Heating 2.1: C4H9Li / -78 - 20 °C 2.2: -78 - 20 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: aq. NH3; KOH / ethanol / Heating 2.1: C4H9Li / -78 - 20 °C 2.2: -78 - 20 °C View Scheme |
benzaldehyde
4'-phenyl-2,2':6',2-terpyridine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NaOH / 0.17 h 2: 4.05 g / NH4OAc / acetic acid / 2 h / Heating View Scheme | |
Multi-step reaction with 2 steps 1: aq. KOH / methanol 2: ammonium acetate / methanol View Scheme |
3-phenyl-1,5-bis(pyridine-2-yl)pentane-1,5-dione
ammonium acetate
4'-phenyl-2,2':6',2-terpyridine
Conditions | Yield |
---|---|
In ethanol for 37h; Reflux; | 9.3 g |
styrene
4'-phenyl-2,2':6',2-terpyridine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: tert.-butylhydroperoxide / acetonitrile / 12 h / 80 °C 2: sodium hydroxide / ethanol View Scheme |
2-acetylpyridine
4′-formyl-2,2′:6′2″-terpyridine
4'-phenyl-2,2':6',2-terpyridine
Conditions | Yield |
---|---|
With ammonium acetate; sodium hydroxide In ethanol Inert atmosphere; Schlenk technique; |
rhenium(I) pentacarbonyl chloride
4'-phenyl-2,2':6',2-terpyridine
[Re(CO)3(4'-phenyl-2,2':6',2''-terpyridine)Cl]
Conditions | Yield |
---|---|
In toluene the mixt. in toluene was refluxed under N2 for 4 h, cooled; ppt. was filtered, stirred in DCM for 10 min, filtered, washed with CH2Cl2 and diethyl ether, dried in vac.; | 99% |
In acetonitrile Reflux; | 75% |
In methanol; toluene for 3h; Reflux; Inert atmosphere; |
Conditions | Yield |
---|---|
at 150℃; for 0.166667h; Inert atmosphere; Sealed tube; | 99% |
Conditions | Yield |
---|---|
at 150℃; for 0.166667h; Inert atmosphere; Sealed tube; | 99% |
Conditions | Yield |
---|---|
at 150℃; for 0.166667h; Inert atmosphere; Sealed tube; | 99% |
Conditions | Yield |
---|---|
at 150℃; for 0.166667h; Inert atmosphere; Sealed tube; | 99% |
Conditions | Yield |
---|---|
at 150℃; for 0.166667h; Inert atmosphere; Sealed tube; | 99% |
Conditions | Yield |
---|---|
at 150℃; for 0.166667h; Inert atmosphere; Sealed tube; | 99% |
Conditions | Yield |
---|---|
at 150℃; for 0.166667h; Inert atmosphere; Sealed tube; | 99% |
Conditions | Yield |
---|---|
at 150℃; for 0.166667h; Inert atmosphere; Sealed tube; | 99% |
Conditions | Yield |
---|---|
at 150℃; for 0.166667h; Inert atmosphere; Sealed tube; | 99% |
Conditions | Yield |
---|---|
at 150℃; for 0.166667h; Inert atmosphere; Sealed tube; | 99% |
Conditions | Yield |
---|---|
at 150℃; for 0.166667h; Inert atmosphere; Sealed tube; | 99% |
Conditions | Yield |
---|---|
at 150℃; for 0.166667h; Inert atmosphere; Sealed tube; | 99% |
Conditions | Yield |
---|---|
With pyridine at 150℃; for 0.166667h; Inert atmosphere; Sealed tube; | 99% |
Conditions | Yield |
---|---|
With pyridine at 150℃; for 0.166667h; Inert atmosphere; Sealed tube; | 99% |
4'-phenyl-2,2':6',2-terpyridine
{Cl2(4'-phenyl-2,2':6',2''-terpyridine)manganese(II)}
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 24h; Inert atmosphere; Schlenk technique; Glovebox; | 98% |
In methanol refluxing for 30 min; concn., washing of the ppt. with MeOH and Et2O and drying (vac.); elem. anal.; |
pyridine
4'-phenyl-2,2':6',2-terpyridine
Conditions | Yield |
---|---|
at 80℃; for 8h; Inert atmosphere; Sealed tube; | 98% |
4'-phenyl-2,2':6',2-terpyridine
{Cl2(4'-phenyl-2,2':6',2''-terpyridine)manganese(II)}
Conditions | Yield |
---|---|
In methanol; acetone ligand dissolved in acetone at 50°C, a soln. of Mn salt in MeOH added, incubated at 50°C; cooled to 0°C, filtered, washed (MeOH/acetone, Et2O), dried (vac., overnight); elem. anal.; | 96% |
In ethanol; chloroform at 20℃; Reflux; | 77% |
RuCl3(isopropyl-S-phenyl)2(CH3OH)
4'-phenyl-2,2':6',2-terpyridine
{Ru(4'-Ph-2,2':6',2''-terpyridine)Cl3}
Conditions | Yield |
---|---|
In acetonitrile for 18h; Reflux; | 96% |
Conditions | Yield |
---|---|
With pyridine at 250℃; for 34h; Inert atmosphere; Sealed tube; | 95% |
4'-phenyl-2,2':6',2-terpyridine
Conditions | Yield |
---|---|
In dichloromethane; acetonitrile at 80℃; for 48h; High pressure; Autoclave; | 94.8% |
trichlorotris(tetrahydrofuran)molybdenum(III)
4'-phenyl-2,2':6',2-terpyridine
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 24h; | 94% |
Conditions | Yield |
---|---|
With pyridine at 250℃; for 34h; Inert atmosphere; Sealed tube; | 94% |
rhenium(I) pentacarbonyl chloride
4'-phenyl-2,2':6',2-terpyridine
Conditions | Yield |
---|---|
In methanol; toluene for 3h; Reflux; Inert atmosphere; | 93% |
4'-phenyl-2,2':6',2-terpyridine
[Pt(4'-phenyl-2,2':6',2''-terpyridine)(Me)]Cl
Conditions | Yield |
---|---|
In methanol byproducts: DMSO; stirring equimolar amts. for 20 min; concn. (vac.), pptn. on Et2O addn. and cooling, collection, washing (Et2O), drying (vac.); elem. anal.; | 92% |
dichloro( 1,5-cyclooctadiene)platinum(ll)
4'-phenyl-2,2':6',2-terpyridine
silver trifluoromethanesulfonate
Conditions | Yield |
---|---|
Stage #1: dichloro( 1,5-cyclooctadiene)platinum(ll); silver trifluoromethanesulfonate In dichloromethane; acetonitrile for 0.5h; Darkness; Stage #2: 4'-phenyl-2,2':6',2-terpyridine In dichloromethane; acetonitrile at 20℃; for 72h; Darkness; | 92% |
rhenium(I) pentacarbonyl bromide
4'-phenyl-2,2':6',2-terpyridine
Conditions | Yield |
---|---|
In toluene for 4h; Reflux; | 91% |
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