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inquiryProduct Name: 1,3-Dicyanobenzene Synonyms: M-PHTHALONITRILE;1,3-Benzendikarbonitril;1,3-benzenedicarbonitrile;1,3-Benzodinitrile;3-Cyanobenzonitrile;Dinitrile of isophthalic acid;dinitrileofisophthalicacid;
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inquiryProduct Name: 1,3-Dicyanobenzene Synonyms: 1,3-benzenedicarbonitrile;1,3-Benzodinitrile;3-Cyanobenzonitrile;Dinitrile of isophthalic acid;dinitrileofisophthalicacid;Isoftalodinitril;isoftalodinitril(czech);
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inquirymoderate price & quick delivery. Appearance:off-white to light brown solid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:100g/bottle,1kg/bottle,25kg/drum or as per your request Application:Is a raw material
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1,3-Dicyanobenzene Basic information Product Name: 1,3-Dicyanobenzene Synonyms: M-PHTHALONITRILE;1,3-Benzendikarbonitril;1,3-benzenedicarbonitrile;1,3-Benzodinitrile;1,3-Dicyanobenzene 98%;1,3-Dicyanobenzene,98%;Between the benzene nitrile;1,4
factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:626-17-5
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:626-17-5
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:626-17-5
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
Conditions | Yield |
---|---|
Stage #1: 1,3-dimethanol benzene With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tert-butylhypochlorite In dichloromethane at 20℃; for 0.5h; Inert atmosphere; Stage #2: With ammonia; iodine In dichloromethane; water at 20℃; for 2h; Inert atmosphere; | 99% |
3-Cyanobenzaldehyde
benzene-1,3-dicarbonitrile
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; triethylamine In ethyl acetate; N,N-dimethyl-formamide at 100℃; | 98% |
With hydroxylamine hydrochloride; zinc(II) oxide for 0.0166667h; Microwave irradiation; neat (no solvent); | 91% |
Multi-step reaction with 2 steps 1: hydroxylamine hydrochloride 2: 19 percent Chromat. / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / acetonitrile / 0.5 h / Photolysis View Scheme |
m-xylene
A
benzene-1,3-dicarbonitrile
B
3-cyanobenzamide
C
3-Methylbenzonitrile
Conditions | Yield |
---|---|
With ammonia; oxygen; B0.5CrK0.02Mo0086Na0009P0.007V at 350 - 420℃; under 1500.15 Torr; Gas phase; Heating / reflux; | A 98% B n/a C n/a |
Conditions | Yield |
---|---|
With aluminum oxide; hydroxylamine hydrochloride; methanesulfonyl chloride at 100℃; for 0.5h; | 97% |
With hydroxylamine hydrochloride; pyrographite; methanesulfonyl chloride at 100℃; for 1h; | 94% |
With hydroxylamine hydrochloride; 2,4,6-triphenylpyrylium tetrafluoroborate In acetonitrile at 40℃; under 750.075 Torr; for 24h; Molecular sieve; Irradiation; Inert atmosphere; | 78% |
1,3-phenylenediboronic acid
A
benzene-1,3-dicarbonitrile
B
4-nitro-N-(4-chlorophenyl)benzenesulfonamide
Conditions | Yield |
---|---|
With Fe3O4/SiO2/(3-chloropropyl)trimethoxysilane/2,2′-(4,4′-(propane-1,3-diyl)bis(piperazine-4,1-diyl))- diethanamine/Pd In acetonitrile for 14h; Catalytic behavior; Reflux; | A 95% B n/a |
Conditions | Yield |
---|---|
