DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:626-67-5
Min.Order:1 Kilogram
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Cas:626-67-5
Min.Order:5 Kiloliter
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Type:Manufacturers
inquiryProduct name N-Methylpiperidine CAS 626-67-5 Synonyms 1-METHYLPIPERDINE;N-METHYL PIPERIDINE 1-METHYL-PIPERIDINE;N-Methylpiperidine,99%;N-Methylpiperidine, 99% 250ML;1-METHYLPIPER
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Cas:626-67-5
Min.Order:100 Kilogram
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Type:Trading Company
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Min.Order:0 Metric Ton
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inquiryProduct name: N-Methylpiperidine CAS No.:626-67-5 Molecule Formula:C6H14N Molecule Weight:100.18 Purity: 99.0% Package: 200kg/drum Description:Colorless liquid Manufacture Standards:Enterprise Standard TESTING ITEM
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Min.Order:1 Kilogram
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inquiryN-Methylpiperidine Basic information Product Name: N-Methylpiperidine Synonyms: 1-METHYLPIPERIDINE;N-METHYLPIPERIDINE;NMPPR;N-MEPIP;1-methyl-piperidin;lk20;Piperidi
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Min.Order:10 Gram
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Conditions | Yield |
---|---|
With P(C4H9)3; ruthenium trichloride at 220℃; for 5h; Product distribution; Mechanism; also with or without other catalyst, other phosphines, other temperatures,; | 100% |
chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II) at 100℃; for 3h; | 100% |
Pt on TiO2 for 20h; Ambient temperature; Irradiation; | 93.4% |
N-methyl-3,4-didehydropiperidine
carbon monoxide
N-methylcyclohexylamine
Conditions | Yield |
---|---|
With hydrogen; di-μ-chlorobis(norbornadiene)dirhodium(I) In benzene at 100℃; under 60004.8 Torr; for 6h; | 100% |
Conditions | Yield |
---|---|
With 1,1,3,3-Tetramethyldisiloxane; [((CH3)5C5)IrCl((CH3)2NC6H3C5H4N)]; trityl tetrakis(pentafluorophenyl)borate In 1,1,2,2-tetrachloroethane at 100℃; for 6h; Inert atmosphere; Schlenk technique; Glovebox; chemoselective reaction; | 99% |
With phenylsilane; caesium carbonate at 25℃; for 30h; Schlenk technique; | 51% |
With lithium aluminium tetrahydride; diethyl ether |
Conditions | Yield |
---|---|
With 3 % platinum on carbon; hydrogen; toluene-4-sulfonic acid at 120℃; under 30003 Torr; for 3h; Reagent/catalyst; Inert atmosphere; Autoclave; | 99% |
Conditions | Yield |
---|---|
With acetic acid at 30℃; for 2h; | 98% |
With diiodo(p-cymene)ruthenium(II) dimer In water at 60℃; for 2h; | 95% |
Stage #1: piperidine; formaldehyd With hydrogenchloride In methanol at 20℃; Stage #2: With N-methylpiperidine zinc borohydride In methanol at 20℃; for 0.1h; | 89% |
Conditions | Yield |
---|---|
at 106℃; for 1h; | A n/a B 96% |
Conditions | Yield |
---|---|
With methylamine | 95% |
1,1'-Dimethyl-3-(2'-piperidyl)-1,4,5,6-tetrahydropyridin
A
N-methylcyclohexylamine
B
1-methylpiperidin-2-one
