1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
Cas:65376-05-8
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inquiryLurasidone Intermediates as follows: (3aR,4S,7R,7aS)-rel-Hexahydro-4,7-methano-1H-isoindole-1,3(2H)-dione[CAS:14805-29-9] (1R,2R)-1,2-Cyclohexanedimethanol[CAS:65376-05-8] HANGZHOU THINK CHEMICAL CO., LTD. (THINKCHEM) is an integrative corporatio
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inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
Cas:65376-05-8
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inquiryManufacturer supply (1R,2R)-1,2-Cyclohexanedimethanol CAS 65376-05-8 with attractive price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its int
Cas:65376-05-8
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:65376-05-8
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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap
Cas:65376-05-8
Min.Order:1 Kilogram
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inquiry1. made in GMP plant, commerially 2. Normal Stock: 500kgs 3. Audit accepted. Related documents are available to offer and audited by many clients, such as Lupin, MSN, Dr reddy etc 4. Chromatographic Purity (HPLC): not less tha
Cas:65376-05-8
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inquiryDayangChem exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product s
Cas:65376-05-8
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:65376-05-8
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Type:Manufacturers
inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/841.html Product Name (1R,2R)-1,2-Bis(hydroxymethyl)cyclohexane CAS No.
Cas:65376-05-8
Min.Order:1 Gram
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inquiryLIDE PHARMACEUTICALS LIMITED is a professional chemicals and APIs leading manufacturer in China. Our core business line covers APIs, Intermediates, Herb extract, etc.
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:65376-05-8
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu
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inquiryWhy is SINOWAY: 1) Specialized in pharmaceutical and healthcare industrial for 34 years. 2) ISO 9001:2015 & SGS audited supplier . 3) Accept various payment terms : T.T 30-60 days. 4) We have warehouse in USA with quickly shipment . 5) We c
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Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryProduct (1R,2R)-1,2-Cyclohexanedimethanol Cas NO 65376-05-8 Product Information: Systematic Name: (1R,2R)-cyclohexane-1,2-diyldimethanol CAS NO: 65376-05-8 Molecular Formula: C8H16O2 Molecular Weight: 144.21 Purity: 99%
Cas:65376-05-8
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Type:Other
inquiryAdvantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best s
Cas:65376-05-8
Min.Order:10 Gram
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Type:Other
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:65376-05-8
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Type:Trading Company
inquiry(1R,2R)-1,2-CYCLOHEXANEDIMETHANOL CAS: 65376-05-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high qualit
Cas:65376-05-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:65376-05-8
Min.Order:1 Kilogram
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inquiryHebei Mojin Biotechnology Co., Ltd, Our company is a professional chemical raw materials and chemical reagents research and development production enterprises. We have several production line,So we can control the lowest price. We also have several
Cas:65376-05-8
Min.Order:25 Gram
FOB Price: $90.0 / 100.0
Type:Trading Company
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Type:Lab/Research institutions
inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Product name: sodium metabisulfite / sodium metabisulphite Molecular weight: 190.10 Specification: 25Kg woven bag Quality guarantee period: 6 months Appearance:white powder Storage:Room Temperature Package:Carton(The aluminum foil
Cas:65376-05-8
Min.Order:10 Gram
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Type:Lab/Research institutions