With aluminum oxide; aminosulfonic acid; urea for 0.116667h; Irradiation; | 93% |
With ammonia at 310 - 400℃; | |
With diammonium phosphate at 370℃; | |
Multi-step reaction with 2 steps 1: ammonium / 0.5 h / Heating 2: phosphorus pentoxide / 1 h / 15 - 37.5 Torr / Heating View Scheme |
1,3-phenylenediboronic acid
A
benzene-1,3-dicarbonitrile
B
4-bromo-benzenesulfonic acid-(4-chloro-anilide)
Conditions | Yield |
---|---|
With Fe3O4/SiO2/(3-chloropropyl)trimethoxysilane/2,2′-(4,4′-(propane-1,3-diyl)bis(piperazine-4,1-diyl))- diethanamine/Pd In acetonitrile for 15h; Catalytic behavior; Reflux; | A 93% B n/a |
Conditions | Yield |
---|---|
With nickel(II) sulphate; sodium hydroxide; dipotassium peroxodisulfate In dichloromethane for 24h; Ambient temperature; | 92% |
With Dess-Martin periodane In dichloromethane at 25℃; for 0.25h; | 90% |
With ammonium hydroxide; iodine at 60℃; for 2h; | 90% |
Conditions | Yield |
---|---|
With palladium diacetate; sodium carbonate; 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride In N,N-dimethyl acetamide at 120℃; for 1h; | 92% |
Conditions | Yield |
---|---|
With sodium carbonate In N,N-dimethyl-formamide at 120℃; for 12h; Inert atmosphere; Schlenk technique; | 92% |
With palladium diacetate; sodium carbonate; 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride In N,N-dimethyl acetamide at 120℃; for 5h; | 89% |
N-(4-chlorophenyl)-N-cyano-4-methylbenzenesulfonamide
1,3-phenylenediboronic acid
A
benzene-1,3-dicarbonitrile
B
4-methyl-N-(4-chlorophenyl)benzenesulfonamide
Conditions | Yield |
---|---|
With Fe3O4/SiO2/(3-chloropropyl)trimethoxysilane/2,2′-(4,4′-(propane-1,3-diyl)bis(piperazine-4,1-diyl))- diethanamine/Pd In acetonitrile for 16h; Catalytic behavior; Reflux; | A 92% B n/a |
Conditions | Yield |
---|---|
With oxygen; ammoxidation catalyst containing 10.2wtpercent V2O5, 8.5wtpercent Cr2O3, 76.2wtpercent TiO2, 0.4wtpercent B2O3, 4.8wtpercent natural diamond at 130 - 380℃; for 24h; Product distribution / selectivity; Inert atmosphere; | 91% |
With ammonia at 425 - 450℃; under 760.051 Torr; for 2h; Reagent/catalyst; Temperature; | 85.4% |
With ammonium hydroxide at 370℃; Flow reactor; | 77% |
sulfolane
isophthalic acid
cyanogen chloride
benzene-1,3-dicarbonitrile
Conditions | Yield |
---|---|
91% |
Conditions | Yield |
---|---|
With 3 A molecular sieve at 280 - 500℃; under 0.003 Torr; for 0.25h; Pyrolysis; | 90% |
With phosphorus pentoxide | |
With phosphorus pentoxide under 15.0015 - 37.5038 Torr; for 1h; Temperature; Heating; |
3-(hydroxyimino)methylbenzonitrile
benzene-1,3-dicarbonitrile
Conditions | Yield |
---|---|
With trichloro(trifluoromethanesulfonato)titanium(IV) at 80℃; for 10h; Dehydration; | 89% |
With thionyl chloride; polyvinylpyrrolidone In dichloromethane at 20℃; for 0.25h; Dehydration; | 84% |
Multi-step reaction with 3 steps 1: Cl(gas) / CHCl3 2: 63 percent 3: cyclohexane / 25 °C / Irradiation View Scheme | |
With fluorosulfonyl fluoride; sodium carbonate In dimethyl sulfoxide at 20℃; for 12h; | 251 mg |
With fluorosulfonyl fluoride; potassium carbonate at 20℃; for 12h; | 212 mg |
Conditions | Yield |
---|---|
