As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
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inquiryProduct Description Name Methyl 4-nitrobenzoate CAS 619-50-1 Assay 99% Appearance
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inquiryOur advantage:Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scient
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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inquiryMethyl 4-nitrobenzoate CAS:619-50-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic int
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
superior quality moderate price & quick delivery Appearance: light yellow to yellow fine crystalline powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your requ
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryMethyl 4-nitrobenzoate Chemical Properties Melting point 94-96 °C (lit.) 94-96 °C Boiling point 314.24°C (rough estimate) density 1.4283 (rough estimate) refractive index 1.5468 (estimate) Fp 94-96°C storage temp.
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inquiryProduct name: Methyl P-Nitrobenzoate CAS No.:619-50-1 Molecule Formula:C8H6NO4 Molecule Weight:180.14 Purity: 99.0% Package: 25kg/drum Description:Yellow powder Manufacture Standards:Enterprise Standard TESTING ITE
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Min.Order:1 Kilogram
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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Triumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Business Custom Synthesis:
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inquiryOur company is engaged in customizing the benzene ring and pyridine derivative organic intermediates, and the quantity is flexible according to customer's needs. It mainly provides high-quality intermediates for domestic and foreign pharmaceutical an
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inquiry1, High quality with competitive price:2, Fast and safe delivery3.Excellent pre-sales and after-sales service4. Well-trained and professional technologist and sales with rich experience in the field for 5-10 yearsAppearance:see detailed specification
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inquiryConditions | Yield |
---|---|
With dmap; 2-chloro-1-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-henicosafluorododecyl)pyridinium trifluoromethanesulfonate; triethylamine In N,N-dimethyl-formamide at 20℃; for 1h; | 100% |
Stage #1: 4-nitro-benzoic acid With 1H-imidazole; iodine; triphenylphosphine In dichloromethane at 20℃; for 0.0833333h; Garegg-Samuelsson type reaction; Stage #2: methanol In dichloromethane at 20℃; Garegg-Samuelsson type reaction; | 100% |
With dmap; 2-chloro-1-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-henicosafluorododecyl)pyridinium trifluoromethanesulfonate; triethylamine In N,N-dimethyl-formamide at 20℃; for 1h; | 100% |
p-nitrobenzene iodide
carbon monoxide
triethylmethoxystannane
4-nitrobenzoic acid methyl ester
Conditions | Yield |
---|---|
With iodophenylbis(triphenylphosphine)palladium under 760 Torr; for 1h; | 100% |
diazomethyl-trimethyl-silane
4-nitro-benzoic acid
4-nitrobenzoic acid methyl ester
Conditions | Yield |
---|---|
In methanol; toluene at 20℃; for 2h; | 100% |
In ethyl acetate | 60% |
In methanol; diethyl ether; hexane at 20℃; for 2h; Inert atmosphere; | 178 mg |
1-(dimethoxymethyl)pyrrolidine
4-nitro-benzoic acid
4-nitrobenzoic acid methyl ester
Conditions | Yield |
---|---|
In 1,2-dichloro-ethane at 30℃; for 25h; | 100% |
methanol
A
4-nitrobenzoic acid methyl ester
B
diethyl [N-(hydroxy)imino](p-fluorophenyl)methylphosphonate
Conditions | Yield |
---|---|
for 6h; Inert atmosphere; Reflux; | A 100% B 100% |
Conditions | Yield |
---|---|
