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Hexa-natrium-benzen-hexathiolat
hexamercaptobenzene
Conditions | Yield |
---|---|
With hydrogenchloride | 96% |
With hydrogenchloride In water | 93% |
hexakis(benzylthio)benzene
hexamercaptobenzene
Conditions | Yield |
---|---|
With ammonia; sodium |
hexakis(isopropylthio)benzene
hexamercaptobenzene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Na, liq. NH3 / -78 °C 2: 96 percent / 5percent aq. HCl View Scheme | |
Stage #1: hexakis(isopropylthio)benzene With sodium at 100℃; Stage #2: With hydrogenchloride In methanol; water |
Hexafluorobenzene
hexamercaptobenzene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1,3-dimethyl-2-imidazolidinone / 0 °C / Inert atmosphere 2: sodium / 100 °C View Scheme | |
Multi-step reaction with 2 steps 1: 1,3-dimethyl-2-imidazolidinone / 0 °C / Inert atmosphere 2: sodium / 100 °C View Scheme | |
Multi-step reaction with 2 steps 1: 1,3-dimethyl-2-imidazolidinone / 0 °C / Inert atmosphere 2: sodium / 100 °C View Scheme |
hexabromobenzene
hexamercaptobenzene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1,3-dimethyl-2-imidazolidinone / 100 °C / Inert atmosphere 2: sodium / 100 °C View Scheme | |
Multi-step reaction with 2 steps 1: 1,3-dimethyl-2-imidazolidinone / 100 °C / Inert atmosphere 2: sodium / 100 °C View Scheme | |
Multi-step reaction with 2 steps 1: 1,3-dimethyl-2-imidazolidinone / 100 °C / Inert atmosphere 2: sodium / 100 °C View Scheme |
hexakis(methylthio) benzene
hexamercaptobenzene
Conditions | Yield |
---|---|
Stage #1: hexakis(methylthio) benzene With sodium at 100℃; Stage #2: With hydrogenchloride In methanol; water |
hexakis(ethylthio)benzene
hexamercaptobenzene
Conditions | Yield |
---|---|
Stage #1: hexakis(ethylthio)benzene With sodium at 100℃; Stage #2: With hydrogenchloride In methanol; water |
pyridine
carbon disulfide
hexamercaptobenzene
7-mercapto-2,5-dithioxobenzo<1,2-d:3,4-d'>bis<1,3>dithiole-8-thiolate
Conditions | Yield |
---|---|
for 0.25h; Ambient temperature; | 97% |
Conditions | Yield |
---|---|
In water; toluene at 60℃; for 49h; | 95% |
Conditions | Yield |
---|---|
Stage #1: tetrakis(acetonitrile)copper(I)tetrafluoroborate In 1,2-dimethoxyethane at 45℃; for 1h; Inert atmosphere; Stage #2: hexamercaptobenzene In 1,2-dimethoxyethane at 45℃; for 168h; Inert atmosphere; | 93.6% |
Conditions | Yield |
---|---|
Stage #1: tetrakis(acetonitrile)copper(I)tetrafluoroborate In methanol at 45℃; for 1h; Inert atmosphere; Stage #2: hexamercaptobenzene In methanol at 45℃; for 168h; Inert atmosphere; | 91% |
bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]
hexamercaptobenzene
Ir3(η5-C5Me5)3(S6C6)
Conditions | Yield |
---|---|
With triethylamine In dichloromethane (under N2, Schlenk); triethylamine added to soln. of C6(SH)6 in CH2Cl2, CH2Cl2 soln. of Ir-complex added, stirred for 2 h at room temp.; filtered, solvent evapd. under vac., alumina column chromy. with CH2Cl2-hexane (1:1), recrystd. from CH2Cl2-hexane; elem. anal.; | 90% |
Conditions | Yield |
---|---|
