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Cas:627-91-8
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This product is used as an intermediate in medicine and organic synthesis. Appearance:Colorless or light pink transparent liquid Storage:Kept in cool and dry place , far away from heat. Package:200kg PE drum Application:This product is used as an i
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Cas:627-91-8
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inquiryProduct Name Monomethyl adipate CAS No. 627-91-8 Appearance Colorless or slightly pink transparent liquid
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Product Name: Monomethyl adipate Synonyms: Hexanedioic acid hydrogen 1-methyl;Adipic acid monometh;MonoMethyl adipate, 98% 5GR;Adipic Acid Monomethyl Ester Methyl Hydrogen Adipate Monomethyl Hexanedioate Hexanedioic Acid Monomethyl Ester;Hexaned
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Min.Order:100 Gram
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
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Min.Order:1 Gram
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Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryProduct name: Adipic Acid Monomethyl Ester CAS No.: 627-91-8 Molecule Formula:C7H11O4 Molecule Weight:159.16 Purity: 99.0% Package: 200kg/drum Description:Colorless transparent liquid Manufacture Standards:Enterprise Standard
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Min.Order:1 Kilogram
Negotiable
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inquiryProduct Name: Monomethyl adipate Synonyms: Hexanedioic acid hydrogen 1-methyl;Adipic acid monometh;MonoMethyl adipate, 98% 5GR;Adipic acid 1-methyl ester;Adipic acid hydrogen 1-methyl;Adipic acid hydrogen 1-methyl ester;Hexanedioic acid 1-meth
Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
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Min.Order:1 Kilogram
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1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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inquiry2-Carboxy-hexanedioic acid 6-methyl ester
adipic acid monomethyl ester
Conditions | Yield |
---|---|
at 160 - 165℃; | 100% |
Conditions | Yield |
---|---|
With porcine liver esterase; sodium hydroxide; phosphate buffer for 6h; | 96% |
With sodium hydroxide; phosphate buffer for 1h; Ambient temperature; pig liver esterase; | 84% |
With potassium hydroxide In methanol; diethyl ether; acetonitrile at 0℃; for 54h; | 71% |
Conditions | Yield |
---|---|
With sulfonated poly-divinylbenzene-co-triallylamine at 24.84℃; for 10h; | 95% |
With acid | 32% |
With hydrogenchloride Heating; | |
With hydrogenchloride In water; toluene at 25 - 85℃; for 8.75h; | 109.6 g |
Conditions | Yield |
---|---|
95% | |
With Jones reagent In acetone at 0℃; for 1h; Inert atmosphere; | 80% |
With Iron(III) nitrate nonahydrate; oxygen In acetonitrile at 25℃; under 760.051 Torr; for 12h; Schlenk technique; | 65% |
adipic acid monomethyl ester
Conditions | Yield |
---|---|
With Iron(III) nitrate nonahydrate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium chloride; oxygen In 1,2-dichloro-ethane at 25℃; for 12h; | 94% |
methanol
Adipic acid
A
hexanedioic acid dimethyl ester
B
adipic acid monomethyl ester
Conditions | Yield |
---|---|
With nickel dichloride for 13h; Heating; | A 81% B 18% |
With aluminum oxide at 25℃; for 48h; Reagent/catalyst; Temperature; Time; Green chemistry; chemoselective reaction; | A 9% B 80% |
With carbonic acid dimethyl ester at 180℃; under 10343.2 Torr; for 5h; Solvent; Inert atmosphere; | A 40% B 60% |
3-iodopropanoic acid
acrylic acid methyl ester
adipic acid monomethyl ester
Conditions | Yield |
---|---|