With water; iodine; sodium nitrite at 20 - 70℃; chemoselective reaction; | 99% |
With ammonium peroxydisulfate at 60℃; for 2.5h; | 99% |
With potassium hydroxide; iodine at 0℃; for 0.0166667h; | 98% |
Conditions | Yield |
---|---|
With sodium carbonate; palladium; silver(l) oxide at 80℃; for 48h; Molecular sieve; | 99% |
With dihydrogen peroxide for 3h; Irradiation; | 95% |
With oxygen; potassium carbonate at 60℃; under 750.075 Torr; for 20h; | 94% |
Conditions | Yield |
---|---|
scandium tris(trifluoromethanesulfonate) at 64℃; for 168h; | 98% |
With dipotassium hydrogenphosphate for 5h; Reflux; | 98% |
With potassium ethoxide | |
acrylonitrile; triphenylphosphine at 25℃; for 24h; | 71 % Chromat. |
N,N-dimethoxyamine
4-nitro-benzoic acid
4-nitrobenzoic acid methyl ester
Conditions | Yield |
---|---|
In benzene for 3h; Heating; | 98% |
In benzene Product distribution; Mechanism; Heating; other nucleophiles; var. reaction conditions; | 98% |
In benzene for 3h; Mechanism; Heating; | 98% |
dimethyl dicarbonate
4-nitro-benzoic acid
4-nitrobenzoic acid methyl ester
Conditions | Yield |
---|---|
magnesium(II) perchlorate In nitromethane at 40℃; for 16h; | 98% |
With 2,6-dimethylpyridine; fac-tris(2-phenylpyridinato-N,C2')iridium(III) In N,N-dimethyl-formamide at 20℃; for 48h; Sealed tube; Inert atmosphere; Irradiation; |
methanol
p-nitrobenzene iodide
carbon monoxide
4-nitrobenzoic acid methyl ester
Conditions | Yield |
---|---|
With palladium diacetate; caesium carbonate; 1,3,5,7-tetramethyl-8-phenyl-2,4,6-trioxa-8-phosphatricyclo[3.3.1.13,7]decane In N,N-dimethyl-formamide at 80℃; under 2327.23 Torr; | 98% |
With triethylamine at 100℃; under 3750.38 Torr; for 1.5h; Inert atmosphere; | 95% |
With palladium diacetate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In N,N-dimethyl-formamide at 100℃; under 5250.53 Torr; continuous flow reactor; | 81% |
N-methyl-N-nitrosotoluene-p-sulfonamide
4-nitro-benzoic acid
4-nitrobenzoic acid methyl ester
Conditions | Yield |
---|---|
With potassium hydroxide In tetrahydrofuran; methanol; water at 20℃; | 98% |
Stage #1: N-methyl-N-nitrosotoluene-p-sulfonamide With potassium hydroxide In methanol; water; N,N-dimethyl-formamide Flow reactor; Stage #2: 4-nitro-benzoic acid In methanol; diethyl ether; water; N,N-dimethyl-formamide at 0 - 25℃; Sonication; | 90% |
methanol
N-amino-(4-nitrophenyl)carboxamide
4-nitrobenzoic acid methyl ester
Conditions | Yield |
---|---|
With ammonium cerium(IV) nitrate at 20℃; for 0.25h; Esterification; | 97% |
With Oxone at 20℃; for 6h; oxidative esterification; | 84% |
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane for 16h; | 97% |
Conditions | Yield |
---|---|
With dmap; triethylamine In acetonitrile | 97% |
tetramethylorthosilicate
4-nitrobenzaldehdye
4-nitrobenzoic acid methyl ester
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride; (t-Bu2POH)2PdCl2 In acetonitrile at 50℃; for 24h; | 97% |
phosphorous acid trimethyl ester
4-nitro-benzoic acid
4-nitrobenzoic acid methyl ester
Conditions | Yield |
---|---|
With diethylazodicarboxylate In tetrahydrofuran for 2h; | 96% |
With diethylazodicarboxylate In tetrahydrofuran for 2h; Mechanism; other phosphite, other carboxylic acid, phenols, imides and C-H acids; | 92% |
methanol
formaldehyd
1,3-diphenylpropanedione
A
4-nitrobenzoic acid methyl ester
B
bis-1,5(4-nitrophenyl)-1,5-pentanedione
Conditions | Yield |
---|---|
hydroxocobalt(III) Schiff base at 60℃; for 1.5h; Product distribution; Mechanism; var. 4-subst. educts; var. reaction conditions; | A 92% B 96% |
Conditions | Yield |
---|---|
With N,N-dimethyl-formamide dimethyl acetal for 16h; Heating; | 95% |
methyl 2-hydroxy-5-nitrobenzoate
4-nitro-benzoic acid
A
4-nitrobenzoic acid methyl ester
B
5-nitrosalicylic acid
Conditions | Yield |
