Dayang Chem (Hangzhou) Co.,Ltd.
Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:2237-30-1
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquirySimagchem Corporation
Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:2237-30-1
Min.Order:0 Metric Ton
Negotiable
Type:Manufacturers
inquiryHenan Allgreen Chemical Co.,Ltd
high quality Appearance:White or off white powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
Chemwill Asia Co., Ltd.
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:2237-30-1
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryHenan Wentao Chemical Product Co., Ltd.
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Changchun Artel lmport and Export trade company
Product Detail Minimum Order Qty. 10 Gram
Cas:2237-30-1
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryHangzhou J&H Chemical Co., Ltd.
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:2237-30-1
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryHenan Tianfu Chemical Co., Ltd.
M-aminobenzonitrile properties Melting point 48-53 ° C (lit.) Boiling point 288-290 ° C Flash point 112 ° C CAS database 2237-30-1 (CAS DataBase Reference) NIST Chemical Information Benzonitrile, 3-amino- (2237-30-1) The use
Siwei Development Group Ltd.
Product name: 3-Aminobenzonitrile CAS No.：2237-30-1 Molecule Formula：C7H6N2 Molecule Weight：118.14 Purity: 99.0% Package: 25kg/drum Description：Slight yellow crystalline powder Manufacture Standards：Enterprise Standard
Cas:2237-30-1
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryWuhan Fortuna Chemical Co.,Ltd
CAS:2237-30-1 EINECS:218-800-5 MW:118.14 MF:C7H6N2 Melting point:48-53 °C(lit.) Boiling point:288-290 °C Appearance:White crystalline powder Package:25kg/drum Transportation:by sea/air/courier Port:Shanghai
Hangzhou Huarong Pharm Co., Ltd.
Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
Hangzhou Zhongqi chem Co.,Ltd.
Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and h
Hunan chemfish Pharmaceutical co.,Ltd
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
HANGZHOU YUNUO CHEMICAL CO.,LTD
Superior quality, moderate price & quick delivery. Appearance:BROWN CRYSTALLINE SOLID Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:as per your request Application:Used as Pharmaceutical Intermediates,ect. T
Kono Chem Co.,Ltd
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
GIHI CHEMICALS CO.,LIMITED
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
JINHUA HUAYI CHEMICAL CO., LTD.
Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Cas:2237-30-1
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou Dingyan Chem Co., Ltd
R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates
Aecochem Corp.
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Cartoon Ingredients Co., Ltd
Cartoon Ingredients Co.,Ltd.is located in NanJing, the capital of Jiangsu Province.with Convenient traffic As a manufacturer, the company mainly engaged in providing Food ingredients, Herbal extracts, Vitamins, APIs and Fine chemicals &a
Zhuozhou Wenxi import and Export Co., Ltd
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:2237-30-1
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiryAntimex Chemical Limied
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Hunan Russell Chemicals Technology Co.,Ltd
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
AstaTech ( Chengdu) BioPharmaceutical Corp.
Quality assurance, stable process and affordable priceAppearance:detailed see specifications Storage:enquiry Package:according to the clients requirement Application:Pharmaceutical intermediates Transportation:Normal Port:chengdu
Bide Pharmatech Ltd
Our mission is to provide high-quality and innovative products to our customers. By offering a broad range of products, custom synthesis and personalized services, Bide can help scientists speeding up their research in the chemical and pharmaceutical
Amadis Chemical Co., Ltd.