C
1-Methyl-3-(5-methylamino-pentyliden)piperidin
Conditions | Yield |
---|---|
With hydrogenchloride; sodium tetrahydroborate In ethanol for 18h; | A n/a B n/a C 88% |
n-decyl magnesium bromide
benzophenone N-methyl-N,N-pentane-1,5-diylhydrazonium iodide
A
N-methylcyclohexylamine
B
Benzophenone imine
C
decane
D
icosane
E
1-Decene
Conditions | Yield |
---|---|
In diethyl ether Product distribution; Mechanism; Heating; other quaternary hydrazonium salts, other alkylmagnesium halides; | A 85% B 84% C 51% D 21% E 25% |
Conditions | Yield |
---|---|
Ambient temperature; | 82% |
N-methylpiperidine-N-oxide
N-methylcyclohexylamine
Conditions | Yield |
---|---|
With titanium tetrachloride; sodium iodide In acetonitrile at 20℃; for 0.0833333h; | 81% |
Erhitzen; |
Conditions | Yield |
---|---|
With 5 wt% Pd/C; hydrogen; 1-butyl-3-methylimidazolium Tetrafluoroborate at 160℃; under 75007.5 Torr; for 6h; Autoclave; | 81% |
Conditions | Yield |
---|---|
With 5 wt% Pd/C; hydrogen; 1-butyl-3-methylimidazolium Tetrafluoroborate at 160℃; under 75007.5 Torr; for 6h; Autoclave; | 77% |
With diphenylsilane; cesium formate In acetonitrile at 50℃; under 750.075 Torr; for 6h; Green chemistry; | 64% |
With iron(II) tetrafluoroborate hexahydrate; phenylsilane; tris(2-diphenylphosphinoethyl)phosphine In tetrahydrofuran at 100℃; under 750.075 - 2250.23 Torr; for 24h; Reagent/catalyst; Schlenk technique; Inert atmosphere; Glovebox; Sealed tube; | 15% |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran for 0.5h; Heating; | 76% |
piperidine
O-methyl adamantane-1-carbothioate
A
N-methylcyclohexylamine
Conditions | Yield |
---|---|
for 0.5h; Heating; | A n/a B 12% C 69% |
O-methyl adamantane-1-carbothioate
A
N-methylcyclohexylamine
Conditions | Yield |
---|---|
With piperidine for 0.5h; Heating; | A n/a B 12% C 69% |
N-Cyan-N-(2,6-dimethylphenyl)-α-alaninmethylester
A
N-methylcyclohexylamine
B
N-(2,6-Dimethylphenyl)-5-methyl-imidazolidin-2,4-dion
Conditions | Yield |
---|---|
With piperidine at 100℃; for 3h; | A n/a B 64% |
sodium tetrahydroborate
A
N-methylcyclohexylamine
B
tri-n-butyl-tin hydride
Conditions | Yield |
---|---|
In diethyl ether boiling (stirring, 4 h); water addn., separation of org. phase, drying over CaCl2, solvent evapn., distn. (vacuum); | A n/a B 60% |
N-methyl-3,4-didehydropiperidine
carbon monoxide
A
N-methylcyclohexylamine
B
N-methyl-piperidine-4-carboxaldehyde
C
1-methylpiperidine-3-carboxaldehyde
Conditions | Yield |
---|---|
With hydrogen; carbonylhydridetris(triphenylphosphine)rhodium(I) In benzene at 100℃; under 60004.8 Torr; for 6h; | A 2% B 59% C 39% |
With hydrogen; di-μ-chlorobis(norbornadiene)dirhodium(I); triphenylphosphine In benzene at 100℃; under 60004.8 Torr; for 6h; Product distribution; various catalysts, formed in situ from various phosphines; | A 3% B 56% C 41% |
sodium tetrahydroborate
triethyltin N,N-pentamethylenecarbamate
A
N-methylcyclohexylamine
B
triethylstannane
Conditions | Yield |
---|---|
In diethyl ether boiling (stirring, 3 h); water addn., separation of org. phase, drying over CaCl2, solvent evapn., distn. (vacuum); | A n/a B 56% |