---|---|
Stage #1: 4-nitro-benzoic acid With potassium carbonate In N,N-dimethyl acetamide at 110℃; for 0.5h; Stage #2: methyl 2-hydroxy-5-nitrobenzoate at 110℃; for 24h; Temperature; | A 95% B n/a |
Conditions | Yield |
---|---|
With C26H28N3O3S(1+)*F6P(1-); nickel diacetate; potassium carbonate; triethylamine at 25℃; for 2h; | 95% |
carbonic acid dimethyl ester
4-nitro-benzoic acid
4-nitrobenzoic acid methyl ester
Conditions | Yield |
---|---|
With sulfuric acid at 80 - 85℃; for 9.5h; Neat (no solvent); | 94.2% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide for 0.0180556h; microwave irradiation; | 90% |
With potassium carbonate In dimethyl sulfoxide at 90℃; for 16h; Inert atmosphere; Green chemistry; | 86% |
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane for 0.166667h; | 94% |
With pyridine at 70℃; for 3h; | 91% |
at 25℃; Thermodynamic data; ΔH; |
Conditions | Yield |
---|---|
With 4-methyl-morpholine; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride at 20℃; for 2.5h; Esterification; | 94% |
methanol
carbon monoxide
para-nitrophenyl bromide
4-nitrobenzoic acid methyl ester
Conditions | Yield |
---|---|
With palladium diacetate; caesium carbonate; 1,3,5,7-tetramethyl-8-phenyl-2,4,6-trioxa-8-phosphatricyclo[3.3.1.13,7]decane In N,N-dimethyl-formamide at 80℃; under 2327.23 Torr; | 94% |
With palladium diacetate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In 1,4-dioxane at 100℃; under 11251.1 Torr; continuous flow reactor; | 77% |
With palladium diacetate; triethylamine; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; hydrazine In tetrahydrofuran; 1,4-dioxane at 100℃; under 11251.1 Torr; Temperature; Flow reactor; | 77% |
With ruthenium(III) trichloride hydrate; 1,4-bis(2'-diphenylphosphino-3'-methylimidazolium)butane triflate; triethylamine In 1-methyl-pyrrolidin-2-one at 140℃; under 15001.5 Torr; for 16h; Autoclave; | 80 %Chromat. |
methanol
1-(4-nitrophenyl)-3-phenyl-1-propanone
A
3-phenyl-propionaldehyde
B
4-nitrobenzoic acid methyl ester
Conditions | Yield |
---|---|
With N,N-dimethyl-formamide dimethyl acetal for 16h; Heating; | A n/a B 93% |
diazomethane
4-nitrobenzyl chloride
4-nitrobenzoic acid methyl ester
Conditions | Yield |
---|---|
Stage #1: 4-nitrobenzyl chloride With sodium chlorite; sodium dihydrogenphosphate; Me-AZADO+Cl- In dichloromethane; water at 25℃; for 1.5h; Stage #2: With 2-methyl-but-2-ene In dichloromethane; water Stage #3: diazomethane With hydrogenchloride; sodium hydroxide Product distribution / selectivity; more than 3 stages; | 93% |
Stage #1: 4-nitrobenzyl chloride With sodium chlorite; sodium dihydrogenphosphate; 2,2,6,6-tetramethylpiperidin-1-oxoammonium chloride In dichloromethane; water at 25℃; for 1.5h; Stage #2: With 2-methyl-but-2-ene In dichloromethane; water Stage #3: diazomethane With hydrogenchloride; sodium hydroxide Product distribution / selectivity; more than 3 stages; | 63% |
4-methoxycarbonylphenylboronic acid
4-nitrobenzoic acid methyl ester
Conditions | Yield |
---|---|
With 1,1,1,3',3',3'-hexafluoro-propanol; N–nitrosaccharin at 60℃; for 19h; Reagent/catalyst; Inert atmosphere; Schlenk technique; | 93% |
With Iron(III) nitrate nonahydrate In toluene at 80℃; for 18h; Inert atmosphere; | 86% |
With dipotassium peroxodisulfate; bismuth (III) nitrate pentahydrate In benzene at 70℃; for 12h; Inert atmosphere; | 74% |
With copper(I) oxide; tetrabutylammonium nitrite In acetonitrile at 20℃; | 53% |
methanol
N-(4-nitrobenzoyl)oxazolidinone
4-nitrobenzoic acid methyl ester
Conditions | Yield |
---|---|
With [t-Bu2SnCl(OH)]2 In toluene at 85℃; for 14h; | 92% |
Conditions | Yield |
---|---|
With tert-butylamine for 10h; Heating; | 100% |