With copper(l) iodide at 80℃; for 0.333333h; Inert atmosphere; Sonication; chemoselective reaction; | 89% |
With sodium carbonate In N,N-dimethyl-formamide at 120℃; for 1h; Inert atmosphere; Green chemistry; | |
With sodium carbonate In N,N-dimethyl-formamide at 120℃; |
Conditions | Yield |
---|---|
With dichloro(2,2-bis(diphenylphosphino)diphenyl ether)palladium(II); potassium acetate In 1,4-dioxane; water at 90℃; for 1.33333h; Sealed tube; | 89% |
Conditions | Yield |
---|---|
With potassium phosphate; ammonium formate In acetonitrile at 115℃; for 16h; Sealed tube; Green chemistry; | 88% |
Multi-step reaction with 3 steps 1: potassium carbonate; fluorosulfonyl fluoride; dimethyl sulfoxide / 12 h / 20 °C 2: hydroxylamine hydrochloride; potassium carbonate / 20 °C 3: potassium carbonate; fluorosulfonyl fluoride / 12 h / 20 °C View Scheme |
3-((hydroxyimino)methyl)benzaldoxime
benzene-1,3-dicarbonitrile
Conditions | Yield |
---|---|
With acetyl chloride; zinc(II) oxide for 0.5h; Heating; | 87% |
With pyrographite; methanesulfonyl chloride at 100℃; for 0.25h; | 85% |
Conditions | Yield |
---|---|
With [(2-di-tert-butylphosphino-2′,4′,6′-triisopropyl-1, 1′-biphenyl)-2-(2′-amino-1,1′-biphenyl)] palladium(II) methanesulfonate In tetrahydrofuran; water at 20℃; for 18h; Inert atmosphere; | 84% |
Conditions | Yield |
---|---|
With ammonia; iodine In water at 60℃; for 4h; | 81% |
Conditions | Yield |
---|---|
With ammonia; oxygen; silica-supported catalyst with 50percentweight silica and V, Cr, Mo and B in a ratio of 1:1:0.1:0.2 at 400℃; under 1125.11 Torr; Product distribution / selectivity; Gas phase; | A 80.2% B 3.7% |
vanadia; zirconium(IV) oxide at 339.85℃; Kinetics; | |
With ammonia; oxygen In water at 470℃; Product distribution / selectivity; | |
With ammonia; oxygen; V4Sb3.1W0.66Cs0.74Ox at 430℃; Steatite spheres; Inert atmosphere; | |
With ammonia at 380℃; for 24h; Catalytic behavior; Reagent/catalyst; Temperature; |
2-methylglutaronitrile
isophthalic acid
A
benzene-1,3-dicarbonitrile
B
3-methyl-piperidine-2,6-dione
Conditions | Yield |
---|---|
With aluminum (III) chloride at 270℃; for 4h; | A 69% B 76% |
tetra-n-butylammonium cyanide
C13H9N3S
A
benzene-1,3-dicarbonitrile
B
3-cyanophenyl phenyl sulfide
Conditions | Yield |
---|---|
In dimethyl sulfoxide at 25℃; for 1h; Irradiation; | A 75% B 17% |
C13H9N3S
A
benzene-1,3-dicarbonitrile
B
3-cyanophenyl phenyl sulfide
Conditions | Yield |
---|---|
With tetra-n-butylammonium cyanide In dimethyl sulfoxide at 25℃; for 1h; Irradiation; | A 75% B 17% |
Conditions | Yield |
---|---|
With 1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione; ammonia In water at 60℃; for 4h; | 75% |
naphthalen-2-yl 4-methylbenzene-1-sulfonate
benzene-1,3-dicarbonitrile
Conditions | Yield |
---|---|
With 2-[2-(dicyclohexylphosphino)-phenyl]-1-methyl-1H-indole; palladium diacetate; potassium carbonate In water at 80℃; for 18h; Inert atmosphere; | 72% |
3-cyanobromobenzene
N,N-dimethyl-formamide
benzene-1,3-dicarbonitrile
Conditions | Yield |
---|---|
Stage #1: 3-cyanobromobenzene; N,N-dimethyl-formamide With magnesium In tetrahydrofuran at 20℃; Stage #2: With ammonia; iodine In tetrahydrofuran; water at 20℃; | 71% |