Stage #1: hexamercaptobenzene With triethylamine In tetrahydrofuran Schlenk technique; Inert atmosphere; Stage #2: dibutyltin chloride for 4h; Inert atmosphere; Schlenk technique; | 85% |
Conditions | Yield |
---|---|
In ethylenediamine for 16 h at 60°C; | 83% |
Conditions | Yield |
---|---|
In chloroform; water for 24h; Inert atmosphere; | 82% |
[(divinyl)(phenyl)phosphine] gold(I) chloride
hexamercaptobenzene
Conditions | Yield |
---|---|
With triethylamine In dichloromethane byproducts: Et3NHCl; stirred at room temp., 2 h; soln. filtered; solvent removed under reduced pressure; residue recrystd. at room temp. (CH2Cl2/hexane); elem. anal.; | 80% |
hexamercaptobenzene
Conditions | Yield |
---|---|
With sodium carbonate; triethylamine In methanol; dichloromethane stirred, room temp., 2 h; solvent removed under reduced pressure; residue dissolved (CH2Cl2); ppt. (hexane), room temp.; elem. anal.; | 80% |
hexamercaptobenzene
Rh3(η5-C5Me5)3(S6C6)
Conditions | Yield |
---|---|
With triethylamine In dichloromethane (under N2, Schlenk); triethylamine added to soln. of C6(SH)6 in CH2Cl2, CH2Cl2 soln. of Rh-complex added, stirred for 2 h at room temp.; filtered, solvent evapd. under vac., alumina column chromy. with CH2Cl2-hexane (1:1), recrystd. from CH2Cl2-hexane; elem. anal.; | 77% |
hexamercaptobenzene
A
benzo<1,2-d><3,4-d'><5,6-d''>-tris-1,2,3-trithiole
Conditions | Yield |
---|---|
With sulfur dichloride; methyllithium 1.) THF, 30 min; 2.) THF, 1 h, r.t.; | A 74% B 20% |
hexamercaptobenzene
Conditions | Yield |
---|---|
With sodium carbonate; triethylamine In methanol; dichloromethane stirred, room temp., 2 h; solvent removed under reduced pressure; residue dissolved (CH2Cl2); ppt. (hexane), room temp.; elem. anal.; | 70% |
hexamercaptobenzene
Conditions | Yield |
---|---|
With sodium carbonate; triethylamine In methanol; dichloromethane stirred, room temp., 2 h; solvent removed under reduced pressure; residue dissolved (CH2Cl2); ppt. (hexane), room temp.; elem. anal.; | 70% |
hexamercaptobenzene
Conditions | Yield |
---|---|
With sodium carbonate; triethylamine In methanol; dichloromethane stirred, room temp., 2 h; solvent removed under reduced pressure; residue dissolved (CH2Cl2); ppt. (hexane), room temp.; | 69% |
hexamercaptobenzene
Conditions | Yield |
---|---|
With triethylamine In acetone (under N2, Schlenk); triethylamine added to soln. of C6(SH)6 in acetone,acetone soln. of Co-complex added, stirred for 2 h at room temp.; filtered, solvent evapd. under vac., alumina column chromy. with CH2Cl2-hexane (1:1), recrystd. from CH2Cl2-hexane; | 59% |
With triethylamine In dichloromethane (under N2, Schlenk); triethylamine added to soln. of C6(SH)6 in CH2Cl2, CH2Cl2 soln. of Co-complex added, stirred for 2 h at room temp.; filtered, solvent evapd. under vac., alumina column chromy. with CH2Cl2-hexane (1:1), recrystd. from CH2Cl2-hexane; elem. anal.; | 53% |
With triethylamine In tetrahydrofuran (under N2, Schlenk); triethylamine added to soln. of C6(SH)6 in THF, THFsoln. of Co-complex added, stirred for 2 h at room temp.; filtered, solvent evapd. under vac., alumina column chromy. with CH2Cl2-hexane (1:1), recrystd. from CH2Cl2-hexane; | 38% |