With sodium tetrahydroborate; azobisisobutyronitrile; tributyltin chloride; sodium fluoride Mechanism; 1) EtOH, 20 deg C, 4 h, 2) H2O; other electrophilic olefins; | 76% |
With sodium tetrahydroborate; azobisisobutyronitrile; tributyltin chloride; sodium fluoride 1) EtOH, r.t., 4 h, 2) H2O; Yield given. Multistep reaction; |
O-methylcaprolactim
Adipic acid
A
caprolactam
B
adipic acid monomethyl ester
Conditions | Yield |
---|---|
at 80 - 85℃; for 16h; | A n/a B 72% |
Conditions | Yield |
---|---|
With chromium(VI) oxide; sulfuric acid In water; acetone for 0.666667h; Ambient temperature; | 46% |
hexanedioic acid dimethyl ester
ethanol
A
adipic acid monomethyl ester
B
diethyl adipate
C
adipic acid ethyl methyl ester
Conditions | Yield |
---|---|
With water; hydrogen In methanol under 37503.8 Torr; | A 11.2% B 43.5% C 40.5% |
hexanedioic acid dimethyl ester
A
6-Hydroxyhexanoic acid
B
adipic acid monomethyl ester
C
adipic anhydride
Conditions | Yield |
---|---|
With hydrogen In 1,4-dioxane under 37503.8 Torr; | A 34.1% B 42.3% C 21% |
2-hydroxy-2-cyclohexen-1-one
A
1,5-pentanedioic acid
B
5-oxopentanoic acid
C
adipic acid monomethyl ester
D
5,5-dimethoxy-1-oxopentanoic acid
E
methyl 5-carboxy-2-hydroxypentanoate
Conditions | Yield |
---|---|
With oxygen; methylene blue In methanol at 30℃; for 10h; Product distribution; Irradiation; yield depends on the reaction conditions (temp., sensitizer, solvent); | A 7% B 9% C 1% D 23% E 33% |
methanol
2-hydroxy-2-cyclohexen-1-one
A
1,5-pentanedioic acid
B
5-oxopentanoic acid
C
adipic acid monomethyl ester
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane; oxygen; rose bengal at 40℃; for 13h; Irradiation; | A 1% B 5% C 27% |
Conditions | Yield |
---|---|
at 230℃; | |
for 24h; Heating; | 35.3 g |
In methanol; water | |
at 160℃; for 24h; |
hexanedioic acid dimethyl ester
A
adipic acid monomethyl ester
B
methyl 2-oxocyclopentane-1-carboxylate
Conditions | Yield |
---|---|
With sodium; toluene |
Conditions | Yield |
---|---|
With aluminum oxide In cyclohexane; N,N-dimethyl-formamide Product distribution; study of selectivity of methylation on alumina surface; |
Conditions | Yield |
---|---|
In tetrahydrofuran at 60℃; for 30h; |
Adipic acid
dimethyl sulfate
A
hexanedioic acid dimethyl ester
B
adipic acid monomethyl ester
Conditions | Yield |
---|---|
aluminum oxide In cyclohexane for 2h; Heating; Yield given. Yields of byproduct given; |
Adipic acid
dimethyl sulfate
A
adipic acid monomethyl ester
B
Monomethyl phthalate
Conditions | Yield |
---|---|
aluminum oxide In cyclohexane for 2h; Heating; Yield given. Yields of byproduct given; |
methyl 6-oxohexanoate
A
methyl hydrogen succinate
B
Pentanedioic acid, monomethyl ester
C
adipic acid monomethyl ester
Conditions | Yield |
---|---|
With oxygen; H5PV2Mo10O40(1,11) In acetic acid at 60℃; under 750.06 Torr; Yield given. Yields of byproduct given; |
Conditions | Yield |
---|---|
With Oxone; potassium hydroxide; sodium hydroxide; disodium hydrogenphosphate; water 1.) 65 deg C, 4 h, 2.) r.t., 4 h; Yield given. Multistep reaction; |
A
icosane
B
hepatdecane
C
n-nonadecane
D
adipic acid monomethyl ester
Conditions | Yield |
---|---|
With air at 1130℃; under 18001.4 Torr; Formation of xenobiotics; high pressure combustion; Further byproducts given. Title compound not separated from byproducts; |
A
Methyl linoleate
B
Tridecane
C
adipic acid monomethyl ester
D
methyl ester of azelaic acid aldehyde
Conditions | Yield |
---|---|
With air at 1130℃; under 18001.4 Torr; Formation of xenobiotics; high pressure combustion; Further byproducts given. Title compound not separated from byproducts; |
adipic acid (4,5-dimethoxy-2-nitrobenzyl) ester methyl ester
adipic acid monomethyl ester
Conditions | Yield |
---|---|
In acetonitrile for 24h; Irradiation; 419 nm irradiation; | 85 % Spectr. |
In acetonitrile for 24h; visible light irradiation; |