Conditions | Yield |
---|---|
With copper diacetate In dichloromethane for 24h; Ambient temperature; | 49% |
1-isopropyl-1-methyl-piperidinium; iodide
A
N-isopropylpiperidine
B
N-methylcyclohexylamine
Conditions | Yield |
---|---|
With sodium thiophenolate In acetonitrile; butanone Heating; | A 45% B 30% |
Conditions | Yield |
---|---|
With copper diacetate In dichloromethane for 24h; Ambient temperature; | 31% |
Conditions | Yield |
---|---|
With diethyl ether; phenyllithium anschliessend mit Methyljodid; | |
Multi-step reaction with 2 steps 1: 1-butyl-3-methylimidazolium chloride; hydrogen; 5 wt% Pd/C / 6 h / 160 °C / 75007.5 Torr / Autoclave 2: hydrogen; 5 wt% Pd/C; potassium tert-butylate; 1-butyl-3-methylimidazolium Tetrafluoroborate / 8 h / 160 °C / 45004.5 Torr / Autoclave View Scheme | |
Multi-step reaction with 2 steps 1: 1-hexyl-3-methylimidazolium tetrafluoroborate; hydrogen; 5 wt% Pd/C / 6 h / 160 °C / 75007.5 Torr / Autoclave 2: hydrogen; 5 wt% Pd/C; potassium tert-butylate; 1-butyl-3-methylimidazolium Tetrafluoroborate / 8 h / 160 °C / 45004.5 Torr / Autoclave View Scheme |
Conditions | Yield |
---|---|
With methanol; kieselguhr; nickel at 220℃; under 58840.6 Torr; Hydrogenation; | |
Multi-step reaction with 2 steps 1: ethanol / 6 h / 80 °C / 3750.38 Torr 2: hydrogen / 12 h / 130 °C / 45004.5 Torr View Scheme | |
Multi-step reaction with 2 steps 1: hydrogen; 5 wt% Pd/C; 1-butyl-3-methylimidazolium Tetrafluoroborate / 6 h / 120 °C / 37503.8 Torr / Autoclave 2: piperidine; hydrogen; 5 wt% Pd/C; 1-butyl-3-methylimidazolium Tetrafluoroborate / 12 h / 160 °C / 45004.5 Torr View Scheme | |
Multi-step reaction with 3 steps 1: hydrogen; 5 wt% Pd/C; 1-butyl-3-methylimidazolium Tetrafluoroborate / 6 h / 120 °C / 37503.8 Torr / Autoclave 2: N-methylcyclohexylamine; hydrogen; 5 wt% Pd/C; 1-butyl-3-methylimidazolium Tetrafluoroborate / 8 h / 160 °C / 45004.5 Torr / Autoclave 3: hydrogen; 5 wt% Pd/C; potassium tert-butylate; 1-butyl-3-methylimidazolium Tetrafluoroborate / 8 h / 160 °C / 45004.5 Torr / Autoclave View Scheme |
Conditions | Yield |
---|---|
at 60℃; elektrochemische Reduktion an einer Cadmium-Kathode; |
N-methyladipinimide
N-methylcyclohexylamine
Conditions | Yield |
---|---|
With tetrahydrofuran; sodium aluminum tetrahydride | |
With lithium aluminium tetrahydride; diethyl ether |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride; diethyl ether |
N-methylcyclohexylamine
2-iodo-propane
1-isopropyl-1-methyl-piperidinium; iodide
Conditions | Yield |
---|---|
In chloroform at 60℃; for 8h; | 100% |
In chloroform Heating; |
N-methylcyclohexylamine
1-iodo-butane
1-butyl-1-methylpiperidinium iodide
Conditions | Yield |
---|---|
In chloroform at 60℃; for 6h; | 100% |
In chloroform Heating; |
Conditions | Yield |
---|---|
100% |
N-methylcyclohexylamine
propyl bromide
1-propyl-1-methyl-piperidinium bromide
Conditions | Yield |
---|---|
In chloroform at 60℃; for 6h; | 100% |
In ethyl acetate at 20℃; for 12h; Solvent; | 98% |