1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
Cas:2237-30-1
Min.Order:10 Milligram
Negotiable
Type:Lab/Research institutions
inquirySynthetic route
| Conditions | Yield |
|---|---|
| With iron(III)-acetylacetonate; hydrazine hydrate In methanol at 150℃; Microwave irradiation; Green chemistry; | 99% |
| With iron(III)-acetylacetonate; hydrazine hydrate In methanol at 150℃; for 0.0333333h; Microwave irradiation; chemoselective reaction; | 99% |
| With maghemite; methylhydrazine In ethanol at 60℃; for 0.2h; Sealed tube; Inert atmosphere; chemoselective reaction; | 99% |
| Conditions | Yield |
|---|---|
| With [(2-di-tert-butylphosphino-2′,4′,6′-triisopropyl-1, 1′-biphenyl)-2-(2′-amino-1,1′-biphenyl)] palladium(II) methanesulfonate In tetrahydrofuran; water at 20℃; for 18h; Inert atmosphere; | 98% |
-
-
2237-30-1
m-cyanoaniline
| Conditions | Yield |
|---|---|
| With hydrogen; palladium dihydroxide In ethanol; ethyl acetate at 20℃; for 2.16667h; Hydrogenolysis; | 97% |
| Conditions | Yield |
|---|---|
| With aluminum oxide; hydroxylamine hydrochloride; methanesulfonyl chloride at 100℃; for 0.333333h; | 97% |
| Multi-step reaction with 2 steps 1: NH2OH*HCl; ZnO / Heating 2: 90 percent / CH3COCl; ZnO / 0.33 h / Heating View Scheme |
-
-
69113-59-3
3-iodobenzonitrile
-
-
2237-30-1
m-cyanoaniline
| Conditions | Yield |
|---|---|
| With copper(l) iodide; ammonia; potassium carbonate; L-proline In water; dimethyl sulfoxide at 25℃; for 24h; Inert atmosphere; | 97% |
| Conditions | Yield |
|---|---|
| Stage #1: 3-cyanobromobenzene With 2,2,2-trifluoroacetamide; potassium carbonate; N,N`-dimethylethylenediamine; copper(l) iodide In 1,4-dioxane at 75℃; Stage #2: With methanol In 1,4-dioxane at 75℃; Further stages.; | 95% |
| With ammonium hydroxide; copper(l) iodide; phosphate potassium salt In N,N-dimethyl-formamide at 20℃; for 48h; Inert atmosphere; | 50% |
| Stage #1: 3-cyanobromobenzene With polystyrene Rink amine resin; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0) In 1,4-dioxane; tert-butyl alcohol at 80℃; for 20h; Stage #2: In dichloromethane for 0.75h; Further stages.; | |
| With sodium azide; copper; L-proline In water; dimethyl sulfoxide at 150℃; under 37503.8 Torr; for 0.583333h; Flow reactor; chemoselective reaction; |
| Conditions | Yield |
|---|---|
| With 2-[2-(dicyclohexylphosphino)-phenyl]-1-methyl-1H-indole; palladium diacetate; sodium carbonate; triethylamine In water; acetonitrile at 70℃; for 18h; | 95% |
| With C42H58NO3PPdS(2-); potassium acetate; tert-butyl XPhos In 1,4-dioxane; water at 100℃; for 1h; Inert atmosphere; Sealed tube; | 91% |
| Conditions | Yield |
|---|---|
| With Aloe vera mediated silver nanoparticles In water at 50℃; for 0.5h; Green chemistry; | 95% |
-
-
31656-78-7
3-azidobenzonitrile
-
-
2237-30-1
m-cyanoaniline
| Conditions | Yield |
|---|---|
| With (1,4-diazabicyclo{2.2.2}-octane)zinc(II) tetrahydoborate In tetrahydrofuran for 2.4h; Heating; | 94% |
| With Zn(BH4)2(Ph3P)2 In tetrahydrofuran for 1h; Reduction; | 93% |
| With Ca(BH2S3)2 In tetrahydrofuran for 0.8h; Reduction; Heating; | 90% |
| With formic acid; 2,6-dimethyl-pyridine-3,5-dicarboxylic acid diethyl ester; N-ethyl-N,N-diisopropylamine In acetonitrile at 25℃; for 12h; Irradiation; | 91 %Chromat. |