inquiryOur Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
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Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiry98%Suzhou Jingye Medicine & Chemical Co., Ltd (Former: Suzhou Daxin Chemical Agent Factory) is a Hi-tech private enterprise, which is a professional manufacturer of hydrogenous products. It is located in Suzhou New District Chemical Area, about
Cas:65376-05-8
Min.Order:1 Metric Ton
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Type:Manufacturers
inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:65376-05-8
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Type:Lab/Research institutions
inquiry(1R,2R)-1,2-cyclohexanedicarboxylic acid dimethyl ester
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
With hydrogen In methanol at 190℃; under 52505.3 Torr; Temperature; Pressure; Solvent; | 94% |
Stage #1: (1R,2R)-1,2-cyclohexanedicarboxylic acid dimethyl ester With diisobutylaluminium hydride In toluene at -5 - 20℃; for 6h; Inert atmosphere; Stage #2: With hydrogenchloride; water In toluene at -5 - 40℃; for 13h; | 74% |
With lithium aluminium tetrahydride In diethyl ether | |
Stage #1: (1R,2R)-1,2-cyclohexanedicarboxylic acid dimethyl ester With diisobutylaluminium hydride In toluene at 0 - 20℃; for 4h; Inert atmosphere; Stage #2: With hydrogenchloride In water at 0 - 40℃; for 18h; | |
With methanol; sodium tetrahydroborate In tetrahydrofuran at 40℃; for 3h; Temperature; Reflux; |
(1R,2R)-(-)-trans-cyclohexane-1,2-dicarboxylic acid
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
With sodium tetrahydroborate; iodine In tetrahydrofuran at 0℃; for 5h; Reflux; | 88.4% |
With Red-Al In tetrahydrofuran; toluene for 5h; Inert atmosphere; Reflux; | 85.2% |
Multi-step reaction with 2 steps 1: diethyl ether 2: LiAlH4 / diethyl ether View Scheme |
(-)-(1R,2R)-trans-2-(hydroxymethyl)cyclohexanoic acid
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In diethyl ether for 12h; Heating; | 80% |
With lithium aluminium tetrahydride |
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In diethyl ether at 0 - 20℃; for 19h; Inert atmosphere; | 76% |
(+/-)-trans-2-(hydroxymethyl)cyclohexylmethanol
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
With C11H19NO |
(+/-)-trans-2-(hydroxymethyl)cyclohexylmethanol
A
trans-2-(hydroxymethyl)cyclohexanecarboxylic acid
B
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
C
(1S,2S)-(–)-1,2-di(hydroxymethyl)cyclohexane
D
(-)-(1R,2R)-trans-2-(hydroxymethyl)cyclohexanoic acid
Conditions | Yield |
---|---|
With sodium hydroxide; NAD; silver nitrate; glycine; Flavin mononucleotide Product distribution; multistep reaction, other trans-diols, stereospecificity; |
diethyl trans-1,2,3,6-tetrahydrophthalate
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
Stage #1: diethyl trans-1,2,3,6-tetrahydrophthalate With hydrogen; palladium on activated charcoal Stage #2: With lithium aluminium tetrahydride |
(3aR,7aS)-1,3,3a,4,7,7a-hexahydroisobenzofuran-1-one
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 86 percent / H2 / Pd/C / methanol 2: 34 percent / NaOH / H2O / 192 h / 130 °C 3: 80 percent / LiAlH4 / diethyl ether / 12 h / Heating View Scheme |
cis-1,2-cyclohexanedimethanol
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 80 percent / NAD+, FMN, pH 9, HLADH, NaOH, glycine / Ambient temperature 2: 34 percent / NaOH / H2O / 192 h / 130 °C 3: 80 percent / LiAlH4 / diethyl ether / 12 h / Heating View Scheme |
cis-1,6-dihydroxymethyl-3-cyclohexene
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 83 percent / NAD+, FMN, pH 9, HLADH, NaOH, glycine / 48 h / 20 °C 2: 86 percent / H2 / Pd/C / methanol 3: 34 percent / NaOH / H2O / 192 h / 130 °C 4: 80 percent / LiAlH4 / diethyl ether / 12 h / Heating View Scheme |
(3aR,7aS)-hexahydroisobenzofuran-1-one
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 34 percent / NaOH / H2O / 192 h / 130 °C 2: 80 percent / LiAlH4 / diethyl ether / 12 h / Heating View Scheme |
1,2-cis-cyclohexanedicarboxylic anhydride
