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inquiryProduct Description Product website: http://www.finerchem.com Product Name N,N-Dimethyloctylamine CAS No.
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inquiryN,N-Dimethyloctylamine Basic information Product Name: N,N-Dimethyloctylamine Synonyms: N1,N1-DIMETHYLOCTAN-1-AMINE;OCTYLDIMETHYLAMINE;N-DIMETHYLOCTYLAMINE;N-N-OCTYLDIMETHYLAMINE;N,N-DIM
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inquiryName:N,N-Dimethyloctylamine CAS No.:7378-99-6 MF: C10H23N Appearance:Clear to slightly hazy liquid Appearance:Clear to slightly hazy liquid Storage:Preserve in well-closed, light-resistant and airtight containers. Package:25kg/drum Application:Inter
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N,N-dimethyloctanamide
Conditions | Yield |
---|---|
With triethyl borane; phenylsilane; sodium hydroxide In tetrahydrofuran; tert-butyl methyl ether at 20℃; Inert atmosphere; Schlenk technique; Sealed tube; chemoselective reaction; | 94% |
With triethyl borane; phenylsilane; sodium hydroxide In tetrahydrofuran; tert-butyl methyl ether at 20℃; for 48h; Inert atmosphere; Schlenk technique; Glovebox; Sealed tube; | 94% |
With water; sodium; sodium chloride In hexane; mineral oil at 0℃; for 3h; Inert atmosphere; | 37% |
With diethyl ether; diisobutylaluminium hydride | |
With hydrogen In 1,2-dimethoxyethane at 70℃; under 22502.3 Torr; for 18h; Autoclave; Molecular sieve; chemoselective reaction; |
Conditions | Yield |
---|---|
With sodium hydroxide In water; toluene for 72h; Autoclave; | 90% |
Conditions | Yield |
---|---|
With hydrogen In water; tert-butyl alcohol at 120℃; under 30003 Torr; for 24h; | 90% |
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol; water at 100℃; for 24h; | 85.2% |
Conditions | Yield |
---|---|
chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II) at 100℃; | 100% |
With 5percent silver supported on titanium oxide at 25℃; for 6h; Inert atmosphere; UV-irradiation; Sealed tube; | 99% |
With [Cp*Ir(2-(1H-benzo[d]imidazol-2-yl)-1H-benzo[d]imidazole)Cl][Cl]; caesium carbonate at 120℃; for 12h; Schlenk technique; | 93% |
methanol
n-Octylamine
A
N,N-dimethyloctanamide
B
N-methyl-N-octylamine
Conditions | Yield |
---|---|
With γ-Al2O3 In gaseous matrix at 280℃; Yield given; Yields of byproduct given; | |
With carbonylhydrido(tetrahydroborato)[bis(2-diphenylphosphinoethyl)amino]ruthenium(II); hydrogen at 110℃; under 30003 Torr; for 24h; Glovebox; | A 7 %Spectr. B n/a |
With platinum on carbon; sodium hydroxide at 150℃; under 750.075 Torr; for 36h; Reagent/catalyst; Inert atmosphere; Autoclave; | A 64 %Chromat. B 23 %Chromat. |
Conditions | Yield |
---|---|
With hydrogen; fused iron catalyst at 250 - 265℃; under 15001.2 - 22501.8 Torr; Mechanism; other alcohols; | 87% |
fused iron catalyst at 250 - 265℃; under 15001.2 - 22501.8 Torr; | 87% |
With C19H32Cl2IrN2; potassium carbonate In water at 120℃; for 40h; Reagent/catalyst; Time; Temperature; Sealed tube; Green chemistry; | 83% |
Conditions | Yield |
---|---|
Stage #1: octyldimethylamine oxide With N,N-Dimethylthiocarbamoyl chloride In dichloromethane at 20℃; for 2h; Stage #2: In acetonitrile for 3h; Reflux; | 92% |
With trimethylacetic formic anhydride In chloroform 1.) 0 deg C, 10 min, 2.) 0 deg C to r.t., 30 min; Yield given; |