adipic acid (3',5'-dimethoxybenzoin) ester methyl ester
adipic acid monomethyl ester
Conditions | Yield |
---|---|
In acetonitrile for 0.166667h; Irradiation; 254 nm irradiation; | 95 % Spectr. |
In acetonitrile for 0.0833333h; visible light irradiation; |
Conditions | Yield |
---|---|
With dihydrogen peroxide; Na12[WZn3(H2O)2(ZnW9O34)2] at 75℃; for 7h; |
adipic acid mono(4,5-dimethoxy-2-nitrobenzyl) ester
adipic acid monomethyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 4.9 mg / benzene; ethanol; hexane / 1 h 2: 85 percent Spectr. / acetonitrile / 24 h / Irradiation; 419 nm irradiation View Scheme | |
Multi-step reaction with 4 steps 1: 76 percent / 4-(N,N-dimethylamino)pyridine; N,N'-dicyclohexylcarbodiimide / CHCl3 / 24 h / 60 °C 2: 87 percent Spectr. / acetonitrile / 24 h / Irradiation; 419 nm irradiation 3: 5.6 mg / benzene; ethanol; hexane / 1 h 4: 95 percent Spectr. / acetonitrile / 0.17 h / Irradiation; 254 nm irradiation View Scheme |
adipic acid monomethyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 5.6 mg / benzene; ethanol; hexane / 1 h 2: 95 percent Spectr. / acetonitrile / 0.17 h / Irradiation; 254 nm irradiation View Scheme |
adipic acid (4,5-dimethoxy-2-nitrobenzyl) ester (3',5'-dimethoxybenzoin) ester
adipic acid monomethyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 78 percent Spectr. / acetonitrile / 0.17 h / Irradiation; 254 nm irradiation 2: 4.9 mg / benzene; ethanol; hexane / 1 h 3: 85 percent Spectr. / acetonitrile / 24 h / Irradiation; 419 nm irradiation View Scheme | |
Multi-step reaction with 3 steps 1: 87 percent Spectr. / acetonitrile / 24 h / Irradiation; 419 nm irradiation 2: 5.6 mg / benzene; ethanol; hexane / 1 h 3: 95 percent Spectr. / acetonitrile / 0.17 h / Irradiation; 254 nm irradiation View Scheme |
adipic acid monomethyl ester
methyl adipoyl chloride
Conditions | Yield |
---|---|
With phosphorus pentachloride In diethyl ether Ambient temperature; | 100% |
With thionyl chloride In benzene | 100% |
With oxalyl dichloride for 2h; Heating; | 94% |
adipic acid monomethyl ester
N2-[2R-isobutyl-3S-(9-fluorenylmethoxycarbonylamino)-4-hydroxysuccinyl]-L-tert-leucine-N1-methylamide
Conditions | Yield |
---|---|
Multistep reaction; | 100% |
Conditions | Yield |
---|---|
With N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline In ethanol for 3h; Heating; | 100% |
adipic acid monomethyl ester
tert-butyl (2S)-2-[[(2S)-2-aminopropanoyl]amino]propanoate
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; | 100% |
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; | 100% |
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; |
adipic acid monomethyl ester
N(ε)-benzoyloxycarbonyl-L-lysine tert-butyl ester hydrochloride
CH3O-Adip-Lys(Z)-OBu-t
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In tetrahydrofuran 1 h, 0 deg C => 6 h, r.t.; | 99% |
biphenyl-2-ylcarbamic acid 1-[2-(methylamino)ethyl]piperidin-4-yl ester
adipic acid monomethyl ester
5-({2-[4-(Biphenyl-2-ylcarbamoyloxy)piperidin-1-yl]ethyl}methylcarbamoyl)pentanoic Acid Methyl Ester
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide for 15h; | 98% |
Trimethyl orthoacetate
adipic acid monomethyl ester
hexanedioic acid dimethyl ester
Conditions | Yield |
---|---|
microwave irradiation; | 96% |
Conditions | Yield |
---|---|
With magnesium hydroxide; lithium hydroxide monohydrate; di-tert-butyl dicarbonate at 25℃; for 24h; Time; | 96% |
adipic acid monomethyl ester
bis(2-tert-butyloxycarbonylaminoethyl)amine
Conditions | Yield |
---|---|
Stage #1: adipic acid monomethyl ester With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 1h; Stage #2: bis(2-tert-butyloxycarbonylaminoethyl)amine In dichloromethane at 20℃; | 96% |
Conditions | Yield |
---|---|