In chloroform Heating; |
Conditions | Yield |
---|---|
In toluene Heating; | 100% |
N-methylcyclohexylamine
triethylene glycol di-(p-toluenesulfonate)
Conditions | Yield |
---|---|
In acetonitrile for 72h; Reflux; | 100% |
N-methylcyclohexylamine
2-(2-(2-methoxyethoxy)ethoxy)ethyl p-toluenesulfonate
1-(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-1-methylpiperidinium p-toluenesulfonate
Conditions | Yield |
---|---|
In acetonitrile at 90℃; for 24h; | 100% |
N-methylcyclohexylamine
[(copper(I)cyanide)(N-methylpiperidine)]
Conditions | Yield |
---|---|
In further solvent(s) suspn. of Cu complex in NMePipd heated in sealed tube under Ar to 70°C overnight, cooled; ppt. filtered off, washed with Et2O, air dried for 15 min; elem. anal.; | 99.3% |
In neat (no solvent) CuCN suspended in N-Me-piperidine in sealed tube under Ar; mixt. heated to 70°C in oil bath overnight without stirring; cooled; alternatively - vapor diffusion reaction; collected by filtration; washed with Et2O; air dried for 15 min; |
Conditions | Yield |
---|---|
In diethyl ether for 4h; Inert atmosphere; Cooling with ice; | 99% |
Conditions | Yield |
---|---|
In diethyl ether for 4h; Inert atmosphere; Cooling with ice; | 99% |
N-methylcyclohexylamine
Conditions | Yield |
---|---|
With ammonium hexafluorophosphate In ethanol for 1h; Reflux; | 99% |
Conditions | Yield |
---|---|
With tetrabenzyl titanium; trityl tetrakis(pentafluorophenyl)borate In toluene at 28℃; for 96h; Inert atmosphere; Sealed tube; Glovebox; regioselective reaction; | 99% |
Conditions | Yield |
---|---|
With P(C4H9)3; ruthenium trichloride at 220℃; for 5h; Product distribution; Mechanism; also with or without other catalyst, other phosphines, other temperatures,; | 100% |
chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II) at 100℃; for 3h; | 100% |
Pt on TiO2 for 20h; Ambient temperature; Irradiation; | 93.4% |
N-methyl-3,4-didehydropiperidine
carbon monoxide
N-methylcyclohexylamine
Conditions | Yield |
---|---|
With hydrogen; di-μ-chlorobis(norbornadiene)dirhodium(I) In benzene at 100℃; under 60004.8 Torr; for 6h; | 100% |
Conditions | Yield |
---|---|
With 1,1,3,3-Tetramethyldisiloxane; [((CH3)5C5)IrCl((CH3)2NC6H3C5H4N)]; trityl tetrakis(pentafluorophenyl)borate In 1,1,2,2-tetrachloroethane at 100℃; for 6h; Inert atmosphere; Schlenk technique; Glovebox; chemoselective reaction; | 99% |
With phenylsilane; caesium carbonate at 25℃; for 30h; Schlenk technique; | 51% |
With lithium aluminium tetrahydride; diethyl ether |
Conditions | Yield |
---|---|
With 3 % platinum on carbon; hydrogen; toluene-4-sulfonic acid at 120℃; under 30003 Torr; for 3h; Reagent/catalyst; Inert atmosphere; Autoclave; | 99% |
Conditions | Yield |
---|---|
With acetic acid at 30℃; for 2h; | 98% |
With diiodo(p-cymene)ruthenium(II) dimer In water at 60℃; for 2h; | 95% |
Stage #1: piperidine; formaldehyd With hydrogenchloride In methanol at 20℃; Stage #2: With N-methylpiperidine zinc borohydride In methanol at 20℃; for 0.1h; | 89% |
Conditions | Yield |
---|---|
at 106℃; for 1h; | A n/a B 96% |