methanol
n-Octylamine
A
N,N-dimethyloctanamide
B
N-methyl-N-octylamine
Conditions | Yield |
---|---|
With platinum on carbon; sodium hydroxide at 150℃; under 750.075 Torr; for 36h; Reagent/catalyst; Inert atmosphere; Autoclave; | A 47 %Chromat. B 29 %Chromat. C 12 %Chromat. |
methanol
n-Octylamine
A
N,N-dimethyloctanamide
B
N-methyl-N-octylamine
C
n-dioctylamine
Conditions | Yield |
---|---|
With rhodium contaminated with carbon; sodium hydroxide at 150℃; under 750.075 Torr; for 36h; Inert atmosphere; Autoclave; | A 62 %Chromat. B 11 %Chromat. C 5 %Chromat. |
methanol
n-Octylamine
A
N,N-dimethyloctanamide
B
N-methyl-N-octylamine
C
methyldioctylamine
Conditions | Yield |
---|---|
With platinum on zirconia; sodium hydroxide at 150℃; under 750.075 Torr; for 36h; Reagent/catalyst; Inert atmosphere; Autoclave; | A 18 %Chromat. B 35 %Chromat. C 20 %Chromat. |
methanol
n-Octylamine
A
N,N-dimethyloctanamide
B
N-methyl-N-octylamine
C
n-dioctylamine
Conditions | Yield |
---|---|
With platinum-doped magnesium oxide; sodium hydroxide at 150℃; under 750.075 Torr; for 36h; Reagent/catalyst; Inert atmosphere; Autoclave; | A 56 %Chromat. B 18 %Chromat. C 10 %Chromat. D 12 %Chromat. |
methanol
n-Octylamine
A
N,N-dimethyloctanamide
B
N-methyl-N-octylamine
C
n-dioctylamine
D
methyldioctylamine
Conditions | Yield |
---|---|
With iridium on carbon; sodium hydroxide at 150℃; under 750.075 Torr; for 36h; Reagent/catalyst; Inert atmosphere; Autoclave; | A 55 %Chromat. B 14 %Chromat. C 6 %Chromat. D 12 %Chromat. |
Conditions | Yield |
---|---|
With tris(triphenylphosphine)ruthenium(II) chloride In tetrahydrofuran at 180℃; for 7h; | A 11 % Chromat. B 85% |
Conditions | Yield |
---|---|
With [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 In hexane; water at 50℃; for 5h; | 98% |
N,N-dimethyloctanamide
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran for 0.5h; Heating; | 82% |
1-Fluoro-octane
N,N,N,N,-tetramethylethylenediamine
A
1-Chlorooctane
B
N,N-dimethyloctanamide
Conditions | Yield |
---|---|
With phenylmagnesium chloride In tetrahydrofuran at 80℃; for 24h; Inert atmosphere; | A 22 %Chromat. B n/a |
methanol
n-Octylamine
A
N,N-dimethyloctanamide
B
methyldioctylamine
Conditions | Yield |
---|---|
With tris(triphenylphosphine)ruthenium(II) chloride at 180℃; for 7h; | A 12 % Chromat. B 75% |
Conditions | Yield |
---|---|
With acetylacetonatodicarbonylrhodium(l); dodecacarbonyl-triangulo-triruthenium; water; triphenylphosphine In N,N-dimethyl-formamide at 170℃; for 6h; Autoclave; Green chemistry; |
N,N-dimethyloctamide
A
octanol
B
N,N-dimethyloctanamide
C
dimethyl amine
Conditions | Yield |
---|---|
With tris(2,4-pentanedionato)ruthenium(III); ytterbium(III) trifluoromethanesulfonate nonohydrate; hydrogen; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine] In tetrahydrofuran at 150℃; under 3750.38 Torr; for 15h; Autoclave; | A n/a B 11 %Chromat. C n/a |
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid; water at 60℃; for 12h; Temperature; Time; Inert atmosphere; | 82% |
Conditions | Yield |
---|---|
With ethanol at 100℃; | |
With PS-triphenylphosphine; di-isopropyl azodicarboxylate In tetrahydrofuran |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 2: 82 percent / LiAlH4 / tetrahydrofuran / 0.5 h / Heating View Scheme |