Stage #1: adipic acid monomethyl ester With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In acetonitrile at 10℃; for 0.166667h; Stage #2: 1-dodecylthiol In acetonitrile at 25℃; for 22h; | 96% |
adipic acid monomethyl ester
aniline
6-oxo-6-(phenylamino)-hexanoic acid methyl ester
Conditions | Yield |
---|---|
Stage #1: adipic acid monomethyl ester With 1-methyl-1H-imidazole; p-toluenesulfonyl chloride In acetonitrile at 0 - 5℃; for 0.5h; Stage #2: aniline In acetonitrile at 0 - 5℃; for 2h; Further stages.; | 95% |
With 1-(tert-butoxy)-2-(tert-butoxy)carbonyl-1,2-dihydroisoquinoline In dichloromethane at 20℃; for 24h; | 92% |
With triethylamine In dichloromethane for 12h; Heating; | 81% |
With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; 1-hydroxybenzotriazol-hydrate In dichloromethane at 20℃; for 4h; | 58% |
adipic acid monomethyl ester
[(glycyl)glycyl]glycine tert-butyl ester
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 25℃; | 95% |
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid; trifluoroacetic anhydride In dichloromethane at 20℃; for 2h; Inert atmosphere; Schlenk technique; | 95% |
1-hydroxy-pyrrolidine-2,5-dione
adipic acid monomethyl ester
1-methyl 6-succinimidyl adipate
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In acetone at 20℃; for 2h; | 94% |
With dicyclohexyl-carbodiimide In tetrahydrofuran at 20℃; Esterification; | |
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine | |
With triethylamine In thionyl chloride; dichloromethane |
Conditions | Yield |
---|---|
Stage #1: adipic acid monomethyl ester With 1-methyl-1H-imidazole; p-toluenesulfonyl chloride In acetonitrile at 0 - 5℃; for 0.5h; Stage #2: piperidine In acetonitrile at 0 - 5℃; for 2h; Further stages.; | 94% |
With 1-(tert-butoxy)-2-(tert-butoxy)carbonyl-1,2-dihydroisoquinoline In dichloromethane at 20℃; for 24h; | 88% |
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 82% |
adipic acid monomethyl ester
1,2,3-trimethoxybenzene
6-Oxo-6-(2,3,4-trimethoxy-phenyl)-hexanoic acid methyl ester
Conditions | Yield |
---|---|
With PPA; Polyphosphoric acid (PPA) at 45℃; for 2.5h; | 93% |
Conditions | Yield |
---|---|
With trifluoroacetic anhydride In dichloromethane for 48h; Reflux; Inert atmosphere; | 93% |
adipic acid monomethyl ester
Conditions | Yield |
---|---|
With 4-methyl-morpholine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol In N,N-dimethyl-formamide at 20℃; for 12h; | 92% |
oxalyl dichloride
adipic acid monomethyl ester
5-Methoxycarbonylpentansaeure-tert-butylester
Conditions | Yield |
---|---|
With pyridine In N-methyl-acetamide; dichloromethane; tert-butyl alcohol | 92% |
With pyridine In N-methyl-acetamide; dichloromethane; tert-butyl alcohol | 92% |
adipic acid monomethyl ester
3-α-acetoxy-4-β-amino-24-norurs-12-ene
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In tetrahydrofuran at 0 - 20℃; for 16.5h; | 92% |
furan
adipic acid monomethyl ester
5-(2-Furoyl)pentansaeure-methylester
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate; trifluoroacetic anhydride In toluene at 0 - 10℃; for 4h; Reagent/catalyst; | 92% |
With boron trifluoride diethyl etherate; trifluoroacetic anhydride In toluene at 0 - 10℃; for 4h; Reagent/catalyst; | 92% |
adipic acid monomethyl ester
N-(tert-butoxycarbonyl)-1,4-phenylenediamine
Conditions | Yield |
---|---|
Stage #1: adipic acid monomethyl ester With 4-methyl-morpholine; chloroformic acid ethyl ester In dichloromethane at 0℃; for 0.25h; Stage #2: N-(tert-butoxycarbonyl)-1,4-phenylenediamine In dichloromethane at 20℃; | 92% |
Conditions | Yield |
---|---|
Stage #1: adipic acid monomethyl ester With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 1h; Stage #2: N,N''-di-Z-diethylenetriamine In dichloromethane at 20℃; for 20h; | 91.6% |
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