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: LiAlH4 2: 80 percent / NAD+, FMN, pH 9, HLADH, NaOH, glycine / Ambient temperature 3: 34 percent / NaOH / H2O / 192 h / 130 °C 4: 80 percent / LiAlH4 / diethyl ether / 12 h / Heating View Scheme |
phthalic acid dimethyl ester
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: Raney nickel; methanol / 50 - 60 °C / 73550.8 Torr / Hydrogenation.Behandeln des Reaktionsprodukts mit methanol. Natriummethylat 2: LiAlH4; diethyl ether 3: (1R)-menthyl isocyanate View Scheme |
dimethyl cyclohexane-trans-1,2-dicarboxylate
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: LiAlH4; diethyl ether 2: (1R)-menthyl isocyanate View Scheme |
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: hydrogenchloride / water 2.1: sulfuric acid / 18 h / 40 °C 3.1: diisobutylaluminium hydride / toluene / 6 h / -5 - 20 °C / Inert atmosphere 3.2: 13 h / -5 - 40 °C View Scheme |
trans-1,2-cyclohexanedicarboxylic acid
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: ethanol / 6.5 h / -70 - 20 °C / Resolution of racemate 2.1: hydrogenchloride / water 3.1: sulfuric acid / 18 h / 40 °C 4.1: diisobutylaluminium hydride / toluene / 6 h / -5 - 20 °C / Inert atmosphere 4.2: 13 h / -5 - 40 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: ethanol / 30 h / 35 - 75 °C 1.2: 1 h 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 65 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: (R)-1-phenyl-ethyl-amine / methanol; isopropyl alcohol / 30 - 40 °C 2.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 1 h / 25 - 30 °C 2.2: 1 h View Scheme | |
Multi-step reaction with 4 steps 1: (R)-1-phenyl-ethyl-amine / methanol; isopropyl alcohol / 30 - 40 °C 2: tetrahydrofuran / 1 h / 25 - 30 °C 3: tetrahydrofuran / 45 - 50 °C 4: sodium tetrahydroborate; water / tetrahydrofuran / 1 h View Scheme |
trans-cyclohex-4-ene-1,2-dicarboxylic acid
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: palladium; hydrogen / methanol / 30 - 35 °C 2.1: ethanol / 30 h / 35 - 75 °C 2.2: 1 h 3.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 65 °C View Scheme |
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: methanol / 0 - 35 °C / Inert atmosphere 1.2: Inert atmosphere 2.1: Red-Al / tetrahydrofuran; toluene / 5 h / Inert atmosphere; Reflux View Scheme | |
Multi-step reaction with 3 steps 1: (R)-1-phenyl-ethyl-amine / 5 °C 2: sulfuric acid / 4 h / Reflux 3: sodium tetrahydroborate; methanol / tetrahydrofuran / 3 h / 40 °C / Reflux View Scheme | |
Multi-step reaction with 3 steps 1.1: diisopropylamine / ethanol / 3 h / -72 - 20 °C 2.1: sulfuric acid / 20 h / 10 - 50 °C 3.1: diisobutylaluminium hydride / toluene / 4 h / 0 - 20 °C / Inert atmosphere 3.2: 18 h / 0 - 40 °C View Scheme |
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sulfuric acid / 20 h / 10 - 50 °C 2.1: diisobutylaluminium hydride / toluene / 4 h / 0 - 20 °C / Inert atmosphere 2.2: 18 h / 0 - 40 °C View Scheme |
dimethyl cis-1,2-cyclohexanedicarboxylate
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium methylate / methanol / 4 h / Inert atmosphere; Reflux 1.2: 4 h / 75 °C / Inert atmosphere 1.3: 0 - 5 °C / pH 2 / Inert atmosphere 2.1: Red-Al / tetrahydrofuran; toluene / 5 h / Inert atmosphere; Reflux View Scheme |
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: tetrahydrofuran / 45 - 50 °C 2: sodium tetrahydroborate; water / tetrahydrofuran / 1 h View Scheme |
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
With sodium tetrahydroborate; water In tetrahydrofuran for 1h; | 15.5 g |
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
tert-butyldimethylsilyl chloride
((1R,2R)-2-(((tert-butyldimethylsilyl)oxy)methyl)cyclohexyl)methanol
Conditions | Yield |
---|---|
Stage #1: (+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane With n-butyllithium In tetrahydrofuran; cyclohexane at 0 - 20℃; for 3.25h; Inert atmosphere; Stage #2: tert-butyldimethylsilyl chloride In tetrahydrofuran; cyclohexane at 20℃; for 1h; Inert atmosphere; | 99% |
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
8-oxabicyclo[4,3,0]nonane-7-one
Conditions | Yield |
---|---|