Conditions | Yield |
---|---|
With methylamine | 95% |
1,1'-Dimethyl-3-(2'-piperidyl)-1,4,5,6-tetrahydropyridin
A
N-methylcyclohexylamine
B
1-methylpiperidin-2-one
C
1-Methyl-3-(5-methylamino-pentyliden)piperidin
Conditions | Yield |
---|---|
With hydrogenchloride; sodium tetrahydroborate In ethanol for 18h; | A n/a B n/a C 88% |
n-decyl magnesium bromide
benzophenone N-methyl-N,N-pentane-1,5-diylhydrazonium iodide
A
N-methylcyclohexylamine
B
Benzophenone imine
C
decane
D
icosane
E
1-Decene
Conditions | Yield |
---|---|
In diethyl ether Product distribution; Mechanism; Heating; other quaternary hydrazonium salts, other alkylmagnesium halides; | A 85% B 84% C 51% D 21% E 25% |
Conditions | Yield |
---|---|
Ambient temperature; | 82% |
N-methylpiperidine-N-oxide
N-methylcyclohexylamine
Conditions | Yield |
---|---|
With titanium tetrachloride; sodium iodide In acetonitrile at 20℃; for 0.0833333h; | 81% |
Erhitzen; |
Conditions | Yield |
---|---|
With 5 wt% Pd/C; hydrogen; 1-butyl-3-methylimidazolium Tetrafluoroborate at 160℃; under 75007.5 Torr; for 6h; Autoclave; | 81% |
Conditions | Yield |
---|---|
With 5 wt% Pd/C; hydrogen; 1-butyl-3-methylimidazolium Tetrafluoroborate at 160℃; under 75007.5 Torr; for 6h; Autoclave; | 77% |
With diphenylsilane; cesium formate In acetonitrile at 50℃; under 750.075 Torr; for 6h; Green chemistry; | 64% |
With iron(II) tetrafluoroborate hexahydrate; phenylsilane; tris(2-diphenylphosphinoethyl)phosphine In tetrahydrofuran at 100℃; under 750.075 - 2250.23 Torr; for 24h; Reagent/catalyst; Schlenk technique; Inert atmosphere; Glovebox; Sealed tube; | 15% |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran for 0.5h; Heating; | 76% |
piperidine
O-methyl adamantane-1-carbothioate
A
N-methylcyclohexylamine
Conditions | Yield |
---|---|
for 0.5h; Heating; | A n/a B 12% C 69% |
O-methyl adamantane-1-carbothioate
A
N-methylcyclohexylamine
Conditions | Yield |
---|---|
With piperidine for 0.5h; Heating; | A n/a B 12% C 69% |
N-Cyan-N-(2,6-dimethylphenyl)-α-alaninmethylester
A
N-methylcyclohexylamine
B
N-(2,6-Dimethylphenyl)-5-methyl-imidazolidin-2,4-dion
Conditions | Yield |
---|---|
With piperidine at 100℃; for 3h; | A n/a B 64% |
sodium tetrahydroborate
A
N-methylcyclohexylamine
B
tri-n-butyl-tin hydride
Conditions | Yield |
---|---|
In diethyl ether boiling (stirring, 4 h); water addn., separation of org. phase, drying over CaCl2, solvent evapn., distn. (vacuum); | A n/a B 60% |
N-methyl-3,4-didehydropiperidine
carbon monoxide
A
N-methylcyclohexylamine
B
N-methyl-piperidine-4-carboxaldehyde
C
1-methylpiperidine-3-carboxaldehyde
Conditions | Yield |
---|---|
With hydrogen; carbonylhydridetris(triphenylphosphine)rhodium(I) In benzene at 100℃; under 60004.8 Torr; for 6h; | A 2% B 59% C 39% |
With hydrogen; di-μ-chlorobis(norbornadiene)dirhodium(I); triphenylphosphine In benzene at 100℃; under 60004.8 Torr; for 6h; Product distribution; various catalysts, formed in situ from various phosphines; | A 3% B 56% C 41% |
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