Stage #1: ethanol With platinum(IV) oxide; hydrogen at 60℃; under 750.075 - 1500.15 Torr; for 2h; Autoclave; Green chemistry; Stage #2: 4-nitrobenzoic acid methyl ester at 60℃; Autoclave; Inert atmosphere; Green chemistry; chemoselective reaction; | 93% |
With dichlorobis(1-butylimidazolium) zinc at 70 - 80℃; | 93% |
4-nitrobenzoic acid methyl ester
N-[(4-methoxycarbonyl)phenyl]hydroxylamine
Conditions | Yield |
---|---|
With 5% rhodium-on-charcoal; hydrazine hydrate In tetrahydrofuran at 0℃; for 5h; Inert atmosphere; | 100% |
With 5% rhodium-on-charcoal; hydrazine hydrate In tetrahydrofuran at 0℃; Inert atmosphere; | 100% |
With rhodium contaminated with carbon; hydrazine hydrate In tetrahydrofuran at 0℃; for 5h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With potassium fluoride; polymethylhydrosiloxane; palladium diacetate In tetrahydrofuran; water at 20℃; for 0.5h; | 100% |
With potassium fluoride; polymethylhydrosiloxane; palladium diacetate In tetrahydrofuran at 20℃; for 0.5h; | 100% |
With sodium tetrahydroborate; water In ethanol at 25℃; for 1h; Solvent; chemoselective reaction; | 100% |
4-nitrobenzoic acid methyl ester
acetonitrile
methyl 4-(ethylamino)benzoate
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; ammonium acetate; hydrogen In methanol at 20℃; under 760.051 Torr; for 24h; | 100% |
Conditions | Yield |
---|---|
With AlBrCl3(1-)*C5H5N*H(1+) at 140℃; for 3h; | 99% |
With methanesulfonic acid; 1-methylimidazolium hydrobromide at 120℃; for 2h; | 96% |
With iron(III) sulfate; water In toluene at 110℃; for 4h; Ionic liquid; | 95% |
Conditions | Yield |
---|---|
With lanthanum(III) nitrate hexahydrate; TOP at 110℃; for 5h; Reagent/catalyst; Molecular sieve; | 99% |
With N,N'-biscyclohexyl-imidazol-2-ylidene; 4 A molecular sieve In tetrahydrofuran at 20℃; for 0.25h; | 96% |
1,3-dicyclohexyl-imidazol-2-ylidene In tetrahydrofuran at 20℃; for 0.25h; | 96% |
1-octadecanol
4-nitrobenzoic acid methyl ester
octadecyl 4-nitro-benzoate
Conditions | Yield |
---|---|
Stage #1: 1-octadecanol; 4-nitrobenzoic acid methyl ester In xylene for 0.5h; Heating; Stage #2: With TiO(acac)2 In xylene for 4.5h; Heating; | 99% |
Conditions | Yield |
---|---|
With caesium carbonate In dimethyl sulfoxide at 25℃; for 1.5h; | 99% |
With magnesium methanolate In N,N-dimethyl-formamide at 80℃; for 8h; | 78% |
Conditions | Yield |
---|---|
With Zn4(OCOCF3)6O In di-isopropyl ether for 40h; Heating; | 99% |
Conditions | Yield |
---|---|
With tetrabutylammonium acetate; oxiranyl-methanol In hexane for 2h; Reflux; | 99% |
4-nitrobenzoic acid methyl ester
dimethyl 4,4'-azoxydibenzoate
Conditions | Yield |
---|---|
With potassium hydroxide In water; isopropyl alcohol at 30℃; under 760.051 Torr; for 10h; Inert atmosphere; | 98% |
With manganese; acetic acid In tetrahydrofuran; water at 20℃; for 15h; | 70% |
With triethylsilane; indium(III) bromide In N,N-dimethyl-formamide at 60℃; for 12h; | 64% |
With bismuth; sodium hydroxide; sodium tetrahydroborate; oxygen 1.) methanol, room temperature, 0.5 h, 2.) methanol, room temperate, 4 h; Yield given. Multistep reaction; | |
Multi-step reaction with 2 steps 1: 78 percent / Sb, NaBH4 / methanol / 1 h / Ambient temperature 2: 88 percent / NaOH, O2 / 4 h / Ambient temperature View Scheme |
4-nitrobenzoic acid methyl ester
propan-1-ol-3-amine
N-(3-Hydroxy-propyl)-4-nitro-benzamid
Conditions | Yield |
---|---|
With ammonium nitrate In neat (no solvent) at 20℃; for 12h; Green chemistry; | 98% |
In toluene at 97℃; for 4h; Acylation; | 79% |
4-nitrobenzoic acid methyl ester
N,N-diethylethylenediamine
N-(2-(diethylamino)ethyl)-4-nitrobenzamide
Conditions | Yield |
---|---|
With ammonium nitrate In neat (no solvent) at 20℃; for 12h; Green chemistry; | 98% |
Conditions | Yield |
---|---|
With ammonia In methanol at 70℃; | 98% |
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