N,N-dimethyloctanamide
Conditions | Yield |
---|---|
With potassium hydroxide In methanol for 0.5h; Heating; Yield given; |
N,N-dimethyloctanamide
Conditions | Yield |
---|---|
With potassium hydroxide In methanol for 0.5h; Heating; Yield given; |
Conditions | Yield |
---|---|
In water at 140 - 150℃; |
Conditions | Yield |
---|---|
With potassium hydroxide at 20℃; for 2h; |
1-Chlorooctane
N,N-dimethyl-formamide
A
octane
B
N,N-dimethyloctanamide
Conditions | Yield |
---|---|
With bis(cyclopentadienyl)titanium dichloride; sodium tetrahydroborate 1.) 96 deg C, 1 h, 2.) 40 deg C, 7 h; Yield given. Yields of byproduct given; |
N,N-dimethyloctamide
A
n-Octylamine
B
octane
C
octanol
D
N,N-dimethyloctanamide
E
Octanoic acid
Conditions | Yield |
---|---|
With hydrogen; Cu-Cr at 260 - 300℃; under 760 Torr; Product distribution; | A 3.9 % Chromat. B 1.8 % Chromat. C 2.9 % Chromat. D 91.8 % Chromat. E 1.1 % Chromat. |
1-bromooct-4-ene
N,N-dimethyloctanamide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: benzene 2: (hydrogenation) View Scheme |
N,N-dimethyloctanamide
(3S,8S,9S,10R,13R,14S,17R)-10,13-dimethyl-17-((R)-6-methylheptan-2-yl)-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl 2-bromoacetate
Conditions | Yield |
---|---|
In acetonitrile for 2h; Reflux; | 99% |
(1R,2S,5R)-1-(chloromethoxy)-2-isopropyl-5-methylcyclohexane
N,N-dimethyloctanamide
Conditions | Yield |
---|---|
In hexane at 20℃; for 0.5h; Menschutkin reaction; | 98.5% |
Conditions | Yield |
---|---|
With dihydrogen peroxide; benzonitrile; Mg-Al-O-t-Bu HT (Catalyst B) In methanol; water at 65℃; for 0.5h; Product distribution / selectivity; | 98% |
With aluminum oxide; Oxone In water at 80℃; Product distribution; Further Variations:; Reagents; Oxidation; | 96% |
With dihydrogen peroxide; sodium dodecylbenzenesulfonate; layered double hydroxide WO4(2-) at 20℃; for 1h; | 95% |
With dihydrogen peroxide In methanol; water | 78% |
Conditions | Yield |
---|---|
In acetonitrile at 82℃; for 48h; Menshutkin Reaction; | 98% |
In ethanol Reflux; | 75% |
N,N-dimethyloctanamide
1-chloromethoxy-heptane
Conditions | Yield |
---|---|
In n-heptane for 0.166667h; Heating; | 95% |
Conditions | Yield |
---|---|
In n-heptane for 0.166667h; Heating; | 95% |
Conditions | Yield |
---|---|
In ethyl acetate at 55℃; for 3h; | 95% |
N,N-dimethyloctanamide
Conditions | Yield |
---|---|
In acetonitrile for 2h; Reflux; | 95% |
N,N-dimethyloctanamide
Conditions | Yield |
---|---|
In acetonitrile for 4h; Reflux; | 95% |
N,N-dimethyloctanamide
Conditions | Yield |
---|---|
In acetonitrile at 85℃; for 24h; Sealed tube; High pressure; | 95% |
1-(bromomethyl)-4-(prop-1-en-2-yl)cyclohexene
N,N-dimethyloctanamide
Conditions | Yield |
---|---|
In benzene at 20℃; | 95% |
1-chloromethoxy-pentane
N,N-dimethyloctanamide
Conditions | Yield |
---|---|
In n-heptane for 0.166667h; Heating; | 94% |
N,N-dimethyloctanamide
1-chloromethoxy-nonane
Conditions | Yield |
---|---|
In n-heptane for 0.166667h; Heating; | 94% |
N,N-dimethyloctanamide
1-chloromethoxy-decane
Conditions | Yield |
---|---|
In n-heptane for 0.166667h; Heating; | 94% |
N,N-dimethyloctanamide
chloromethoxy-cyclooctane
Conditions | Yield |
---|---|
In n-heptane for 0.166667h; Heating; | 94% |
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