| Conditions | Yield |
|---|---|
| With lead acetate In dichloromethane for 12h; Reflux; | 93% |
| With thionyl chloride In toluene at 90 - 100℃; Temperature; Solvent; | 91.3% |
| With 3 Angstroem melecular sieves at 180 - 500℃; under 0.005 Torr; for 0.5h; Pyrolysis; | 79% |
| Stage #1: 3-Aminobenzamide With C39H45N2 In acetonitrile at 20℃; Schlenk technique; Glovebox; Inert atmosphere; Stage #2: With phenylsilane In acetonitrile at 20℃; for 12h; Schlenk technique; Inert atmosphere; Sealed tube; | 40% |
| Conditions | Yield |
|---|---|
| With C68H64Cl2N6P2Ru2(4+)*2F6P(1-)*2Cl(1-); caesium carbonate In N,N-dimethyl-formamide at 100℃; for 24h; Inert atmosphere; Green chemistry; | 92.8% |
| With HRu(1,3-bis(6'-methyl-2'-pyridylimino)isoindoline)(PPh3)2 In toluene at 110℃; for 24h; Inert atmosphere; Glovebox; chemoselective reaction; | 54% |
| Conditions | Yield |
|---|---|
| With 2-(2-methoxyphenyl)-1-methyl-3-(diphenylphosphino)-1H-indole; potassium tert-butylate; triethylamine; bis(dibenzylideneacetone)-palladium(0) In dichloromethane; water; acetonitrile at 50℃; for 24h; Inert atmosphere; | 91% |
| With sodium carbonate In water; N,N-dimethyl-formamide at 120℃; for 15h; | 87% |
| Conditions | Yield |
|---|---|
| With graphitic carbon nitride; hydrazine hydrate In water at 80℃; for 20h; Irradiation; Sealed tube; Green chemistry; chemoselective reaction; | A 91% B 9% |
| Conditions | Yield |
|---|---|
| With acetyl chloride; zinc(II) oxide for 0.333333h; Heating; | 90% |
| Conditions | Yield |
|---|---|
| With ferrous(II) sulfate heptahydrate; CH5NO3S*CHF3O3S at 60℃; for 2h; | 89% |
| Multi-step reaction with 2 steps 1: concentrated sulfuric acid; KNO3 2: tin dichloride; concentrated hydrochloric acid View Scheme |
-
-
2237-30-1
m-cyanoaniline
| Conditions | Yield |
|---|---|
| With ammonium hydroxide; copper(ll) sulfate pentahydrate; sodium hydroxide In water at 25℃; for 24h; | 88% |
-
-
26177-43-5
3-nitrobenzylamine hydrochloride
-
-
2237-30-1
m-cyanoaniline
| Conditions | Yield |
|---|---|
| With caesium carbonate In N,N-dimethyl-formamide at 100℃; for 24h; Inert atmosphere; | 87% |
| Conditions | Yield |
|---|---|
| With 2-[2-(dicyclohexylphosphino)-phenyl]-1-methyl-1H-indole; palladium diacetate; potassium carbonate In water; tert-butyl alcohol at 80℃; for 18h; Inert atmosphere; | 85% |
| Conditions | Yield |
|---|---|
| With C46H71Cl3N2Pd; ammonia; sodium t-butanolate In 1,4-dioxane at 80℃; for 4h; Inert atmosphere; Schlenk technique; | A n/a B 85% |
| Conditions | Yield |
|---|---|
| With sodium carbonate In N,N-dimethyl-formamide at 120℃; for 5h; | 79% |
| Conditions | Yield |
|---|---|
| With ammonium cerium (IV) nitrate; copper(II) bis(trifluoromethanesulfonate); potassium carbonate at 130℃; for 24h; | 78% |
-
-
54060-30-9
3-acetylenephenylamine
-
-
2237-30-1
m-cyanoaniline
| Conditions | Yield |
|---|---|
| With trimethylsilylazide; silver carbonate In dimethyl sulfoxide at 100℃; for 12h; | 77% |
| Conditions | Yield |
|---|---|
| Stage #1: potassium cyanide With acetic acid In ethylene glycol at 20℃; Sealed tube; Stage #2: m-Bromoaniline With P(t-Bu)3 Palladacycle Gen. 3; potassium acetate In 1,4-dioxane; water at 60℃; for 16h; Sealed tube; | 77% |