With (CH3)5C5*Ir(-OCH2C(C6H5)2NH-) In acetone at 20℃; for 36h; | 98% |
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
p-methoxybenzyl chloride
Conditions | Yield |
---|---|
Stage #1: (+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane With sodium hydride In N,N-dimethyl-formamide; mineral oil at -20℃; for 0.5h; Inert atmosphere; Stage #2: p-methoxybenzyl chloride In N,N-dimethyl-formamide; mineral oil at 20℃; for 1h; Inert atmosphere; | A 97% B 2% |
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
Stage #1: (+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane With oxalyl dichloride; dimethyl sulfoxide In dichloromethane at -60℃; Inert atmosphere; Stage #2: With triethylamine In dichloromethane at -50 - 20℃; Inert atmosphere; | 94% |
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
methanesulfonyl chloride
(1R,2R)-(-)-trans-cyclohexane-1,2-diylbis(methylene)dimethanesulfonate
Conditions | Yield |
---|---|
With triethylamine at 0 - 5℃; Industrial scale; | 92.6% |
With triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere; | 92% |
With triethylamine In chloroform at 0 - 20℃; for 5h; | 90.8% |
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
p-toluenesulfonyl chloride
(R)-trans-1,2-bis-(toluene-4-sulfonyloxymethyl)-cyclohexane
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at -10 - 0℃; for 3h; Concentration; | 92.5% |
Conditions | Yield |
---|---|
Stage #1: (+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane With sodium hydroxide In tetrahydrofuran Stage #2: C18H17N3O2S In tetrahydrofuran at 70℃; for 2h; Reagent/catalyst; Solvent; Temperature; | 74% |
Conditions | Yield |
---|---|
Stage #1: (+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane With sodium hydroxide In tetrahydrofuran Stage #2: C18H17N3O2S In tetrahydrofuran at -10℃; | 32% |
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In water; dimethyl sulfoxide at 23℃; for 2h; |
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: o-iodoxybenzoic acid / dimethylsulfoxide; H2O / 2 h / 23 °C 2: benzene / 16 h / Heating View Scheme |
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: o-iodoxybenzoic acid / dimethylsulfoxide; H2O / 2 h / 23 °C 2: benzene / 16 h / Heating 3: 94 percent / triethylamine / CH2Cl2 / 0 °C 4: 84 percent / sodium iodide / acetone / 14 h / Heating View Scheme |
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: o-iodoxybenzoic acid / dimethylsulfoxide; H2O / 2 h / 23 °C 2: benzene / 16 h / Heating 3: 94 percent / triethylamine / CH2Cl2 / 0 °C View Scheme |
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: o-iodoxybenzoic acid / dimethylsulfoxide; H2O / 2 h / 23 °C 2: benzene / 16 h / Heating 3: 94 percent / triethylamine / CH2Cl2 / 0 °C 4: 84 percent / sodium iodide / acetone / 14 h / Heating 5: 97 percent / ethanol / 120 h / Heating 6: 75 percent / potassium hydroxide; water / 8 h / Heating View Scheme |
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: o-iodoxybenzoic acid / dimethylsulfoxide; H2O / 2 h / 23 °C 2: benzene / 16 h / Heating 3: 94 percent / triethylamine / CH2Cl2 / 0 °C 4: 84 percent / sodium iodide / acetone / 14 h / Heating 5: 97 percent / ethanol / 120 h / Heating 6: 10 percent Chromat. / potassium hydroxide; water / 8 h / Heating View Scheme |
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: o-iodoxybenzoic acid / dimethylsulfoxide; H2O / 2 h / 23 °C 2: benzene / 16 h / Heating 3: 94 percent / triethylamine / CH2Cl2 / 0 °C 4: 84 percent / sodium iodide / acetone / 14 h / Heating 5: 70 percent / triethylamine / 120 h / Heating View Scheme |
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: o-iodoxybenzoic acid / dimethylsulfoxide; H2O / 2 h / 23 °C 2: benzene / 16 h / Heating 3: 94 percent / triethylamine / CH2Cl2 / 0 °C 4: 84 percent / sodium iodide / acetone / 14 h / Heating 5: 97 percent / ethanol / 120 h / Heating View Scheme |
(+)-(1R,2R)-trans-1,2-bis(hydroxymethyl)cyclohexane
(3aR)-trans-octahydro-isobenzofuran
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: pyridine 2: aqueous KOH-solution View Scheme |
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