Conditions | Yield |
---|---|
Stage #1: 3-cyanobromobenzene With isopropylmagnesium chloride; lithium chloride In tetrahydrofuran at -15℃; for 0.25h; Stage #2: With N,N-dimethyl-formamide In tetrahydrofuran at 0℃; for 2h; Stage #3: With ammonia; iodine In tetrahydrofuran; water at 20℃; for 2h; | 71% |
Conditions | Yield |
---|---|
With ammonia; hydrogen In methanol at 100℃; under 22502.3 Torr; for 2h; Pressure; Reagent/catalyst; Temperature; | 99% |
With hydrogen; cobalt/diatomaceous earth catalyst "G67", cobalt content=56percent; pretreatment is given in full text In 1,2,4-Trimethylbenzene; ammonia at 100℃; for 50h; Product distribution / selectivity; | 96.2% |
With hydrogen; Ni(NO3)2, Cu(NO3)2, Cr(NO3)3, Na2CO3; calcined at 380 deg C for 18 h; pretreatment is given in full text In 1,2,4-Trimethylbenzene; ammonia at 80℃; for 24h; Product distribution / selectivity; | 95.2% |
Conditions | Yield |
---|---|
With dihydrogen peroxide; potassium carbonate In dimethyl sulfoxide for 0.166667h; Ambient temperature; | 99% |
With [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; water; 1-benzyl-1-azonia-3,5-diaza-7-phosphaadamantyl chloride for 1h; Catalytic behavior; Reagent/catalyst; Schlenk technique; Reflux; Green chemistry; | 99% |
With dihydrogen peroxide; sodium carbonate In dimethyl sulfoxide at 60℃; for 3h; Reagent/catalyst; Temperature; | 98.7% |
benzene-1,3-dicarbonitrile
tert-butylmercury chloride
2,4-dicyano-1,5-bis(1,1-dimethylethyl)benzene
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane In dimethyl sulfoxide at 35℃; for 4.5h; Irradiation; | 99% |
benzene-1,3-dicarbonitrile
tert-butylmercury iodide
2,4-dicyano-1,5-bis(1,1-dimethylethyl)benzene
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane; potassium iodide In dimethyl sulfoxide at 25℃; for 19h; Irradiation; | 99% |
benzene-1,3-dicarbonitrile
3-(1H-tetrazole-5-yl)benzonitrile
Conditions | Yield |
---|---|
With sodium azide In N,N-dimethyl-formamide at 120℃; for 3h; | 99% |
With sodium azide In N,N-dimethyl-formamide for 24h; Reflux; | 95% |
With sodium azide In N,N-dimethyl-formamide at 110 - 120℃; for 24h; | 95% |
benzene-1,3-dicarbonitrile
Conditions | Yield |
---|---|
With hydrogenchloride; hydrogen In propan-1-ol; water at 60℃; under 375.038 Torr; for 18h; Flow reactor; | 99% |
Stage #1: benzene-1,3-dicarbonitrile With ammonia; hydrogen In water; isopropyl alcohol at 110℃; under 15001.5 Torr; for 24h; Autoclave; Stage #2: With hydrogenchloride In methanol; ethyl acetate Cooling with ice; | 66% |
Multi-step reaction with 2 steps 1: tris(pentafluorophenyl)borate / chloroform-d1 / 4 h / 25 °C / Inert atmosphere 2: hydrogenchloride; water / diethyl ether / 1 h / 20 °C View Scheme |
benzene-1,3-dicarbonitrile
propan-1-ol-3-amine
3-(5,6-dihydro-4H-1,3-oxazine-2-yl)benzonitrile
Conditions | Yield |
---|---|
With Montmorillonite KSF for 2h; Microwave irradiation; chemoselective reaction; | 98% |
With phosphotungstic acid for 0.0333333h; Microwave irradiation; chemoselective reaction; | 98% |
With montmorillonite KSF at 30℃; for 0.25h; Sonication; chemoselective reaction; | 98% |