-
-
585-79-5
3-Bromonitrobenzene
-
-
75-86-5
2-hydroxy-2-methylpropanenitrile
-
A
-
98-95-3
nitrobenzene
-
B
-
2237-30-1
m-cyanoaniline
-
C
-
619-24-9
3-nitrobenzonitrile
| Conditions | Yield |
|---|---|
| Stage #1: m-nitrobromobenzene With copper(l) iodide; 1,10-Phenanthroline; potassium iodide In N,N-dimethyl-formamide at 110℃; for 6h; Stage #2: 2-hydroxy-2-methylpropanenitrile With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 110℃; for 60h; | A 10.0 % Chromat. B 3.5 % Chromat. C 75% |
| Conditions | Yield |
|---|---|
| With [Pd(cinnamyl)Cl]2; N-ethyl-N,N-diisopropylamine; XPhos In butan-1-ol at 100℃; for 2h; Inert atmosphere; | 73% |
-
-
66152-74-7
3-<(trifluoromethanesulfonyl)oxy>benzonitrile
-
-
2237-30-1
m-cyanoaniline
| Conditions | Yield |
|---|---|
| Stage #1: 3-<(trifluoromethanesulfonyl)oxy>benzonitrile With bis(bis(trimethylsilyl)amido)zinc(II); tri-tert-butyl phosphine; tetrabutylammomium bromide; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran at 50℃; for 12h; Stage #2: With hydrogenchloride In tetrahydrofuran; diethyl ether | 70% |
| Conditions | Yield |
|---|---|
| With L-proline In N,N-dimethyl-formamide at 120℃; for 45h; Rosenmund-von Braun reaction; | 69% |
| Conditions | Yield |
|---|---|
| With 1,3,5-trichloro-2,4,6-triazine; palladium on activated charcoal; potassium carbonate; triphenylphosphine at 25 - 130℃; for 12.1667h; | 69% |
| Conditions | Yield |
|---|---|
| With C18H14CuIN4 In acetonitrile at 20℃; for 24h; Inert atmosphere; Sealed tube; UV-irradiation; | 63% |
| Conditions | Yield |
|---|---|
| With sodium cyanoborohydride In acetonitrile at 20℃; for 2h; | 100% |
| With sodium cyanoborohydride; acetic acid In tetrahydrofuran at 23 - 50℃; for 18h; Inert atmosphere; | 95% |
| With sodium cyanoborohydride; acetic acid In acetonitrile for 2h; | 94% |
| With sodium cyanoborohydride; acetic acid In water; acetonitrile for 2.5h; Ambient temperature; | 94% |
| With sodium cyanoborohydride In water; acetonitrile at 0 - 20℃; for 4h; | 92.9% |
| Conditions | Yield |
|---|---|
| With dihydrogen peroxide; hexadecyltrimethylammonium methanesulfonate; sodium hydroxide In water at 25℃; for 1h; | 100% |
| With Amberlyst A-26 (OH- form); dihydrogen peroxide In methanol at 20℃; for 1.7h; Hydrolysis; | 95% |
| With water at 150℃; under 5171.62 - 6205.94 Torr; for 0.5h; Inert atmosphere; Microwave irradiation; | 94% |
| Conditions | Yield |
|---|---|
| With hydrogen; palladium on activated charcoal In methanol | 100% |
| With C28H29Cl2CoNP2; hydrogen; sodium triethylborohydride In 1,4-dioxane at 80℃; under 37503.8 Torr; for 6h; | 75% |
| In methanol; palladium-carbon | 0.516 g (~100%) |
-
-
2237-30-1
m-cyanoaniline
| Conditions | Yield |
|---|---|
| Stage #1: m-cyanoaniline With hydrogenchloride; sodium nitrite In water at 0℃; for 0.5h; Stage #2: With hydrogenchloride; tin(ll) chloride In water at 0℃; for 2h; | 100% |
| Stage #1: m-cyanoaniline With hydrogenchloride; sodium nitrite Stage #2: With hydrogenchloride; tin(ll) chloride | 78% |
| Stage #1: m-cyanoaniline With hydrogenchloride; sodium nitrite In water at 0 - 5℃; for 1h; Stage #2: With hydrogenchloride; tin(II) chloride dihdyrate In water at 0 - 20℃; for 2h; | |