With NaOCH3 In methanol; dichloromethane (under N2, Schlenk); NaOCH3 added to soln. of C6(SH)6 in CH2Cl2-MeOH, CH2Cl2-MeOH soln. of Co-complex added, stirred for 2 h at room temp.; filtered, solvent evapd. under vac., alumina column chromy. with CH2Cl2-hexane (1:1), recrystd. from CH2Cl2-hexane; | 32% |
With Na2CO3 In methanol; dichloromethane (under N2, Schlenk); Na2CO3 added to soln. of C6(SH)6 in CH2Cl2-MeOH, CH2Cl2-MeOH soln. of Co-complex added, stirred for 2 h at room temp.; filtered, solvent evapd. under vac., alumina column chromy. with CH2Cl2-hexane (1:1), recrystd. from CH2Cl2-hexane; | 11% |
hexamercaptobenzene
Co3(η5-C5H5)3(S6C6)
Conditions | Yield |
---|---|
With triethylamine In dichloromethane (under N2, Schlenk); triethylamine added to soln. of C6(SH)6 in CH2Cl2, CH2Cl2 soln. of Co-complex added, stirred for 2 h at room temp.; filtered, solvent evapd. under vac., alumina column chromy. with CH2Cl2-hexane (1:1), recrystd. from CH2Cl2-hexane; elem. anal.; | 58% |
(triphenylphosphine)gold(I) chloride
hexamercaptobenzene
Conditions | Yield |
---|---|
With NEt3 In dichloromethane molar ratio Au-complex:thiol:NEt3=6:1:6; stirring (room temp., 2 h); filtration, solvent removal (vac.), recrystn. (CH2Cl2/hexane=1:1); | A 30% B n/a |
Conditions | Yield |
---|---|
In toluene at 130℃; for 2h; | 17% |
hexamercaptobenzene
acetonitrile
Conditions | Yield |
---|---|
In not given reaction of nickel compd. with hexamercaptobenzene in presence of base; chromy. (alumina), NMR and MS; | 14% |
cyclohexane
hexamercaptobenzene
Conditions | Yield |
---|---|
In not given reaction of ruthenium compd. with hexamercaptobenzene in presence of base; chromy. (alumina), NMR annd MS; | 5% |
hexamercaptobenzene
[((4,4'-di-tert-butyl-2,2'-pyridine)Pt)3(hexathiolatobenzene)]
Conditions | Yield |
---|---|
In not given reaction of platinum compd. with hexamercaptobenzene in presence of base; chromy. (alumina), NMR and MS; | 1% |
carbon disulfide
diiodomethane
hexamercaptobenzene
1,3,4,6,7,9-Hexathia-trindene-2,5-dithione
Conditions | Yield |
---|---|
With pyridine 1) RT, 15 min, 2) 10 min; Yield given. Multistep reaction; |
carbon disulfide
amyl iodide
hexamercaptobenzene
4,5-Bis-pentylsulfanyl-benzo[1,2-d;3,4-d']bis[1,3]dithiole-2,7-dithione
Conditions | Yield |
---|---|
With pyridine 1) RT, 15 min, 2) 10 min; Yield given. Multistep reaction; |
carbon disulfide
hexamercaptobenzene
ethyl iodide
4,5-Bis-ethylsulfanyl-benzo[1,2-d;3,4-d']bis[1,3]dithiole-2,7-dithione
Conditions | Yield |
---|---|
With pyridine 1) RT, 15 min, 2) 10 min; Yield given. Multistep reaction; |
carbon disulfide
hexamercaptobenzene
methyl iodide
4,5-Bis-methylsulfanyl-benzo[1,2-d;3,4-d']bis[1,3]dithiole-2,7-dithione
Conditions | Yield |
---|---|
With pyridine 1) RT, 15 min, 2) 10 min; Yield given. Multistep reaction; |
4-methyl-benzaldehyde
hexamercaptobenzene
Conditions | Yield |
---|---|
With zinc trifluoromethanesulfonate In chloroform Heating; |
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