With sulfur; cobalt(II) nitrate In neat (no solvent) at 90℃; for 0.0333333h; Time; Microwave irradiation; | 89% |
benzene-1,3-dicarbonitrile
dimethyl 2,2-di(but-2-yn-1-yl)malonate
tetramethyl 1,1',4,4'-tetramethyl-3,3'-(1,3-phenylene)bis(6,7-dihydro-5H-cyclopenta[c]pyridine-6,6-dicarboxylate)
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; bis(1,5-cyclooctadiene)diiridium(I) dichloride In benzene for 3h; Inert atmosphere; Reflux; | 98% |
2-(4-cyanophenyl)-5,5-dimethyl[1,3,2]dioxaborinane
benzene-1,3-dicarbonitrile
Conditions | Yield |
---|---|
With 4-(diphenylphosphino)morpholine; bis(triphenylphosphine)nickel(II) chloride; copper(II) bis(trifluoromethanesulfonate) at 85℃; for 7h; Reagent/catalyst; Solvent; Inert atmosphere; | 97.8% |
benzene-1,3-dicarbonitrile
2-(4-methoxyphenyl)-5,5-dimethyl-1,3,2-dioxaborolane
Conditions | Yield |
---|---|
With 4-(diphenylphosphino)morpholine; bis(triphenylphosphine)nickel(II) chloride; copper(II) bis(trifluoromethanesulfonate) In 1,4-dioxane at 90℃; for 7h; Reagent/catalyst; Solvent; Inert atmosphere; | 97.6% |
Conditions | Yield |
---|---|
With 4-(diphenylphosphino)morpholine; bis(triphenylphosphine)nickel(II) chloride; copper(II) bis(trifluoromethanesulfonate); N-fluorobis(benzenesulfon)imide In 1,4-dioxane at 80℃; for 8h; Reagent/catalyst; Solvent; Inert atmosphere; | 97.4% |
benzene-1,3-dicarbonitrile
5,5-dimethyl-2-(4-nitrophenyl)-1,3,2-dioxaborinane
Conditions | Yield |
---|---|
With 4-(diphenylphosphino)morpholine; bis(triphenylphosphine)nickel(II) chloride; copper(II) bis(trifluoromethanesulfonate) In 1,4-dioxane at 100℃; for 6h; Reagent/catalyst; Solvent; Inert atmosphere; | 97.3% |
benzene-1,3-dicarbonitrile
(SnCl4)2(((C2H5OCO)2CC(NH2))2C6H4)
Conditions | Yield |
---|---|
In 1,2-dichloro-ethane react. at 80°C for 5 h, all operations in dry atmosphere; filtn., washing with C2H4Cl2 or CCl4, drying in vacuum, elem. anal.; | 97% |
benzene-1,3-dicarbonitrile
ethylenediamine
3-(4,5-dihydro-1H-imidazol-2-yl)benzonitrile
Conditions | Yield |
---|---|
With bis(2-hydroxy-κO-2-phenylacetato)copper(II); iodine; sodium acetate In toluene at 90℃; for 0.25h; Time; Microwave irradiation; chemoselective reaction; | 97% |
With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione at 110℃; for 2.5h; chemoselective reaction; | 96% |
With trichloroisocyanuric acid In neat (no solvent) at 110℃; for 0.333333h; chemoselective reaction; | 92% |
benzene-1,3-dicarbonitrile
Cysteamine
1,3-bis(4,5-dihydrothiazol-2-yl)benzene
Conditions | Yield |
---|---|
With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione at 110℃; for 0.15h; chemoselective reaction; | 97% |
With trichloroisocyanuric acid In neat (no solvent) at 110℃; for 0.116667h; chemoselective reaction; | 95% |
benzene-1,3-dicarbonitrile
Trimethylenediamine
3-(2-(1,4,5,6-tetrahydropyrimidinyl))benzonitrile
Conditions | Yield |
---|---|
With bis(2-hydroxy-κO-2-phenylacetato)copper(II); iodine; sodium acetate In toluene at 90℃; for 0.333333h; Time; Microwave irradiation; chemoselective reaction; | 97% |
With phosphotungstic acid for 0.116667h; Microwave irradiation; chemoselective reaction; | 96% |