| Stage #1: m-cyanoaniline With hydrogenchloride; sodium nitrite In water for 0.25h; Cooling with ice; Stage #2: With tin(ll) chloride In water for 1h; Cooling with ice; | 118 mg |
| Conditions | Yield |
|---|---|
| In 2-methoxy-ethanol at 100 - 110℃; for 3h; | 100% |
-
-
15568-85-1
5-methoxymethylene-2,2-dimethyl-1,3-dioxane-4,6-dione
-
-
2237-30-1
m-cyanoaniline
-
-
1186230-83-0
3-(((2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-ylidene)methyl)amino)benzonitrile
| Conditions | Yield |
|---|---|
| In acetonitrile at 20℃; for 0.25h; | 100% |
-
-
32315-10-9
bis(trichloromethyl) carbonate
-
-
1400997-47-8
(+)-(R)-2-(4-amino-3-fluorophenyl)-morpholine-4-carboxylic acid tert-butyl ester
-
-
2237-30-1
m-cyanoaniline
-
-
1415757-41-3
(R)-2-{4-[3-(3-cyano-phenyl)-ureido]-3-fluoro-phenyl}-morpholine-4-carboxylic acid tert-butyl ester
| Conditions | Yield |
|---|---|
| Stage #1: bis(trichloromethyl) carbonate; (+)-(R)-2-(4-amino-3-fluorophenyl)-morpholine-4-carboxylic acid tert-butyl ester With sodium carbonate In dichloromethane; water at 20℃; for 2.5h; Stage #2: m-cyanoaniline In dichloromethane; water at 20℃; for 2h; | 100% |
| Stage #1: bis(trichloromethyl) carbonate; (+)-(R)-2-(4-amino-3-fluorophenyl)-morpholine-4-carboxylic acid tert-butyl ester With sodium carbonate In dichloromethane; water at 20℃; for 2.5h; Stage #2: m-cyanoaniline In dichloromethane; water at 20℃; for 2h; | 100% |
-
-
32315-10-9
bis(trichloromethyl) carbonate
-
-
1400997-62-7
tert-butyl (RS)-2-(4-amino-3-chlorophenyl)morpholine-4-carboxylate
-
-
2237-30-1
m-cyanoaniline
-
-
1415757-42-4
tert-butyl (RS)-2-(3-chloro-4-(3-(3-cyanophenyl)ureido)phenyl)morpholine-4-carboxylate
| Conditions | Yield |
|---|---|
| Stage #1: bis(trichloromethyl) carbonate; tert-butyl (RS)-2-(4-amino-3-chlorophenyl)morpholine-4-carboxylate With sodium carbonate In dichloromethane; water at 20℃; for 2.5h; Stage #2: m-cyanoaniline In dichloromethane; water at 20℃; for 2h; | 100% |
| Stage #1: bis(trichloromethyl) carbonate; tert-butyl (RS)-2-(4-amino-3-chlorophenyl)morpholine-4-carboxylate With sodium carbonate In dichloromethane; water at 20℃; for 2.5h; Stage #2: m-cyanoaniline In dichloromethane; water at 20℃; for 2h; | 100% |
-
-
1267993-72-5
4-chloro-7-isothiocyanato-7-de(acetamide)colchicine
-
-
2237-30-1
m-cyanoaniline
-
-
1267990-93-1
4-chloro-N-[(3-cyanophenyl)thiocarbamoyl]deacetyl colchicine
| Conditions | Yield |
|---|---|
| In dichloromethane at 0 - 20℃; Inert atmosphere; | 100% |
| Conditions | Yield |
|---|---|
| In ethanol; water at 150℃; for 1h; Microwave irradiation; | 100% |
-
-
2237-30-1
m-cyanoaniline
-
-
73183-34-3
bis(pinacol)diborane
-
-
214360-46-0
3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzonitrile
| Conditions | Yield |
|---|---|
| With tert.-butylnitrite In acetonitrile at 0 - 80℃; for 2h; | 99.8% |
| With tert.-butylnitrite In acetonitrile at 0 - 80℃; for 2h; | 99.8% |
| With tert.-butylnitrite In acetonitrile at 80℃; for 2h; | 64% |
| With tert-butyl nitrite; benzoyl peroxide In acetonitrile MeCN, (CN)C6H4NH2 (1 mmol) and tBuONO (1.5 mmol) added to B2pin2 (1.2 mmol) and benzoyl peroxide (0.01 mmol), mixt. stirred at room temp. for 2 h; soln. concd. (under reduced pressure), residue chromd.; | 22% |
-
-
124-63-0
methanesulfonyl chloride