With Montmorillonite K-10 at 125℃; for 5.8h; chemoselective reaction; | 95% |
With C37H38Cu2O11; sodium acetate In toluene for 4h; Reflux; | 95% |
benzene-1,3-dicarbonitrile
A
1,3-di(aminomethyl)benzene
B
3-methyl-benzenemethanamine
Conditions | Yield |
---|---|
With hydrogen; Ni(NO3)2, Cu(NO3)2, Cr(NO3)3, Na2CO3; calcined at 380 deg C for 18 h; pretreatment is given in full text In 1,2,4-Trimethylbenzene; ammonia at 80℃; for 24h; Product distribution / selectivity; | A 96.8% B 0.1% |
With hydrogen; Ni(NO3)2, Cu(NO3)2, Cr(NO3)3, Na2CO3; calcined at 380 deg C for 18 h; activated with H2 In 1,2,4-Trimethylbenzene; ammonia at 80℃; for 24h; Product distribution / selectivity; | A 92.1% B 0.1% |
benzene-1,3-dicarbonitrile
N-Cyanoguanidine
3-(4,6-diamino-1,3,5-triazin-2-yl)benzonitrile
Conditions | Yield |
---|---|
With potassium hydroxide In isopropyl alcohol at 110℃; for 12h; | 96.5% |
With potassium hydroxide In butan-1-ol at 120℃; for 1h; | 81% |
at 230 - 250℃; |
benzene-1,3-dicarbonitrile
2,2'-di(prop-1-ynyl)biphenyl
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; bis(1,5-cyclooctadiene)diiridium(I) dichloride In benzene for 24h; Inert atmosphere; Reflux; | 96% |
benzene-1,3-dicarbonitrile
terephthalonitrile
furan-2,5-dicarbonitrile
2,5-thiophenedicarbonitrile
4-(4'-cyanophenoxy)benzonitrile
Conditions | Yield |
---|---|
With hydrogenchloride In 1,4-dioxane; ethanol; 2-methoxy-ethanol; acetone | 95.5% |
Conditions | Yield |
---|---|
With water at 30℃; for 25h; bacterial hydrolysis with cells of Rhodococcus rhodochrous NCIB 11,216; 0.25 M phosphate buffer, pH 7; | 95% |
With water; nitrile hydratase SP361 at 30℃; for 48h; in potassium phosphate buffer (pH = 7); | 91% |
With water; nitrile hydratase SP361 at 30℃; for 48h; in potassium phosphate buffer (pH = 7); | 91% |
With sodium hydroxide; sulfuric acid; sodium nitrite In water | 52% |
benzene-1,3-dicarbonitrile
ethylenediamine
1,3-bis(4,5-dihydro-1H-imidazol-2-yl)benzene
Conditions | Yield |
---|---|
With tetraphosphorus decasulfide for 0.025h; microwave irradiation; | 95% |
With cupric indole-3-acetate at 80℃; for 0.333333h; Neat (no solvent); Microwave irradiation; | 89% |
With toluene-4-sulfonic acid for 1.83333h; Reflux; neat (no solvent); | 87% |
Conditions | Yield |
---|---|
With trichloroisocyanuric acid In neat (no solvent) at 110℃; for 0.166667h; chemoselective reaction; | 95% |
With tris(trifluoroacetato)bismuth(III) for 0.6h; Heating; | 92% |
With sulfur; cobalt(II) nitrate In neat (no solvent) at 90℃; for 0.05h; Time; Microwave irradiation; | 83% |
With sodium acetate at 100℃; |
Conditions | Yield |
---|---|
With sodium azide; ammonium chloride In N,N-dimethyl-formamide at 120℃; for 14h; Inert atmosphere; | 94% |
With indium(III) chloride; sodium azide In water; isopropyl alcohol at 160℃; for 1h; Microwave irradiation; | 86% |
With sodium azide; triethylamine hydrochloride In N,N-dimethyl-formamide at 130℃; for 2h; Microwave irradiation; Inert atmosphere; | 81% |
Conditions | Yield |
---|---|
With ammonia; hydrogen; catalyst A In mata-xylene at 80 - 110℃; Conversion of starting material; | A 93.1% B 5.5% |
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