-
-
2237-30-1
m-cyanoaniline
-
-
50790-30-2
N-(3-cyanophenyl)methanesulfonamide
| Conditions | Yield |
|---|---|
| With pyridine In dichloromethane at 0 - 20℃; for 4h; | 99% |
| With pyridine In dichloromethane at 0 - 20℃; for 4h; | 99% |
| Conditions | Yield |
|---|---|
| With triethylamine In dichloromethane at 20℃; for 0.5h; | 99% |
| Conditions | Yield |
|---|---|
| With [(9,9-Me2-4,5-(PPh2)2-xanthene]Pd(η3-allyl)Cl In tetrahydrofuran at 25℃; for 24h; | 99% |
| Conditions | Yield |
|---|---|
| With sodium hydroxide In neat (no solvent) at 80℃; for 0.5h; | 99% |
| With tetrakis(μ2-α-methacrylate-O,O')-bis(H2O)-dicopper(II); sodium acetate at 80℃; for 5h; Neat (no solvent); | 84% |
| Conditions | Yield |
|---|---|
| In acetonitrile for 0.166667h; Milling; Green chemistry; | 99% |
-
-
2237-30-1
m-cyanoaniline
-
-
58202-84-9
N-(3-cyanophenyl)acetamide
| Conditions | Yield |
|---|---|
| With acetic anhydride In methanol at 20℃; for 1h; | 98.52% |
-
-
2237-30-1
m-cyanoaniline
-
-
1005-56-7
phenylcarbonochloridothioate
-
-
302577-09-9
((3-cyanophenyl)amino)phenoxymethane-1-thione
| Conditions | Yield |
|---|---|
| In tetrahydrofuran at 20℃; for 0.5h; Condensation; | 98% |
-
-
2237-30-1
m-cyanoaniline
-
-
31656-78-7
3-azidobenzonitrile
| Conditions | Yield |
|---|---|
| Stage #1: m-cyanoaniline With hydrogenchloride In water at 0 - 5℃; Stage #2: With sodium nitrite In water Stage #3: With sodium azide In water at 0 - 5℃; for 1h; Further stages.; | 98% |
| Stage #1: m-cyanoaniline With hydrogenchloride; sodium nitrite In methanol; water at 0℃; for 0.333333h; Stage #2: With sodium azide In methanol; water at 20℃; for 2h; | 90% |
| Stage #1: m-cyanoaniline With hydrogenchloride; sodium nitrite In water Stage #2: With sodium azide In water at 0 - 5℃; for 24h; | 85% |
| Conditions | Yield |
|---|---|
| With 2-amino-4(3H)-quinazolinone; phenylsilane; acetic acid In neat (no solvent) at 20℃; for 5h; Green chemistry; | 98% |
| With copper(I) iodide; phenylsilane In ethanol at 80℃; for 4h; | 85% |
-
-
2237-30-1
m-cyanoaniline
-
-
177533-37-8
2-amino-6-O-(p-toluenesulfonyl)-9-[2-deoxy-3,5-di-O-(tert-butyldimethylsilyl)-β-D-ribofuranosyl]purine
| Conditions | Yield |
|---|---|
| With palladium diacetate; potassium phosphate; DavePhos In 1,4-dioxane; tert-butyl alcohol at 110℃; for 0.5h; | 97% |
-
-
87-13-8
diethyl 2-ethoxymethylenemalonate
-
-
2237-30-1
m-cyanoaniline
-
-
59551-10-9
diethyl 2-[((3-cyanophenyl)amino)methylene]malonate
| Conditions | Yield |
|---|---|
| at 110℃; for 0.75h; | 97% |
| In toluene at 110℃; | 95% |
| at 80℃; for 1h; |
| Conditions | Yield |
|---|---|
| With potassium carbonate; potassium iodide In acetonitrile for 6h; Heating / reflux; | 97% |
| With sodium carbonate In N,N-dimethyl-formamide at 70℃; for 5h; | 76% |
-
-
2033-24-1
cycl-isopropylidene malonate
-
-
122-51-0
orthoformic acid triethyl ester
-
-
2237-30-1
m-cyanoaniline
-
-
1186230-83-0
3-(((2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-ylidene)methyl)amino)benzonitrile
| Conditions | Yield |
|---|---|
| In ethanol at 90℃; for 2h; | 97% |
| In ethanol for 2h; Reflux; | 87% |
| Conditions | Yield |
|---|---|
| With acetic anhydride | 96.3% |
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